LaMotte 1200-MN User Manual

Page 1
1200 COLORIMETER
MANGANESE
MODEL 1200-MN · CODE 3682-01
QUANTITY CONTENTS CODE
2 x 100 mL *Hardness Buffer Reagent *4255-J 2 x 30 mL *Manganese Indicator Reagent *3956-G 15 mL *Sodium Cyanide, 10% *6565-E 1 Pipet, 0.5 mL, plastic, w/cap 0369 1 Pipet, 1.0 mL, plastic 0354 6 Colorimeter Tubes, with caps 0290-6 1 Water Sample Collecting Bottle 0688 1 1200 Colorimeter for Manganese 26739
*WARNING: Reagents marked with a * are considered to be potential health hazards. To view or print a Material Safety Data Sheet (MSDS) for these reagents see MSDS CD or www.lamotte.com. To obtain a printed copy, contact LaMotte by email, phone or fax.
To order individual reagents or test kit components, use the specified code number.
INTRODUCTION
Manganese is present in ground water in the divalent state due to the lack of oxygen. In surface waters, manganese may be in various oxidation states as soluble complexes or as suspended compounds. Manganese is rarely present in excess of 1 mg/L. It may cause an objectionable taste or cause staining problems in laundry, but manganese levels normally encountered in water seldom produce any health hazard.
Manganese is removed from water by various means including chemical precipitation, pH adjustment, aeration, superchlorination and the use of ion exchange resins.
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MANGANESE TEST PROCEDURE - PAN METHOD
4.
Push the READ button to turn the meter on. Press the
ZERO button
and hold it for 2 seconds until bla is displayed. Release the button to take a blank reading (0.0 ppm).
I200 COLORIMETER
• • • • • • • • • • • • • • • • • •
READ
ZERO
bla
Insert the tube into the chamber, being
3.
Rinse and fill a colorimeter tube (0290) to the
10 mL line with sample water. Cap and wipe dry.
2.
Fill the Water Sample Collecting Bottle (0688) with sample water. This will be used to dispense sample water for the tests.
1.
Use the 1.0 mL pipet (0354) to add 2.0 mL of *Hardness Buffer Reagent (4255).
5.
6.
Swirl the tube to mix.
8.
7.
Add two drops of *Sodium Cyanide, 10% (6565).
Swirl the tube to mix.
sure to align the index line with the arrow on the meter. Close the lid. This tube is the blank or zero.
L
Mott
Read the 1200 Colorimeter Manual before proceeding. Carefully wipe tubes dry before inserting into the colorimeter chamber.
MANGANESE
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10.9.
Cap tube and invert to mix.
11.
Align the index line with the arrow on the meter, insert
tube into chamber. Close the lid. Push the READ button. Record results as ppm Manganese.
Note:
For the best possible results, carry a reagent blank through the procedure. After scanning the blank in Step 4, perform the test procedure on clear, colorless, distilled or deionized water. Subtract results of reagent blank from all subsequent test results.
12.
Use the 0.5 mL pipet (0369) to add 0.5 mL of *Manganese Indicator Reagent (3956).
Wipe tube dry.
CAL
I200COLORIMETER
• • • • • • • • • • • • • • • • • •
READ
L
Mott
If the reading displays Er2, repeat procedure on diluted sample, and multiply the result by the appropriate dilution factor. See 1200 Colorimeter Instruction Manual for procedure.
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MANGANESE TEST METHOD SPECIFICATIONS
APPLICATION
Drinking and surface; domestic and industrial wastewaters.
RANGE
0.0 - 0.7 mg/L Manganese
METHOD
PAN, (1-[2-Pyridylazo]-2-Naphthol), forms a red complex with Manganese (Mn+2) at a pH of 8 to 10.
HANDLING & PRESERVATION
Manganese may oxidize readily in neutral water and precipitate from solution. It may adhere to or be absorbed by container walls, especially glass. Acidified sample can be stored in plastic.
INTERFERENCES
None. Test is quite specific.
LaMOTTE COM PANY
Helping Peo ple Solve An a lyt i cal Chal lenges
PO Box 329 • Chestertown • Mary land • 21620 • USA
800-344-3100 • 410-778-3100 (Out side U.S.A.) • Fax: 410-778-6394
Visit us on the web at www.lamotte.com
®
63682-01 · 10.08
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