LaMotte 3240-LI User manual

Page 1
DC1500 CHLORINE
Chlorine Colorimeter Kit • DPD Liquid
Code 3240-LI
Firmware Version 2.10 or greater
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CONTENTS
Chlorine & Bromine DPD Liquid Kit
Test Method Specications
Analysis
 Bromine ............................................................................................... 10
Calibration
 Chlorine Standards ...........................................................................12
 Chlorine Calibration Procedure ....................................................... 12
Set Up
 Setting the Clock ...............................................................................15
 Logging Data ......................................................................................16
 Factory Setup .....................................................................................17
 Setting Power Save ...........................................................................17
 Setting Backlight Time .....................................................................18
 Selecting A Language .......................................................................19
 Looping Menus ................................................................................... 20
Computer Connection
 Output ..................................................................................................21
 Computer Connection ....................................................................... 21
Battery
 Battery/AC Operation ........................................................................21
 Battery Replacement ........................................................................ 22
Maintenance
 Cleaning ..............................................................................................22
 Repairs ................................................................................................22
 Meter Disposal ...................................................................................23
General Operating Information
 Overview .............................................................................................. 24
 General Operating Information .......................................................24
 The Keypad .........................................................................................24
 The Display and Menus ..................................................................... 25
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 Tubes and Chambers.........................................................................27
 Sample Dilution Techniques ............................................................27
General information
 Packaging and Delivery ....................................................................28
 General Precautions .......................................................................... 28
 Safety Precautions ............................................................................ 28
 Limits of Liability ...............................................................................29
Specications ....................................................................................29
 CE .........................................................................................................30
 IP67 ...................................................................................................... 30
 Warranty .............................................................................................30
 Register Your Meter...........................................................................30
Trouble Shooting Guide
 Error Messages ..................................................................................31
 Calibration ..........................................................................................31
 Stray Light ..........................................................................................31
 Troubleshooting Guide ......................................................................32
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DC1500 Chlorine & Bromine DPD Liquid Kit
 Kit Contents
QUANTITY CONTENTS CODE
30 mL DPD 1A Free Chlorine Reagent P-6740-G
30 mL *DPD 1B Free Chlorine Reagent *P-6741-G
30 mL *DPD 3 Total Chlorine Reagent *P-6743-G
1 Colorimeter Tubes, w/caps,set of 6 0290-6
1 Water Sample Collecting Bottle 0688
1 1500 Colorimeter for Chlorine DPD 27926-CL
1 USB Wall Adapter 1721
1 USB Cable 1720
1 DC1500-CL Chlorine Colorimeter, DPD
Liquid Manual
1 DC1500-CL Chlorine Colorimeter, DPD
Liquid Quick Start Guide
*WARNING: Reagents marked with an * are considered to be potential health hazards.
reagent label, in the contents that follows or precedes the four digit code number. For example if code is 4450WT-H, search 4450. To obtain a printed copy, contact LaMotte by e-mail, phone or fax.
To view or print a Safety Data Sheet (SDS) for these reagents go to
Search the four digit reagent code number listed on the
list or in the test procedures. Omit any letter
3240-LI-MN-CL
3240-LI-QG-CL
To order individual reagents or test kit components, use the specied code
number.
 Accessories
DESCRIPTION CODE
Test Tubes, with Caps 0290-6
Replacement Chamber 3-0038
USB Cable 1720
USB Wall Adapter 1721
Car Charger 5-0132
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TEST METHODS SPECIFICATIONS
 APPLICATION
Drinking water supplies and distribution systems, swimming pool and spas, sewage and chlorinated waste waters, process waters and sanitizing solutions.
 RANGE
0 to 4.0 ppm Chlorine (may be extended by dilution) 0 to 7.0 ppm Bromine (may be extended by dilution)
 METHOD
In the absence of Iodide, Free Available Chlorine reacts instantly with the
buered diethyl-p-phenylenediamine indicator (DPD) to produce a pink-red
color in proportion to the amount of chlorine present. Subsequent addition of potassium iodide produces a rapid color response from the combined forms
of chlorine (chloramines). In buered samples, bromine reacts with disthyl-
p-phenylene diamine (DPD) to produce a pink-red color in proportion to the concentration of bromine present.
 HANDLING & PRESERVATION
Chlorine and bromine in aqueous solutions, particularly weak solutions, are not stable. Exposure to sunlight or agitation will accelerate the reduction of
chlorine and bromine. For chlorine samples, ll sample containers to the top
and cap tightly. Analyze samples as soon as possible after collection. Samples to be analyzed for bromine cannot be preserved or stored.
