LaMotte CHLORIDE IN WATER TEST KIT User Manual

CHLO RIDE IN WA TER TEST KIT
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CODE 7172-01
QUANTITY CONTENTS CODE
30 mL *Hydrogen Peroxide, 3% *6091WT-G 30 mL *Chloride Reagent A *4069WT-G 30 mL *Sulfuric Acid, 0.5N *6090WT-G 15 mL *Phenolphthalein Indicator, 0.5% *2258-E 2 x 30 mL *Silver Nitrate, 0.171 N *3824WT-G 1 Sample Tube, 5-10-25 mL, w/cap 0715
*WARNING: Reagents marked with an * are considered to be potential health hazards. To view or print a Material Safety Data Sheet (MSDS) for these reagents go to www.lamotte.com. To obtain a printed copy, contact LaMotte by e-mail, phone or fax.
To order individual reagents or test kit components, use the specified code number.
NOTE: This test allows the analyst to use different sample volumes to vary equivalencies. Select the appropriate sample volume from the table below and add reagents as specified.
SAMPLE SIZE
25 mL 1 dr = 10 ppm 10 mL 1 dr = 25 ppm 5 mL 1 dr = 50 ppm
EQUIVALENCE (ppm Per Drop)
PRO CE DURE
1. Rinse sample tube with sample water. Fill with desired sample size selected from table above.
2. If sulfites are present, add 5 drops of *Hydrogen Peroxide, 3% (6091WT). Swirl for 30 seconds.
3. Add *Phenolphthalein Indicator, 0.5% (2258) as follows:
25 mL 2 drops 10 mL 1 drop 5 mL 1 drop
Mix. If solution is pink add *Sulfuric Acid, 0.5N (6090WT), one drop at a time, swirling after each drop, until pink color changes to colorless. If solution is colorless, proceed to Step 4.
4. Add *Chloride Reagent A (4069WT) as follows:
25 mL 5 drops 10 mL 2 drops 5 mL 1 drop
Mix. Solution will turn yellow.
5. Add *Silver Nitrate, 0.171N (3824WT), one drop at a time, swirling and counting the number of drops, until the color turns orange-brown.
6. Multiply number of drops used in Step 5 as follows:
25 mL multiply by 10 10 mL multiply by 25 5 mL multiply by 50
Record as ppm Chloride.
LaMOTTE COM PANY
Helping Peo ple Solve An a lyt i cal Challenges
PO Box 329 • Chestertown • Mary land • 21620 • USA
800-344-3100 • 410-778-3100 (Out side U.S.A.) • Fax 410-778-6394
Visit us on the web at www.lamotte.com
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