LaMotte Tracer DO PockeTester, 1761 User Manual

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Tracer DO PockeTesterTM
Code 1761
FILL - Before first use
POLARIZE - Weekly
CALIBRATE - Daily
Water Testing Leader Since 1919!
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WARNING! This set contains chemicals
that may be harmful if misued. Read
cautions on individual containers
carefully. Not to be used by children
except under adult supervision.
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TRACER
DISSOLVED OXYGEN • CODE 1761
Introduction .....................................................................................4
Specifi cations ..................................................................................4
Contents ..........................................................................................4
Parts & Accessories ........................................................................5
Meter Description
Front Panel Description ............................................................... 5
Display .......................................................................................... 5
Operation
Filling the Electrode ..................................................................... 6
Powering the TRACER ................................................................. 6
Startup Polarization Period .......................................................... 6
Turn-on Diagnostics .................................................................... 6
Changing the Temperature Units ................................................ 6
Changing Salinity Compensation................................................ 7
Changing the Altitude Compensation ......................................... 7
Changing Measurement Units ..................................................... 7
Auto-Power Off Feature ............................................................... 8
Disabling Auto-Power Off Feature ............................................... 8
Low Battery Indicator ................................................................... 8
Storing Readings ......................................................................... 8
Recalling Stored Readings .......................................................... 8
Clearing Stored Readings ........................................................... 8
Set Up
Membrane Cap Assembly - Filling and Replacement ................ 9
Polarization ................................................................................. 10
Calibration ................................................................................... 10
Optional Zero Oxygen Calibration.............................................. 11
Dissolved Oxygen Measurement ...................................................12
Operational Matrix ..........................................................................13
Troubleshooting .............................................................................16
Maintenance
Battery Replacement ..................................................................17
Battery Safety .............................................................................. 17
Electrode Replacement ............................................................. 17
Replacing the Membrane Cap .................................................... 17
Electrode Storage ....................................................................... 18
Warranty ...................................................................................... 18
Short Form Instructions (back cover)
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INTRODUCTION
Congratulations on your purchase of the Dissolved Oxygen/Temperature TRACER. Units of measure are % saturation, mg/L or ppm for dissolved oxygen for temperature. Advanced features include data hold, 25 point memory, automatic temperature compensation, and salinity/altitude compensation. Careful use and maintenance will provide years of reliable service.
and C° or F°
auto shut off,
SPECIFICATIONS
Display 2000 count, Dual function 3 ½ digit LCD
Display size 24 mm x 20 mm
Sensor Polarographic type
Membrane Bonded membrane cap with threaded f tting
Operating Temp. Range 0 to 50°C (32 to 122°F)
ATC Range 0 to 50°C (32 to 122°F)
Salinity Compensation 0 to 50 ppt in 1 ppt (part per thousand) increments
Altitude compensation 6000 m (0 to 20,000 ft) in 300m (1000 ft) increments
Measurement Storage 25 tagged (numbered) data sets with recall
Battery Power Four (4) CR2032 button batteries
Low Battery Indication ‘BAT’ appears on the LCD
Auto Power Off
Dimensions/Weight 36 x 173 x 41mm (1.4 x 6.8 x 1.6”); 110g (3.8 oz)
Measurement Range Resolution Accuracy
% Saturation 0 to 200.0% 0.1% ±2.0% FS (full scale) Dissolved Oxygen 0 to 20.00 mg/l 0.01 mg/l ±2% FS Concentration 0 to 20.00 ppm 0.01 ppm ±2% FS Temperature 0 to 50 °C 0.1 °C ±1.0 °C
with Bar graph
After 10 minutes of inactivity (APO override available)
32 to 122°F 0.1 °F (0 to 99ºF);
1.0 °F (>100°F)
±1.8°F
CONTENTS
Dissolved Oxygen TRACER Kit Code 1761 Includes:
DO TRACER Body DO Bonded Membrane Cap Assembly Electrolyte Solution Code DO600-EL Sample cup and Lanyard
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PARTS & ACCESSORIES
DO Replacement Sensor Kit (sensor module, membrane cap assembly, electrolyte solution) DO Membrane Cap Kit (6 membrane cap assemblies, electrolyte solution, Polishing Strips) DO Extension Cable, 1 meter (with probe guard and weight) DO Extension Cable, 1 meter (with probe guard and weight)
METER DESCRIPTION
Front Panel Description
1. Battery compartment cover
2. LCD Display
3. MODE button
4. CAL button
5. ON/OFF button
6. Electrode Retaining Collar
7. Dissolved Oxygen Sensor
8. Bonded membrane cap assembly
9. Membrane & cathode (Note: The Electrode storage cap is not shown)
Code 1762
Code 1761M
Code 1763 Code 1764
Display
1. Bar graph display
2. Measurement units
3. Main display
4. Low Battery indicator
5. Temperature display
6. Reading Hold indicator
7. Polarization indicator (meter off)
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10
7
t
2
mg/L
10 20 12
%
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5
*
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OPERATION
Filling the Electrode
The electrode is shipped dry and requires f lling with the supplied electrolyte solution before the f rst use. The membrane should be in place and does not need to be replaced. Follow the procedure on page 9 for f lling the membrane cap.
