Lovibond SensoDirect Oxi200 Operating Instructions Manual

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GB
SensoDirect Oxi200
Dissolved Oxygen Meter
Operating instructions
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Declaration of CE-Conformity
The manufacturer: Tintometer GmbH
Schleefstraße 8 a
Deutschland
declares that this product
Product name: SensoDirect Oxi200
with all optional items conforms to the following regulations:
EMC EN 55 022 : 6 / 1993 class B EN 50 082-1 (EN 61000-4-6, EN 61000-4-4, EN 61000-4-3, EN 61000-4-2)
The product conforms to the regulations of the EMC Directive 89/336/EEC and 73/23/EEC.
Dortmund, March 12, 2003
2
Cay-Peter Voss, Managing Direc-
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Table of Contents Page
1. Scope of delivery ..............................................................4
2. System description ............................................................4
3. Connections ......................................................................6
4. Display ..............................................................................6
5. Keypad ..............................................................................8
6. Startup ..............................................................................8
7. Measurement ...................................................................10
8. Conguration of the unit ...................................................10
8.1 Resolution of display for oxygen measurement ................11
8.2 Zero point temperature oset ...........................................11
8.3 Salinity: salinity correction ................................................12
8.4 Display of sensor status ..................................................12
8.5 Pressure Absolute, display of absolute pressure .............13
8.6 Selection of temperature unit °C /°F .................................13
8.7 Selection of unit for oxygen partial pressure .....................13
8.8 “Power o”: automatic unit switch-o ..............................13
9. Oxygen measurement .....................................................14
9.1 Absolute pressure ............................................................14
9.2 Salinity correction.............................................................15
10. Calibration of oxygen measurement ................................15
10.1 Performing calibration ......................................................15
11. Oxygen sensor.................................................................16
11.1 Technical data ..................................................................16
11.2 Operating notes ...............................................................17
11.3 Design of the sensor ........................................................18
11.4 Care and maintenance .....................................................19
12. Result memory ................................................................21
12.1 Storing results ..................................................................21
12.2 Displaying stored results ..................................................21
12.3 Deleting stored results .....................................................21
13. Error messages and troubleshooting ................................22
14. Technical data ..................................................................23
15. Accessories .....................................................................26
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1. Scope of Delivery
Standard:
• Lovibond® SensoDirect Oxi200
• Measuring cell
• Batteries, 4*AA 1,5 V Cells
• Operating instructions
Set:
®
• Lovibond
• Batteries, 4*AA 1,5 V Cells
• Measuring probe
• Carrying case
• Operating instructions
SensoDirect Oxi200
2. System description
The Lovibond® SensoDirect Oxi200 is a sturdy, water-
tight handheld meter designed for daily measurements
in the area of eld or laboratory analysis.
It is used to measure oxygen concentration in surface waters and groundwater as well as for waste water and service water analysis.
The system complies with the requirements in EN 60529 relating to protection class IP67 and water­proof/dustproof properties.
The permanent protective plating on the unit serves not just as impact protection but also as a storage compartment for the sensor and as an anti-slip device when the meter is used in an upright position.
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Microprocessor technology and 4*AA 1,5 V batteries
allow unit operation without battery change for 12,000 hours or more.
A „Low Bat” indicator in the display shows the user
when it is time to change the batteries.
The required temperature compensation for the system is performed automatically following connection of the temperature sensor (NTC, 10 kOhm) that is integrated as standard in the Tintometer oxygen sensor.
The AUTO HOLD feature enables the user to identify
stable results and call them up on the display.
The standard MEAS measuring function is for conti­nuous measurement of oxygen concentrations, partial pressures or saturations.
The absolute atmospheric pressure is measured in the unit and is automatically used, for among other things, calculation of the oxygen partial pressure or calibration of the system.
The integrated automatic salinity correction feature is based on the „International Oceanographic Tables“ and is user-selectable in the range from 0% to 70% via the
conguration function of the unit.
The system is calibrated using the oxygen in the air.
A sensor evaluation is automatically shown in the display (or can be called up via the menu) after each calibration.
An internal memory for 20 results is integrated in the unit as standard. The memory stores location, result and temperature.
The memory is called up via the display.
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3. Connections
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Oxygen sensor
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4. Display
Main Display: Result or user prompt
[mmHg] Oxygen partial pressure in mmHg [hPa] Oxygen partial pressure in hPa [mg/l] Oxygen concentration [%O2] Oxygen saturation
Secondary display: Result - temperature or user prompt
[%] Percent (sensor evaluation) [°C/°F] Temperature unit
!
