LaMotte 1740-KIT-01 User manual

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TracerTM Total Chlorine
PockeTester
Code 1740
Water Testing Leader Since 1919!
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INTRODUCTION
Congratulations on your purchase of the TRACER Total Chlorine PockeTester. The
TRACER is a revolutionary, rst of its kind measurement device that oers direct reading of Total Chlorine from 0.01 to 10.00 ppm. The TRACER is easy to use and maintain, and oers high accuracy, automatic calibration, with fast response and simultaneous Chlorine and Temperature displays and a 15-reading memory storage. Careful use and maintenance will provide years of reliable service. The TRACER testing procedure complies with the electrode method described in EPA 40 CFR Part 136.3, Table 1B (1994) and Standard Methods for the Examination of
Wastewater,
a buer be added to the sample before testing.
18th Ed., 4500-Cl I, p 4-65, which requires that potassium iodide and
that may be harmful if misued. Read
cautions on individual containers
carefully. Not to be used by children
except under adult supervision.
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TRACER
Introduction ............................................................................................. 4
Specifications .......................................................................................... 4
Contents................................................................................................... 4
Parts & Accessories ................................................................................. 5
Meter Description
Basic Operation
Testing
Validation Procedure
Maintenance
TM
TOTAL CHLORINE POCKETESTER • CODE 1740
Front Panel Description .................................................................................... 5
TRACER Display ................................................................................................... 5
Powering the TRACER ........................................................................................ 6
Electrode Recognition ....................................................................................... 6
Automatic Calibration........................................................................................6
Changing the Display Temperature Units .....................................................6
Low Battery Indicator ........................................................................................ 6
Conditioning the Electrode...............................................................................7
Measurement ...................................................................................................... 7
Storing Readings ................................................................................................ 7
Recalling Stored Readings ............................................................................... 8
For Best Accuracy ...............................................................................................8
Offset Adjustment Procedure .......................................................................... 9
Required Materials ............................................................................................10
Preparation of 1ppm Standard ......................................................................10
Procedure ............................................................................................................10
Notes ....................................................................................................................11
Storage ................................................................................................................12
Battery Replacement ........................................................................................12
Cleaning the Electrode ....................................................................................12
Replacing the Electrode ...................................................................................13
Troubleshooting .................................................................................................13
Expanding Your TRACER...................................................................................14
Warranty ..............................................................................................................14
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SPECIFICATIONS
Display Multifunction display with bar graph Operating conditions 32 to 122°F (0 to 50°C) and < 80% RH
Chlorine range 0.01 to 10.00 ppm (Total Chlorine) Chlorine accuracy 0.5 to 5.00 ppm; ± (10% reading + 0.01 ppm)
Temperature 23 to 194°F ( 5 to 90°C) measurement range Temperature range for 32 to 122°F (0 to 50°C)
Chlorine
Temperature resolution 0.1 up to 99.9, then 1 Temperature accuracy ± 1.8F (1°C) from 23 to 122°F ( 5 to 50°C)
Measurement storage 15 readings can be stored and recalled Low battery indicator ‘BAT’ appears on the display Power Four CR 2032 button batteries Auto power o After 10 minutes of inactivity
5.00 to 10.00 ppm; ± (15% reading + 0.05 ppm)
± 5.4F (3°C) from 122 to 194°F (50 to 90°C)
CONTENTS
Total Chlorine TRACER Kit, 0-10.00ppm Range Code 1740 Includes: TRACER TCL Tablets (100) Code 7044A-J Tablet Crusher Code 0175 Sample Cup w/cap†
† not sold individually.