 INTERFERENCES
The only interfering substance likely to be encountered is oxidized manganese. The extent of this interference can be determined by treating a sample with sodium arsenite to destroy the chlorine or bromine present, so that the amount of interference can be estimated. Chlorine, bromine, and iodine will give a positive result and should be considered an interference
unless the test is being performed specically for that parameter.
 CALIBRATION
The colorimeter is precalibrated. In order to comply with NPDWR or NPDES reporting regulations, the calibration should be checked periodically by using a set of reference standards including a 0 mg/L blank and 0.3, 1.0, and 3.5 mg/L chlorine. To prepare these standards, a LaMotte 1000 mg/L standard chlorine equivalent solution (Code 3858) is available. Consult with your local regulatory agency to determine standardization frequency.
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ANALYSIS - CHLORINE
PROCEDURE – FREE CHLORINE
1. Fill the Water Sample Collecting Bottle (0688) with sample water.
Chlorine
2. Press and hold until colorimeter turns on.
3. Press
ENTER
to select Testing
Menu.
4. Scroll to and select 024 Chlorine L DPD from menu.
Main Menu
Testing Menu
Editing Menu
12:00:00 001/500
All Tests
015 Bromine L DPD
016 Bromine T DPD
024 Chlorine L DPD
025 Chlorine T DPD
12:00:00 001/500
024 Chlorine L DPD
Scan Blank
Scan Sample
12:00:00 001/500
5. Rinse a clean tube (0290) with sample water. Fill to the 10 mL line with sample. Cap and wipe dry.
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6. Insert tube into chamber, close lid and select Scan Blank.
Chlorine
7. Remove tube from colorimeter. Add 5 drops of DPD 1A Free Chlorine Reagent (P-6740) and add 5 drops of *DPD 1B Free Chlorine Reagent (P-6741), Cap and invert to mix. The solution will be pink if chlorine is present. Read within 30 seconds.
8. Immediately insert tube into chamber. Close lid. Select Scan Sample. Record result as Free Chlorine.
0.99 ppm
Scan BLank
Scan Sample
12:00:00 001/500
PROCEDURE – COMBINED CHLORINE
9. Remove tube from colorimeter. Add 5 drops of *DPD 3 Total Chlorine Reagent (P-6743). Cap and invert to mix. An increase in color represents Combined Chlorine.
DPD
DPD
024 Chlorine L DPD
1A
DPD
3
1B
NOTE: For wastewater samples, Standard Methods for the Examination of Water and Wastewater recommends waiting 2 minutes for full color development when testing
total chlorine.
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10. Insert tube into chamber, close lid and select Scan Sample. Record result as Total Chlorine (Monochloramine, Dichloramine, and Nitrogen Trichloride) present in the water sample.
11. Subtract free chlorine reading from total chlorine reading to obtain concentration of combined chlorine.
Chlorine
12. Press to turn o the colorimeter or press
EXIT
to exit to a
previous menu or make another menu selection.
Levels of chlorine about 4 mg/L will cause a bleaching eect on the DPD
indicator, and may give a false indication that no chlorine is present. If if is possible that the chlorine concentration is greater than 4 mg/L, perform test on a diluted sample and multiply the result by appropriate dilution factor.
CAUTION: DO NOT leave reacted samples in test tubes. Discard sample and thoroughly rinse tubes. If allowed to remain, DPD wil stain tubes, signigicantly impairing the operation of the colorimeter. If necessary, acid wash, and vigorously clean glassware with test tube brush and detergent.
NOTE: For the most accurate results, samples over 4 ppm chlorine should be diluted with chlorine demand free water and re-tested.
NOTE: The meter will remember the last scanned blank reading. It is not necessary to scan a blank each time the test is performed. To use the previous blank reading, instead of scanning a new one, scroll to Scan Sample and proceed. For the most accurate results, the meter should be blanked before each test and the same tube should be used for the blank and the reacted sample.
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ANALYSIS - BROMINE
PROCEDURE
1. Fill the Water Sample Collecting Bottle (0688) with sample
Bromine
water.
2. Press and hold until colorimeter turns on.
3. Press
ENTER
to select Testing
Menu.
