LaMotte MOLYBDENUM KIT User Manual

MOLYBDENUM
1200 COLORIMETER, 0-30 ppm
CODE 3676-01
QUANTITY CONTENTS CODE
60 mL *Mo Buffer *3997-H 2 x 30 mL *Molybdenum Oxidizing Reagent *6485-G
2.5 g *Molybdenum Indicator Powder *6486-S 1 Colorimeter Tubes 10 mL, w/cap, set of 6 0290-6 1 Spoon, 0.05g, plastic 0696 1 Pipets, 1.0 mL, plastic, w/cap 0372 1 Pipet, 1.0 mL 0354 1 Water Sample Collecting Bottle 0688 1 1200 Colorimeter for Molybdenum 26729
*WARNING: Reagents marked with an * are considered to be potential health hazards. To view or print a Material Safety Data Sheet (MSDS) for these reagents go to www.lamotte.com. To obtain a printed copy, contact LaMotte by e-mail, phone or fax.
To order individual reagents or test kit components, use the specifi ed code number. NOTE: After use, return *MO Buffer (3997) to zipper top storage bag to reduce
exposure to corrosive reagent.
INTRODUCTION
Molybdenum occurs naturally in the earth’s crust as molybdenite and wolfenite, and is an important element in many biochemical reactions, including nitrogen fi xation. In industrial processes, such as the operation of boilers and cooling towers, molybdenum, in the form of sodium molybdate, is used as an environmentally safe corrosion inhibitor.
MOLYBDENUM PROCEDURE - Thioglycolate Method
Read the 1200 Colorimeter Manual before proceeding. Carefully wipe tubes dry before inserting into the colorimeter chamber
MOLYBDENUM
12
Fill theWater Sample Collecting Bottle (0688) with sample water. This will be used to dispense sample water for the tests.
Rinse and fi ll a colorimeter tube (0290) to the 10mL line with sample water.
34
Use the 1.0 mL pipet (0372) to add1mLof *Mo Buffer (3997). Cap and mix.
Use the 1.0 mL pipet (0354) to add 1mL of *Molybdenum Oxidizing Reagent (6485). Cap and mix.
5
Wipe the tube dry.
7
Push the READ button to turn the meter on. Press the ZERO button and hold it for 2 seconds until is displayed. Release the button to take a blank reading (0.0 ppm).
6
8
Insert the tube into the chamber, being sure to align the index line with the arrow on themeter. Close the lid. This tube is the sample blank.
Use the 0.05 spoon (0696) to add 0.05g of *Molybdenum Indicator Powder (6486).
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