·TEST KIT PROCEDURE 121
TITRATION OF OAKITE ALKALINE PRODUCTS WITH N ACID USING
PHENOLPHTHALEIN INDICATOR
(THIS PROCEDURE REPLACES PREVIOUS OAKITE PROCEDURE 92)
Test Kit: - OAKITE ALKALINE TEST KIT (CODE OKT 9205)
Reagents and Equipment:
Code Quantity Description
OKT 6130-J 100 ml 1 N Hydrochloric Acid
OKT 6131-J 100 ml 0.1 N Hydrochloric Acid
OKT 2246-G 25 ml Phenolphthalein
OKT 2207-G 25 ml Bromcresol Green
OKT 2292-G 25 ml Methyl Red
0376 2 Direct Reading Titrator; 0-1 ml
0778 1 Titration Tube marked at 5, 10 and
15 ml, with cap
0354 1 Plastic dropper marked at 1 ml
TK 121
Step 1: Using the 1 ml dropper, pipet the appropriate sample volume of Oakite solution
listed in the table below into the empty titration tube. Add water to this solution
until the volume is at least to the 5 ml mark. For 5 and 10 ml sample volumes,
use the graduations on the titration tube. No water need be added.
Step 2: Add 1 or 2 drops of Phenolphthalein Indicator. Swirl to mix. The color will be
red. Place the cap on the titration tube.
Step 3: Fill the Direct Reading Titrator* to the zero mark with 1N Acid.
Step 4: Insert tip of Titrator into the central hole in the titrating tube cap. While holding
the Titrator assembly in one hand, slowly depress the plunger of the Titrator
with the other hand to dispense the titrating solution. Swirl the solution gently
after each drop has been added. When the red color of the solution disappears
completely, stop any further movement of the plunger. Record the reading on
the Titrator in ml. Call this Titration T. This completes the analysis.
Calculation: T x F = % by vol, g/l or oz/gal of Oakite product.
*NOTE: For complete instructions on how to use the Direct Reading Titrator please
refer to the enclosed instruction sheet.
(con tin ued)
Test Kit procedure 121 continued
Use Concentration Sample Volume Multiplying Factor (F)
Oakite Material
24 30-90 (4-12) 1 75 (10)
45 1.5-15 (0.2-2) 10 6.3 (0.83)
62 3.8-15 (0.5-2) 5 11 (1.4)
77 15-60 (2-8) 2 51 (6.8)
90 45-90 (6-12) 1 64 (8.5)
94 7.5-30 (1-4) 10 13 (1.8)
100 15-60 (2-8) 2 24 (3.2)
145 0.5-2 10 0.80
160 15-45 (2-6) 2 22 (3.0)
161 3.8-15 (0.5-2) 10 15 (2.0)
162 7.5-30 (1-4) 5 16 (2.2)
190 60-120 (8-16) 1 54 (7.2)
245 0.5-2 10 0.95
295 30-45 (4-6) 2 42 (5.6)
g/l (oz/gal)
15-90 (2-12) 1 63 (8.3)
% by vol in ml % by vol
g/l (oz/gal)
345 0.5-2 10 1.7
360 L 2-8 1 5.7
990 45-90 (6-12) 1 54 (7.2)
2327 30-60 (4-8) 2 42 (5.6)
ALC-1
Alclean NS
Aluminum
Cleaner 164
Anodet
Anoprep
Dynadet
Dynamerse
Enprox 714
Enprox Tow e r
Cleaner
FiSan-500
FiSan-500M
1.9-7.5 (0.25-1) 10 6.6 (0.88)
15-60 (2-8) 10 30 (4.0)
45-75 (6-10) 2 82 (11)
45-90 (6-12) 1 71 (9.5)
15-60 (2-8) 2 44 (5.9)
22-90 (3-12) 2 42 (5.6)
22-90 (3-12) 2 47 (6.2)
2-8 1 6.0
3.8-15 (1.5-2) 10 15 (2.0)
0.5-2 5 1.2
0.5-2 5 1.2
FiSan-Bottle
Clean
15-60 (2-8) 10 20 (2.7)
(con tin ued)
Test Kit Procedure 121 continued