4. Scroll to and select 015 Bromine L DPD from menu.
Main Menu
Testing Menu
Editing Menu
12:00:00 001/500
All Tests
015 Bromine L DPD
016 Bromine T DPD
024 Chlorine L DPD
025 Chlorine T DPD
12:00:00 001/500
015 Bromine L DPD
Scan Blank
Scan Sample
12:00:00 001/500
5. Rinse a clean tube (0290) with sample water. Fill to the 10 mL line with sample. Cap and wipe dry.
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6. Insert tube into chamber, close lid and select Scan Blank.
Bromine
7. Remove tube from colorimeter. Add 5 drops of DPD 1A Free Chlorine Reagent (P-6740) and add 5 drops of *DPD 1B Free Chlorine Reagent (P-6741), Cap and invert to mix. The solution will be pink if bromine is present. Read within 30 seconds.
8. Immediately insert tube into chamber. Close lid. Select Scan Sample. Record result as Bromine.
NOTE: For the most accurate results, samples over 7 ppm bromine should be diluted with chlorine demand free water and re-tested.
NOTE: The meter will remember the last scanned blank reading. It is not necessary to scan a blank each time the test is performed. To use the previous blank reading, instead of scanning a new one, scroll to Scan Sample and proceed. For the most accurate results, the meter should be blanked before each test and the same tube should be used for the blank and the reacted sample.
0.99 ppm
Scan BLank
Scan Sample
12:00:00 001/500
DPD
DPD
015 Bromine L DPD
1A
1B
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CALIBRATION
 CHLORINE STANDARDS
The meter should be calibrated with free chlorine standards. The calibration should be done with a distilled or deionized water blank and one chlorine standard of known concentration. The concentration of the calibration
Calibration
standard should be similar to the expected concentration of the sample that will be tested.
To perform a bromine calibration, prepare a bromine with a concentration that is equivenlent to a chlorine dioxide standard that is within the range of the chlorine dioxide test. (1 ppm chlorine = 1.9 ppm bromine). Follow the procedure below but select the bromine test.
Chlorine Secondary Standards (Code 4140-03) are available to verify the performance of the meter.
CHLORINE CALIBRATION PROCEDURE
1. Press and briey hold to turn the meter on. The LaMotte logo screen will appear for about 3 seconds and the Main Menu will appear.
2. Press
3. Scroll to and select 024 Chlorine
ENTER
to select Testing
Menu.
L DPD from menu.
Main Menu
Testing Menu
Editing Menu
12:00:00 001/500
All Tests
015 Bromine L DPD
016 Bromine T DPD
024 Chlorine L DPD
025 Chlorine T DPD
12:00:00 001/500
024 Chlorine L DPD
Scan Blank
Scan Sample
12:00:00 001/500
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4. Rinse a clean tube (0290) three times with the chlorine standard. Fill to the 10 mL line with the chlorine standard. Cap the tube. Dry the tube with a lint-free cloth.
5. Insert tube into chamber, close lid and select Scan Blank.
Calibration
6. Remove tube from colorimeter. Add 5 drops of DPD 1A Free Chlorine Reagent (P-6740) and add 5 drops of *DPD 1B Free Chlorine Reagent (P-6741), Cap and invert to mix. The solution will be pink if chlorine is present. Read within 30 seconds.
7. Immediately insert tube into chamber. Close lid. Select Scan Sample.
8. Press to scroll to Calibrate.
DPD
DPD
024 Chlorine L DPD
1A
1B
0.99 ppm
Scan BLank
Scan Sample
12:00:00 001/500
024 Chlorine L DPD
0.99 ppm
%T/Abs
Calibrate
12:00:00 001/500
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9. Press A reverse font (light background with dark characters) will appear to indicate that the reading can be adjusted.
Calibration
ENTER
to select Calibrate.
024 Chlorine L DPD
0.99 ppm
∧, ∨=Edit, ENTER=Save
+ENTER=Default
12:00:00 001/500
10. Press or to adjust the value shown to the concentration of the prepared standard, 1.00 in this example. NOTE: A maximum adjustment of 25% is possible.
11. Press
ENTER
to save the value.
To leave the Calibration procedure without saving the adjustment, press
Press time to return to the default value.
The calibration has now been standardized and can be used for testing. Scroll to Scan Blank and begin testing.
and
EXIT
ENTER
.
at any
024 Chlorine L DPD
1.00 ppm
∧, ∨=Edit, ENTER=Save
+ENTER=Default
12:00:00 001/500
024 Chlorine L DPD
1.00 ppm
%T/Abs
Calibrate
12:00:00 001/500
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SET UP
 SETTING THE CLOCK
Setting the clock allows the correct time and date stamp to be stored with each reading in the data logger.
