Lovibond PoolDirect Instruction And Operation Manual

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GB
V4_11/2015
Lovibond
®
The Instruments of Choice The Test of Quality
Instruction/Operator Manual
Lovibond® Water Testing
Tintometer® Group
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Important steps before using the photometer
Please carry out the following steps as described in the In­struction manual. Become familiar with your new photometer before starting with the first tests:
• Unpacking and inspection of delivery contents, see page 72.
• Install the rechargeable batteries/batteries and the Lithium­battery, see page 36, 37.
• Using rechargeable batteries: Charge the rechargeable batteries in the instrument for 5 days (it is possible to continue using the instrument). Now use the instrument without mains power until the first battery warning comes up. Charge again, for 4 days this time. Repeat this cycle four times.
Perform the following settings in the Mode-Menu; Instruction manual from page 44 and following:
• MODE 10: select language
• MODE 12: set date and time
• MODE 34: perform “Delete data“
If required set other functions.
IMPORTANT NOTE:
The Lithium battery (for saving data and clock) works for ap­prox. ½ year in case of no power from mains adapter or re­chargeable batteries/batteries.
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Wichtige Information
Um die Qualität unserer Umwelt zu erhalten, beschützen und zu verbessern
Entsorgung von elektronischen Geräten in der Europäischen Union
Aufgrund der Europäischen Verordnung 2012/19/EU darf Ihr elektronisches Gerät
nicht mit dem normalen Hausmüll entsorgt werden!
Tintometer GmbH entsorgt ihr elektrisches Gerät auf eine professionelle und für die Umwelt verantwortungsvolle Weise. Dieser Service ist, die Transportkosten
nicht inbegriffen, kostenlos. Dieser Service gilt ausschließlich für elektrische Geräte
die nach dem 13.08.2005 erworben wurden. Senden Sie Ihre zu entsorgenden
Tintometer Geräte frei Haus an Ihren Lieferanten.
Important Information
To Preserve, Protect and Improve the Quality of the Environment
Disposal of Electrical Equipment in the European Union
Because of the European Directive 2012/19/EU your electrical instrument must not
be disposed of with normal household waste!
Tintometer GmbH will dispose of your electrical instrument in a professional
and environmentally responsible manner. This service, excluding the cost of
transportation is free of charge. This service only applies to electrical instruments
purchased after 13th August 2005. Send your electrical Tintometer instruments for
disposal freight prepaid to your supplier.
Notice importante
Conserver, protéger et optimiser la qualité de l’environnement
Élimination du matériel électrique dans l’Union Européenne
Conformément à la directive européenne nº 2012/19/UE, vous ne devez plus jeter
vos instruments électriques dans les ordures ménagères ordinaires !
La société Tintometer GmbH se charge d’éliminer vos instruments électriques de
façon professionnelle et dans le respect de l’environnement. Ce service, qui ne
comprend pas les frais de transport, est gratuit. Ce service n’est valable que
pour des instruments électriques achetés après le 13 août 2005. Nous vous prions
d’envoyer vos instruments électriques Tintometer usés à vos frais à votre fournisseur.
Belangrijke informatie
Om de kwaliteit van ons leefmilieu te behouden, te verbeteren en te
beschermen is voor landen binnen de Europese Unie de Europese richtlijn
2012/19/EU voor het verwijderen van elektronische apparatuur opgesteld.
Volgens deze richtlijn mag elektronische apparatuur niet met het huishoudelijk afval
worden afgevoerd.
Tintometer GmbH verwijdert uw elektronisch apparaat op een professionele en
milieubewuste wijze. Deze service is, exclusief de verzendkosten, gratis en alleen geldig voor elektrische apparatuur die na 13 augustus 2005 is gekocht. Stuur uw te
verwijderen Tintometer apparatuur franco aan uw leverancier.
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Información Importante
Para preservar, proteger y mejorar la calidad del medio ambiente
Eliminación de equipos eléctricos en la Unión Europea
Con motivo de la Directiva Europea 2012/19/UE, ¡ningún instrumento eléctrico
deberá eliminarse junto con los residuos domésticos diarios!
Tintometer GmbH se encargará de dichos instrumentos eléctricos de una manera
profesional y sin dañar el medio ambiente. Este servicio, el cual escluye los gastos de transporte, es gratis y se aplicará únicamente a aquellos instrumentos eléctricos
adquiridos después del 13 de agosto de 2005. Se ruega enviar aquellos instrumentos
eléctricos inservibles de Tintometer a carga pagada a su distribuidor.
Informazioni importanti
Conservare, proteggere e migliorare la qualità dell’ambiente
Smaltimento di apparecchiature elettriche nell’Unione Europea
In base alla Direttiva europea 2012/19/UE, gli apparecchi elettrici non devono essere
smaltiti insieme ai normali rifiuti domestici!
Tintometer GmbH provvederà a smaltire i vostri apparecchi elettrici in maniera
professionale e responsabile verso l’ambiente. Questo servizio, escluso il trasporto,
è completamente gratuito. Il servizio si applica agli apparecchi elettrici acquistati
successivamente al 13 agosto 2005. Siete pregati di inviare gli apparecchi elettrici
Tintometer divenuti inutilizzabili a trasporto pagato al vostro rivenditore.
Informação Importante
Para Preservar, Proteger e Melhorar a Qualidade do Ambiente
Remoção de Equipamento Eléctrico na União Europeia
Devido à Directiva Europeia 2012/19/UE, o seu equipamento eléctrico naõ deve ser
removido com o lixo doméstico habitual!
A Tintometer GmbH tratará da remoção do seu equipamento eléctrico de forma
profissional e responsável em termos ambientais. Este serviço, não incluindo
os custos de transporte, é gratuito. Este serviço só é aplicável no caso de
equipamentos eléctricos comprados depois de 13 de Agosto de 2005. Por favor,
envie os seus equipamentos eléctricos Tintometer que devem ser removidos ao seu
fornecedor (transporte pago).
Istotna informacja
Dla zachowania, ochrony oraz poprawy naszego środowiska
Usuwanie urządzeń elektronicznych w Unii Europejskiej
Na podstawie Dyrektywy Parlamentu Europejskiego 2012/19/UE nie jest
dozwolone usuwanie zakupionych przez Państwo urządzeń elektronicznych wraz z
normalnymi odpadami z gospodarstwa domowego!
Tintometer GmbH usunie urządzenia elektrycznego Państwa w sposób
profesjonalny i odpowiedzialny z punktu widzenia środowiska. Serwis ten jest,
za wyjątkiem kosztów transportu, bezpłatny. Serwis ten odnosi się wyłącznie do
urządzeń elektrycznych zakupionych po 13.08.2005r. Przeznaczone do usunięcia
urządzenia rmy Tintometer mogą Państwo przesyłać na koszt własny do swojego
dostawcy.
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Wichtiger Entsorgungshinweis zu Batterien und Akkus
Jeder Verbraucher ist aufgrund der Batterieverordnung (Richtlinie 2006/66/
EG) gesetzlich zur Rückgabe aller ge- und verbrauchten Batterien bzw. Akkus
verpflichtet. Die Entsorgung über den Hausmüll ist verboten. Da auch bei Produkten
aus unserem Sortiment Batterien und Akkus im Lieferumgang enthalten sind, weisen
wir Sie auf folgendes hin:
Verbrauchte Batterien und Akkus gehören nicht in den Hausmüll, sondern können
unentgeltlich bei den öffentlichen Sammelstellen Ihrer Gemeinde und überall
dort abgegeben werden, wo Batterien und Akkus der betreffenden Art verkauft
werden. Weiterhin besteht für den Endverbraucher die Möglichkeit, Batterien und
Akkus an den Händler, bei dem sie erworben wurden, zurückzugeben (gesetzliche
Rücknahmepflicht).
Important disposal instructions for batteries and accumulators
EC Guideline 2006/66/EC requires users to return all used and worn-out batteries
and accumulators. They must not be disposed of in normal domestic waste. Because
our products include batteries and accumulators in the delivery package our advice is
as follows :
Used batteries and accumulators are not items of domestic waste. They must be
disposed of in a proper manner. Your local authority may have a disposal facility;
alternatively you can hand them in at any shop selling batteries and accumulators.
You can also return them to the company which supplied them to you; the company
is obliged to accept them.
Information importante pour l'élimination des piles et des accumulateurs
En vertu de la Directive européenne 2006/66/CE relative aux piles et accumulateurs,
chaque utilisateur est tenu de restituer toutes les piles et tous les accumulateurs
utilisés et épuisés. L'élimination avec les déchets ménagers est interdite. Etant donné
que l'étendue de livraison des produits de notre gamme contient également des piles
et des accumulateurs, nous vous signalons ce qui suit :
les piles et les accumulateurs utilisés ne sont pas des ordures ménagères, ils peuvent
être remis sans frais aux points de collecte publics de votre municipalité et partout où sont vendus des piles et accumulateurs du type concerné. Par ailleurs, l'utilisateur final a la possibilité de remettre les piles et les accumulateurs au commerçant auprès
duquel ils ont été achetés (obligation de reprise légale).
Belangrijke mededeling omtrent afvoer van batterijen en accu’s
Ledere verbruiker is op basis van de richtlijn 2006/66/EG verplicht om alle gebruikte
batterijen en accu’s in te leveren. Het is verboden deze af te voeren via het huisvuil.
Aangezien ook onze producten geleverd worden met batterijen en accu’s wijzen wij
u op het volgende; Lege batterijen en accu’s horen niet in het huisvuil thuis. Men
kan deze inleveren bij inzamelpunten van uw gemeente of overal daar waar deze
verkocht worden. Tevens bestaat de mogelijkheid batterijen en accu’s daar in te
leveren waar u ze gekocht heeft. (wettelijke terugnameplicht)
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Indicación importante acerca de la eliminación de pilas y acumuladores
Basado en la norma relativa a pilas/ baterías (directiva 2006/66/CE), cada consumidor,
está obligado por ley, a la devolución de todas las pilas/ baterías y acumuladores usados y
consumidos. Está prohibida la eliminación en la basura doméstica. Ya que en productos de
nuestra gama, también se incluyen en el suministro pilas y acumuladores, le sugerimos lo
siguiente:
Las pilas y acumuladores usados no pertenecen a la basura doméstica, sino que pueden
ser entregados en forma gratuita en cada uno de los puntos de recolección públicos de su
comunidad en los cuales se vendan pilas y acumuladores del tipo respectivo. Además, para
el consumidor final existe la posibilidad de devolver las pilas y baterías recargables a los
distribuidores donde se hayan adquirido (obligación legal de devolución).
