Labconco Fume Adsorbers User Manual

Fume Adsorbers
Models
115V 230V
3955200 Organic 30" 3955220 Organic 30"
3955400 Organic 60" 3955420 Organic 60" 3955201 Formaldehyde 30" 3955221 Formaldehyde 30" 3955401 Formaldehyde 60" 3955421 Formaldehyde 60" 3955202 Ammonia 30" 3955222 Ammonia 30" 3955402 Ammonia 60" 3955422 Ammonia 60"
Labconco Corporation
HOME PAGE www.labconco.com
Please read the User’s Manual before operating the equipment.
User’s Manual
8811 Prospect Avenue Kansas City, MO 64132-2696 800-821-5525, 816-333-8811 FAX 816-363-0130 E-MAIL labconco@labconco.com
Warranty
Labconco provides a warranty on all parts and factory workmanship. The warranty includes areas of defective material and workmanship, provided such defect results from normal and proper use of the equipment. Glassware is not warranted from breakage when dropped or mishandled.
The warranty for a Labconco Fume Adsorber will expire one year from date of installation or two years from date of shipment from Labconco, whichever is sooner.
This limited warranty covers parts and labor, but not transportation and insurance charges. In the event of a warranty claim, contact Labconco Corporation or the dealer who sold you the product. If the cause is determined to be a manufacturing fault, the dealer or Labconco Corporation will repair or replace all defective parts to restore the unit to operation. Under no circumstances shall Labconco Corporation be liable for indirect, consequential, or special damages of any kind. This statement may be altered by a specific published amendment. No individual has authorization to alter the provisions of this warranty policy or its amendments. Lamps and filters are not covered by this warranty. Damage due to corrosion or accidental breakage is not covered.
Copyright © 2005, 2007, 2014 Labconco Corporation. All rights reserved.
The information contained in this manual and the accompanying products are copyrighted and all rights reserved by Labconco Corporation. Labconco Corporation reserves the right to make periodic design changes without obligation to notify any person or entity of such change.
Returned or Damaged Goods
Do not return goods without the prior authorization from Labconco. Unauthorized returns will not be accepted. If your shipment was damaged in transit, you must file a claim directly with the freight carrier. Labconco Corporation and its dealers are not responsible for shipping damages.
The United States Interstate Commerce Commission rules require that claims be filed with the delivery carrier within fifteen (15) days of delivery.
Limitation of Liability
The disposal and/or emission of substances used in connection with this equipment may be governed by various federal, state, or local regulations. All users of this equipment are required to become familiar with
any regulations that apply in the user’s area concerning the dumping of waste materials in or upon water,
land, or air and to comply with such regulations. Labconco Corporation is held harmless with respect to user’s compliance with such regulations.
Contacting Labconco Corporation
If you have questions that are not addressed in this manual, or if you need technical assistance, contact Labconco’s Customer Service Department or Labconco’s Product Service Department at 1-800-821-5525 or 1-816-333-8811, between the hours of 7:00 a.m. and 6:00 p.m., Central Standard Time.
Part #6960400, Rev. E
ECO J105
ORIGINAL INSTRUCTIONS
TABLE OF CONTENTS
CHAPTER 1: INTRODUCTION 1
About This Manual 2 Typographical Conventions 3
CHAPTER 2: PREREQUISITES 5
Support Requirements 5 Location and Air Current Requirements 6 Electrical Requirements 6 Space Requirements 6
CHAPTER 3: GETTING STARTED 7
Unpacking Your Enclosure 7 Installing the Enclosure on a Supporting Structure 8 Installation of Carbon Filters 8 Connect the Electrical Supply Source to the Enclosure 9 Validating the Fume Adsorber Face Velocity 9
CHAPTER 4: PERFORMANCE FEATURES AND SAFETY
PRECAUTIONS 10
Performance Features 10 Safety Precautions 11
CHAPTER 5: APPROPRIATE APPLICATIONS FOR YOUR
ENCLOSURE 14
Routine Daily Work Procedures 14 Suitable Applications 15 Appropriate Chemicals for Carbon Filters 15 Definition of Terms 16 Hazardous Misapplications for Carbon Filters with Volatile Chemicals 17 Chemical Carcinogen Use with Carbon Filters 17 Prohibited Acid Use 17
CHAPTER 6: MAINTAINING YOUR ENCLOSURE 18
Routine Maintenance Schedule 18 Determination of When to Replace Carbon Filters and How to Replace 19 Calculating Carbon Filter Life 21
CHAPTER 7: TROUBLESHOOTING 23
APPENDIX A: ENCLOSURE COMPONENTS
AND REPLACEMENT PARTS 25
APPENDIX B: DIMENSIONS 28
APPENDIX C: FUME ADSORBER SPECIFICATIONS 29
APPENDIX D: QUICK CHART FOR THE FUME ADSORBER 30
APPENDIX E: REFERENCES 31
DECLARATION OF CONFORMITY 33
1
CHAPTER 1 INTRODUCTION
Congratulations on your purchase of a Labconco Fume Adsorber. Your enclosure uses carbon filtration to provide personnel protection of annoying solvents, formaldehyde or ammonia vapors generated by histology and pathology operations.