Powering the Tracer
The Tracer uses four (4) CR2032 Lithium Ion Batteries. Press the ON/OFF button to turn the meter on or off. If the batteries are weak, the ‘BAT’ indicator will appear on the display. The auto power off feature shuts the Tracer off automatically after approximately 10 minutes of inactivity. The auto power off feature may be temporarily disabled for convenience or for extended polarization time.
Startup Polarization Period
When the DO Tracer is powered up for the f rst time, the electrode requires polarization. In order for this to occur a polarization period of approximately three minutes must elapse before measurements can be made. After the meter has been turned on, a special circuit in the meter will maintain a very small biasing current to the electrode for a period of seven days. This will keep the electrode polarized and enables the user to make immediate measurements within a 7 day period without waiting for the electrode to re-polarize. Each time the Tracer is turned on, the polarization timer is reset and the 7 day polarization period is initiated. A small asterisk at the bottom right corner of the display will indicate that the polarization timer circuit is active only when the meter is off. If the Tracer is not used for more than seven days, a 3 minute waiting period is required before a measurement can be made.
Turn-On Diagnostics
1. When the meter is turned on ‘SELF’ and ‘CAL’ will be displayed while the meter runs a diagnostic routine.
2. During this time the meter is recalling the User Calibration data, performing self diagnostics & initializing the circuitry.
3. After this function is complete, the meter proceeds to the normal measurement mode.
Changing the T
emperature Units
To change the displayed temperature units between °F and °C
1. With the unit OFF, press and hold CAL.
2. With CAL depressed, momentarily press
ON/OFF
to turn the Tracer ON.
3. Release CAL. ‘SELF CAL’ will be displayed.
4. Repeat Steps 1 – 3 to change to the other temperature unit.
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Changing the Salinity Compensation
1. With the Tracer ON, momentarily press CAL twice in quick succession. ‘SAL’ will be shown on the lower part of the display.
2. Momentary press MODE. Each press of MODE increases the salinity compensation by 1ppt (part per thousand); the available range is 0 to 50ppt.
3. Momentarily press CAL to save the compensation setting and return to the normal measurement mode.
Changing the Altitude Compensation
1. With the Tracer ON, momentarily press CAL twice in quick succession. ‘SAL’ will be shown in the lower part of the display.
2. Press and hold CAL again for 2 seconds to enter the Altitude Mode. ‘Ald’ will be shown in the lower part of the display.
3. The factory default value is sea level. Each press of MODE increases the altitude compensation by 1000ft. The maximum value is 20 presses (20,000ft above sea level).
4. Momentarily press CAL to save the compensation setting and return to the normal measurement mode.
Changing the Measurement Units
The meter can be set to measure % saturation, dissolved oxygen in mg/l, and dissolved oxygen in parts per million (ppm).
To change the mode:
1. Press and hold MODE for 2 seconds and the display will begin to scroll through the available units of measure :
• % saturation
• dissolved oxygen, mg/L (milligrams per liter)
• dissolved oxygen, ppm (parts per million)
2. When the desired units are displayed, release MODE and the unit will return to normal operating mode.
Note: The ‘HOLD’ function cannot be on when changing the measurement function. If ‘HOLD’ is displayed in the lower left corner of the display, brief y press the MODE button to turn it off.
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Auto-Power Off Feature
The auto power off feature automatically shuts the meter off 10 minutes after the most recent button press. To disable this feature, refer to the Disable Auto-Power Off section.
Disable Auto-Power Off Feature
With the meter ON, momentarily press CAL, then quickly press and hold both MODE and ON/OFF until ‘oFF’ is displayed. To restore the Auto Power Off Feature turn the meter off and on again using ON/OFF.
Low Battery Indicator
When the battery voltage falls below the operating threshold, ‘BAT’ will appear on the display. Refer to the Maintenance section for battery replacement information.