*WARNING: Reagents marked with an * are considered to be potentail health hazards. To view or print Safety Data Sheet (SDS) for these reagetns
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PARTS & ACCESSORIES
Total Chlorine Replacement Electrode Code 1732 Weighted Stand w/ Sample Cups (5) Code 1746 Sample Cups w/caps (24) Code 1745
METER DESCRIPTION
Front Panel Description
1. Battery compartment cover
2. LCD Display
3. MODE/HOLD button
4. CAL/RECALL button
5. ON/OFF button
6. Electrode Retaining Collar (ring)
7. Electrode Sensor (Note: The Electrode storage cap is not shown)
LCD Display
1. Bargraph reading
2. Bar graph scale designations
3. Measurement reading
4. BAT (low battery) and HOLD (data hold) indicator
5. Temperature display
6. Units of measure
0
500
1000
mv
10.04
HOLDBAT
78.6
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BASIC OPERATION
Powering the TRACER
If the batteries are weak, the BAT indicator will appear on the display. Press the ON/OFF key to turn the TRACER on or o. The auto power o feature will shut the TRACER o automatically after 10 minutes of inactivity.
Electrode Recognition
When the TRACER is turned on, it will recognize the type of electrode that is connected and will display the appropriate unit of measure.
Automatic Calibration
NOTE: The automatic calibration process calibrates internal circuitry for drift. This does not calibrate the electrode.
The TRACER should not be immersed in a solution until after the unit is turned on. When the TRACER is turned on, it will automatically self calibrate and the
SELF and CAL icons will be displayed. These icons will disappear after the self
calibration is complete. The main display and bar graph will then read the Total Chlorine concentration in ppm units. The bar graph will read 0 ppm (far left), 5 ppm (center), and 10 ppm (far right). The unit of measure for the lower temperature display will be °C or °F as selected. The readings on the display will ash until they have stabilized.
Changing the Displayed Temperature Units
Press and hold the CAL/RECALL button for approximately 3 seconds. The °C or °F icon will change rst and temperature readings will change only after the button has been released.
Low Battery Indicator
The “BAT” indicator will be displayed when the batteries become weak. Refer to the Maintenance Section for battery replacement information.
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TESTING
Conditioning the Electrode
The TRACER electrode comes in a factory cleaned condition. If the meter is new or has been in storage for an extended period of time, at least two tests should be performed to condition the electrode. The electrode will perform best when in continuous use. Gently wipe the electrode surface with a paper towel between uses.
Measurement
1. Fill a sample cup with exactly 20 ml of the sample water. NOTE: Turbidity of the solution has no eect on the reading.
2. Add one TRACER TCL Tablet (7044A).
3. Use the tablet crusher (0175) to crush the tablet.
4. Cap and shake vigorously for 20-30 seconds. The tablet should be completely disintegrated.
5. Turn the TRACER on. Wait 3 seconds for self-calibration. Immediately immerse in the sample.
6. Stir the sample with the TRACER for 10 seconds. Stop stirring.
The sample and the electrode must remain still and stable during the entire measurement.
7. The display will ash while readings are changing rapidly. The result should be read when the display stabilizes. The reading will be held and the HOLD annunciator will come on after 120 seconds.
8. Remove the TRACER from the sample. Turn the unit o. Replace electrode cap.
NOTE: If a series of subsequent measurements is to be carried out, briey rinse the electrode with water (deionized, if available) and shake o. Gently wipe the electrode surface with a paper towel between uses.
9. The TRACER must be turned o and on again between samples.
Storing Readings
1. When the display is steady and not ashing, press the MODE/HOLD button to store the data. The storage location number, the stored reading and HOLD will be displayed. Press MODE/HOLD to return to the current reading.
2. Only one reading can be stored during the 120 second measurement cycle.
3. After fteen readings are stored, the sixteenth stored reading will over-write the rst stored reading.
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Recalling Stored Readings
NOTE: The HOLD symbol should not be displayed. If it is, exit the HOLD function by pressing the MODE button.
1. Press the CAL/RECALL button and then press the MODE/HOLD button immediately after will ash.
2. The last stored reading taken will be displayed rst. To advance through the stored readings, press the MODE/HOLD button. The location number is displayed rst, followed by the reading stored in that location.
3. To exit the storage mode, press the CAL/RECALL button and the meter will return to normal operation.
4. If the batteries are removed, all stored readings will be lost.
For Best Accuracy
1. Remove TRACER from sample when power is o. Even though power is o, leaving TRACER in solution can shorten unit life.
2. Wash sample cups and caps and rinse completely before use.
3. If measuring solutions with large dierences in chlorine concentration, for example, 0.1 ppm and 5.0 ppm, use a separate sample cup for each
concentration.