Indicazioni importanti sullo smaltimento di pile e accumulatori
In base alla normativa concernente le batterie (Direttiva 2006/66/CE) ogni consumatore
è tenuto per legge alla restituzione di tutte le batterie o accumulatori usati ed esauriti. È
vietato lo smaltimento con i rifiuti domestici. Dato che anche alcuni prodotti del nostro assortimento sono provvisti di pile e accumulatori, vi diamo di seguito delle indicazioni:
Pile e accumulatori esauriti non vanno smaltiti insieme ai rifiuti domestici, ma depositati
gratuitamente nei punti di raccolta del proprio comune o nei punti vendita di pile e
accumulatori dello stesso tipo. Inoltre il consumatore finale può portare batterie e
accumulatori al rivenditore presso il quale li ha acquistati (obbligo di raccolta previsto per
legge).
Instruções importantes para a eliminação residual de pilhas e acumuladores
Os utilizadores finais são legalmente responsáveis, nos termos do Regulamento relativo
a pilhas e acumuladores (Directiva 2006/66/CE), pela entrega de todas as pilhas e
acumuladores usados e gastos. É proibida a sua eliminação juntamente com o lixo
doméstico. Uma vez que determinados produtos da nossa gama contêm pilhas e/ou
acumuladores, alertamos para os seguintes aspectos:
As pilhas e acumuladores usados não podem ser eliminados com o lixo doméstico, devendo sim ser entregues, sem encargos, junto dos pontos de recolha públicos do seu município, ou em qualquer ponto de venda de pilhas e acumuladores. O utilizador final
dispõe ainda da possibilidade de entregar as pilhas e/ou acumuladores no estabelecimento
comerciante onde os adquiriu (dever legal de aceitar a devolução).
Istotna wskazówka dotycząca utylizacji baterii i akumulatorów
Każdy użytkownik na mocy rozporządzenia w sprawie baterii (wytyczna 2006/66/WE)
jest ustawowo zobowiązany do oddawania wszystkich rozładowanych i zużytych baterii
lub akumulatorów. Utylizacja wraz z odpadkami domowymi jest zabroniona. Ponieważ
także w produktach z naszego asortymentu zawarte są w zakresie dostawy baterie i
akumulatory, zwracamy uwagę na poniższe zasady:
zużyte baterie i akumulatory nie mogą być wyrzucane wraz z odpadkami domowymi,
lecz powinny być bezpłatnie przekazywane w publicznych miejscach zbiórki
wyznaczonych przez gminę lub oddawane w punktach, gdzie sprzedawane są baterie i
akumulatory danego rodzaju. Poza tym użytkownik końcowy ma możliwość zwrócenia baterii i akumulatorów do przedstawiciela handlowego, u którego je nabył (ustawowy
obowiązek przyjęcia).
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Safety precautions
CAUTION
Reagents are formulated exclusively for chemical analysis and must not be used for
any other purpose. Reagents must not get into the hands of children. Some of the
reagents contain substances which are not entirely harmless environmentally. Be
aware of the ingredients and take proper care when disposing of the test solution.
CAUTION
Please read this instruction manual before unpacking, setting up or using the
photometer. Please read the method description completely before performing the
test. Be aware of the risks of using the required reagents by reading the MSDS
(Material Safety Data Sheets). Failure could result in serious injury to the operator or
damage to the instrument.
MSDS: www.lovibond.com
CAUTION
Use the charger unit only with rechargeable Ni-MH batteries. Failure can result in
serious injury to the operator or damage to the instrument.
Do not use charger with non rechargeables batteries.
CAUTION
The accuracy of the instrument is only valid if the instrument is used in an environment
with controlled electromagnetic disturbances according to DIN 61326.
Wireless devices, e.g. wireless phones, must not be used near the instrument.
Revision_4i 11/2015
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Table of contents
Part 1 Methods ................................................................................................. 13
1.1 Table of Methods ................................................................................................... 14
Free Chlorine .................................................................................................................. 15
Total Chlorine ................................................................................................................. 16
pH Value ......................................................................................................................... 18
Total Alkalinity ................................................................................................................ 20
Calcium Hardness ........................................................................................................... 22
Bromine .......................................................................................................................... 24
Ozone ............................................................................................................................. 26
Free Copper .................................................................................................................... 28
Total Copper ................................................................................................................... 29
CyA-Test (Cyanuric acid) .................................................................................................. 30
Water Balance (Langelier Saturation Index) ...................................................................... 32
Guidelines for photometric measurements ...................................................................... 34
Part 2 Operator manual .............................................................................. 35
2.1 Operation ..................................................................................................... 36
2.1.1 Commissioning .............................................................................................. 36
2.1.2 Saving data – Important Notes ....................................................................... 36
2.1.3 Replacement of rechargeable batteries and/ or Lithiumbattery ........................ 36
2.1.4 Charging the rechargeable batteries ............................................................... 36
2.1.5 Fuse ............................................................................................................... 37
2.1.6 Protective caps ............................................................................................... 37
2.1.7 Instrument view ............................................................................................. 37
2.2 Overview of function keys ......................................................................... 39
2.3 Operation mode .......................................................................................... 40
2.3.1 Automatic switch off ...................................................................................... 40
2.3.2 Selecting a method ........................................................................................ 40
2.3.3 Blank because of technical requirements ........................................................ 40
2.3.4 Performing Zero ............................................................................................. 40
2.3.5 Performing Tests ............................................................................................. 41
2.3.6 Ensuring reaction periods (countdown) ........................................................... 41
2.3.7 Blank because of technical requirements ........................................................ 41
2.3.8 Storing results ................................................................................................ 42
2.3.9 Printing results ............................................................................................... 43
2.3.10 Perform additional measurements .................................................................. 43
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2.4 Photometer settings: Table of Mode Functions ........................................ 44
2.4.1 blank because of technical requirements ........................................................ 45
2.4.2 Instrument basic settings 1 ............................................................................. 45
2.4.3 Printing of stored results ................................................................................. 49
2.4.4 Recall / delete stored results............................................................................ 54
2.4.5 Calibration ..................................................................................................... 58
2.4.6 Lab function ................................................................................................... 63
2.4.7 blank because of technical requirements ........................................................ 65
2.4.8 User operation ............................................................................................... 66
2.4.9 Instrument basic settings 2 ............................................................................. 68
2.4.10 Instrument special functions /service ............................................................... 68
2.5 Data transfer ................................................................................................ 69
2.5.1 Connection to a printer .................................................................................. 69
2.5.2 Data transfer to a personal computer ............................................................. 69
2.5.3 Internet Updates ............................................................................................ 69
Part 3 Enclosure ................................................................................................ 71
3.1 Unpacking .................................................................................................... 72
3.2 Contents ....................................................................................................... 72
3.3 blank because of technical requirements .................................................. 72
3.4 Technical data .............................................................................................. 73
3.5 Abbreviations .............................................................................................. 74
3.6 Troubleshooting .......................................................................................... 75
3.6.1 Operating messages in the display / error display ............................................ 75
3.6.2 General .......................................................................................................... 76
3.7 Declaration of CE-Conformity .................................................................... 77
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Part 1
Methods
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1.1 Table of Methods
Test Analysis Reagent Range Displayed Method OTZ
1 2
Free Chlorine Total Chlorine
tablet tablet
0.01-6
0.01-6
mg/l Cl
2
mg/l Cl
2
DPD
1, 2, 3
DPD
1, 2, 3
3 pH-Value tablet 6.5-8.4 Phenol red
5
4 Total Alkalinity tablet 5-200 mg/l CaCO
3
Acid / Indicator
1, 2, 5
5 Cal Hardness tablet 0-500 mg/l CaCO
3
Murexide
4
6 Bromine tablet 0.05-13 mg/l Br
2
DPD
5
7 Ozone (DPD) tablet 0.02-2 mg/l O
3
DPD
5
8 Copper tablet 0.05-5 mg/l Cu Biquinoline
4
9 CyA-TEST tablet 0-160 mg/l CyA Melamine
OTZ (OneTimeZero) switching on and off, see Mode 55, page 65
The precision of Lovibond® Reagent Systems (tablets, powder packs and tube tests) is identical to the precision specified in standards literature such as American Standards (AWWA), ISO etc.
Most of the data referred to in these standard methods relates to Standard Solutions. Therefore they are not readily applicable to drinking-, boiler- or waste-water, since various interferences can have a major influence on the accuracy of the method. Due to the fact that each sample is different, the only way to check the tolerances (‘precision’) is the Standard Additions Method. According to this method, first the original sample is tested. Then further samples (2 to
4) are taken and small amounts of a Standard Solution are added, and further results are obtained. The amounts added range from approximately half, up to double the amount present in the sample itself. These supplementary results make it possible to estimate the actual concentration of the original sample by comparison.
Literature
The reagent formulations are based on internationally recognised test methods. Some are described in national and/or international guidelines.
1. Deutsche Einheitsverfahren zur Wasser-, Abwasser- und Schlammuntersuchung
2. Standard Methods for the Examination of Water and Wastewater; 18th Edition, 1992
3. Photometrische Analysenverfahren, Schwedt, Wissenschaftliche Verlagsgesellschaft mbH, Stuttgart 1989
4. Photometrische Analyse, Lange / Vejdelek, Verlag Chemie 1980
5. Colorimetric Chemical Analytical Methods, 9th Edition, London
Notes for searching:
Alkalinity, total -> Alkalinity-m Calcium Hardness -> Hardness, Calcium Cyanuric Acid -> CyA-TEST m-Value -> Alkalinity, total
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1.1 Methods
Free Chlorine
0.01 – 6 mg/l Cl
2
1. Select the method required on keypad.
2. Fill a clean vial (24 mm Ø) with 10 ml of the water sample, close tightly with the cap.
3. Place the vial in the sample chamber making sure that the marks are aligned.
4. Press ZERO key.
5. Remove the vial from the sample chamber and empty
it, leaving a few drops remaining in the vial.