1. From the Editing Menu, press
or to scroll to Set
Clock.
2. Press
ENTER
to select Set Clock.
The year is displayed. Press
or to scroll to the
appropriate character. Press
ENTER
to select the character. The month, day, hour, format hour, minute, second, AM/PM will be dislpayed. Repeat for each.
3. Press
ENTER
to select the nal
character. The time and date will be saved and the meter will return to the Editing Menu.
Editing Menu
Set Clock
Logging
Factory Setup
Set Power Save
12:00:00 001/500
Set Time
Year: 2000
12:00:00 001/500
Editing Menu
Set Clock
Logging
Factory Setup
Set Power Save
12:00:00 001/500
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 LOGGING DATA
The default setting for the data logger is enabled. The meter will log the last 500 data points. The counter in the center bottom of the display will show how many data points have been logged. The display will show 500+ when the data logger has exceeded 500 points and the data points are being overwritten.
1. From the Editing Menu, press or to scroll to
Logging.
2. Press
ENTER
to select Logging.
3. Press or to scroll to
desired function.
Editing Menu
Set Clock
Logging
Factory Setup
Set Power Save
12:00:00 001/500
Logging
Display Test Log
Logging Enabled
Logging Disabled
Erase Log
12:00:00 001/500
Logging
Display Test Log
Logging Enabled
Logging Disabled
Erase Log
12:00:00 001/500
4. Press
ENTER
. The screen will display Storing... for about 1 second and return to the Editing Menu.
Set Clock
Logging
Editing Menu
Factory Setup
Set Power Save
12:00:00 001/500
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 FACTORY SETUP
The Factory Setup menu is used in manufacturing of the colorimeter. This
menu is not for use by the operator in the eld.
 SETTING POWER SAVE
The power saving Auto Shuto feature will turn the meter o when a button
has not been pushed for a set amount of time. The default setting is disabled. To change the setting:
1. From the Editing Menu, press or to scroll to Set
Power Save.
2. Press
ENTER
to select Set Power
Save.
3. Press or to scroll to
desired function.
Editing Menu
Set Clock
Logging
Factory Setup
Set Power Save
12:00:00 001/500
Set Power Save
Disable
5 Minutes
15 Minutes
30 Minutes
12:00:00 001/500
Set Power Save
Disable
5 Minutes
15 Minutes
30 Minutes
12:00:00 001/500
4. Press
ENTER
. The screen will
display Storing.... for about 1
second and the meter will retun to the Editing Menu.
Set Clock
Logging
Editing Menu
Factory Setup
Set Power Save
12:00:00 001/500
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 SETTING THE BACKLIGHT TIME
The backlight illuminates the display for enhanced viewing. The default setting is 10 seconds. If Button Control is chosen the backlight button on the key pad
will act as an on/o switch and the backlight will remain on or o when the
meter is being used. When one of the other settings – 10, 20 or 30 seconds –
is chosen, the display will be illuminated for the specied amount of time after
any button is pressed.
NOTE: The backlight feature uses a signicant amount of power. The longer
the backlight is on, the more frequently the battery will have to be charged if the USB/Wall Adapter is not being used.
1. From the Editing Menu, press or to scroll to
Backlight Time.
2. Press
ENTER
to select Set
Backlight Time.
3. Press or to scroll to
desired option.
Editing Menu
Logging
Factory Setup
Set Power Save
Set Backlight Time
12:00:00 001/500
Set Backlight Time
Button Control
10 seconds
20 seconds
30 seconds
12:00:00 001/500
Set Backlight Time
Button Control
10 seconds
20 seconds
30 seconds
12:00:00 001/500
4. Press
ENTER
. The screen will display Storing... for about 1 second and the meter will return to the Editing Menu.
Logging
Factory Setup
Editing Menu
Set Power Save
Set Backlight Time
12:00:00 001/500
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 SELECTING A LANGUAGE
There are seven languages available: English, Spanish, French, Portuguese, Italian, Chinese, and Japanese.
1. From the Editing Menu, press or to scroll to
Select Language.
2. Press
ENTER
to select Select
Language.
3. Press or to scroll to
desired language.
Editing Menu
Factory Setup
Set Power Save
Set Backlight Time
Select Language
12:00:00 001/500
Select Language
English
Spanish
French
Portugese
12:00:00 001/500
Select Language
English
Spanish
French
Portugese
12:00:00 001/500
4. Press
ENTER
. The screen will display Storing... for about 1 second and the meter will return to the Editing Menu.