4. Discard the sample cup when it becomes stained.
5. The process requires an acidic solution. The reagent tablet provides sucient buering capacity to deal with alkalinity, calculated as calcium carbonate, up to and in excess of 500 ppm. This will cover all common water samples.
6. When the electrode is new or after dry storage, chlorine measurements should be repeated at least twice until a repeatable reading is obtained.
7. Gently wipe the electrode surface with a paper towel between uses.
8. When measuring a lower chlorine concentration after a higher concentration, the meter will temporarily give slightly elevated readings.
9. All oxidizing species that interfere with other chlorine methods, such as manganese, iodine and bromine will interfere. Silver and mercuric ions over 20 ppm will also interfere.
10. Do not touch the tablets. It can contaminate them.
11. Do not touch the sensor surface.
CAL is displayed; the location number (1 through 15)
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Total Chlorine Tracer Offset Adjustment Procedure
1. Obtain a sample with a known concentration of total chlorine.
2. Follow the Chlorine Measurement procedure on page 7.
3. Wait for the display to read HOLD. This may take approximately 2 minutes.
4. Press the MODE/HOLD button for approximately 5 seconds until “C_O” appears at the bottom of the display.
5. IMMEDIATELY press the MODE/HOLD button repeatedly to increase the value or press the CAL/RECALL button repeatedly to decrease the value on the display until it matches the known concentration of the sample.
6. Once the value is adjusted, IMMEDIATELY press the ON/OFF button to save the adjusted value to memory. “SA” will appear on the display.
7. Turn the meter o and proceed with the Chlorine Measurement procedure.
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VALIDATION PROCEDURE
Perform this procedure or an appropriate calibration procedure when TRACER is used for compliance monitoring or before the rst use after replacing the Total Chlorine TRACER electrode.
Required Materials and Chemicals
1 Analytical Balance, Readability 0.0005g 5 g Chloramine-T trihydrate, Analytical grade, 98% 1 Pipet, or Pipettor with disposable plastic tips, 1 mL 3 Volumetric asks, 100 mL 2 Amber glass bottles, 100 mL 1 Sample cup (included in kit) 5 TRACER TCl Tablets (included in kit) Deionized or distilled water
Preparation of 1ppm Standard Solution
1. Fill a 100 mL volumetric ask approximately half full with deionized water. Weigh and add exactly 4.050 g Chloramine-T trihydrate. Dissolve. Dilute to the 100 mL line with deionized water. Cap and mix. This standard is 10,000 ppm.
2. Pipet exactly 1.00 mL of the 10,000 ppm standard into another 100 mL volumetric ask. Dilute to the 100 mL line with deionized water. Cap and mix. This standard is 100 ppm.
3. Pipet exactly 1.00 mL of the 100 ppm solution into a third 100 mL volumetric ask. Dilute to the 100 mL line with deionized water. Cap and mix. This standard is 1 ppm.
4. Add 5 TRACER TCl Tablets (7044A) to the ask of 1 ppm standard from Step 3. Cap and mix until the tablets disintegrate. The tablets contain a small amount of insoluble material and will not dissolve completely. This standard is 1 ppm Converted Chlorine.
Procedure
1. Mix the 1 ppm Converted Chlorine standard.
2. Fill a sample cup with 20 ml of newly prepared 1 ppm Converted Chlorine standard. Tightly cap the standard immediately after use.
3. Turn the TRACER on. Wait 3 seconds for auto-calibration (circuit’s not electrode). Immediately immerse in the standard.
4. Stir the standard with the TRACER for 10 seconds. Stop stirring. The standard and the TRACER must remain still and stable during measurement.
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5. The display will ash while readings are changing rapidly. The result should be read when the display stabilizes. The reading will be held and the HOLD annunciator will come on after 120 seconds.