6. Add one DPD No. 1 tablet straight from the foil to the water sample and crush the tablet using a clean stirring rod.
7. Add the water sample to the 10 ml mark.
8. Close the vial tightly with the cap and swirl gently several times until the tablets are dissolved.
9. Place the vial in the sample chamber making sure that the marks are aligned.
10. Press TEST key.
The result is shown in the display as free Chlorine in
mg/l.
Note:
See page 17
prepare Zero press ZERO
Zero accepted prepare Test press TEST
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1.1 Methods
Total Chlorine
0.01 – 6 mg/l Cl
2
1. Select the method required on keypad.
2. Fill a clean vial (24 mm Ø) with 10 ml of the water sample, close tightly with the cap.
3. Place the vial in the sample chamber making sure that the marks are aligned.
4. Press ZERO key.
5. Remove the vial from the sample chamber and empty
it, leaving a few drops remaining in the vial.
6. Add one DPD No. 1 and one DPD No. 3 tablet straight from the foil to the water sample and crush the tablets using a clean stirring rod.
7. Add the water sample to the 10 ml mark.
8. Close the vial tightly with the cap and swirl gently several times until the tablets are dissolved.
9. Place the vial in the sample chamber making sure that the marks are aligned.
10. Press TEST key.
Wait for a reaction period of 2 minutes.
After the reaction period is finished the measurement
starts automatically.
The result is shown in the display as total Chlorine in
mg/l.
Note:
Instead of using DPD No. 1 plus DPD No. 3 you can use DPD No. 4.
prepare Zero press ZERO
Zero accepted prepare Test press TEST
Countdown 2:00
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1.1 Methods
Notes:
1. Vial cleaning: As many household cleaners (e.g. dishwasher detergent) contain reducing substances, the subsequent determination of Chlorine may show lower results. To avoid any measurement errors, only use glassware free of Chlorine demand. Preparation: Put all applicable glassware into Sodium hypochlorite solution (0.1 g/l) for one hour, then rinse all glassware thoroughly with deionised water.
2. For individual testing of free and total Chlorine, the use of different sets of glassware is recommended (EN ISO 7393-2, 5.3)
3. Preparing the sample: When preparing the sample, the lost of Chlorine, e.g. by pipetting or shaking, must be avoided. The analysis must take place immediately after taking the sample.
4. The DPD colour development is carried out at a pH value of 6.2 to 6.5. The reagents therefore contain a buffer for the pH adjustment. Strong alkaline or acidic water samples must be adjusted between pH 6 and pH 7 before the reagent is added (use 0.5 mol/l Sulfuric acid resp. 1 mol/l Sodium hydroxide).
5. Exceeding the measuring range: Concentrations above: 10 mg/l Chlorine using tablets can lead to results showing 0 mg/l. In this case, the water sample must be diluted with water free of Chlorine. 10 ml of the diluted sample should be mixed with the reagent and the measurement repeated.
6. Turbidity (can lead to errors): The use of the DPD No. 1 tablet in samples with high Calcium ion content* and/or high conductivity* can lead to turbidity of the sample and therefore incorrect measurements. In this case, the reagent tablet DPD No. 1 High Calcium should be used as an alternative. If turbidity does occur after the DPD No. 3 tablet has been added, this can be prevented by using the DPD No. 1 HIGH CALCIUM tablet and the DPD No.3 High Calcium tablet. The DPD No. 1 High Calcium should only be used in combination with the DPD No.3 High Calcium.
* it is not possible to give exact values, because the development of turbidity depends on the nature of the sample.
7. combined Chlorine = total Chlorine – free Chlorine
8. Oxidising agents such as Bromine, Ozone etc. interfere as they react in the same way as Chlorine.
Precision
An educated operator obtained under laboratory conditions exemplary for 2 different (one) standard solutions the following standard deviations using different lots of reagent: Chlorine 0.20 ± 0.02 mg/l; 2.00 ± 0.05 mg/l
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1.1 Methods
pH Value
6.5 – 8.4
1. Select the method required on keypad.
2. Fill a clean vial (24 mm Ø) with 10 ml of the water sample, close tightly with the cap.
3. Place the vial in the sample chamber making sure that the marks are aligned.
4. Press ZERO key.
5. Remove the vial from the sample chamber.
6. Add one PHENOL RED PHOTOMETER tablet straight from the foil to the water sample and crush the tablet using a clean stirring rod.
7. Close the vial tightly with the cap and swirl gently several times until the tablet is dissolved.
8. Place the vial in the sample chamber making sure that the marks are aligned.
9. Press TEST key.
The result is shown in the display as pH-Value.
prepare Zero press ZERO
Zero accepted prepare Test press TEST
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1.1 Methods
Notes:
1. For photometric determination of pH values only use PHENOL RED tablets in black printed foil pack and marked with PHOTOMETER.
2. Water samples with low values of Alkalinity-m (below 35 mg/l CaCO3) may give wrong pH readings.
3. pH values below 6.5 and above 8.4 can produce results inside the measuring range. A plausibility test (pH-meter) is recommended.
4. The accuracy of the colorimetric determination of pH values depends on various boundary conditions (buffer capacity of the sample, salt content etc.).
5. Salt error Correction of test results (average values) for samples with salt content of:
Indicator Salt content
Phenol red 1 molar 2 molar 3 molar
– 0.21 – 0.26 – 0.29
The values of Parson and Douglas (1926) are based on the use of Clark and Lubs buffers. 1 Mol NaCl = 58.4 g/l = 5.8 %
Precision
An educated operator obtained under laboratory conditions exemplary for 2 different (one) standard solutions the following standard deviations using different lots of reagent:
7.50 ± 0.01 mg/l
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1.1 Methods
Total Alkalinity
5 – 200 mg/l CaCO
3
1. Select the method required on keypad.
2. Fill a clean vial (24 mm Ø) with 10 ml of the water sample, close tightly with the cap.
3. Place the vial in the sample chamber making sure that the marks are aligned.
4. Press ZERO key.
5. Remove the vial from the sample chamber.
6. Add one ALKA-M-PHOTOMETER tablet straight from the foil to the water sample and crush the tablet using a clean stirring rod.
7. Close the vial tightly with the cap and swirl gently several times until the tablet is dissolved.
8. Place the vial in the sample chamber making sure that the marks are aligned.
9. Press TEST key.
The result is shown in the display as Total Alkalinity.
prepare Zero press ZERO
ZERO accepted prepare test press Test
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1.1 Methods
Notes:
1. The terms total Alkalinity, Alkalinity-m, m-Value and Alkalinity to pH 4.3 are identical.
2. For accurate results exactly 10 ml of water sample must be taken for the test.
3. Conversion table:
Acid demand to pH 4.3
DIN 38 409 (KS
4.3
)
German
°dH*
English
°eH*
French
°fH*
1 mg/l CaCO
3
0.02 0.056 0.07 0.1
*Carbonate hardness (reference = Hydrogencarbonate-anions) Example: 10 mg/l CaCO3 = 10 mg/l x 0.056 = 0.56 °dH 10 mg/l CaCO3 = 10 mg/l x 0.02 = 0.2 mmol/l
4. CaCO3 °dH °eH °fH
°aH
Precision
An educated operator obtained under laboratory conditions exemplary for 2 different (one) standard solutions the following standard deviations using different lots of reagent:
140.00 ± 4.00 mg/l
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1.1 Methods
Calcium Hardness
0 – 500 mg/l CaCO
3
1. Select the method required on keypad.
2. Fill a clean vial (24 mm Ø) with 10 ml of the water sample, close tightly with the cap.
3. Place the vial in the sample chamber making sure that the marks are aligned.
4. Press ZERO key.
5. Remove the vial from the sample chamber.
6. Add one CALCIO H No. 1 tablet straight from the foil to the 10 ml water sample, crush the tablet using a clean stirring rod and dissolve the tablet completely.
7. Add one CALCIO H No. 2 tablet straight from the foil to the same water sample and crush the tablet using a clean stirring rod.
8. Close the vial tightly with the cap and swirl gently several times until the tablet is completely dissolved.
9. Place the vial in the sample chamber making sure that the marks are aligned.
10. Press TEST key.
Wait for a reaction period of 2 minutes.
After the reaction period is finished the measurement
starts automatically.
The result is shown in the display as Calcium Hard-
ness.
Zero accepted prepare Test press TEST
prepare Zero press ZERO
Countdown 2:00
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1.1 Methods
Notes:
1. To optimise the readings an optional batch related calibration can be performed using Mode 40, see page 58.
2. Strong alkaline or acidic water samples must be adjusted to a pH-value between pH 4 and 10 before the tablets are added (use 1 mol/l Hydrochloride acid resp. 1 mol/l Sodium hydroxide).
3. For accurate test results exactly 10 ml of water sample must be taken for the test.
4. This method was developed from a volumetric procedure for the determination of Calcium Hardness. Due to undefined conditions, the deviations from the standardised method may be greater.
5. The tolerance of the method is increasing with higher concentrations. When diluting samples, this should be taken in account, always measuring in the first third of the range.
6. Interferences:
• Magnesium hardness up to 200 mg/l CaCO3 does not interfere.
• Iron concentration above 10 mg/l may cause low results.
• Zinc concentration above 5 mg/l may cause high results.
7. CaCO
3
°dH °eH °fH °aH
Precision
An educated operator obtained under laboratory conditions exemplary for 2 different (one) standard solutions the following standard deviations using different lots of reagent:
100.00 ± 10.00 mg/l; 500.00 ± 50.00 mg/l
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1.1 Methods
Bromine
0.05 – 13 mg/l Br
2
1. Select the method required on keypad.
2. Fill a clean vial (24 mm Ø) with 10 ml of the water sample, close tightly with the cap.
3. Place the vial in the sample chamber making sure that the marks are aligned.
4. Press ZERO key.
5. Remove the vial from the sample chamber and empty
it, leaving a few drops remaining in the vial.