Use Concentration Sample Volume Multiplying Factor (F)
Oakite Material
FiSan Brite
FiSan-CQD
Fleetline TC
FM 183
Liqualin
Low Heat
Cleaner 1
Low Heat
Cleaner 3
LRS
Okemclean
Rustripper
Rustripper M
Solventol 530
Solventol 530
Solventol 828
g/l (oz/gal)
% by vol in ml % by vol
g/l (oz/gal)
7.5-30 (1-4) 2 24 (3.2)
7.5-30 (1-4) 2 24 (3.2)
60-120 (8-16) 1 72 (9.6)
30-120 (4-16) 2 82 (11)
1-4 10 4.0
22-90 2 66 (8.8)
2-8 5 2.8
1-4 5 2.5
2.8 5 6.5
30-90 (4-12) 1 60 (8.0)
15-45 (2-6) 2 26 (3.5)
7.5-15 (1-2) 10 15 (1.9)
30-60 (4-8) 5 29 (3.9)
7.5-30 (0.5-2) 10 10 (1.3)
Solventol 3641
Solventol 3830
Solventol
Actostrip 3929FB
Solventol ES
3899
STC
Stripper M3
Stripper Q5
Stripper Q9
Stripper Q9L
Stripper Q9L
Special
Stripper Q10
Stripper R6
Stripper R8
Super Rustripper
3.8-15 (0.5-2) 10 9.7 (1.3)
3-10 1 7.1
40-60 1 28
45-90 (6-12) 2 48 (6.4)
2-8 5 3.0
22-90 (3-12) 1 47 (6.3)
22-90 (3-12) 1 45 (6.0)
22-90 (3-12) 1 52 (7.0)
5-20 1 8.4
5-20 1 8.5
10-40 1 23
30-120 (4-16) 1 48 (6.4)
30-120 (4-16) 1 52 (7.0)
30-120 (4-16) 1 75 (10)
9/1/87
Supersedes 1/22/87 Ptd. in U.S.A.
TP/TK 121
·TEST KIT PROCEDURE 122
TITRATION OF OAKITE ALKALINE PRODUCTS WITH N ACID USING
BROMCRESOL GREEN INDICATOR
(THIS PROCEDURE REPLACES PREVIOUS OAKITE PROCEDURES 1 AND 56)
Test Kit: - OAKITE ALKALINE TEST KIT (CODE OKT 9205)
Reagents and Equipment:
Code Quantity Description
OKT 6130-J 100 ml 1 N Hydrochloric Acid
OKT 6131-J 100 ml 0.1 N Hydrochloric Acid
OKT 2246-G 25 ml Phenolphthalein
OKT 2207-G 25 ml Bromcresol Green
OKT 2292-G 25 ml Methyl Red
0376 2 Direct Reading Titrator; 0-1 ml
0778 1 Titration Tube marked at 5, 10 and
15 ml, with cap
0354 1 Plastic dropper marked at 1 ml
TK 122
Step 1: Using the 1 ml dropper, pipet the appropriate sample volume of Oakite solution
listed in the table below into the empty titration tube. Add water to this solution
until the volume is at least to the 5 ml mark. For 5 and 10 ml sample volumes,
use the graduations on the titration tube. No water need be added.
Step 2: Add 1 or 2 drops of Bromcresol Green Indicator. Swirl to mix. The color will be
blue. Place the cap on the titration tube.
Step 3: Fill the Direct Reading Titrator* to the zero mark with 1N Acid.
Step 4: Insert tip of Titrator into the central hole in the titrating tube cap. While holding
the Titrator assembly in one hand, slowly depress the plunger of the Titrator
with the other hand to dispense the titrating solution. Swirl the solution gently
after each drop has been added. When the color of the solution changes from
blue to a distinct yellow, stop any further movement of the plunger. Record the
reading on the Titrator in ml. Call this Titration T. This completes the analysis.
Calculation: T x F = % by vol, g/l or oz/gal of Oakite product.
*NOTE: For complete instructions on how to use the Direct Reading Titrator please
refer to the enclosed instruction sheet.