[Δ
] Warning index - battery
[SAL] Salinity correction on/o
[OK] Measuring signal stable
[CAL] Auto. oxygen calibration
[hPa] Absolute air pressure
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5. Keypad
[Meas] Continuous measurement -
standard
[Hold] Auto-Hold: Automatic
retaining of stable result
[On/O] On / O
[] [] Display change: partial pressure,
concentration or saturation. Leaf
through menu or display
[Rcl] Display of stored results
[Cal] Calibration mode
[Store] Storage of current result or acceptance of
unit conguration
[Menu] Unit conguration
6. Startup
The unit is supplied with integrated batteries as stan­dard and is therefore ready for immediate use. You have to unscrew the unit to insert or change the batteries.
When inserting the batteries, ensure correct polarity!
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Screw the unit back together carefully without exerting too much pressure on the gasket seal.
!
If the
[Δ
] symbol appears together with „bAt” in the
lower section of the display, this means that the bat­teries are nearly empty and need replacing.
However, the unit will continue to function for a certain period of time.
If „bAt“ appears in the upper section of the display, this means that the batteries are completely empty.
Only use the matching Tintometer oxygen sensors!
Other sensors may cause serious damage to the meter and the sensor.
The sensor or temperature sensor must be plugged in before the unit is switched on.
Switch the unit on via the [On/O] key.
The system must be calibrated when the system is
rst used.
Following measurement, please switch the unit o using the [On/O] key.
See the enclosed Operating Instructions for more detailed information on storage and care of the sen­sors.
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7. Measurement
Measuring mode MEAS
After the unit is switched on, it is automatically in the standard measuring mode (MEAS).
You can switch to the standard MEAS measuring mode by pressing the [Meas] key.
The display shows the current, possibly still uctuating
result and [Meas].
If the result is stable, the [ok] arrow appears in the display.
Measuring mode HOLD
Pressing the [Hold] key takes you into the AUTO HOLD
measuring mode.
In this mode, the recorded result is checked by the
system in line with the predened stability criteria until
these criteria are met.
The display shows Auto/HOLD in alternating mode
together with the result.
Once a stable reproducible value is present, the result
is shown permanently in the display („frozen”).
The display also shows HOLD and the temperature.
If you press the [Hold] key again, the measuring cycle starts again and runs until the stability criteria are met.
8. Conguration of the unit
To congure the unit, press the [Menu] key.
The rst menu item appears.
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If you press the [Menu] key again, the display jumps to the next menu item.
+
You can set the various parameters using the
keys.
Press the [Store] key to store and conclude congu­ration.
The unit then switches back to measuring mode.
You can terminate the conguration process by pres­sing the [Meas] or [Hold] key.
Settings made up to this point are not stored.
The unit retains the previous settings.
8.1 Resolution: resolution of display for oxygen measurement
Hi: high resolution, restricted measuring
ranges
Lo: low resolution, maximum measuring ranges
Auto: automatic, maximum measuring ranges
8.2 [Offset] = Zero point temperature offset
-10.0°C...10.0°C or -18.0°F...18.0°F:
The zero point for temperature measurement is offset by this value.
This enables the user to balance out any occurring sensor deviations:
Displayed temperature = measured temperature offset
Off: zero point offset is inactive (=0.0°)
[] [].
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8.3 Salinity: salinity correction
0...70,0 ‰: Selection of salinity correction
off: Salinity correction inactive
8.4 Display of sensor status
Indication of the sensor status that is computed internally during every calibration depending on the sensor used.
100% The electrode is in excellent condition.
30...90% The condition of the electrode is ade-
quate.
<30% The electrode is old from use or soiled.
If there is no improvement after you have cleaned and recalibrated the sensor (see operating instructions for electrode), you need to replace the sensor.
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8.5 Pressure Absolute, display of ab­solute pressure
Display of the absolute atmospheric pressure in hPa.
8.6 Selection of temperature unit °C /°F
°C All temperature values in degrees Celsius
°F All temperature values in degrees Fahrenheit
(°C = 0.556*°F-17.8 or °F = 1.8*°C+32)
8.7 Selection of unit for oxygen partial pressure
hPa: Oxygen partial pressure in hPascal
mmHg: Oxygen partial pressure in mm
mercury column
8.8 “Power off”: automatic unit switch-off
If no key is pressed during the switch-o delay period, the unit switches o automatically after the selected
time has run down.
The desired delay time is entered in minutes.
If P.oFF = oFF, automatic unit switch-o is inactive.