6. Add one DPD No. 1 tablet straight from the foil to the water sample and crush the tablet using a clean stirring rod.
7. Add the water sample to the 10 ml mark.
8. Close the vial tightly with the cap and swirl gently several times until the tablets are dissolved.
9. Place the vial in the sample chamber making sure that the marks are aligned.
10. Press TEST key.
The result is shown in the display as Bromine in mg/l.
prepare Zero press ZERO
Zero accepted prepare Test press TEST
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1.1 Methods
Notes:
1. Vial cleaning: As many household cleaners (e.g. dishwasher detergent) contain reducing substances, the subsequent determination of Bromine may show lower results. To avoid any measurement errors, only use glassware free of Chlorine demand. Preparation: Put all applicable glassware into Sodium hypochlorite solution (0.1 g/l) for one hour, then rinse all glassware thoroughly with deionised water.
2. Preparing the sample: When preparing the sample, the lost of Bromine, e.g. by pipetting or shaking, must be avoided. The analysis must take place immediately after taking the sample.
3. The DPD colour development is carried out at a pH value of 6.2 to 6.5. The reagent tablet therefore contains a buffer for the pH adjustment. Strong alkaline or acidic water samples must be adjusted between pH 6 and pH 7 before the reagent is added (use 0.5 mol/l Sulfuric acid resp. 1 mol/l Sodium hydroxide).
4. Exceeding the measuring range: Concentrations above 22 mg/l Bromine can lead to results showing 0 mg/l. In this case, the water sample must be diluted with water free of Bromine. 10 ml of the diluted sample should be mixed with the reagent and the measurement repeated.
Oxidising agents such as Chlorine, Ozone etc. interfere as they react in the same way as Bromine.
Precision
An educated operator obtained under laboratory conditions exemplary for 2 different (one) standard solutions the following standard deviations using different lots of reagent:
0.40 ± 0.04 mg/l; 5.00 ± 0.15 mg/l
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1.1 Methods
Ozone, in the absence of Chlorine
0.02 – 2 mg/l O
3
1. Select the method required on keypad.
2. Fill a clean vial (24 mm Ø) with 10 ml of the water sample, close tightly with the cap.
3. Place the vial in the sample chamber making sure that the marks are aligned.
4. Press ZERO key.
5. Remove the vial from the sample chamber and empty it, leaving a few drops remaining in the vial.
6. Add one DPD No. 1 and one DPD No. 3 tablet straight from the foil to the water sample and crush the tablets using a clean stirring rod.
7. Add the water sample to the 10 ml mark.
8. Close the vial tightly with the cap and swirl gently several times until the tablets are dissolved.
9. Place the vial in the sample chamber making sure that the marks are aligned.
10. Press TEST key.
Wait for a reaction period of 2 minutes.
After the reaction period is finished the measurement
starts automatically.
The result is shown in the display as Ozone in mg/l.
Note:
Instead of using DPD No. 1 plus DPD No. 3 you can use DPD No. 4.
prepare Zero press ZERO
Zero accepted prepare TEST press TEST
Countdown 2:00
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1.1 Methods
Notes:
1. Vial cleaning: As many household cleaners (e.g. dishwasher detergent) contain reducing substances, the subsequent determination of Ozone may show lower results. To avoid any measurement errors, only use glassware free of Chlorine demand. Preparation: Put all applicable glassware into Sodium hypochlorite solution (0.1 g/l) for one hour, then rinse all glassware thoroughly with deionised water.
2. Preparing the sample: When preparing the sample, the lost of Ozone, e.g. by pipetting or shaking, must be avoided. The analysis must take place immediately after taking the sample.
3. The DPD colour development is carried out at a pH-value of 6.2 to 6.5. The reagent tablet therefore contains a buffer for the pH adjustment. Strong alkaline or acidic water samples must be adjusted between pH 6 and pH 7 before the tablet is added (use 0.5 mol/l Sulfuric acid resp. 1 mol/l Sodium hydroxide).
4. Turbidity (can lead to errors): The use of the DPD No. 1 tablet in samples with high Calcium ion content* and/or high conductivity* can lead to turbidity of the sample and therefore incorrect measurements.
*it is not possible to give exact values, because the developement of turbidity depends on the nature of the sample.
5. Exceeding of the measuring range: Concentrations above 6 mg/l Ozone can lead to results showing 0 mg/l. In this case, the water sample must be diluted with water free of Ozone. 10 ml of the diluted sample should be mixed with the reagent and the measurement repeated.
Oxidising agents such as Bromine, Chlorine etc. interfere as they react in the same way as Ozone.
Precision
An educated operator obtained under laboratory conditions exemplary for 2 different (one) standard solutions the following standard deviations using different lots of reagent:
0.10 ± 0.02 mg/l; 1.50 ± 0.05 mg/l
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1.1 Methods
Free Copper
0.05 – 5 mg/l Cu
1. Select the method required on keypad.
2. Fill a clean vial (24 mm Ø) with 10 ml of the water sample, close tightly with the cap.
3. Place the vial in the sample chamber making sure that the marks are aligned.
4. Press ZERO key.
5. Remove the vial from the sample chamber.
6. Add one COPPER No. 1 tablet straight from the foil to the water sample and crush the tablet using a clean stirring rod.
7. Close the vial tightly with the cap and swirl gently several times until the tablet is dissolved.
8. Place the vial in the sample chamber making sure that the marks are aligned.
9. Press TEST key.
The result is shown in the display as free Copper in
mg/l.
Precision
An educated operator obtained under laboratory conditions exemplary for 2 different (one) standard solutions the following standard deviations using different lots of reagent:
0.30 ± 0.03 mg/l; 3.50 ± 0.07 mg/l
prepare Zero press ZERO
Zero accepted prepare Test press TEST
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1.1 Methods
Total Copper
0.05 – 5 mg/l Cu
1. Select the method required on keypad
2. Fill a clean vial (24 mm Ø) with 10 ml of the water sample, close tightly with the cap.
3. Place the vial in the sample chamber making sure that the marks are aligned.
4. Press ZERO key.
5. Remove the vial from the sample chamber.
6. Add one COPPER No. 1 tablet and one COPPER No. 2 tablet straight from the foil to the water sample and crush the tablets using a clean stirring rod.
7. Close the vial tightly with the cap and swirl gently several times until the tablet is dissolved.
8. Place the vial in the sample chamber making sure that the marks are aligned.
9. Press TEST key.
The result is shown in the display as Total Copper in
mg/l.
Precision
An educated operator obtained under laboratory conditions exemplary for 2 different (one) standard solutions the following standard deviations using different lots of reagent:
0.30 ± 0.03 mg/l; 3.50 ± 0.07 mg/l
prepare Zero press ZERO
Zero accepted prepare Test press TEST
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1.1 Methods
CyA-TEST (Cyanuric acid)
0 – 160 mg/l CyA
1. Select the method required on keypad
2. Fill a clean vial (24 mm Ø) with 5 ml of the water sample and 5 ml deionised water (Note 1), close tightly with the cap.
3. Place the vial in the sample chamber making sure that the marks are aligned.
4. Press ZERO key.
5. Remove the vial from the sample chamber.
6. Add one CyA-TEST tablet straight from the foil to the water sample and crush the tablet using a clean stirring rod.
7. Close the vial tightly with the cap and swirl gently several times until the tablet is dissolved.
8. Place the vial in the sample chamber making sure that the marks are aligned.
9. Press TEST key.
The result is shown in the display as Cyanuric Acid in
mg/l.
prepare Zero press ZERO
Zero accepted prepare Test press TEST
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1.1 Methods
Notes:
1. Use deionised water or tap water free of Cyanuric acid.
2. If Cyanuric acid is present a cloudy solution will occur. Small single particles are not necessarily caused by Cyanuric acid.
3. Dissolve the tablet completely (therefore swirl the vial approx. 1 Minute). Un-dissolved particles of the tablet can cause results that are too high.
Precision
An educated operator obtained under laboratory conditions exemplary for 2 different (one) standard solutions the following standard deviations using different lots of reagent: 0 – 50 ± 10 mg/l; 50 – 100 ± 15 mg/l; 100 – 160 ± 20 mg/l
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Water Balance (Langelier Saturation Index)
When water is in balance, it is said to be neither corrosive nor scale-forming. In other words, it will not deposit a layer of calcium scale neither will it dissolve an existing layer of scale.
For Langelier calculation the following tests are required:
• pH Value
• Temperature
• Calcium hardness
• Total Alkalinity
• TDS (Total Dissolved Solids) Run each test separately and note the results.
Calculate the Langelier Saturation Index as described below:
Calculation of Water Balance (Langelier Saturation Index):
If you want to enter values like 7.5 use the store key as decimal point. With Mode 71 (see below) it is possible to select between degree Celsius or degree Fahren-
heit.
Press [Balance] key
The display shows:
Enter the temperature value (T) in the range between 3 and 53°C and confirm with [ ] key.
If °F was selected, enter the temperature value in the range between 37 and 128°F.
The display shows:
Enter the value for Calcium hardness (CH) in the range bet­ween 50 and 1000 mg/l CaCO3 and confirm with [ ] key.
The display shows:
Enter the value for Total Alkalinity (TA) in the range between 5 and 800 mg/l CaCO3 and confirm with [ ] key.
The display shows:
Enter the value for TDS (Total Dissolved Solids) in the range between 0 and 6000 mg/l and confirm with [ ] key.
calcium hardness 50<=CH<=1000 +_ _ _ _
<Langelier> temperature °C: 3°C <=T<=53°C +_ _ _ _
tot. alkalinity 5<=TA<=800 +_ _ _ _
total dissol. solids 0<=TDS<=6000 +_ _ _ _
Balance
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The display shows:
Enter the pH Value in the range between 0 and 12 and confirm with [ ] key.
The display shows the Langelier Saturation Index.
Press [ ] key to start new calculation.
Return to mode menu by pressing [ESC] key.
Operating error:
Values out of defined range:
The entered value is too high.
The entered value is too low.
Confirm display message with [ ] key and enter a value in the defined range.
Notes:
If the index is zero the water is in perfect balance. If the index is minus the water is aggressive and tends to be corrosive. If the index is positive the water is non aggressive but could be scale-forming.
For Swimming pool water an index value in the range of zero to + 0.3 is considered satisfactory.
Selection of temperature unit
Entering the temperature value is possible in degrees Celsius or degrees Fahrenheit. Therefore the following preselection is (once) required.
Press [MODE] [7] [1] keys.
Confirm with [ ] key.
The display shows:
Press [1] key to select degrees Celsius.
