SINGLE PARAMETER
DIGITAL COLORIMETER
FLUORIDE
MODEL DC1100-FL · CODE 3674
QUANTITY CONTENTS CODE
2 x 100 mL *Acid-Zirconyl-SPADNS Reagent *3875-J
2 x 60 mL *Sodium Arsenite Solution *4128-H
1 Pipet, 0.5 mL, plastic 0353
1 Pipet, 1.0 mL, plastic 0354
6 Colorimeter Tubes, 10 mL, glass, w/ caps 0967
1 Colorimeter, DC1100 for Fluoride 26714
*WARNING: Reagents marked with an * are considered hazardous
substances. Material Safety Data Sheets (MSDS) are supplied for these
reagents. For your safety, read label and accompanying MSDS before using.
To order individual reagents or test kit components, use the specified code
number.
NOTE: This procedure uses the EPA approved SPADNS Reagent
System for fluoride found in method 4500-F-D, 17th Edition of Standard
Methods for the Examination of Water and Wastewater, page 4 - 89.
PRO CE DURE
NOTE: Read the Model DC1100 Colorimeter Instruction Manual
before proceeding. Carefully wipe tubes dry before inserting into the
colorimeter chamber.
1. Rinse and fill a clean colorimeter tube (0967) to the 10 mL line
with fluoride-free demineralized water.
2. Use the 0.5 mL pipet (0353) to add 0.5 mL of *Sodium Arsenite
Solution (4128). Cap and mix contents.
3. Use the 1.0 mL pipet (0354) to add 2 measures of *Acid-Zirconyl
SPADNS Reagent (3875). Cap and mix thoroughly. This is the
reagent blank.
4. Insert tube into the colorimeter chamber. Press the “ON/OFF”
button and adjust to 0 ppm with the “SET BLANK” knob. Remove
blank sample.
5. Rinse and fill a second colorimeter tube to 10 mL line with sample
water.
6. Use the 0.5 mL pipet (0353) to add 0.5 mL of *Sodium Arsenite
Solution (4128). Cap and mix contents.
7. Use the 1.0 mL pipet (0354) to add 2 measures of *Acid-Zirconyl
SPADNS Reagent (3875). Cap and mix thoroughly.
8. Insert the tube into the colorimeter chamber and press the
“ON/OFF” button. Record result in (ppm) Fluoride as soon as
reading stabilizes.
LaMOTTE COM PANY
Helping Peo ple Solve An a lyt i cal Chal lenges
PO Box 329 • Chestertown • Mary land • 21620 • USA
800-344-3100 • 410-778-3100 (Out side U.S.A.) • Fax 410-778-6394
Visit us on the web at www.lamotte.com
SM
11/98