9. Oxygen measurement
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Please note the following when measuring dissolved oxygen:
The sensor should be calibrated after the unit is swit­ched on.
The sensor and the liquid to be measured must have the same temperature (leave until the temperatures match if necessary)
Measurements are only suciently accurate if perfor­med with a minimum ow rate of approx. 30 cm/sec;
in other words, the liquid must be constantly stirred or a suitable stirring mechanisms must be used.
Remove the protective cap prior to measurement.
The oxygen partial pressure, the oxygen concentration [mg/l] and the oxygen saturation [%] are calculated on the basis of the sensor signal and the temperature.
The measurement is based on steam-saturated air in accordance with DIN38408-C22.
9.1 Absolute pressure
The absolute atmospheric pressure is measured in the unit.
The measured air pressure primarily aects saturation
measurement [%] but also plays a major role during automatic oxygen calibration.
During depth measurements, there are dierent pres­sure conditions at the sensor and it is necessary to correct the oxygen saturation [%].
The results for oxygen concentration [mg/l] and oxygen
partial pressure are not aected by this.
9.2 Salinity correction
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The higher the salinity, the lower the solubility of oxy-
gen in water; in other words, fewer mg of oxygen are
dissolved per litre of water at the same oxygen partial pressure.
It is therefore necessary to rst enter the salinity of
the medium in order to determine the oxygen con­centration.
The salinity correction feature is adjusted for aqueous media whose chemical composition corresponds to that of seawater.
Correction is based on the „International Oceanogra-
phic Tables” (IOT).
10. Calibration of oxygen measurement
The sensor data of oxygen sensors are aected by
ageing and manufacturing tolerances that result in
uctuations. You should therefore calibrate the unit
with the sensor on a regular basis.
The sensor is automatically adjusted to the oxygen
content of the air (20.95%; 1-point calibration).
We recommend calibration prior to each series of measurement.
10.1 Performing calibration
Remove the protective cap from the sensor prior to calibration.
Pat the diaphragm dry using a soft cloth.
Starting calibration: -Press [Cal] key.
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‘CAL’ appears in the display.
As soon as the results for oxygen, temperature and air pressure are constant, calibration is terminated automatically.
The sensor status (‘ELEC’, valuation in 10% steps) is then briey displayed.
Depending on the temperature, a correctly calibrated sensor shows a result of 102..114% (oxygen satu­ration).
If error messages occur during calibration, please see the troubleshooting tips.
If calibration is not completed after you have waited a lengthy period of time, at least one of the three measu­ring signals (oxygen partial pressure, temperature or air pressure) is not stable.
In this event, you should check the measuring setup.
11. Oxygen sensor
11.1 Technical data:
Measuring range of the unit:
Oxygen partial pressure: 0 ... 1200 hPa O
Temperature: -5.0 ... 50.0 °C
Sensor: Galvanic, active dia­ phragm-covered sen­ sor, with integrated NTC resistor
Response time: 95% in 10 sec., tem-
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perature-dependent
Operating pressure: max. 3 bar.
Installation diameter: Ø 12.0 ±0.2 mm (ts a 1/2 „ screw connection, for example)
Overall length: approx. 220 mm (incl. anti-kink protection)
Installation length: approx. 110 mm
Weight: approx. 180 g
Operating temperature: 0 to +40°C
Storage temperature: 0 to +60°C
The galvanic self-polarising sensor with silver cathode and lead anode with potassium hydroxide as an elec­trolyte, is an active system.
The lead anode, the silver cathode and the electrolyte are used up during operation.
The sensor is aected by ageing over time.
Continuous maintenance of the sensor is therefore necessary.
11.2 Operating notes
a.) The oxygen sensor must always be kept moist to prevent the membrane from drying out. To this end, you should place the sensor in deionised water in the supplied storage cap.
If the diaphragm has dried out, the sensor needs to be watered for approx. 2 hours prior to measurement. It
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then needs to be recalibrated.
b.) The sensors may only be used with the correspon­ding units. The use of the sensors in combination with unsuitable units can destroy the unit and the sensors! c.) Unit and sensor must be handled with care and used in accordance with the technical data outlined above. Always protect the connector and connection socket against soiling and dirt.
d.) Do not insert the connector at an angle. If the connector is inserted properly, you should be able to press it in without using force.
When disconnecting the sensor, do not pull it by the cable but always by the connector sleeve.
e.) Remove the sensor storage cap before performing measurements.
11.3 Design of the sensor
The housing of the sensor probe is made of PVC. With the exception of the sensor shaft, all parts must be serviced regularly and replaced if necessary.
