LaMotte BOTTLE 3-0026 User Manual

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WA TER SAM PLER – FLUSHING STYLE
L
Mott
CODE 1060
QUANTITY CONTENTS CODE
1 Water Sampling Bottle Body 1080 3 Test Tubes, glass 0829 1 Rod, w/Stopper 1059 1 Sounding Weight 1068 1 Center Plug, w/Inlet Tube 1089 2 Stoppers, cork 0658
IN TRO DUC TION
This device is designed for use in the field and is a simplified water sampler. The sample is collected in a removable inner chamber which is overflowed ten times to insure a representative sample. Samples may be taken at a controlled depth by using a calibrated line. Attaching the two pound weight to the bottom of the sampling device insures rapid descent and minimizes the amount of drift due to currents. More weight should be attached to the sampling device in strong currents.
It is necessary to maintain a position directly over the Water Sampler when lowering it so that it remains in an upright position. This permits the displacement of all of the air in the sampler so that it will fill completely.
It should be noted that the bubbles of air displaced from the sampler will be observed downstream.
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PRO CE DURE
CENTER PLUG
INNER CHAMBER
WEIGHT
TEST TUBE
INLET TUBING
BOTTOM BRIDLE
SNAP CLAMP
TOP BRIDLE
A. COLLECTING A WATER SAMPLE
1. Re move the plas tic cen ter plug with in let tub ing at tached. In sert a test tube (0829), with the stop per re moved, into the in ner cham ber of the cyl in der.
2. Re place the plas tic cen ter plug and make sure the in let tub ing is in the test tube.
3. At tach the two pound weight (1068) to the bot tom bri dle of the sam pler by the snap clamp.
4. At tach the snap clamp on the cal i brated line to the top bri dle of the sam pler.
5. Quickly lower the wa ter sam pler to the de sired depth and leave un til full. This can be de ter mined when the bub bles from the dis placed air in the sam pler cease to ap pear. This usu ally takes from 3-5 min utes.
6. Care fully re trieve the wa ter sam pler.
7. Re move the plas tic cen ter plug to ex pose the test tube in the in ner cham ber.
8. Care fully re trieve the test tube from the cham ber us ing the rod with stop per (1059).
9. If a dissolved oxygen test is to be performed on this sample, proceed immediately to Part B.
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B. COLLECTING A DISSOLVED OXYGEN WATER SAMPLE
The dissolved oxygen test is performed with reagents furnished in LaMotte’s Dissolved Oxygen Kits, Code 7414 or 5860.
*WARNING: Reagents marked with an * are considered to be potential health hazards. To view or print a Material Safety Data Sheet (MSDS) for these reagents go to www.lamotte.com. To obtain a printed copy, contact LaMotte by e-mail, phone or fax.
1. Remove the rod with stopper from the test tube.
2. To the sample, add 8 drops of *Manganous Sulfate Solution (4167)
and 8 drops of *Alkaline Potassium Iodide Azide (7166).
3. Stopper the tube and gently mix by inverting.
4. Allow the test tube to stand undisturbed until the precipitate settles
two inches below the top of the tube.
5. Use a 1.0 g spoon (0697) to add one measure of *Sulfamic Acid Powder (6286), or add 8 drops of *Sulfuric Acid, 1:1 (6141WT). Cap the test tube and mix until the precipitate has completely dissolved.
Contact of the water sample with air will not affect it now. By following instructions provided with the Dissolved Oxygen Kit, the “fixed” sample may either be titrated in the field or returned to the laboratory for final titration.
C. TAKING SOUNDINGS WITH THE GRADUATED LINE
The two pound weight can be used for taking soundings. Attach the weight to the graduated line by the snap clamp and lower it into the water. Measure the depth at which the sounding lead strikes the bottom. The line is graduated in meters with every fifty meters marked by a plastic band.
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LaMOTTE COM PANY
Helping Peo ple Solve An a lyt i cal Chal lenges
PO Box 329 • Chestertown • Mary land • 21620 • USA
800-344-3100 • 410-778-3100 (Out side U.S.A.) • Fax 410-778-6394
Visit us on the web at www.lamotte.com
®
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