When properly installed and operated, these enclosures will effectively contain low concentrations of noxious fumes and chemicals. Each enclosure uses carbon filtration and is only intended for chemical use with a time weighted exposure limit (TWA) of 100 ppm or greater (Reference the NIOSH Pocket Guide, www.cdc.gov/niosh/npg/npg.html). The carbon filters are available with three different carbons for adsorbing organic vapors, formaldehyde or ammonia and amines.
Please acquaint yourself with this manual and keep it handy for future reference to review all the Fume Adsorber’s features. If you are unfamiliar with how Fume Adsorbers operate, please review Chapter 4: Performance Features and Safety Precautions before you begin working in the enclosure. Even if you are an experienced user, please review Chapter 5: Using Your Fume Adsorber, which describes the features so that you can use the enclosure efficiently.
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Chapter 1: Introduction
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Width
Fume Adsorber
Model No’s.
Filter
Blower
Application
Exhaust
30"
3955200 (115V) 3955220 (230V)
Carbon Filter* Organic Vapor
Built-In Integral Motorized Impeller
When ducting to the outside is not feasible, the filters keep low level concentrations below OSHA recommended time weighted averages, restoring clean air to the laboratory.
To the room
60"
3955400 (115V) 3955420 (230V)
Width
Fume Adsorber
Model No’s.
Filter
Blower
Application
Exhaust
30"
3955201 (115V) 3955221 (230V)
Carbon Filter*,
Formaldehyde
Built-In Integral Motorized Impeller
When ducting to the outside is not feasible, the filters keep low level concentrations below OSHA recommended time weighted averages, restoring clean air to the laboratory.
To the room
60"
3955401 (115V) 3955421 (230V)
Width
Fume Adsorber
Model No’s.
Filter
Blower
Application
Exhaust
30"
3955202 (115V) 3955222 (230V)
Carbon Filter*,
Ammonia
Built-In Integral Motorized Impeller
When ducting to the outside is not feasible, the filters keep low level concentrations below OSHA recommended time weighted averages, restoring clean air to the laboratory.
To the room
60"
3955402 (115V) 3955422 (230V)
!
!
Note: Formaldehyde filters can adsorb up to 30% organic vapors.
Note: Ammonia filters can adsorb up to 30% organic vapors.
* It is recommended that a Labconco product specialist review the chemical application to determine if it is suitable. Consult Chapter 5 and Chapter 6.
Acids must not be used in Fume Adsorbers.
About This Manual
This manual is designed to help you learn how to install, use, and maintain your enclosure. Instructions for installing accessory carbon filters on your filtered enclosure are also included. Your Fume Adsorber ships with either one or two organic vapor carbon filters depending on the model width.
If the unit is not operated as specified in this manual it may impair the protection provided by the unit.
Si l'unité n'est pas utilisée comme spécifié dans ce manuel il peut diminuer la protection fournie par l'unité.
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Chapter 1: Introduction
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Chapter 1: Introduction provides a brief overview of the enclosure, explains the organization of the manual, and defines the typographical conventions used in the manual.
Chapter 2: Prerequisites explains what you need to do to prepare your site before you install the enclosure. Electrical and service requirements are discussed.
Chapter 3: Getting Started contains the information you need to properly unpack, inspect, install, and certify the enclosure.
Chapter 4: Performance Features and Safety Precautions explains how the enclosure operates and the appropriate precautions you should take when using it.
Chapter 5: Appropriate Applications for Your Enclosure discusses the basic operation of how to prepare, use and shut down your enclosure.
Chapter 6: Maintaining Your Enclosure explains how to perform routine maintenance on the enclosure.
Chapter 7: Troubleshooting contains a table of problems you may encounter while using the enclosure including the probable causes of the problems and suggested corrective actions.