(con tin ued)
Test Kit Procedure 122 continued
Use Concentration Sample Volume Multiplying Factor (F)
Oakite Material
20 7.5-30 (1-4) 5 12 (1.7)
30 15-60 (2-8) 2 28 (3.8)
61B 22-60 (3-8) 2 45 (6.0)
67 7.5-30 (1-4) 5 16 (2.2)
91 38-45 (5-6) 1 64 (8.5)
91A 7.5-15 (1-2) 10 26 (3.5)
92 7.5-15 (1-2) 10 11 (1.4)
195 38-60 (5-8) 1 56 (7.5)
220 NP 5-20 10 10
420 ML 5-20 10 15
443 2.8 10 5.1
444 15-60 (2-8) 2 31 (4.1)
BCR
BP 181
Buff Brite NR
g/l (oz/gal)
7.5-30 (1-4) 10 14 (1.9)
% by vol in ml % by vol
3-12 5 6.8
2-8 10 4.4
g/l (oz/gal)
DZL
FiSan-Guard
FiSan-HD
Fleetline 213
FM 103
Foam-Det
General
Cleaner
HD 126
Industrial
(Red Label)
LFL
Liqualin CC
LSD
Penetrant
2-5 10 1.6
7.5-30 (1-4) 5 20 (2.6)
7.5-30 (1-4) 5 9.8 (1.3)
3-12 10 8.4
7.5-15 (1-2) 10 11 (1.5)
2-8 10 6.0
1-15 (0.12-2) 10 6.2 (0.82)
30-60 (4-8) 1 60 (8.0)
7.5-30 (1-4) 10 17 (2.3)
1-4 10 2.5
1-4 10 2.9
1-4 10 2.4
1-15 (0.12-2)
15-75 (2-10)
10
2
7 (0.93)
35 (4.7)
(con tin ued)
Test Kit Procedure 122 continued
Use Concentration Sample Volume Multiplying Factor (F)
Oakite Material
Power-Det
Renovator
SC 129
SC 225
Solventol 3130
Solventol 3249
Speedet
Super
Turbo-Det
Te st X
Turbo-Det
g/l (oz/gal)
% by vol in ml % by vol
g/l (oz/gal)
15-60 (2-8) 5 34 (4.6)
60-90 (8-12) 5 53 (7.1)
7.5-22 (1.3) 5 16 (2.2)
7.5-30 (1-4) 5 17 (2.3)
3.8-22.5(0.5-3) 10 7.7 (1.0)
5.6-22.5 (0.75-3) 10 11 (1.5)
3-12 10 8.6
45-75 (6-10) 2 45 (6.0)
30-90 (4-12) 1 52 (7.0)
15-60 (2-8) 2 37 (4.9)
9/1/87
Supersedes 1/22/87 Ptd. in U.S.A.
TP/TK 122
·PROCEDURE 123
DETERMINING FREE AND TOTAL ALKALI IN CLEANING SOLUTIONS
(THIS PROCEDURE REPLACES PREVIOUS OAKITE PROCEDURE 13)
Test Kit: - OAKITE ALKALINE TEST KIT (CODE OKT 9205)
Reagents and Equipment:
Code Quantity Description
OKT 6130-J 100 ml 1 N Hydrochloric Acid
OKT 6131-J 100 ml 0.1 N Hydrochloric Acid
OKT 2246-G 25 ml Phenolphthalein
OKT 2207-G 25 ml Bromcresol Green
OKT 2292-G 25 ml Methyl Red
0376 2 Direct Reading Titrator; 0-1 ml
0778 1 Titration Tube marked at 5, 10 and
15 ml, with cap
0354 1 Plastic dropper marked at 1 ml
TK 123
Step 1: Using the 1 ml dropper, pipet the appropriate sample volume of Oakite solution
listed in the table below into the empty titration tube. Add water to this solution
until the volume is at least to the 5 ml mark. For 5 and 10 ml sample volumes,
use the graduations on the titration tube. No water need be added. For
appropriate sample volumes see notes 4, 5 and 6 below.
Step 2: Add 1 or 2 drops of Phenolphthalein Indicator. Swirl to mix. The color will be
red. Place the cap on the titration tube.
