LaMotte 4140-03 User manual

Page 1
COLORIMETER
Code 4140-03 | Chlorine Secondary Standards
QUANTITY CONTENTS CODE
1 DPD Chlorine Color Standard Blank 4136-E 1 DPD Chlorine Color Standard A 4147-E 1 DPD Chlorine Color Standard B 4138-E 1 DPD Chlorine Color Standard C 4139-E To order individual reagents or test kit components, use the
specified code number.
These color standards are to be used as Chlorine Secondary Standards and are not intended to be used as calibration standards.
These color standards are to be used as Chlorine Secondary Standards to verify the performance of the meter and are not intended to be used as calibration standards. The meter is calibrated at the time of manufacture. The standards should be read on when they are received and the results should be recorded. Periodically, as by the user, the standards should be read on the same meter and the results should be compared to the initial readings. The meter is performing satisfactorily the difference between the initial readings and the current readings is within the specified tolerances on the data sheet.
The initial readings for the standards should be approximately:
the meter
determined
if
Standard A 0.1 - 0.4 ppm
Standard B 0.9 - 1.2 ppm
Standard C 2.2 - 3.2 ppm
The exact value of the standards will vary on different types of meters. The critical measurement is the change in the readings over time, not the value of readings.
Continued on next page...
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Page 2
DC1200 - INITIAL DETERMINATION OF STANDARD VALUE
Perform this procedure once, when standards are received.
1.
Follow the Calibration Procedure in the Colorimeter manual. Use two standards, as described, that have been titrated by an EPA accepted method (such as LaMotte Method 3176-02).
3.
Insert the DPD Chlorine Color Standard Blank into the chamber, being sure to align the index line with the arrow on the meter. Close the lid.
5.
Wipe the DPD Chlorine Color Standard A (4147-E) with a clean, lint-free cloth.
2.
Wipe the DPD Chlorine Color Standard Blank (4136-E) with a clean, lint-free cloth.
4.
Push the READ button to turn the meter on. Press the ZERO button and hold it for 2 seconds until bLA is displayed. Release the button to take a zero reading ( 0 ppm).
6.
Insert DPD Chlorine Color Standard A into the chamber, being sure to align the index line with the arrow on the meter. Close the lid.
7.
Press the READ button. The concentration in ppm will be displayed within 2 seconds.
9.
Repeat steps 5-8 for DPD Chlorine Color Standard B (4138-E) and DPD Chlorine Color Standard C (4139-E).
8.
Record the actual reading on the DPD Chlorine Color Standard A cap and on the Data Sheet, under initial reading.
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Page 3
DC1200 - INSTRUMENT PERFORMANCE CHECK
Perform this procedure at specified intervals to verify instrument performance.
1.
Wipe the DPD Chlorine Color Standard Blank (4136-E) with a clean, lint-free cloth.
3.
Push the READ button and hold it for 2 seconds until bLA is displayed. Release the button to take a zero reading.
5.
Insert the DPD Chlorine Color Standard Blank into the chamber, being sure to align the index line with the arrow on the meter. Close the lid.
2.
Insert the DPD Chlorine Color Standard Blank into the chamber, being sure to align the index line with the arrow on the meter. Close the lid.
4.
Wipe the DPD Chlorine Color Standard A (4147-E) with a clean, lint-free cloth.
6.
Press the READ button. The concentration in ppm will be displayed within 2 seconds. The reading should be within the tolerance limits given on the Data Sheet.
7.
Repeat steps 4-6 with DPD Chlorine Color Standard B (4138-E) and DPD Chlorine Color Standard C (4139-E).
NOTE: Store standards in a cool place out of direct light. Exposure to excessive heat or light may cause degradation of the standards.
8.
If the readings are not within the tolerance limits, standardize the meter calibration by following the Calibration Procedure in the meter manual. If the readings are still not within the tolerance limits, the standards are no longer valid and should be replaced.
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Page 4
SMART 2 - INITIAL DETERMINATION OF STANDARD VALUE
Perform this procedure once, when standards are received.
1. Follow the Calibration Procedure in the Colorimeter manual. Use two standards, as described, that have been titrated by an EPA accepted method (such as LaMotte Method 3176-02)..
3. Insert the DPD Chlorine Color Standard Blank into the chamber, being sure to align the index line with the arrow on the meter. Close the lid.