Storing Readings
1. Press
MODE
to store a reading. The storage location number will be shown on the lower display and the main display will show the stored reading. The meter will enter the HOLD mode and ‘HOLD’ will appear on the display.
2. Press
MODE
The next time stored
and so on.
again to exit the
MODE
is momentarily pressed another reading will be
HOLD
mode and return to normal operation.
3. If more than 25 readings are stored, previously stored readings, starting with reading number 1, will be overwritten.
Recalling Stored Readings
1. Momentarily press the
CAL
and then, within 4 seconds, momentarily press
MODE. The last stored data point location will be displayed (1 to 25). Each time MODE is momentarily pressed the next most recently stored data point will be displayed.
After the last data point stored is displayed, press MODE again to return
2. the display to the beginning of the list.
3. Press
CAL
at any time to stop the data retrieval process and return the meter
to the normal measurement mode.
Clearing Stored Readings
1. With the meter ON press and hold ON/OFF for 4 seconds.
When ‘clr’ is shown on the display the memory is cleared.
2.
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SET UP
Membrane Cap Assembly - Filling and Replacement
The electrode is shipped dry and requires f lling with the supplied electrolyte solution before the f rst use. The membrane should be in place and does not need to be replaced.
Important Note: Do not touch the membrane as skin oils will interfere with the oxygen permeability rate of the membrane.
1. The electrode should remain attached to the meter during the process.
2. Carefully remove the membrane cap assembly from the electrode by f rmly unscrewing it in a counter-clockwise direction.
3. Discard the used membrane cap assembly.
NOTE: When a membrane cap is installed the membrane must tightly stretch over the cathode. If a membrane cap is removed, it can not be reinstalled because the membrane will no longer stretch properly over the cathode.
4. Rinse the cathode and anode with deionized water.
5. Set the membrane cap assembly on a f at surface.
6. Fill the membrane cap assembly with Electrolyte Solution (DO600-EL) to the bottom of the threads on the inside of the cap. To remove air bubbles hold the cap steady with one hand and tap the side of the assembly sharply with a pen.
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FILL
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7. Do not move the membrane cap assembly. Dip the electrode into the assembly and remove it. Repeat this step several times. With each dip, progressively push the electrode deeper into the electrode solution in the assembly. This dipping technique will minimize the introduction of air bubbles into the electrolyte solution. Air bubbles can compromise dissolved oxygen measurements.
8. Carefully pick up the membrane cap assembly and slowly screw it onto the electrode in a counter-clockwise direction until it is fully tightened. While tightening the cap, excess electrolyte solution will leak out.
This is normal and desirable since it will minimize air pockets in the solution. Air pockets can compromise dissolved oxygen measurements. If the electrode solution does not overf ow, an insuf
f cient amount was added. Repeat the process with a new membrance cap assembly if air bubbles or air pockets are visible when the meter is inverted. Membrane cap assemblies can not be reused.
NOTE: Air bubbles outside the cathode (6 mm in diameter in the center of the probe) will not interfere.
9. Rinse excess electrolyte from the outside of the membrane cap assembly and the electrode.
P
olarization
If the meter has not been used for seven (7) days or longer the electrode will not be fully polarized. A
fully polarized electrode is indicated by a small, f ashing, asterisk in the lower right corner of the display when the meter is OFF. If the asterisk is absent, turn the meter ON and allow the electrode to fully polarize. This may take 2-3 minutes. The asterisk will appear to indicate full polarization.
Calibration
Calibration should be performed daily. (Be sure the electrode is f lled and fully polarized before calibrating)
1. Turn the meter ON.
2. Press and hold MODE until ‘%’ is displayed.
3. Remove the electrode cap. The electrode membrane must be clean and
dry or the calibration will be incorrect. Do not touch the membrane. Skin oil will affect the electrode response.
CALIBRATE
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4. Moisten the sponge in the electrode cap with distilled water or tap water.
Do not soak the sponge.
5. Replace the electrode cap on the electrode. There must be an air gap
between the membrane and the sponge.
6. Wait until the reading stabilizes. Press and hold CAL until ‘CAL’ is
shown on the display. The readings will blink ‘101.7’ and ‘SA’ will appear. ‘SA’ will not appear if the calibration fails.
7. When the calibration is complete ‘End’ will appear and the meter will
return to the measurement mode.
Optional Zero Oxygen Calibration
The zero oxygen calibration will improve the measurement accuracy for very low or very high dissolved oxygen samples.