Set Power Save
Set Backlight Time
Editing Menu
Bluetooth Menu
Select Language
12:00:00 001/500
NOTE: If meter unintentionally switches to another language, use the procedure above to reset the meter to the desired language. For example, to reset the meter to English:
Turn meter on.
1. Press one time. Press
2. Press ve times. Press
3. Press
ENTER
.
ENTER
ENTER
.
.
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 LOOPING MENUS
Long menus, such as All Tests, incorporate a looping feature which allows
the user to quickly reach the last choice in the menu from the rst choice. In a looping menu the last choices in the menu are above the rst choice
and scrolling upward moves through the menu in reverse order. Scrolling
downward moves through the menu from rst choice to last but the menu
starts over following the last choice. So all menu choices can be reached by scrolling in either direction. The diagrams below demonstrate a looping menu.
AND SO ON AND SO ON AND SO ON
: : : : : : : : :
: : : : : : : : :
THIRD TO LAST LAST CHOICE LAST CHOICE
SECOND TO LAST AND SO ON AND SO ON
LAST CHOICE : : : : : :
TESTING MENU TESTING MENU TESTING MENU
FIRST CHOICE : : : : : :
SECOND CHOICE THIRD TO LAST THIRD TO LAST
THIRD CHOICE
ANOTHER LAST CHOICE LAST CHOICE
12:00:00 001/500 12:00:00 001/500 12:00:00 001/500
AND ANOTHER FIRST CHOICE FIRST CHOICE
AND SO ON SECOND CHOICE SECOND CHOICE
: : : THIRD CHOICE THIRD CHOICE
: : : ANOTHER ANOTHER
LAST CHOICE AND ANOTHER AND ANOTHER
SECOND TO LAST SECOND TO LAST
The feature called Looping Menu can be turned on and o in the Editing Menu. The default setting is ON.
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COMPUTER CONNECTION
 OUTPUT
USB
 COMPUTER CONNECTION
USB Type A, USB mini B, Order Cable Code 1720.
 WATERLINK CONNECT
The meter may be interfaced with any Windows-based 64 bit computer by using the LaMotte WaterLink Connect program and a USB cable. The program will store test information and results in a local database, and allow
for exporting this data to a comma separated value (CSV) le. The meter
will send the following data: time/date stamp, name of test, sample value, sample units, meter name, and location. To download WaterLink go t
BATTERY
 BATTERY/AC OPERATION
The colorimeter may be operated on battery power using a USB wall adapter or USB computer connection. If using the meter as a bench top unit, use the wall adapter if possible to extend the battery life. The meter will remain on when the USB adapter is used.
To charge the battery with the wall adapter, plug the smaller end of the USB cable (USB mini B connector) into the meter and the larger end of the USB cable (USB type A connector) into the wall adapter. Plug the wall adapter into an AC outlet. Reinsert the rubber USB port plug after charging. To charge the battery from a computer, plug the smaller end of the USB cable (USB mini B connector) into the meter and the larger end of the USB cable (USB Type A connector) into a USB port on a computer. The battery icon will show no bars
and ash when the unit rst turns on. Then the indicator will indicate the
battery status by showing 0, 1, 2, 3, or 4 bars.
It will take 6 hours to fully charge a low battery. The battery icon will ash
when the battery is charging. The battery icon will show four bars and stop
ashing when it is fully charged. The charging circuit will automatically switch to a oat charge when the battery is fully charged. The charger may remain
connected. Some computers will NOT supply power to their USB ports during standby operation. The wall adapter will charge the unit continuously.
Storing the meter above ambient room temperature will decrease the battery charge more quickly than storage at room temperature. If the meter does not turn on, it means that the battery is at a very low charge. Charging the battery with the wall adapter in this state may take up to 10 hours. At low temperatures, approaching 0 °C, the battery will charge more slowly. It will not charge at all below 0 °C. The battery icon will show no bars and continuously
ash if the battery is getting low but the unit will still operate normally. A
“Low Battery” message on the status bar of the display will replace the time
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when the battery voltage is too low for proper operation and accuracy may be degraded. A “Shutdown Low Batt” message on the display will appear for
a few seconds before the power is switched o when the battery is too low to operate the unit. When the battery icon simultaneously ashes bars 1 and 2
followed by bars 3 and 4, it is an indication that the battery is damaged and technical support should be contacted.
To extend the battery life:
• Shut down the unit with the power switch when not taking measurements or use the power save option to have the unit
automatically turn o after 5 minutes.