5. Wipe the DPD Chlorine Color Standard A (4147-E) with a clean, lint-free cloth.
2. Wipe the DPD Chlorine Color Standard Blank (4136-E) with a clean, lint-free cloth.
4. Press ON to turn the meter on. Press */ ENTER to select START. Press */ENTER to select Testing Menu. Press */ENTER to select All Tests. Press or to scroll to 015 Chlorine. Press */ENTER to select 015 Chlorine. Press */ENTER to scan the blank..
6. Insert DPD Chlorine Color Standard A into the chamber, being sure to align the index line with the arrow on the meter. Close the lid.
7. Press */ENTER to scan the sample. The concentration will be displayed.
015 Chlorine
*Scan Sample
9. Repeat steps 5-8 for DPD Chlorine Color Standard B (4138-E) and DPD Chlorine Color Standard C (4139-E).
8. Record the actual reading on the DPD Chlorine Color Standard A cap and on the Data Sheet, under initial reading.
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Page 5
SMART 2 - INSTRUMENT PERFORMANCE CHECK
Perform this procedure at specified intervals to verify instrument performance.
1.
Wipe the DPD Chlorine Color Standard Blank (4136-E) with a clean, lint-free cloth.
3.
Press ON to turn the meter on. Press */ ENTER to select START. Press */ENTER to select Testing Menu. Press */ENTER to select All Tests. Press or to scroll to 015 Chlorine. Press */ENTER to select 015 Chlorine. Press */ENTER to scan the blank..
5.
Insert DPD Chlorine Color Standard A into the chamber, being sure to align the index line with the arrow on the meter. Close the lid.
2..
Insert the DPD Chlorine Color Standard Blank into the chamber, being sure to align the index line with the arrow on the meter. Close the lid.
4.
Wipe the DPD Chlorine Color Standard A (4147-E) with a clean, lint-free cloth.
6.
Press */ENTER to scan the sample. The concentration will be displayed.
015 Chlorine
*Scan Sample
7.
Repeat steps 4-6 with DPD Chlorine Color Standard B (4138-E) and DPD Chlorine Color Standard C (4139-E).
NOTE: Store standards in a cool place out of direct light. Exposure to excessive heat or light may cause degradation of the standards.
8.
If the readings are not within the tolerance limits, standardize the meter calibration by following the Calibration Procedure in the meter manual. If the readings are still not within the tolerance limits, the standards are no longer valid and should be replaced.
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Page 6
SMART 3 - INITIAL DETERMINATION OF STANDARD VALUE
Perform this procedure once, when standards are received.
1.
Follow the Calibration Procedure in the Colorimeter manual. Use one standard, as described, that has been titrated by an EPA accepted method (such as LaMotte Method 3176-02).
3.
Insert the DPD Chlorine Color Standard Blank into the chamber, being sure to align the index line with the arrow on the meter. Close the lid.
5.
Wipe the DPD Chlorine Color Standard A (4147-E) with a clean, lint-free cloth.
2.
Wipe the DPD Chlorine Color Standard Blank (4136-E) with a clean, lint-free cloth.
4.
Press to turn the meter on. Press
ENTER
to select Testing Menu. Press
to select All Tests Menu. Press
ENTER
ENTER
to select All Tests. Press or to scroll to 014 Chlorine. Press 014 Chlorine. Press
ENTER
ENTER
to select
to scan the
blank.
6.
Insert DPD Chlorine Color Standard A into the chamber, being sure to align the index line with the arrow on the meter. Close the lid.
7.
Press to scan the sample. The concentration will be displayed.
014 Chlorine
Scan Blank
Scan Sample
12:00:00 001/500
8.
Record the actual reading on the DPD Chlorine Color Standard A cap and on the Data Sheet, under initial reading.
9.
Repeat steps 5-8 for DPD Chlorine Color Standard B (4138-E) and DPD Chlorine Color Standard C (4139-E).
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Page 7
SMART 3 - INSTRUMENT PERFORMANCE CHECK
Perform this procedure at specified intervals to verify instrument performance.
1.
Wipe the DPD Chlorine Color Standard Blank (4136-E) with a clean, lint-free cloth.
3.
Press to turn the meter on. Press
ENTER
to select Testing Menu. Press
to select All Tests Menu. Press
ENTER
ENTER
to select All Tests. Press or to scroll to 014 Chlorine. Press 014 Chlorine. Press
ENTER
ENTER
to select
to scan the
blank.
5.