Step 3: Fill the Direct Reading Titrator* to the zero mark with 1N Acid. Insert tip of
Titrator into the central hole in the titrating tube cap. While holding the Titrator
assembly in one hand, slowly depress the plunger of the Titrator with the other
hand to dispense the titrating solution. Swirl the solution gently after each drop
has been added. When the red color of the solution disappears completely,
stop any further movement of the plunger. Record the reading on the Titrator in
ml. Call this Titration A.
Step 4: Into the mixture from Step 3, add 1 or 2 drops of Bromcresol Green Indicator.
Swirl to mix. The color of the solution will be blue.
Step 5: Again, fill the Direct Reading Titrator to the zero mark with 1N Acid and titrate
the blue solution until the color changes to a distinct yellow. Record the reading
on the Titrator in ml. Call this Titration B.
Calculations: A + B = Total Alkali
A - B = Free Alkali
A - B = Ratio of Free Alkali
A + B Total Alkali
(con tin ued)
Test Kit Procedure 123 continued
Example:
A B A-B A+B
A-B
A+B
1st Titration (fresh tank)
2nd Titration (after use)
3rd Titration (after much more use)
1.75 .025 1.50 2.00 0.75
1.50 0.50 1.00 2.00 0.50
1.00 1.00 0.00 2.00 0.00
NOTES:
*1. For complete instructions on how to use the Direct Reading Titrator please refer to the
enclosed instruction sheet.
2. The ratio is constant and specific for fresh solutions of each Oakite product regardless of the
absolute concentration used.
3. The ratio reduces with use. As the ratio approaches zero it indicates a spent tank.
4. A suggested sample volume for highly concentrated alkaline solutions is 1 ml and for weaker
solutions, up to 10 ml.
5. The ratio of Free to Total Alkali should first be determined on a fresh solution. An appropriate
sample volume should be chosen so as to yield a Titration “A” somewhere between 1 and 2
ml of 1N Acid in Step 3.
6. Once the appropriate sample volume has been chosen, it must remain constant for
subsequent titrations of the Oakite solution after use.
2/6/86
Supersedes 4/16/84 Ptd. in U.S.A.
TP/TK 123
·PROCEDURE 124
TITRATION OF OAKITE ALKALINE PRODUCTS WITH 0.1 N ACID USING
PHENOLPHTHALEIN INDICATOR
(THIS PROCEDURE REPLACES PREVIOUS OAKITE PROCEDURE 94)
Test Kit: - OAKITE ALKALINE TEST KIT (CODE OKT 9205)
Reagents and Equipment:
Code Quantity Description
OKT 6130-J 100 ml 1 N Hydrochloric Acid
OKT 6131-J 100 ml 0.1 N Hydrochloric Acid
OKT 2246-G 25 ml Phenolphthalein
OKT 2207-G 25 ml Bromcresol Green
OKT 2292-G 25 ml Methyl Red
0376 2 Direct Reading Titrator; 0-1 ml
0778 1 Titration Tube marked at 5, 10, and 15
ml, with cap
0354 1 Plastic dropper marked at 1 ml
TK 124
Step 1: Using the 1 ml dropper, pipet the appropriate sample volume of Oakite solution
listed in the table below into the empty titration tube. Add water to this solution
until the volume is at least to the 5 ml mark. For 5 and 10 ml sample volumes,
use the graduations on the titration tube. No water need be added.
Step 2: Add 1 or 2 drops of Phenolphthalein Indicator. Swirl to mix. The color will be
red. Place the cap on the titration tube.
Step 3: Fill the Direct Reading Titrator* to the zero mark with 0.1N Acid.
Step 4: Insert tip of Titrator into the central hole in the titrating tube cap. While holding
the Titrator assembly in one hand, slowly depress the plunger of the Titrator
with the other hand to dispense the titrating solution. Swirl the solution gently
after each drop has been added. When the red color of the solution disappears
completely, stop any further movement of the plunger. Record the reading on
the Titrator in ml. Call this Titration T. This completes the analysis.
Calculation: T x F = % by vol, g/l or oz/gal of Oakite product.
*NOTE: For complete instructions on how to use the Direct Reading Titrator please
refer to the enclosed instruction sheet.