Storage cap: The storage cap is used to moisten the membrane. This increases the service life of the sensor. The storage cap contains deionised water.
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Rell
opening
Sensor shaft
O-Ring­seal
membrane cap
Membrane cap: the diaphragm head is covered with
a Teon membrane.
The diaphragm cap is lled with KOH electrolyte and
screwed onto the sensor shaft in such a way that there are no air bubbles.
Damaged membrane or air bubbles in the membrane
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cap cause incorrect results.
The membrane cap is listed in the spare parts list.
Refill opening: if the sensor is used at excessive temperatures or stored outside the storage bottle for lengthy periods of time, this will result in electrolyte evaporation losses.
If necessary, you should therefore unscrew the dia-
membrane head, remove the sealing screw, and ll
up the electrolyte using a syringe.
Then screw the sealing screw back in place.
11.4 Care and maintenance
If the sensor is not needed, it should be stored either
in the storage cap (lled with water) or directly in a
container full of deionised water.
If a bacterial, fungal or algae coating has formed on
the membrane, you should wipe o the coating using
a soft paper cloth prior to measurement.
If it is no longer possible to calibrate the sensor or if the membrane is damaged, the sensor needs servicing.
Air bubbles in the membrane cap can aect measu­rements. Please remove carefully.
! Exercise caution during maintenance work – the electrolyte is caustic !
Wear disposable gloves when servicing the sensor and wash your hands thoroughly with water afterwards.
Servicing the sensor:
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Unscrew the membrane head and wipe o the elec­trolyte solution carefully using a paper cloth.
Do not allow the electrolyte to come into contact with your hands. If it does come into contact with your skin,
rinse the aected area thoroughly in water.
To clean the silver cathode, sand lightly using sand­paper (240 grit). Do not sand the silver cathode to a smooth nish. It needs to be rough so that the electro­lyte is distributed evenly. Carefully remove the sanding dust after sanding.
Unscrew the rell screw and ll up carefully with elec­trolyte until it just overows (disposable syringe). Screw the rell screw back in place.
Fill new membrane cap with electrolyte, avoiding air bubbles.
Screw the sensor vertically into the cap from above. When you insert the sensor, the electrolyte is displaced
from the membrane head and overows.
Remove excess electrolyte using a paper cloth.
Turn the sensor upside down and check for air bubbles. If there are no air bubbles, servicing is complete.
If air bubbles are still present, please remove carefully.
If the O-ring seal is damaged it needs replacing.
Important note: leave the sensor to settle for at least 1 hour before performing recalibration.
If it is still not possible to calibrate the sensor despite servicing, the sensor needs to be checked at the fac­tory and replaced if necessary.
12. Result memory
A maximum 20 results with the corresponding tempe-
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ratures can be stored.
12.1 Storing results
You can store the current result in the result memory by pressing the [Store] key.
[Stor] and the number of the memory location appear
briey in the display.
12.2 Displaying stored results
You can call the stored results up in the display by pressing the [Rcl] (=Recall) key.
The rst time you press the [Rcl] key, the number of
the memory location and the corresponding oxygen­value are displayed.
The second time you press the key, the temperature for this result is displayed, the third time the air pressure is displayed.
You can use the stored results.
As soon as you press the [Store], [Meas] or [Hold] key,
+
the unit reverts to the corresponding measuring mode.
[] [] keys to switch between the
12.3 Deleting stored results
If you press the [Store] key for longer than 2 seconds,
the unit switches to the delete menu [CLR].
You can use the and press the [Store] key to execute it.
+
The unit then returns to the corresponding measuring mode.
[] [] keys to select the desired action
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[CLr-ALL]: delete all stored results.
[CLr-LASt]: delete the last-stored result.
[CLr-nonE]: do not delete any result.
13. Error messages and troubleshooting
Display Cause Remedy
Weak battery vol- Insert new batteries
tage the unit will only
continue to function
for a short time
Batteries empty Insert new batteries
No display or Batteries empty Insert new batteries
strange symbols. Batteries incorrectly Check batteries
inserted
Unit does not react System error Disconnect batteries, when keys are wait for a short time, pressed reconnect the batteries
Unit defective Send in for repair
Display Cause Remedy
Err.1 Exceeds Check: can value be
measuring range exceed admissible
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measuring range?
-> Result too high!
Sensor defective Replace sensor
Err.2 Below Check: can value be
measuring range below admissible measuring range?
-> Result too low!