Press [2] key to select degrees Fahrenheit. The instrument goes back to mode menu automatically.
pH value 0<=pH<=12 +_ _ _ _
<Langelier> Langelier saturation index 0,00 Esc
CH<=1000 mg/l CaCO3!
CH>=50 mg/l CaCO3!
Mode
2
1
1
7
<temperature> 1: °C 2: °F
Examples:
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Guidelines for photometric measurements
1. Vials, caps and stirring rods should be cleaned thoroughly after each analysis to prevent interferences. Even minor reagent residues can cause errors in the test result.
2. The outside of the vial must be clean and dry before starting the analysis. Clean the outside of the vials with a towel. Fingerprints or other marks will be removed.
3. If there is no defined vial for the blank, the zeroing and the test must be carried out with the same vial as there may be slight differences in optical performance between vials.
4. The vials must be positioned in the sample chamber for zeroing and test with the mark on the vial aligned with the mark on the instrument.
5. Always perform zeroing and test with closed vial cap. Only use cap with sealing ring.
6. Bubbles on the inside of the vial may also lead to errors. To prevent this, remove the bubbles by swirling the vial before performing the test.
7. Avoid spillage of water in the sample chamber. If water should leak into the instrument housing, it can destroy electronic components and cause corrosion.
8. Contamination of the lens in the sample chamber can result in errors. Check at regular intervals and – if necessary – clean the light entry surfaces of the sample chamber using a moist cloth or cotton buds.
9. Large temperature differences between the instrument and the environment can lead to errors – e.g. due to the formation of condensation in the area of the lens or on the vial.
10. To avoid errors caused by stray light do not use the instrument in bright sunlight.
Correct position of the vial (ø 24 mm):
Correct filing of the vial:
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Part 2
Operator manual
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2.1 Operation
2.1.1 Commissioning
Before working with the photometer insert the rechargeable batteries and the Lithium battery (included with instrument). The rechargeable batteries are not charged. See chapter 2.1.2 Saving data – Important Notes, 2.1.3 Replacement of rechargeable batteries resp. Lithium battery. and 2.1.4 Charging the rechargeable batteries.
Before using the photometer perform the following settings in the Mode-Menu:
• MODE 10: select language
• MODE 12: set date and time
• MODE 34: perform „Delete data“
See chapter 2.4 Photometer settings.
2.1.2 Saving data – Important Notes
The Lithium battery saves data (stored results and photometer setting) if there is no power from the power supply from the rechargeable batteries or the mains adapter. Recommendation: Change the lithium battery every 5 years. Note: When neither mains adapter nor batteries supply energy to the instrument, all stored data and settings will be lost if the lithium battery is taken out. Recommendation: Keep the instrument connected to mains adapter supply while changing the lithium battery to maintain stored data.
2.1.3 Replacement of rechargeable batteries and/or Lithium-
battery
1. Switch the instrument off.
2. If necessary remove vial from the sample chamber.
3. Place the instrument upside down on a clean and even surface.
4. Unscrew the two screws (A) of the battery compartment cover (B).
5. Lift off battery compartment cover.
6. If necessary remove old rechargeable batteries (C) and/or the Lithium-battery (D) (See 2.1.4).
7. Place 7 new rechargeable batteries and/or the Lithium-battery.
Ensuring the correct polarity!
8. Replace the battery compartment cover.
9. Tighten the screws carefully.
CAUTION
Dispose of used rechargeable batteries and Lithium-batteries in accordance with all legal requirements.
2.1.4 Charging the rechargeable batteries
The rechargeable batteries are charged in the instrument. As soon the photometer is connected with the mains adapter to the mains the rechargeable batteries are charged. Empty rechargeable batteries should be charged in the instrument for at least 5 days. 10 charging and discharging cycles are necessary before the rechargeable batteries obtain their full capacity.
it is possible to operate the instrument with the adapter with or without inserted rechargeable batteries.
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2.1.5 Fuse
The instrument contains a fuse (E) (type: 1 A, inert, 20 mm). If an replacement is necessary proceed as described in “Replacement of rechargeable batteries resp. Lithium-battery". If the instrument can be operated with the mains adapter but not with the rechargeable batteries, the fuse could be defective (try new rechargeable batteries first).
2.1.6 Protective caps
If not in use protect the two connections against damage (e.g. corrosion) caused by environmental influences (e.g. dust or splashing) keep the protective caps in place (G).
2.1.7 Instrument view
(A) screws (B) battery compartment cover (C) rechargeable batteries 7 Ni-MH-rechargeable batteries (Typ AA, 1100 mAh) (D) battery Lithium-battery (Type CR 2032, 3V) (E) fuse 1 A, inert, 20 mm (F) instrument
(B) battery compartment cover
(C) rechargeable batteries
(D) battery
(E) fuse
(F) instrument back
(G) connections
protective caps
(A) screws
power supply
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2.2 Overview of function keys
Switching the photometer on or off
Returning to selection of methods or previous menu
Send data to printer
Confirming - 'enter'
Menu of photometer settings and further functions
Moving the cursor “>>” up or down
Storing of displayed test result
Performing Zero or used as number key
Performing Test
Water balance calculation key
Print
Esc
ON OFF
Mode
Store
Zero
Test
Balance
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2.3 Operation mode
Switch the photometer on by pressing the [ON/OFF] key.
The photometer performs an electronic self-test.
2.3.1 Automatic switch off
The instrument switches off automatically after 20 minutes. This is indicated 30 seconds before by a beeper. Press any key to avoid the instrument switching off. As long as the instrument is working (for example countdown or printing) the automatic switch off is inactive.
2.3.2 Selecting a method
The display shows:
Select method you require by pressing one of the 9 keys as below:
2.3.3 Blank because of technical requirements
2.3.4 Performing Zero
The display shows:
Prepare a clean vial as described in Methode" and place the vial in the sample chamber and making sure that the marks are aligned.
Press [ZERO] key.
The display shows:
Autotest ...
select
method
Prepare zero press zero
Zero accepted prepare Test press TEST
Zero
ON OFF
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2.3.5 Performing Tests
When zero calibration is complete, remove the vial from the sample chamber and perform the tests as described under "Method".
When the results have been displayed:
• with some methods you can change between different chemical species
• you can store and/or print out the results
• perform further analysis with the same zero
• select a new method
2.3.6 Ensuring reaction periods (countdown)
To ensure compliance with reaction periods there is incorporated a time delay, the countdown.
• Press [TEST] key. Prepare the water sample/blank as described in the method description and place the vial in the sample chamber. The display shows the countdown by pressing the [TEST] key and the countdown is started automatically. After the reaction period is finished the reading starts automatically.
Notes:
1. It is possible to finish the working countdown by pressing the [ ] key. Reading starts immediately. In this case the operator is responsible for ensuring the necessary reaction period by himself.
Non-compliance with reaction periods leads to incorrect test results.
2. The time remaining is displayed continuously. The beeper indicates the last 10 seconds.
2.3.7 blank because of technical requirements
Test
Countdown 1:59
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2.3.8 Storing results
Press [STORE] key while the test result is displayed.
The display shows:
• We advise you to enter a numeric code (up to 6 places). (A Code No. can contain references to the operator or the sample-taking place.)
After entering confirm with [ ] key.
• If a code number is not necessary confirm by pressing [ ] directly. (The assignment for the Code No. is then 0 automatically.)
The entire data set is stored with date, time, Code No., method and test result.
The display shows:
The test result is then shown again.
Note:
The display shows the number of free data sets.
If there are less than 30 data sets free the display shows:
Clear the memory as soon as possible (see “Deleting stored results”). If memory capacity is used up it is impossible to save additional test results.
Stored!
Storage: only 29 free records left
Storage: 900 free records left
Code No.: _ _ _ _ _ _
Store
0 0 0 0 01
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2.3.9 Printing results
If a printer is installed and switched on, it is possible to print out the test results (without saving it beforehand).
Press [Print] key.
The entire data set is printed with date, time, Code No., method and test result. Printing example:
Chlorine T
0.01-6 mg/l Cl2 Profi-Mode: no 2008-07-01 14:53:09 Test No.: 1 Code No.: 007
4.80 mg/l free Cl
2
The test No. is an internal number that is set automatically if a test result is stored. It appears only on the print out.
2.3.10 Perform additional measurements
To perform additional tests using the same method:
• Press [TEST] key
The display shows:
Confirm with [TEST] key
or
• Press [ZERO] key to perform a new zero calibration.
The display shows:
2.3.11 Selecting a new method
Press [ESC] key to return to method selection.
Test
Test
Zero accepted prepare Test press TEST
Zero
prepare Zero press ZERO
Esc
Print
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2.4 Photometer settings: Table of Mode Functions
MODE-Function No. Description Page
Abs Measurement 51 Measuring the absorbance 65
Calibration 40 Special method calibration 58
Clear calibration 46 Deleting user calibration 62
Clock 12 Setting date and time 47
Countdown 13
Switching the countdown on/off to ensure reaction times
48
Delete data 34 Deleting all stored results 57
Key beep 11
Switching the acoustic signal on/off to indicate key-pressing
46
Langelier 70
Calculation of Langelier saturation Index (Water Balance)
66
Temperature 71 Selection of °C or °F for Langelier Mode 70 67
Language 10 Selecting language 45
LCD contrast 80 Setting the display contrast 68
OTZ 55 One Time Zero (OTZ) 65
Print 20 Printing all stored results 49
Print code no. 22 Print only results of a selected code no. range 51
Print date 21 Print only results of a selected time period 50
Print method 23 Print only results of one selected method 52
Printing parameters
29 Setting of printing options 53
Profi-Mode 50 Switching the detailed operator instructions on/off 63
Signal beep 14
Switching the acoustic signal on/off to indicate end of reading
48
Storage 30 Displaying all stored results 54
Storage Code No. 32 Displaying only results of a selected code no. range 56
Storage date 31 Displaying only results of a selected time period 55
Storage method 33 Displaying only results of one selected method 57
System info 91
Information about the instrument e.g. current software version
68
User calibration 45 Storage of user calibration 61
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2.4.1 Blank because of technical requirements
2.4.2 Instrument basic settings 1
Selecting a language
Press [MODE] [1] [0] keys in sequence.
Confirm with [ ] key.
The display shows:
Press arrow key [ ] or [ ] to select the required language from the displayed list.
Confirm with [ ] key.