(con tin ued)
Test Kit Procedure 124 continued
Use Concentration Sample Volume Multiplying Factor (F)
Oakite Material
3 15-60 (2-8) 1 27 (3.6)
21 0.9-7.5 (0.12-1) 2 5.2 (0.69)
302 2-8 5 4.8
FiSan-Bottle
Clean
FiSan-Guard LT
PK 244
Solventol ES
3449
Super Foam-Det
g/l (oz/gal)
% by vol in ml % by vol
g/l (oz/gal)
7.5-22.5 (1-3) 1 10 (1.4)
15-60 (2-8) 1 20 (2.8)
3.8-15 (0.5-2) 2 7.5 (1.0)
1.9-7.5 (0.25-1) 2 5.2 (0.70)
2-10 2 3.5
2-8 1 6.4
9/1/87
Supersedes 11/20/95 Ptd. in U.S.A.
TP/TK 124
·PROCEDURE 125
TITRATION OF OAKITE ALKALINE PRODUCTS WITH 0.1 N ACID
USING BROMCRESOL GREEN INDICATOR
(THIS PROCEDURE REPLACES PREVIOUS OAKITE PROCEDURES 1, 56 AND 91)
Test Kit: - OAKITE ALKALINE TEST KIT (CODE OKT 9205)
Reagents and Equipment:
Code Quantity Description
OKT 6130-J 100 ml 1 N Hydrochloric Acid
OKT 6131-J 100 ml 0.1 N Hydrochloric Acid
OKT 2246-G 25 ml Phenolphthalein
OKT 2207-G 25 ml Bromcresol Green
OKT 2292-G 25 ml Methyl Red
0376 2 Direct Reading Titrator; 0-1 ml
0778 1 Titration Tube marked at 5, 10 and
15 ml, with cap
0354 1 Plastic dropper marked at 1 ml
TK 125
Step 1: Using the 1 ml dropper, pipet the appropriate sample volume of Oakite solution
listed in the table below into the empty titration tube. Add water to this solution
until the volume is at least to the 5 ml mark. For 5 and 10 ml sample volumes,
use the graduations on the titration tube. No water need be added.
Step 2: Add 1 or 2 drops of Bromcresol Green Indicator. Swirl to mix. The color will be
blue. Place the cap on the titration tube.
Step 3: Fill the Direct Reading Titrator* to the zero mark with 0.1N Acid.
Step 4: Insert tip of Titrator into the central hole in the titrating tube cap. While holding
the Titrator assembly in one hand, slowly depress the plunger of the Titrator
with the other hand to dispense the titrating solution. Swirl the solution gently
after each drop has been added. When the color of the solution changes from
blue to a distinct yellow, stop any further movement of the plunger. Record the
reading on the Titrator in ml. Call this Titration T.
Step 5: Wash out the titration tube used in Steps 1 thru 4 and refill it to the same mark
as in Step 1 with water used to make up the sample solution. Follow Steps 2, 3,
and 4 above and record the number of ml used. Call this Titration B. This
completes the analysis.
Calculation: (T - B) x F = % by vol, g/l or oz/gal of Oakite product.
(con tin ued)
Test Kit Procedure 125 continued
NOTE 1: Step 5 is very important to the accuracy of the titration and should always be
performed. The reason for this is due to the natural occurring alkalinity in the
water used to dilute the Oakite Product. This alkalinity will give erroneously
higher concentration values unless corrected.
*NOTE 2: For complete instructions on how to use the Direct Reading Titrator please
refer to the enclosed instruction sheet.
Use Concentration Sample Volume Multiplying Factor (F)
Oakite Material
53 3.8-15(0.5-2) 2 8.2 (1.1)
101 2-8 5 4.9
202 1-4 10 4.2
FiSan-LC66
FiSan-LC99
FiSan-Panacea
Fleetline JC5
Fleetline 170
Fleetline 205
Fleetline 205
Special
FM 403
Liqui-Det
Liqui-Det 2
Liquid Power-Det
Solventol
Hydra-Clean
g/l (oz/gal)
% by vol in ml % by vol
g/l (oz/gal)
0.5-2 10 0.87
0.5-1.5 10 0.93
1-4 5 1.4
5-20 2 9.1
7.5-30 (1-4) 2 22 (2.9)
5-20 2 11
5-20 2 11
1-4 5 1.6
2-8 5 3.7
0.5-2 10 2.0
2-8 2 5.0
3-10 1 6.2
Versadet
7/26/83
Supersedes 11/20/80 PTD. in U.S.A.