Sensor defective Replace sensor
Err.7 System error Send in for repair
Err.9 Sensor not present Connect sensor
Sensor defective Replace sensor
Err.11 Value could not Temperature outside
be calculated the admissible temperature measuring range
Oxygen calibration
Display Cause Remedy
CAL.-Err.1 Wrong temperature Temperature must
be between
5 and 40°C
CAL.-Err.2 Wrong air pressure Air pressure must
be between 500 and 1100hPa
Display Cause Remedy
CAL.-Err.3 Sensor signal Membrane dried
too low dried out?
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-> Place sensor in water for 2 hours (waterxx)
Repair or replace sensor
Check calibration environment
CAL.-Err.4 Sensor signal Air bubbles in the
too high diaphragm head?
Check calibration environment
14. Technical data
Indicating ranges
High resolution Low resolution, Auto Range
Oxygen partial 0.0...570.0 hPa 0...1200 hPa
pressure 0.0...427.5 mmHg 0...900 mmHg
Oxygen concentration 0.00...25.00 mg/l 0.0...70.0 mg/l
Oxygen saturation 0.0...250.0 % 0...600 %
Temperature -5,0 ... +50,0°C/
23.0 ... 122.0°F
Abs. pressure 500..1100 hPa
Accuracy:
(at nominal temperature, ±1digit)
Oxygen measuring +/-1.5% +/-0.2mg/l (0...25 mg/l) or ranges +/-2.5% +/-0.3mg/l (25...70 mg/l)
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Temperature ±0,1°C
Abs. pressure +/- 0,5% full scale
Nominal temperature: 25°C Operating temperature: 0 to +50°C Storage temperature: -20 to +70°C
Memory: 20 result memory locations
Power supply: 4 x 1.5 V -batteries, Type AA
operating life up to 2000h (depending on measuring mode and battery type)
Power consumption: max. 0.25 mA (depending on measuring mode
– MEAS or AUTOHOLD)
Battery change indicator: ‚bAt‘
Automatic „Off” function: if no key is pressed and no data transfer is
occurring, the unit switches o after the switch-o delay time. May be set between
1 and 120 minutes or inactive.
Housing: water-tight in accordance with IP67 Integral protective plating
LCD
Film keypad
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Sensor: self-polarising galvanic oxygen sensor with integrated NTC sensor
Connection: 7-pin DIN socket
Installation diameter: 12.0 +/- 0.2mm (also ts 1/2“ screw
connections) Overall length: approx. 220 mm (incl. anti-kink protection) Operating temperature: 0...40°C
15. Accessories
723200 Lovibond® SensoDirect Oxi200 Basic Instrument
®
723220 Lovibond
723201 SensoDirect Oxygen Sensor 1 m cable
723210 SensoDirect Oxygen Sensor 10 m cable
723230 SensoDirect Oxygen Sensor 30 m cable
723250 Service Set Oxygen Sensor
723260 Armature for Depth Measurement
725020 Case SensoDirect
SensoDirect Oxi200 Set
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Tintometer GmbH
®
Water Testing
Lovibond Schleefstraße 8-12 44287 Dortmund Tel.: +49 (0)231/94510-0 Fax: +49 (0)231/94510-20 sales@tintometer.de www.lovibond.com
Germany
Tintometer Inc. (dba Orbeco-Hellige Inc.) 6456 Parkland Drive Sarasota, FL 34243 Tel: 941.756.6410 Fax: 941.727.9654 sales@tintometer.us www.lovibond.us
USA
The Tintometer Limited Lovibond House / Solar Way Solstice Park / Amesbury, SP4 7SZ Tel.: +44 (0)1980 664800 Fax: +44 (0)1980 625412 water.sales@tintometer.com www.lovibond.com
UK
Tintometer China Room 1001, China Life Tower 16 Chaoyangmenwai Avenue, Beijing, 100020 Tel.: +86 10 85251111 App. 330 Fax: +86 10 85251001
China
Technical changes without notice Printed in Germany 10/14 No.: 00 38 60 65 Lovibond® and Tintometer® are Trademarks of the Tintometer Group of Companies
Tintometer AG
Hauptstraße 2 5212 Hausen AG Tel.: +41 (0)56/4422829 Fax: +41 (0)56/4424121 info@tintometer.ch www.tintometer.ch
Switzerland
Tintometer South East Asia Unit B-3-12, BBT One Boulevard, Lebuh Nilam 2, Bandar Bukit Tinggi, Klang, 41200, Selangor D.E Tel.: +60 (0)3 3325 2285/6 Fax: +60 (0)3 3325 2287 lovibond.asia@tintometer.com www.lovibond.com
Malaysia
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