• Store the unit at a moderate temperature.
• Fully charge the battery before storing the unit for extended periods of time.
• Fully charge the battery at least once per year. Failure to do so may result in a permanently drained battery.
• Limit backlight use. The unit consumes 3X normal power with the backlight on. Set the backlight time option to 10 seconds, or select
“Button Control” and keep the backlight o.
BATTERY REPLACEMENT
The lithium ion battery used in this unit should last for many years with normal use. When it no longer powers the unit long enough to meet testing requirements it will need to be replaced. Lithium ion batteries that are properly charged and stored do not usually lose all capacity; they just have less capacity after hundreds of charge cycles. This unit uses a custom battery assembly that is only available from LaMotte Company. Battery replacement must be performed at a LaMotte authorized repair facility. The water resistant housing of this meter should not be opened by the user
MAINTENANCE
 CLEANING
Clean the exterior housing with a damp, lint-free cloth. Do not allow water to enter the light chamber or any other parts of the meter. To clean the light chamber and optics area, point a can of compressed air into the light chamber and blow the pressurized air into the light chamber. Use a cotton swab dampened with Windex® window cleaner to gently swab the interior of the chamber. Do not use alcohol; it will leave a thin residue over the optics when dry.
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 METER DISPOSAL
Waste Electrical and Electronic Equipment (WEEE) Natural resources were used in the production of this equipment. This
equipment may contain materials that are hazardous to health and the environment. To avoid harm to the environment and natural resources, the use of appropriate take-back systems is recommended. The crossed out wheeled bin symbol on the meter encourages the use of these systems when disposing of this equipment.
Take-back systems will allow the materials to be reused or recycled in a way that will not harm the environment. For more information on approved collection, reuse, and recycling systems contact local or regional waste administration or recycling services.
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GENERAL OPERATING INFORMATION
 OVERVIEW
The meter is a portable, microprocessor controlled, direct reading colorimeter. It has a graphical liquid crystal display and 6 button keypad. These allow the user to select options from the menu driven software, to directly read test results or to review stored results of previous tests in the data logger. The
menus can be displayed in seven dierent languages.
The LaMotte tests are precalibrated for LaMotte reagent systems. The colorimeter displays the result of these tests directly in units of concentration.
The optics feature a colored LED. The LED has a corresponding silicon
photoiode with an integrated interference lter. The interference lter selects
a narrow band of light from the corresponding LED for the colorimetric measurements.
A USB wall adapter, USB computer connection or lithium battery powers the colorimeter.
GENERAL OPERATING INFORMATION
The operation of the colorimeter is controlled by the menu driven software and user interface. A menu is a list of choices. This allows a selection of various tasks for the colorieter to perform, such as scan blank and scan sample. The keypad is used to make menu selections that are viewed on the display.
 THE KEYPAD
The keypad has 6 buttons which are used to perform specic tasks.
ENTER
EXIT
This button will scroll up through a list of menu selections.
The button is used to select choices in a menu viewed on the display.
This button controls the backlight on the display.
This button will scroll down through a list of menu selections.
This button exits to the previous menu.
This button turns the meter on or o.
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Page 24
ENTER
EX IT
 THE DISPLAY AND MENUS
The display allows menu selections to be viewed and selected. These
selections instruct the colorimeter to perform specic tasks. The menus are
viewed in the display using two general formats that are followed from one menu to the next. Each menu is a list of choices or selections.
The display has a header line at the top and a footer line at the bottom. The header displays the title of the current menu. The footer line displays the time and the date, the data logger status and the battery status. The menu selection window is in the middle of the display between the header and the footer.
The menu selection window displays information in two general formats. In
the rst format only menu selections are displayed. Up to 4 lines of menu
selections may be displayed. If more selections are available they can be viewed by pressing the arrow buttons to scroll the other menu selections into the menu selection window. Think of the menu selections as a vertical list in the display that moves up or down each time an arrow button
is pressed. Some menus in the colorimeter are looping menus. The top and bottom menu choices are connected in a loop. Scrolling down past the bottom of the menu will lead to the top of the menu. Scrolling up past the top of the menu will lead to the bottom of the menu.