Insert DPD Chlorine Color Standard A into the chamber, being sure to align the index line with the arrow on the meter. Close the lid.
2.
Insert the DPD Chlorine Color Standard Blank into the chamber, being sure to align the index line with the arrow on the meter. Close the lid.
4.
Wipe the DPD Chlorine Color Standard Blank (4136-E) with a clean, lint-free cloth.
6.
ENTER
Press
to scan the sample. The
concentration will be displayed.
014 Chlorine
Scan Blank
Scan Sample
12:00:00 001/500
7.
Repeat steps 4-6 with DPD Chlorine Color Standard B (4138-E) and DPD Chlorine Color Standard C (4139-E).
8.
If the readings are not within the tolerance limits, standardize the meter calibration by following the Calibration Procedure in the meter manual. If the readings are still not within the tolerance limits, the standards are no longer valid and should be replaced.
NOTE: Store standards in a cool place out of direct light. Exposure to excessive heat or light may cause degradation of the standards.
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Page 8
1500 - INITIAL DETERMINATION OF STANDARD VALUE
Perform this procedure once, when standards are received.
1.
Follow the Calibration Procedure in the Colorimeter manual. Use one standard, as described, that has been titrated by an EPA accepted method (such as LaMotte Method 3176-02).
3.
Insert the DPD Chlorine Color Standard Blank into the chamber, being sure to align the index line with the arrow on the meter. Close the lid.
5.
Wipe the DPD Chlorine Color Standard A (4147-E) with a clean, lint-free cloth.
2.
Wipe the DPD Chlorine Color Standard Blank (4136-E) with a clean, lint-free cloth.
4.
Press to turn the meter on. Press
ENTER
to select Testing Menu. Press
to select All Tests Menu. Press
ENTER
ENTER
to select All Tests. Scroll to and select Chlorine TT or Chlorine Liq DPD. Select Scan Blank.
6.
Insert DPD Chlorine Color Standard A into the chamber, being sure to align the index line with the arrow on the meter. Close the lid.
7.
Select Scan Sample. The concentration will be displayed.
Chlorine TT
Scan Blank
Scan Sample
12:00:00 001/500
8.
Record the actual reading on the DPD Chlorine Color Standard A cap and on the Data Sheet, under initial reading.
9.
Repeat steps 5-8 for DPD Chlorine Color Standard B (4138-E) and DPD Chlorine Color Standard C (4139-E).
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Page 9
1500 - INSTRUMENT PERFORMANCE CHECK
Perform this procedure at specified intervals to verify instrument performance.
1.
Wipe the DPD Chlorine Color Standard Blank (4136-E) with a clean, lint-free cloth.
3.
Press to turn the meter on. Press
ENTER
to select Testing Menu. Press
to select All Tests Menu. Press
ENTER
ENTER
to select All Tests. Scroll to and select Chlorine TT or Chlorine Liq DPD. Select Scan Blank.
5.
Insert DPD Chlorine Color Standard A into the chamber, being sure to align the index line with the arrow on the meter. Close the lid.
2.
Insert the DPD Chlorine Color Standard Blank into the chamber, being sure to align the index line with the arrow on the meter. Close the lid.
4.
Wipe the DPD Chlorine Color Standard Blank (4136-E) with a clean, lint-free cloth.
6.
Select Scan Sample. The concentration will be displayed.
Chlorine TT
Scan Blank
Scan Sample
12:00:00 001/500
7.
Repeat steps 4-6 with DPD Chlorine Color Standard B (4138-E) and DPD Chlorine Color Standard C (4139-E).
8.
If the readings are not within the tolerance limits, standardize the meter calibration by following the Calibration Procedure in the meter manual. If the readings are still not within the tolerance limits, the standards are no longer valid and should be replaced.
NOTE: Store standards in a cool place out of direct light. Exposure to excessive heat or light may cause degradation of the standards.
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Page 10
DATA SHEET
Due to changes in the optics, meters that were manufactured at different times will have a different response to the Chlorine Secondary Standards. The variation is due to the spectral qualities of the dye standards being slightly different from the spectral qualities of DPD. Readings of actual DPD chlorine reactions will not differ significantly between meters.
Serial Number:
Kit Lot Number:
Expiration Date:
Code Lot # Initial Reading Tolerance
4136-E Blank
4147-E ±0.05
4138-E ±0.1
4139-E ±0.2
Colorimeter Reading
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