Appendix A: Components and Replacement Parts contains labeled diagrams of all of the components of the enclosures.
Appendix B: Dimensions contains comprehensive diagrams showing all of the dimensions for the enclosures.
Appendix C: Specifications contains the electrical requirements for enclosures. Wiring diagrams are also included.
Appendix D: Quick Chart provides an airflow table and test data for the enclosures.
Appendix E: References lists the various resources available that address laboratory ventilation.
Typographical Conventions
Recognizing the following typographical conventions will help you understand and use this manual:
Book, chapter, and section titles are shown in italic type (e.g., Chapter 3:
Getting Started).
Steps required to perform a task are presented in a numbered format. Comments located in the margins provide suggestions, reminders, and
references.
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Chapter 1: Introduction
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!
!
Critical information is presented in boldface type in paragraphs that are
preceded by the exclamation icon. Failure to comply with the information following an exclamation icon may result in injury to the user or permanent damage to the enclosure.
Critical information is presented in boldface type in paragraphs that are
preceded by the wrench icon. Only a trained certifier or contractor should perform these operations. Failure to comply with the information following a wrench icon may result in injury to the user or permanent damage to your enclosure.
Important information is presented in capitalized type in paragraphs that are
preceded by the pointer icon. It is imperative that the information contained in these paragraphs be thoroughly read and understood by the user.
CAUTION – See Manual. When this symbol is on the unit it indicates a
caution that is detailed in this manual.
ATTENTION - Voir manuel. Lorsque ce symbole est sur l'unité, il indique une
mise en garde qui est indiqué dans ce manuel.
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CHAPTER 2
PREREQUISITES
Before you install the Fume Adsorber, prepare your site for installation. A source of electrical power should be located near the installation site to power the enclosure. Additionally, the enclosure should be strategically placed in the lab to provide efficient workflow.
Carefully read this chapter to learn the requirements for your installation site:
The support requirements. The location and air current requirements. The electrical power requirements. The space requirements.
Refer to Appendix B: Dimensions for complete enclosure dimensions.
Refer to Appendix C: Specifications for complete enclosure electrical and environmental conditions, specifications and requirements.
Support Requirements
At a minimum, the supporting structure usually consists of a work surface in the laboratory. See Chapter 3 for setting up installation.
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Chapter 2: Prerequisites
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Location and Air Current Requirements
The Fume Adsorbers have been designed to contain hazardous fumes by negating typical cross drafts and turbulence within the opening. As precautionary safety measure and a higher level of quality management, it is recommended that the Fume Adsorber be placed in an area to avoid:
High traffic areas where walking might cause an air disturbance or be a
nuisance.
Overhead or wall HVAC diffusers, fans, radiators or other lab equipment
producing air currents.
Next to doorways or windows that may be opened.
Do not position the unit so that it is difficult to operate the main disconnect device.
Ne placez pas l'appareil de sorte qu'il est difficile de faire fonctionner le dispositif principal de déconnexion.
Electrical Requirements
Standard duplex electrical receptacles should be nearby for connecting the Fume Adsorber. See the nameplate on the rear of the enclosure for rated electrical service.
Space Requirements
The dimensions for the different Fume Adsorber models are shown in Appendix B: Dimensions.
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The United States Interstate Commerce Commission rules require that claims be filed with the delivery carrier within fifteen (15) days of delivery.
CHAPTER 3
GETTING STARTED
Now that the site for your Fume Adsorber is properly prepared, you are ready to unpack, inspect and install the enclosure. Read this chapter to learn how to:
Unpack and move the enclosure. Set up the enclosure with the proper supporting structure. Installation of carbon filter(s). (Fume Adsorbers ship with organic vapor
filter(s).
Connect the electrical supply. Validate the enclosure face velocity.
Unpacking the Enclosure
Carefully remove the shrink-wrap and carton on the unit and inspect it for damage that may have occurred in transit. If damaged, notify the delivery carrier immediately and retain the entire shipment intact for inspection by the carrier.
DO NOT RETURN GOODS WITHOUT THE PRIOR AUTHORIZATION OF LABCONCO. UNAUTHORIZED RETURNS WILL NOT BE ACCEPTED.
IF ENCLOSURE WAS DAMAGED IN TRANSIT, YOU MUST FILE A CLAIM DIRECTLY WITH THE FREIGHT CARRIER. LABCONCO CORPORATION AND ITS DEALERS ARE NOT RESPONSIBLE FOR SHIPPING DAMAGE.