Mode
1
0
<Language> Deutsch >> English Francais
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Key beep
Press [MODE] [1] [1] keys in sequence.
Confirm with [ ] key.
The display shows:
• Press [0] key to switch the key beep off.
• Press [1] key to switch the key beep on.
Confirm with [ ] key.
Note:
In the case of methods with reaction periods, an acoustic signal still sounds during the last 10 seconds of the countdown even if the key beep is switched off.
<Key Beep> ON: 1 OFF: 0
Mode
1
1
1
0
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Setting Date and time
Press [MODE] [1] [2] keys in sequence.
Confirm with [ ] key.
The display shows:
The entry comprises two digits each.
Enter year, month and day,
e.g.: 14. May 2008 = [0][8][0][5][1][4]
Enter hours and minutes
e.g.: 3.07 p.m. = [1][5][0][7]
Confirm with [ ] key.
Note:
While confirming date and time with [ ] key the seconds are adjusted to zero automatically.
Mode
1
2
<clock> yy-mm-dd hh:mm _ _-_ _-_ _ _ _:_ _
yy-mm-dd hh:mm 08-05-14 _ _:_ _
yy-mm-dd hh:mm 08-05-14 15:07
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Countdown (Ensuring reaction periods)
Some methods require a reaction period. This reaction period is incorporated in the method as standard with the countdown function. It is possible to switch the countdown off for all methods:
Press [MODE] [1] [3] keys in sequence.
Confirm with [ ] key.
The display shows:
• Press [0] key to switch the countdown off.
• Press [1] key to switch the countdown on.
Confirm with [ ] key.
Notes:
1. It is possible to interrupt the working countdown by pressing the [ ] key (application e.g. serial analysis). The “user countdown” is also available if the countdown is switched off.
2. If the countdown function is switched off, the operator is responsible for ensuring the necessary reaction period. Non-compliance with reaction periods leads to incorrect
test results.
Signal beep
Performing a zero or a measurement takes 8 seconds. The photometer indicates the end of zeroing or measuring by a short beep.
Press [MODE] [1] [4] keys in sequence.
Confirm with [ ] key.
The display shows:
<Countdown> ON: 1 OFF: 0
Mode
1
3
1
0
<Signal Beep> ON: 1 OFF: 0
Mode
1
4
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Press [0] key to switch the signal beep off.
Press [1] key to switch the signal beep on.
Confirm with [ ] key.
Note:
In the case of methods with reaction periods, an acoustic signal still sounds during the last 10 seconds of the countdown even if the key beep / signal beep is switched off.
2.4.3 Printing of stored results
Printing all results
Press [MODE] [2] [0] keys in sequence.
Confirm with [ ] key.
The display shows:
Press [ ] key for printing out all stored test results.
The display shows e.g.:
After printing the photometer goes back to <Mode Menu> automatically.
Note:
It is possible to cancel the entry by [ESC]. All stored data are printed out.
<Print> Print all Data Start: cancel: ESC
Test No.:
1
0
Mode
2
0
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Printing results of a selected time period
Press [MODE] [2] [1] keys in sequence.
Confirm with [ ] key.
The display shows:
Enter year, month and day for the first day of the required period, e.g.: 14 May 2008 = [0][8][0][5][1][4]
Confirm with [ ] key.
The display shows:
Enter year, month and day for the last day of the required period, e.g.: 19 May 2008 = [0][8][0][5][1][9]
Confirm with [ ] key.
The display shows:
Press [ ] key and all stored results in the selected date range are printed.
After printing the photometer goes back to mode menu automatically.
Note:
It is possible to cancel the entry by [ESC]. If you want to print only results of one day enter the same date twice to determine the period.
<Print> sorted: date from yy-mm-dd __-__-__
from yy-mm-dd __-__-__
from 2008-05-14 to 2008-05-19 Start: cancel: ESC
Mode
2
1
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Printing results of a selected Code No. range
Press [MODE] [2] [2] keys in sequence.
Confirm with [ ] key.
The display shows:
Enter numeric code number (up to 6 places) for the first required Code No., e.g.: [1].
Confirm with [ ] key.
The display shows:
Enter numeric code number (up to 6 places) for the last required Code No., e.g.: [1] [0].
Confirm with [ ] key.
The display shows:
Press [ ] key and all stored results in the selected Code number range are printed.
After printing the photometer goes back to mode menu automatically.
Note:
It is possible to cancel the entry by [ESC]. If you want to print only results of one code number enter the same code number twice. If you want to print all results without code no. (code no. is 0) enter Zero [0] twice.
Mode
2
2
from 000001 to 000010 Start: cancel: ESC
<Print> sorted: Code No. from_ _ _ _ _ _
to _ _ _ _ _ _
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Printing results of one selected method
Press [MODE] [2] [3] keys in sequence.
Confirm with [ ] key.
The display shows:
Select the required method from the keypad
The display shows:
Press [ ] key and all stored results of the selected method are printed.
After printing the photometer goes back to mode menu automatically.
<Print> select method
<Print> method Alkalinity-total Start: cancel: ESC
Mode
2
3
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Printing Parameter
Press [MODE] [2] [9] keys in sequence.
Confirm with [ ] key.
The display shows:
Press [1] key to select ”Protocol”.
The display shows:
Press arrow key [ ] or [ ] to select the required Protocol (Xon/Xoff, Hardware, no control)
Confirm with [ ] key.
Finish with [ESC] key. Flow Control will be set to the selection displayed at "is".
Press [2] key to select ”Baud rate”.
The display shows:
Mode
2
9
Esc
1
2
<printing parameter> 1: Flow control 2: Baud rate
cancel: ESC
<Flow Control> is: Hardware select: [ ] [ ] save: cancel: ESC
<Baud rate> is: 19200 select: [ ] [ ] save: cancel: ESC
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Press arrow key [ ] or [ ] to select the required Baud rate. (600, 1200, 2400, 4800, 9600, 14400, 19200)
Confirm with [ ] key.
End with [ESC] key.
Back to Mode Menu with [ESC] key.
Back to Method selection with [ESC] key.
Note:
Select “Hardware” as Protocol and “9600” as Baud rate if you use the printer DP 2335. For setting of the printer see chapter 2.5.1 Connection to a printer.
2.4.4 Recall / delete stored results
Recall all stored results
Press [MODE] [3] [0] keys in sequence.
Confirm with [ ] key.
The display shows:
The stored data sets are displayed in chronological order, starting with the latest stored test result. Press [ ] key and all stored results are displayed.
Press [Print] key to print the displayed result.
End with [ESC].
Press arrow key [ ] to display the following test result.
Press arrow key [ ] to display the previous test result.
If there are no test results in memory the display shows:
Mode
3
0
no data
<Storage> display all data Start: cancel: ESC print: Print
Esc
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Recall results of a selected time period
Press [MODE] [3] [1] keys in sequence.
Confirm with [ ] key.
The display shows:
Enter year, month and day for the for the first day of the required period, e.g.: 14 May 2008 = [0][8][0][5][1][4]
Confirm with [ ] key.
The display shows:
Enter year, month and day for the last day of the required period, e.g.: 19 May 2008 = [0][8][0][5][1][9]
Confirm with [ ] key.
The display shows:
Press [ ] key and all stored results in the selected date range are displayed.
Press [Print] key to print the displayed result.
End with [ESC].
Notes:
It is possible to cancel the entry by [ESC]. If you want to recall only results of one day enter the same date twice to determine the time period.
<Storage> sorted: date from yy-mm-dd __-__-__
Mode
3
1
from yy-mm-dd __-__-__
from 2008-05-14 to 2008-05-19 Start: cancel: ESC print: Print
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Recall results of a selected Code No. range
Press [MODE] [3] [2] keys in sequence.
Confirm with [ ] key.
The display shows:
Enter numeric code number (up to 6 places) for the first required Code No., e.g.: [1].
Confirm with [ ] key.
The display shows:
Enter numeric code number (up to 6 places) for the last required Code No., e.g.: [1] [0].
Confirm with [ ] key.
The display shows:
Press [ ] key and all stored results in the selected Code No. range are displayed.
Press [Print] key to print the displayed result.
End with [ESC].
Notes:
It is possible to cancel the entry by [ESC]. If you want to recall only results of one code number enter the same code number twice. If you want to recall all results without code no. (code no. is 0) enter Zero [0] twice.
Mode
3
2
<Storage> sorted: Code No. from_ _ _ _ _ _
to _ _ _ _ _ _
from 000001 to 000010 Start: cancel: ESC print: Print
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Recall results of one selected method
Press [MODE] [3] [3] keys in sequence.
Confirm with [ ] key.
The display shows:
Select the required method from the keypad
The display shows:
• Press [ ] key and all stored results of the selected method are displayed.
Press [Print] key to print the displayed result.
End with [ESC].
<Storage> select method
Mode
3
3
<Storage> method Alkalinity-total Start: cancel: ESC print: Print
Delete stored results
Press [MODE] [3] [4] keys in sequence.
Confirm with [ ] key.
The display shows:
• Press [0] key to retain the data sets in memory.
• After pressing key [1] the following acknowledgment is displayed:
Press [ ] key to delete.
ATTENTION: All stored test results are deleted
or cancel without deleting data by pressing [ESC] key.
Note:
All stored test results are deleted.
Mode
3
4
<Delete data> Delete all data? YES : 1 NO : 0
1
0
<Delete data> Delete data Do not delete: ESC
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2.4.5 Calibration
Calcium Hardness Method – Calibration of a method blank
Press [MODE] [4] [0] keys in sequence.
Confirm with [ ] key.
The display shows:
Press [1] key.
The display shows:
1. Fill a clean vial (24 mm Ø) with exactly 10 ml of deio- nised water, close tightly with the cap.
2. Place the vial in the sample chamber making sure that the marks are aligned.
3. Press ZERO key.
4. Remove the vial from the sample chamber.
5. Pipette 100 ml of water free of calcium to an appropriate beaker (note 2, 3).
6. Add 10 CALCIO H No. 1 tablets straight from the foil to the 100 ml of water, crush the tablets using a clean stirring rod and dissolve the tablets completely.
7. Add 10 CALCIO H No. 2 tablets straight from the foil to the same water, crush the tablets using a clean stirring rod and dissolve the tablets completely.
8. Press [ ] key.
Wait for a reaction period of 2 minutes.