1. Place the electrode in a zero dissolved oxygen calibration solution, such
as 5% sodium sulf te.
2. Slowly stir the sample with the electrode and wait for the reading to
stabilize. This may take a while, depending on the electrode history.
3. Press CAL until ‘CAL’ is shown on the display. The readings will blink
‘101.7’ and ‘SA’ will appear. ‘SA’ will not appear if the calibration fails.
4. When the calibration is complete ‘End’ will appear and the meter will
return to the measurement mode.
NOTE: Sodium Sulf te can become deposited on the electrode and on the coined surface of the electrode retaining collar. The presence of the Sodium Sulf te will negatively affect dissolved oxygen measurements unless it is removed completelyfrom the electrode.
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CALIBRATE
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DISSOLVED OXYGEN MEASUREMENT
(Be sure the electrode is f lled and fully polarized. Calibrate daily.)
1. Cover the electrode with the electrode cap. The sponge in the electrode
cap should be moistened (not soaked) with distilled water or tap water.
2. Press ON/OFF to turn the meter ON. The meter will self calibrate.
3. Press and hold MODE to select the desired unit of measure.
4. Remove the electrode cap.
5. Place the electrode in the sample to be measured. Stir the sample with
the electrode.
6. Wait for the reading to stabilize.
7. Press ON/OFF to turn the meter OFF. Rinse the electrode with distilled
water or tap water. Replace the electrode cap.
NOTE:
- The unit of measure selected when the meter was last turned OFF will be retained.
- Stir the sample with the electrode to remove any air bubbles that may be trapped on the membrane surface and to obtain accurate results.
- Do not submerse the electrode above the bottom edge of the electrode collar.
- For maximum accuracy, allow suff cient time for the temperature of the probe to reach the temperature of the sample before taking a reading. The larger the difference in temperature between the electrode and the sample the longer it will take for the reading to stabilize. Stabilization will be indicated by a stable temperature reading on the display. Stabilization time can vary from ten (10) seconds to f ve (5) minutes.
-The DO Tracer uses a polarographic sensor, which consumes oxygen at the sensing surface. This requires a constant movement of the sample across the membrane to maintain a constant dissolved oxygen level. It is recommended that the sample be stirred gently with the electrode as the measurement is made, or if in a laboratory environment, the sample should be stirred using a stir plate.
MEASURE
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OPERATIONAL MATRIX
Function / Resulting Action
Power Status
Mode Setting
Required Button Press Sequence
ON/OFF Any Any Momentary press of
the ON/OFF button
Water Saturated Air Calibration
On Any Place electrode in
electrode cap. Press & hold CAL button for 2 seconds.
Zero Calibration
On Any Place electrode in
zero DO solution. Wait for stability. Press & hold CAL button for 2 seconds.
Store Reading On Any Momentary press
of MODE button.
Hold Release On While In
Hold Mode
Enter Memory
On Any Momentary press
Retrieval
Momentary press of the MODE button.
of CAL button followed by a momentary press of the MODE button within 4 seconds.
Scroll Stored Readings
Exit Memory Retrieval
Clear Stored Memory
On Memory
Recall
On Memory
Recall
On Any
Measure­ment Mode
Momentary press of MODE button.
Momentary press of CAL button.
Press and hold ON/OFF button for 4 seconds
Comments
Also works with probe removed. (Cal at zero current)
Stores and holds reading. ‘HOLD’ displayed
If no data is stored in memory, ‘End’ is displayed brief y, and then returns to last mode.
‘clr’ is displayed.
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0
Function / Resulting Action
Change Measurement Mode
Enter Salinity Compensation
Changing Salinity Compensation
Exit Salinity Compensation
Enter Altitude Compensation
Power Status
Mode Setting
Required Button Press Sequence
On Any Press and hold
MODE button for at least two seconds. Modes will scroll until button is released.
On Any Press and release
the CAL button twice quickly in succession.
On SAL Momentary press
of MODE button.
On SAL Press and release
CAL button for 2 seconds to enter Altitude Compensation. Or press and release CAL button one more time to enter measurement mode.
On Any
or SAL
Press CAL button twice quickly. Unit enters Salinity Mode. Press CAL button for 2 seconds to enter Altitude Compensation Mode.
Comments
‘SAL’ is displayed.
Each button press increases the ratio by 1 ppt (part per thousand). The value cycles from 0 to 50 ppt.
It is necessary to press CAL button to save changes. If the unit times out, no changes are saved.