6. Remove the TRACER from the standard. Rinse in deionized water and shake dry.
7. Repeat steps 2 - 6 three more times on the same sample cup of standard.
8. After the fourth time, press and hold the CAL key. While continuing to hold the CAL key, press the MODE key. Immediately release both keys. The main display should ash electrode in standard and press the CAL key again until then press the CAL and MODE keys again simultaneously. Immediately release both keys.
9. After approximately 5 to 7 seconds the display will briey ash Rinse the TRACER in deionized water and shake dry.
Notes
1. The 1 ppm Converted Chlorine standard should be at room temperature (23 ±2°C) during the validation procedure.
2. The 10,000 ppm Standard Solution can be stored for up to one year in a tightly sealed, amber, glass bottle.
3. The 10 ppm Standard Solution can be stored for up thirty days in a tightly sealed, amber, glass bottle.
4. The 1 ppm Converted Chlorine Standard is stable for up to approximately 30 minutes. Discard the standard after use.
1.00. If 1.00 is not displayed, keep the CAL is displayed,
END.
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MAINTENANCE
Storage
When not in use, the TRACER should be stored dry with the electrode cap in place. Cover the connector with the clear cover whenever the electrode is removed from the meter body.
Battery Replacement
1. Twist o the battery compartment cap.
2. Hold the battery housing in place with one nger. Remove the battery carrier by pulling on the small tabs.
3. Replace the four CR2032 batteries. Observe polarity.
4. Replace the battery compartment cap.
Cleaning the Electrode
The TRACER Chlorine Electrode arrives in a factory-cleaned condition and is ready to be used. The electrode will perform better and yield more stable readings after the rst few tests. Firmly wipe the electrode surface with a clean, dry paper towel before and after use to remove any compounds that may have formed. Rinse the electrode in deionized water to clean it. When not in use, the TRACER should be stored with the electrode cap in place.
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Replacing the Electrode
The TRACER is shipped with an electrode attached. If the electrode needs to be replaced or changed, follow these steps.
1. Press the ON/OFF button to turn the meter o.
2. To remove an electrode, unscrew and completely remove the electrode collar. Turn the collar counter-clockwise.
3. Gently rock the electrode from side to side, pulling it downwards, until it disconnects from the meter.
4. To attach an electrode, align the slots and carefully plug the electrode into the meter socket. CAUTION: Take care to align pins carefully. Bent or broken pins will cause the meter to malfunction.
5. Firmly tighten the electrode collar to create a seal with the rubber gasket between the electrode and the meter. Do not over tighten.
6. Cover the connector end of the removed electrode with the clear plastic cap.
TROUBLESHOOTING
Problem Check Action
Power on but no display Batteries Insert batteries
Verify correct polarity
Replace
Unstable reading Electrode Immerse probe more deeply
Slow response Electrode Clean electrode
Unexpected low results Tablet Conrm tablet has been added
Unexpected high results Tablet Dissolve tablet completely
Display frozen HOLD function Press MODE/HOLD or turn
Button press Remove batteries (stored data
in sample
Remove air bubbles caught under electrode
Clean electrode
Replace electrode
meter o.Restart.
will be lost)
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EXPANDING YOUR TRACER
0
Interchangeable electrodes are available to convert the Total Chlorine TRACER to a pH TRACER or an ORP TRACER.
Remember to ask for instructions and appropriate reagent or buer tablets when ordering pH or ORP electrodes.
pH TRACER Electrode, 0.00-14.00 pH Code 1733
The pH TRACER Electrode is used with pH 4.0, 7.0 and 10.0 buers. Order using the following codes:
pH 4.0 Mini Buer Tablets (100) Code 3983A-J
pH 7.0 Mini Buer Tablets (100) Code 3984A-J
pH 10.0 Mini Buer Tablets (100) Code 3985A-J
ORP TRACER Electrode,±999 mV Code 1734
The ORP TRACER Electrode (code1734) requires an initial soaking in a pH 4.0 buer solution. Order pH 4.0 Mini Buer Tablets/100 pack (Code 3893A-J).
WARRANTY
The TRACER PocketTester is specically calibrated for use with the TRACER TC1 Tablets (Code 7044A). Use with other reagent systems will void the warranty and may damage the meter.
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