Header Menu Title
Main Window Selection First Choice
Second Choice
Third Choice
Another
Footer
12:00:00 001/500 P
And Another
And So On
A light bar will indicate the menu choice. As the menu is scrolled through, the
light bar will highlight dierent menu choices. Pressing the
ENTER
button will
select the menu choice that is indicated by the light bar. In the second format the menu choice window takes advantage of the
graphical capabilities of the display. Large format graphic information, such as test results or error messages or the LaMotte logo is displayed. The top two lines of the display are used to display information in a large, easy to read
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Page 25
format. The menus work in the same way as previously described but two lines of the menu are visible at the bottom of the display.
Header Menu Title
Message or Result Window
Result or Message
Another
Main Window Selection And Another
Footer
As described previously, the current menu and a return to the previous menu. This allows a rapid exit from an inner menu to the main menu by repeatedly pushing the Pushing at any time will turn the colorimeter o.
The display may show the following messages:
Battery Status
More choices are available and can be viewed by scrolling up and/or down through the display.
EXIT
12:00:00 001/500
And So On
Last Choice
button allows an exit or escape from the
EXIT
button.
Header Identies the current menu and information on units and
reagent systems if applicable.
Footer In the data logging mode the number of the data point
is displayed and the total number of data points in the memory will be shown. The footer also shows current time and battery status
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Page 26
 TUBES AND CHAMBERS
The colorimeter uses one type of tube (Code 0290) for all test factors. The handling of the tubes is of utmost importance. Tubes must be clean and
free from lint, ngerprints, dried spills and signicant scratches, especially
the central zone between the bottom and the sample line.
Scratches, ngerprints and water droplets on the tube can cause stray light
interference leading to inaccurate results. Tubes that have been scratched in the light zone through excessive use should be discarded and replaced with new ones.
Tubes should always be washed on the inside and outside with mild detergent
prior to use to remove dirt or ngerprints. The tubes should be allowed to air-
dry in an inverted position to prevent dust from entering the tubes. Dry tubes should be stored with the caps on to prevent contamination.
After a tube has been lled and capped, it should be held by the cap and the
outside surface should be wiped with a clean, lint-free absorbent cloth until it is dry and smudge-free. Handling the tube only by the cap will avoid problems
from ngerprints. Always set the clean tube aside on a clean surface that will
not contaminate the tube. It is imperative that the tubes and light chamber be clean and dry. The outside of the tubes should be dried with a clean, lint-free cloth or disposable wipe before they are placed in the meter chamber.
Tubes should be emptied and cleaned as soon as possible after reading a sample to prevent deposition of particulates on the inside of the tubes.
Variability in the geometry of the glassware and technique is the predominate cause of variability in results. Slight variations in wall thickness and the diameter of the tubes may lead to slight variations in the test results. To eliminate this error the tubes should be placed in the chamber with the same orientation each time.
Chambers which have been scratched through excessive use should be discarded and replaced with a new one.
 SAMPLE DILUTION TECHNIQUES
If a test result is out of the range of the meter, it must be diluted. The test should then be repeated on the diluted sample. The following table gives quick reference guidelines for dilutions of various proportions.
Amount of Sample Deionized Water to Bring
Final Volume to 10 mL
10 mL 0 mL 1
5 mL 5 mL 2
2.5 mL 7.5 mL 4
1 mL 9 mL 10
0.5 mL 9.5 mL 20
All dilutions are based on a nal volume of 10 mL, so several dilutions will
require small volumes of the water sample. Graduated pipets should be used for all dilutions. If volumetric glassware is not available, dilutions can
28
Multiplication Factor
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Page 27
be made with the colorimeter tube. Fill the tube to the 10 mL line with the sample and then transfer it to another container. Add 10 mL volumes of deionized water to the container and mix. Transfer 10 mL of the diluted sample to the colorimeter tube and follow the test procedure. Repeat the dilution and testing procedures until the result falls within the range of the calibration. Multiply the test result by the dilution factor. For example, if 10 mL of the sample water is diluted with three 10 mL volumes of deionized water, the dilution factor is four. The test result of the diluted sample should be multiplied by four.
GENERAL INFORMATION
 PACKAGING AND DELIVERY
Experienced packaging personnel at LaMotte Company assure adequate protection against normal hazards encountered in transportation of shipments.
After the product leaves LaMotte Company, all responsibility for safe delivery
is assured by the transportation company. Damage claims must be led
immediately with the transportation company to receive compensation for damaged goods.
 GENERAL PRECAUTIONS
READ THE INSTRUCTION MANUAL BEFORE ATTEMPTING TO SET UP OR
OPERATE THE METER. Failure to do so could result in personal injury or damage to the meter. The meter should not be used or stored in a wet or corrosive environment. Care should be taken to prevent water from wet tubes from entering the meter chamber.