‘Ald” is displayed. Unit times out in 5 seconds if no button is pressed, reverts to previous mode.
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0
Function / Resulting Action
Changing Altitude
Power Status
Mode Setting
Required Button Press Sequence
On Ald Momentary press of
the MODE button.
Compensation
Exit Altitude Compensation
On Ald Momentary press
CAL button to exit and save changes.
Change Temperature Units
Off OFF mode Press and hold the
CAL button then momentarily press the ON/OFF button. Release the CAL button after ‘SELF CAL’ appears.
Override Auto Power Off
On Any
Press CAL button momentarily then simultaneously press and hold MODE and ON/OFF buttons for 2 seconds.
Default Reset Off OFF mode Simultaneously
press ON/OFF, CAL and MODE buttons momentarily.
Comments
Each button­press increases altitude by 1,000 ft. The value cycles from 0 to 20,000 ft.
It is necessary to press the CAL button to save changes. If the unit times out, no changes are saved.
‘dFLt’ will be displayed.
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TROUBLESHOOTING
- If the display appears to be frozen, it is possible that the Data Hold mode has been inadvertently activated. This is indicated by ‘HOLD’ in the bottom left of the display. To exit the Data Hold mode press MODE or turn the meter off and back on again.
- If the meter locks up and pressing any buttons fails to revive it, remove the batteries and then reinsert the batteries.
Symptom Possible Cause Action
Unit will not power on
“BAT” indicator shown on display
Unstable readings Insuff cient electrolyte
Readings drift down Insuff cient
Slow response Dirty or damaged
Electrode can not be calibrated
Electrode can not be calibrated
after replacing electrolyte and membrane cap
Sample reading is frozen
Batteries not in place
Dead batteries
Insert, replace, or reorient batteries
Batteries polarity incorrect
Batteries are weak Replace batteries
Replace electrolyte, and
in probe. Air bubbles
membrane cap assembly visible when probe inverted.
Electrolyte is depleted
Stir sample with meter or stirring
move probe in sample
Replace electrolyte and membrane
Depleted electrolyte
Dirty or damaged
membrane cap
Replace electrolyte and
membrane cap
membrane
Dirty probe.
Cathode is not a shiny gold color.
Meter is in HOLD mode
Meter is locked
Clean cathode with cleaning
cloth or cleaning paper. Do not
over polish.
Release HOLD by momentarilly
pressing MODE button.
Remove batteries. Press ON/
OFF button. Replace batteries
and press ON/OFF button.
Stored readings will be lost.
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MAINTENANCE
Battery Replacement
1. Twist off the battery compartment cover.
2. Holding the battery housing in place with a f nger, pull out the battery carrier using the two small tabs.
3. Replace the four (4) CR2032 batteries observing proper polarity.
4. Replace the battery carrier, reattach the battery compartment cap and tighten securely.
Battery Safety
- Dispose of batteries responsibly; observe local, state, and federal regulations.
- Never dispose of batteries in a f re; batteries may explode or leak.
- Never mix battery types; install new batteries of the same type.
Electrode Replacement
1. Turn the meter OFF. Turn the electrode retaining collar clock-wise and remove it.
2. Gently rock the electrode from side to side, pulling it away from the meter until it disconnects.
3. Align the positioning “keys” of the replacement electrode and the main body housing. Carefully push the electrode into the meter socket until it is fully seated.
4. Tighten the electrode retaining collar until the electrode is f rmly sealed to the meter.
Replacing the Membrane Cap Assembly
See page 9.
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Electrode Storage
Store the TRACER with the Electrode Storage Cap in place. The sponge in the cap should always be moist without excess liquid.
Electrode Cleaning Recommendations
Contaminant Cleaning Solution Procedure
Salt build-up Deionized water Soak in 20% or weaker
Acetic Acid solution for 1 minute. Rinse thoroughly with DI water.
Oil Warm water and
household detergent
Clean with mild detergent solution. Rinse thoroughly with DI water.
NOTE: Do not contact the membrane with the cleaning solution. Install a new membrane after cleaning the electrode.
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Short Form Instructions
Fill the membrane cap assembly before the f rst use. Follow Set Up instructions before the f rst use. Read the entire manual before the f rst use. Calibrate daily. Polarize weekly.
Dissolved Oxygen Measurement Procedure
1. Press ON/OFF button to turn meter ON.
2. Place TRACER in sample. Stir.
3. Wait for reading to stabilize.
4. Record result.
5. Press ON/OFF to turn meter off.
6. Rinse electrode.
7. Replace electrode cap.
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