After the reaction period is finished proceed as follows:
<Calibration> M191 Calcium Hardness 2T prepare ZERO press ZERO
<Calibration> 1: M191 Ca-Hardness 2 2: M191 0 Jus. Reset
Mode
4
0
1
Zero accepted Countdown 2:00 start:
Zero
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9. Rinse the vial (24 mm Ø) with the coloured sample from the beaker and fill with 10 ml of the sample.
10. Press TEST key.
The batch related method blank is saved.
Press [ ] key,
to go back to mode menu.
Notes:
1. If a new batch of CALCIO tablets is used a calibration of the method blank has to be performed to optimise the results.
2. Deionised or tap water
3. If no water free of Calcium is available these ions can be masked by using EDTA. Preparation: Add 50 mg (a spatula-tipful) EDTA to 100 ml water and dissolve.
4. To achieve the most accurate method blank it is important to adhere exactly to the sample volume of 100 ml.
Calcium Hardness Method – Reset method blank to factory calibration
Press [MODE] [4] [0] keys in sequence.
Confirm with [ ] key.
The display shows:
Press [2] key.
The display shows:
Press [0] key to keep the method blank.
Press [1] key to erase the method blank and set the value back to factory calibration.
The instrument goes back to mode menu automatically.
<Calibration> M191 Calcium Hardness 2T Reset? YES: 1, NO: 0
<Calibration> 1: M191 Ca-Hardness 2 2: M191 0 Jus. Reset
Mode
4
0
2
0
1
prepare TEST press TEST
stored
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User Calibration
If a test method is user calibrated the method name is displayed inverse.
Procedure:
• Prepare a standard of known concentration and use this standard instead of the sample according to the test procedure.
• It is recommend to use well known standards which are formulated according to DIN EN, ASTM or other international norms or to use certified standards which are commercially available.
• After measuring this standard solution it is possible to change the displayed results to the required value.
• If a method uses a mathematic equation for the calculation of the result, it is only possible to calibrate the basic tests since all the other tests use the same polynomial.
• The same applies for some test procedures which use a polynomial from another test procedure.
Return to factory calibration: If the user calibration is deleted the factory calibration is automatically activated.
Table
Method Recommended range for user user-calibration
Alkalinity-total 50–150 mg/l CaCO
3
Bromine Calibration with basic test Chlorine free Chlorine, free 0,5–1,5 mg/l Cl
2
Chlorine, total Calibration with basic test Chlorine free CyA-TEST 30–60 mg/l CyA Hardness, Calcium 100–200 mg/l CaCO
3
Copper 0,5–1,5 mg/l Cu Ozone (DPD) Calibration with basic test Chlorine free pH-Value 7,6–8,0
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Store user calibration
Perform the required method as described in the manual using a standard of know concentration instead of the water sample.
If the test result is displayed press [MODE] [4] [5] keys in sequence and confirm with [ ] key.
The display shows:
Pressing the arrow key [ ] once increases the displayed result.
Pressing the arrow key [ ] once decreases the displayed result.
Press keys as long as the displayed result corresponds to the value of the standard.
Confirm with [ ] key to store the new calibration factor.
Cancel user calibration by pressing [ESC] key.
The display shows:
Now the method name is displayed inverse and the test result is calculated with the new calibration factor.
Mode
4
5
Chlorine T
0.01-6 mg/l Cl2
0.90 mg/l free Cl2
<user calibration> Chlorine T
0.01-6 mg/l Cl2
0.90 mg/l free Cl2 up: , down: save:
Jus Factor saved
Chlorine T
0.01-6 mg/l Cl2
1.00 mg/l free Cl2
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Delete user calibration
This chapter only applies for methods which can be user calibrated.
Select the required method.
Instead of zeroing the instrument press [MODE] [4] [6] keys in sequence and confirm with [ ] key.
The display shows:
Press [1] key to delete user calibration.
Press [0] key to keep the valid user calibration.
The instrument goes back to Zero-query automatically.
Mode
<user calibration> Chlorine T
0.01-6 mg/l Cl2
clear user calibration? YES: 1, NO: 0
Chlorine T
0.01-6 mg/l Cl2
0
1
6
4
prepare ZERO press ZERO
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2.4.6 Lab functions
Reduced operator guidance => “Profi-Mode“
This function may be used for routine analyses with many samples of one method. The following information is always stored in the methods:
a) Method b) Range c) Date and time d) Detailed operator instruction e) Compliance with reaction periods
If the Profi-Mode is active, the photometer provides only a minimum of operator instructions. The criteria specified above in d, e are no longer included.
Press [MODE] [5] [0] keys in sequence.
Confirm with [ ] key.
The display shows:
• Press [0] key to switch the Profi-Mode off.
• Press [1] key to switch the Profi-Mode on.
The display shows:
Confirm with [ ] key.
Note:
Storage of test results is possible. When results are stored the display shows “Profi-Mode”. The selected settings are kept by the photometer even when it is switched off. To change photometer setting a new setting is required.
Mode
5
0
<Profi-Mode> ON : 1 OFF : 0
1
0
switched off
or
switched on
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Measuring the absorbance
Press [MODE] [5] [1] keys in sequence.
Confirm with [ ] key.
Enter the required wavelength, e.g.: [2] for 560 nm.
The display shows:
Place a vial with the blank (e.g. deionised water) into the sample chamber.
Press [Zero] key.
The display shows:
Place the vial with the coloured test solution into the sample chamber.
Press [Test] key.
The result is shown in the display in mAbs. 1000 mAbs = 1 A (Absorbance unit)
Press [ESC] key to get back to wavelength selection. Press [ESC] again to get back to mode menu.
Note:
1. It is not possible to print or store the test results.
2. Range: -2600 mAbs to +2600 mAbs
< Abs Measurement > choose wavelength: 1: 530 nm 2: 560 nm 3: 610 nm
< Abs Measurement > 560 nm
prepare Zero press ZERO
Zero accepted prepare Test press TEST
__ mAbs
2
Mode
5
1
Esc
Test
Zero
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One Time Zero (OTZ)
OneTimeZero is available for all methods where zero is performed in a 24 mm Ø round vial with sample water (see chapter 1.1 Table of Methods).
OneTimeZero can be used for different tests providing the tests are performed with the same sample water and under the same test conditions. When changing the method, it is not necessary to perform a new Zero. The test can be carried out straight away.
When the instrument is first being used for an OTZ compatible method and OneTimeZero is activated, the instrument will request a new Zero with “prepare OT-Zero”. Perform Zero as described in the method. This Zero will be stored and used for all methods with OTZ function until the instrument is switched off.
If necessary, a new Zero can be performed by pressing [Zero] key at any time.
Switching the “OTZ-Function“ on and off:
Press [MODE] [5][5] keys in sequence.
Confirm with [ ] key.
The display shows:
• Press [0] key to switch the OTZ off.
• Press [1] key to switch the OTZ on.
The display shows:
Confirm with [ ] key.
The instrument goes back to mode menu automatically.
Note:
The specified accuracy is valid for all test results when Zero is performed for each test (OneTimeZero function is switched off).
2.4.7 blank because of technical requirements
Mode
5
5
<OneTimeZero> ON : 1 OFF : 0
1
0
switched off
or
switched on
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2.4.8 User operations
Langelier Saturation Index (Water Balance)
For Langelier calculation the following tests are required:
• pH Value
• Temperature
• Calcium hardness
• Total Alkalinity
• TDS (Total Dissolved Solids)
Run each test separately and note the results. Calculate the Langelier Saturation Index as described below:
Calculation of Water Balance (Langelier Saturation Index):
If you want to enter values like 7.5 use the store key as decimal point. With Mode 71 (see below) it is possible to select between degree Celsius or degree Fahren-
heit.
Press [MODE] [7] [0] keys in sequence.
Confirm with [ ] key.
The display shows:
Enter the temperature value (T) in the range between 3 and 53°C and confirm with [ ] key.
If °F was selected, enter the temperature value in the range between 37 and 128°F.
The display shows:
Enter the value for Calcium hardness (CH) in the range bet­ween 50 and 1000 mg/l CaCO3 and confirm with [ ] key.
The display shows:
Enter the value for Total Alkalinity (TA) in the range between 5 and 800 mg/l CaCO3 and confirm with [ ] key.
The display shows:
Enter the value for TDS (Total Dissolved Solids) in the range between 0 and 6000 mg/l and confirm with [ ] key.
Mode
7
0
calcium hardness 50<=CH<=1000 +_ _ _ _
<Langelier> temperature °C: 3°C <=T<=53°C +_ _ _ _
tot. alkalinity 5<=TA<=800 +_ _ _ _
total dissol. solids 0<=TDS<=6000 +_ _ _ _
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The display shows:
Enter the pH Value in the range between 0 and 12 and confirm with [ ] key.
The display shows the Langelier Saturation Index.
Press [ ] key to start new calculation.
Return to mode menu by pressing [ESC] key.
Operating error:
Values out of defined range:
The entered value is too high.
The entered value is too low.
Confirm display message with [ ] key and enter a value in the defined range.
Notes:
If the index is zero the water is in perfect balance. If the index is minus the water is aggressive and tends to be corrosive. If the index is positive the water is non aggressive but could be scale-forming.
For Swimming pool water an index value in the range of zero to + 0.3 is considered satisfactory.
Selection of temperature unit
Entering the temperature value is possible in degrees Celsius or degrees Fahrenheit. Therefore the following preselection is (once) required.
Press [MODE] [7] [1] keys in sequence.
Confirm with [ ] key.
The display shows:
Press [1] key to select degrees Celsius.
Press [2] key to select degrees Fahrenheit. The instrument goes back to mode menu automatically.
pH value 0<=pH<=12 +_ _ _ _
<Langelier> Langelier saturation index 0,00 Esc
CH<=1000 mg/l CaCO3!
CH>=50 mg/l CaCO3!
Mode
2
1
1
7
<temperature> 1: °C 2: °F
Examples:
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2.4.9 Instrument basic settings 2
Adjusting display contrast
Press [MODE] [8] [0] keys in sequence.
Confirm with [ ] key.
The display shows:
• Press arow key [ ] to increase contrast of the LCD
display.
• Press arrow key [ ] to decrease contrast of the LCD
display.
Confirm with [ ] key.