NEVER PUT WET TUBES IN THE METER.
 SAFETY PRECAUTIONS
Read the labels on all LaMotte reagent containers prior to use. Some
containers include precautionary notices and rst aid information. Certain
reagents are considered hazardous substances and are designated with a * in the instruction manual. Safety Data Sheets (SDS) can be found at
Keep equipment and reagent chemicals out of the reach of young children. Ensure that the protection provided by this equipment is not impaired. Do not
intall or use this equipment in a manner that is not indicated in this manual.
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 LIMITS OF LIABILITY
Under no circumstances shall LaMotte Company be liable for loss of life,
property, prots, or other damages incurred through the use or misuse of its
products.
 SPECIFICATIONS & RANGES
INSTRUMENT TYPE: Colorimeter
Readout 160 x 100 backlit LCD, 20 x 6 line graphical
display
Wavelengths 525 nm
Wavelength Accuracy ±2% FS
Readable Resolution Determined by reagent system
Wavelength Bandwidth 10 nm typical
Photometric Range –2 to +2 AU
Photometric Precision ± 0.001 AU at 1.0 AU
Photometric Accuracy ±0.005 AU at 1.0 AU
Sample Chamber Accepts 25 mm diameter at-bottomed test
tubes
Light Sources 1 LEDs
Detectors 1 silicon photodiode
Modes Pre-programmed tests, absorbance, %T
Pre-Programmed Tests YES, with automatic wavelength selection
Languages English, Spanish, French, Portuguese, Italian,
Chinese, Japanese
Temperature Operation: 0-50 °C; Storage: -40-60 °C
Operation Humidity Range
USB Port Mini B
Power Requirements USB wall adapter, USB computer connection or
Battery Charge Life: Approximately 380 tests with
Electrical Rating Rated voltage (5V), Rated power of input current
Data Logger 500 test results
Waterproof IP67 with USB port plug in place
Dimensions (LxWxH) 3.5 x 7.5 x 2.5 inches, 8.84 x 19.05 x 6.35 cm
0-90 % RH, non-condensing
lithium ion rechargeable battery
backlight on to 1000 tests with backlight o.
Battery Life: Approximately 500 charges.
(1.0A) at mini-USB input port
Weight 13 oz, 362 g (meter only)
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 CE COMPLIANCE
The colorimeter has been independently tested and has earned the European CE Mark of compliance for electromagnetic compatibility and safety. To view
certicates of compliance, go t
IP67 Certication
The meets IP67 standards for protection against dust and immersion only when the USB port plug is in place. Documentation is available at www.
TROUBLESHOOTING
 ERROR MESSAGES
Over Range
If the message OVERRANGE is displayed when scanning a sample, the sample may be over range or under range. If the sample is over range the sample should be diluted and tested again (see Sample Dilution Techniques and Volumetric Measurements, page 27).
If overrange is displayed, press
ENTER
to continue testing on diluted
samples.
Note: After pressing overrange cncentration will be displayed. This concentration is an approximation only.
ENTER
, the
Overrange
<Enter> continue
Scan Blank
Scan Sample
12:00:00 001/500
31
025 Chlorine T DPD
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Page 30
 CALIBRATION
As with all pre-calibrated meters, it is highly recommended, even if not required by regulations, that the user periodically verify the performance of the meter by running standards with a predetermined concentration. Results
outside of specication are an indication that the meter needs to be adjusted.
This can be done following the user calibration described on page 24. If the user calibration fails to properly adjust the meter then the meter should be returned to LaMotte Company for recalibration. (See page 30).
 STRAY LIGHT
The colorimeter should have no problems with stray light. Make sure that the sample compartment lid is always fully closed.
 TROUBLESHOOTING GUIDE
PROBLEM REASON SOLUTION
Flashing
“Low Battery” Battery voltage is very
“Shut Down Low Batt” Shut Down
“Overrange” Sample is outside of
Low battery. Readings are reliable.
low. Readings are not reliable.
Battery is too low to operate the unit.
acceptable range.
Charge battery or use USB wall/computer adapter.
Charge battery or use USB wall/computer adapter.
Charge battery or use USB wall/computer adapter.
Dilute sample and test again.
Unusually large negative or positive readings when performing calibration
Incorrect standards used to calibrate meter.
Use fresh 0.0 standard in clean tube. Reset meter to factory default settings. Recalibrate meter.
3240-LI-MN-CL 08.19
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