TP/TK 125
3.8-15 (0.5-2) 1 11 (1.5)
·PROCEDURE 126
TITRATION OF OAKITE ALKALINE PRODUCTS WITH 0.1 N ACID USING
MIXED INDICATOR
(THIS PROCEDURE REPLACES PREVIOUS OAKITE PROCEDURE 91)
Test Kit: - OAKITE ALKALINE TEST KIT (CODE OKT 9205)
Reagents and Equipment:
Code Quantity Description
OKT 6130-J 100 ml 1 N Hydrochloric Acid
OKT 6131-J 100 ml 0.1 N Hydrochloric Acid
OKT 2246-G 25 ml Phenolphthalein
OKT 2207-G 25 ml Bromcresol Green
OKT 2292-G 25 ml Methyl Red
0376 2 Direct Reading Titrator; 0-1 ml
0778 1 Titration Tube marked at 5, 10 and
15 ml, with cap
0354 1 Plastic dropper marked at 1 ml
TK 126
Step 1: Using the 1 ml dropper, pipet the appropriate sample volume of Oakite solution
listed in the table below into the empty titration tube. Add water to this solution
until the volume is at least to the 5 ml mark. For 5 and 10 ml sample volumes,
use the graduations on the titration tube. No water need be added.
Step 2: Add 1 or 2 drops of Bromcresol Green Indicator followed by 1 or 2 drops of
Methyl Red Indicator. Swirl to mix. The color will be green. Place the cap on the
titration tube.
Step 3: Fill the Direct Reading Titrator* to the zero mark with 0.1N Acid.
Step 4: Insert tip of Titrator into the central hole in the titrating tube cap. While holding
the Titrator assembly in one hand, slowly depress the plunger of the Titrator
with the other hand to dispense the titrating solution. Swirl the solution gently
after each drop has been added. When the color of the solution changes from
green to a distinct pink, stop any further movement of the plunger. Record the
reading on the Titrator in ml. Call this Titration T.
Step 5: Wash out the titration tube used in Steps 1 thru 4 and refill it to the same mark
as in Step 1 with water used to make up the sample solution. Follow Steps 2, 3,
and 4 above and record the number of ml used. Call this Titration B. This
completes the analysis.
Calculation: (T - B) x F = % by vol, g/l or oz/gal of Oakite product.
(con tin ued)
Test Kit Procedure 126 continued
NOTE 1: Step 5 is very important to the accuracy of the titration and should always be
performed. The reason for this is due to the natural occurring alkalinity in the
water used to dilute the Oakite Product. This alkalinity will give erroneously
higher concentration values unless corrected.
*NOTE 2: For complete instructions on how to use the Direct Reading Titrator please
refer to the enclosed instruction sheet.
Use Concentration Sample Volume Multiplying Factor (F)
Oakite Material
6 3.8-15 (0.5-2) 10 6.0 (0.80)
542 NN
Aluminum
Cleaner 166
Aluminum
Cleaner NSS
Aluminum
Cleaner NST
CPA
Felt Life
FiSan-Lube
FiSan-Panacea
Formula B-50
Formula C
Formula L
Formula MM
g/l (oz/gal)
% by vol in ml % by vol
g/l (oz/gal)
5-10 1 9.5
45-60 (6-8) 1 18 (2.4)
1-4 10 1.8
5-10 2 7.5
0.5-2 5 0.86
0.5-2 10 1.1
3.8-15 (0.5-2) 10 7.5 (1.0)
0.25-1 10 0.70
2-8 5 3.2
1-4 5 4.3
2-5 1 4.3
3-10 1 7.3
Formula MM-OF
Formula P-Q
5/20/88
Supersedes 1/22/87 Ptd. in U.S.A.
TP/TK 126
3-10 1 8.5
2-10 2 3.7
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