2.4.10 Instrument special functions / service
Photometer-Information
Press [MODE] [9] [1] keys in sequence.
Confirm with [ ] key.
This method informs you about the current software version, about the current detected mains power supply, about the number of performed tests and free memory capacity.
Press arrow key [ ] to display the number of performed tests and free memory capacity.
Finish with [ESC] key.
<LCD contrast>
<System-Info> Software: V012.002.3.003.002 mains power: yes more: , cancel: Esc
<Sysem-Info> Number of Tests: 139 free records left 999 cancel: Esc
Mode
8
0
Mode
9
1
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2.5 Data transfer
Switch the photometer and the personal computer or printer off. Connect the photometer (RS232 interface) and the serial interface of the personal computer or printer using a cable in line with the specified assignment (see technical data). The cable for connection to a personal computer is included in delivery contents.
2.5.1 Connection to a printer
Print with a serial connection are suitable for connection with the photometer (see chapter 3.4 Technical data interface).
A suitable paper tabel printer is the printer DPN 2335.
Before using the printer DPN 2335 with the Photometer you should change the following standard adjustments: (Detailed information of changing the adjustment you will find in the printer manual).
Baudrate: 9600 Parity: None Data bits: 8
Note: The printer must be connected and switched on before printing.
Caution: Adjust printing parameter in Mode 29. See chapter 2.4.3 Printing of stored
results.
2.5.2 Data transfer to a personal computer
Transferring test results from the photometer to a personal computer requires a transfer program, e.g. HyperTerminal. Please find detailed information at our homepage on the download-area.
2.5.3 Internet Updates
It is possible to update new software applications and additional languages via the internet. Please find detailed information at our homepage in the download-area.
Remark:
To prevent loss of stored test results store or print them out before performing an Update.
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Part 3
Enclosure
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3.1 Unpacking
Carefully inspect all items to ensure that every part of the list below is present and no visible damage has occurred during shipment. If there is any damage or something is missing, please contact your local distributor immediately.
3.2 Contents
Standard contents for PoolDirect 9in1:
1 Photometer in plastic case 2 Protective caps for connections 1 Rechargeable battery set (7 Ni-MH cells; Type AA; 1100 mAh) 1 Lithium battery (CR 2032; 3V) 1 Mains adapter, 100 – 240 V, 50 – 60 Hz 1 Cable for connection to PC 3 Round vials with cap and seal, height 48 mm, ø 24 mm 1 Beaker cup, plastic, 100 ml 1 Cleaning brush 1 Stirring rod, plastic 1 Syringe, plastic, 5 ml 1 Instruction manual 1 Guarantee declaration
Tablet reagents:
DPD No. 1 – 2 x 100 tablets DPD No. 3 – 100 tablets DPD No. 4 – 100 tablets PHENOL RED PHOTOMETER – 100 tablets CyA-TEST – 100 tablets ALKA-M-PHOTOMETER – 100 tablets CALCIO H No. 1 – 50 tablets CALCIO H No. 2 – 50 tablets COPPER No.1 – 100 tablets COPPER No.2 – 100 tablets
3.3 blank because of technical requirements
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3.4 Technical data
Display Graphic Display (7-line, 21-characters) Serial Interface serial RS232 for printer- and PC-connection;
9-pin D-sub-mail connector, data format ASCII, 8-bit Data, no parity, 1 start-bit, 1 stop-bit, baud rate and protocol: adjustable
Pin assignation: Pin 1 = free Pin 6 = free Pin 2 = Rx Data Pin 7 = RTS Pin 3 = Tx Data Pin 8 = CTS Pin 4 = free Pin 9 = free Pin 5 = GND
Light source LEDs and photo sensor amplifier in protected cell compartment. Wave length ranges: 1 = 530 nm IF = 5 nm 2 = 560 nm IF = 5 nm 3 = 610 nm IF = 6 nm IF = Interference filter
Photometric 0.100 Abs ± 0.008 Abs accuracy* 1.000 Abs ± 0.020 Abs
Operation Acid and solvent resistant touch-sensitive keyboard with integral beeper as acoustic indicator.
Power supply 7 Ni-MH cells (Type AA with 1100 mAh); external main adapter (Input: 100 –240 V, 50–60 Hz; Output: 15V= / 530 mA) Lithium battery (CR 2032, 3V); for keeping data if there is no power supply from the rechargeable batteries or the main adapter
Auto off 20 minutes after last function, 30 seconds acoustical signal before switch off
Charging time approx. 10 hours Dimensions approx. 265 x 195 x 70 mm (unit)
approx. 440 x 370 x 140 mm (case) Weight (unit) approx. 1000 g (with main adapter and rechargeable
batteries) Working condition 5 – 40°C at max. 30–90% relative humidity
(without condensation) Language options English, German, French, Spanish, Italian, Portuguese,
Polish; further languages via Internet Update Storage capacity ca. 1000 data sets
* measured with standard solutions
Subject to technical modification!
To ensure maximum accuracy of test results, always use the reagent systems supplied by the instrument manufacturer.
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3.5 Abbreviations
Abbreviation Definition
°C degree Celsius (Centigrade)
°F degree Fahrenheit °F = (°C x 1,8) + 32
°dH degree German Hardness
°fH degree French hardness
°eH degree English Hardness
°aH degree American Hardness
Abs Absorption unit
μg/l (= ppb) Microgram per litre
mg/l (= ppm) Milligram per litre
g/l (= ppth) Gram per litre <
KI Potassium Iodide
TDS Total Dissolved Solids
LR Low Range
MR Medium Range
HR High Range
T Tablet
DPD Diethyl-p-phenylendiamine
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3.6 Troubleshooting
3.6.1 Operating messages in the display / error display
Display Possible Causes Elimination
Overrange reading is exceeding the range
water sample is too cloudy
to much light on the photo cell
if possible dilute sample or use other measuring range filtrate water sample seal on the cap? Repeat measurement with seal on the cap of the vial
Underrange result is under the detection limit indicate result with lower x mg/l
x = low end of measuring range; if necessary use other analytical method
Storage­system error use Mode 34
mains power fails or is not connected
insert or change Lithium battery Delete Data with Mode 34.
Battery warning
warning signal every 3 minutes warning signal every 12 seconds
capacity of the battery is too low; change the batteries
warning signal, the instrument switches itself off
change the batteries
Jus Overrange E4
The user calibration is out of the accepted range
Please check the standard, reaction time and other possible faults. Repeat the user calibration.
Jus Underrange E4
Overrange E1
The concentration of the
standard
is too high/too low, so
that
during user calibration the
limit
of the range was exceeded
Perform the test with a standard of higher/lower concentration
Underrange E1
E40 user calibration not possible
If the display shows Overrange/ Underrange for a test result a user calibration is not possible
Perform the test with a standard of higher/lower concentration
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Display Possible Causes Elimination
Zero not accepted
Light absorption is too great or too low
Refer to chapter 2.3.4 Performing Zero. Clean sample chamber. Repeat zeroing.
Printer „Timeout“
printer switched off; no connection
Connect printer Check connections Switch printer on
3.6.2 General
Finding Possible Causes Elimination
Test result deviates from the expected
Chemical species not as required
Press arrow keys to select the required chemical species
The pre-programmed countdown is not displayed.
Countdown is not activated and/or the Profi-Mode is activated.
Switch the countdown on with Mode 13 and/or switch the Profi-Mode off with Mode 50.
Instrument can be operated with the mains adapter but not with the rechargeable batteries.
Rechargeable batteries are not charged or defect. Fuse (Type A, inert, 20 mm) may be defect.
Charge rechargeable batteries or change them. If the problem still exists change fuse.
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3.7 Declaration of CE-Conformity
Declaration of EC-Conformity according to
DIRECTIVE 2004/108/EG OF THE EUROPEAN PARLIAMENT
AND OF THE COUNCIL of 2004, December the 15
th
Name of manufacturer: Tintometer GmbH
Schleefstraße 8-12 44287 Dortmund Germany
declares that this product
Product name: Lovibond® PoolDirect 9in1
meets the requirements of the following product family standard:
DIN EN 61326-1:2006
Basic immunity test requirements (Table1)
Emission according to the requirements for class B equipment
Dortmund, 1th July 2010
Cay-Peter Voss, Managing Director
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Technical changes without notice Printed in Germany 11/15
Lovibond® and Tintometer® are registered trademarks of the Tintometer group of companies
Tintometer China
Room 1001, China Life Tower 16 Chaoyangmenwai Avenue, Beijing, 100020 Tel.: +86 10 85251111 App. 330 Fax: +86 10 85251001
China
Tintometer South East Asia
Unit B-3-12, BBT One Boulevard, Lebuh Nilam 2, Bandar Bukit Tinggi, Klang, 41200, Selangor D.E Tel.: +60 (0)3 3325 2285/6 Fax: +60 (0)3 3325 2287 lovibond.asia@tintometer.com www.lovibond.com
Malaysia
Tintometer GmbH
Lovibond® Water Testing Schleefstraße 8-12 44287 Dortmund Tel.: +49 (0)231/94510-0 Fax: +49 (0)231/94510-20 sales@tintometer.de www.lovibond.com
Germany
Tintometer AG
Hauptstraße 2 5212 Hausen AG Tel.: +41 (0)56/4422829 Fax: +41 (0)56/4424121 info@tintometer.ch www.tintometer.ch
Switzerland
The Tintometer Ltd
Lovibond® House Sun Rise Way Amesbury Salisbury SP4 7GR Tel.: +44 (0)1980 664800 Fax: +44 (0)1980 625412 sales@tintometer.com www.lovibond.com
UK
Tintometer Inc.
6456 Parkland Drive Sarasota, FL 34243 Tel: 941.756.6410 Fax: 941.727.9654 sales@tintometer.us www.lovibond.com
USA
Tintometer Brasilien
Caixa Postal: 271 CEP: 13201-970 Jundiaí – SP ­Tel.: +55 (11) 3230-6410 sales@tintometer.com.br www.lovibond.com.br
Brazil
Tintometer Indien Pvt. Ltd.
B-91, A.P.I.E. Sanath Nagar, Hyderabad, 500018 Tel: +91 (0) 40 4647 9911 Toll Free: 1 800 102 3891 indiaoffice@tintometer.com www.lovibondwater.in
India
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