Do not discard the packing material until you have checked all of the components and tested the enclosure. We recommend that you do not remove the enclosure from its shipping container until it is ready to be placed in its final location.
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Chapter 3: Getting Started
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Filter Type
Appropriate Use
Organic Vapor
Activated Carbon
6961300
6.0 lbs.
Adsorbs organic compounds designated by NIOSH guidelines as acceptable for use with chemical cartridge-type respirators. Concentrations in the
enclosure’s work area must not exceed the IDLH for
the chemical and the exhaust from the enclosure must be monitored not to exceed the TWA.
Formaldehyde
(Formalin)
6961301
7.5 lbs.
Formaldehyde requires the use of an impregnated
carbon. Concentrations in the enclosure’s work area
must not exceed the IDLH for the chemical and the exhaust from the enclosure must not exceed the TWA.
Ammonia and
Amines
6961302
8.7 lbs.
Treats ammonia, low molecular weight amines and other bases designated by NIOSH as acceptable for use with ammonia cartridge type respirators. Requires the use of an impregnated carbon. Concentrations in the
enclosure’s work area must not exceed the IDLH for
the chemical and the exhaust from the enclosure must not exceed the TWA.
!
Installing the Enclosure on a Supporting Structure
Use caution when lifting or moving the enclosure.
When installing the enclosure onto a chemical-resistant work surface or benchtop, ensure that the structure can safely support the weight of the enclosure. The 30" wide Fume Adsorber weighs 62 lbs, and the 60" wide Fume Adsorber-2 weighs 125 lbs. The work surface should be at least as wide as the enclosure to properly support it.
Installation of Carbon Filters
For carbon filter installation, first remove the four (or eight) Phillips screws on the perforated baffle located inside the enclosure. Slowly remove the perforated baffle. See the following list of available carbon filters below. All carbon filters are installed with the gasket side on the downstream exhaust side. The carbon filters are installed behind the upper and lower filter clamps and are removed by Phillips screws. Install the correct carbon filter for the application. In choosing the correct filter for your application call Labconco for assistance. See Figures A-1, A-2 and A-3 in Appendix A and Figure 4-2 in Chapter 4 for installation diagrams.
Important: Carbon filters do not provide any particulate protection, but provide odor control for low level concentrations below OSHA recommended time weighted averages.
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!
115V
Maximum
is 2 amps.
230V
is 1 amp.
!
circuit load
Maximum circuit load
Chapter 3: Getting Started
Connecting the Electrical Supply Source to the Enclosure
115V Models
Simply connect the 115V power cord supplied to the IEC electrical supply plug on the back of the enclosure.
230V Models
The same procedure applies for the 230V except it is shipped without a plug. Install the appropriate plug for your electrical specifications per local codes.
Do not use any detachable power cord that is not adequately rated
for the unit.
Ne pas utliser un fil électrique amovible qui n’est pas du tension
nominale de l’appareil.
Validating the Fume Adsorber Face Velocity
To determine the actual face velocity at the sash opening, airflow velocity readings
are taken. The “average face velocity” is achieved by taking readings in two rows
across the enclosure with the readings 6" from the ends and evenly spaced every 12". The average velocity across the opening of the enclosure is 35 fpm and should be validated. Do not use the enclosure with an average velocity of less than 25 fpm. Consult your safety officer.
NOTE: Face velocity profiles and smoke testing should be performed at least monthly.
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Figure 4-1
Performance Features
3
2
4
CHAPTER 4 PERFORMANCE
FEATURES AND SAFETY
PRECAUTIONS
Performance Features
The Fume Adsorbers are designed to meet the needs of the laboratory scientist and provide containment of light emissions of solvents, formaldehyde and ammonia vapors. Annoying vapors, such as xylene and toluene fumes used in cover slipping operations are efficiently adsorbed by the Fume Adsorber carbon filter(s). The Fume Adsorber uses a carbon filter to collect low concentrations and exhaust filtered air back into the room.
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Chapter 4: Performance Features & Safety Precautions
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Figure 4-2
Performance Features, Exploded View
2 5 3
1
1. Built-In Motorized Impeller Provides up to 35 fpm average face velocity.
Airflow capacity is 100 CFM on the 30" wide unit and 200 CFM on the 60" wide unit.
2. Perforated Baffle provides uniform removal of noxious fumes. Remove
this baffle to access the carbon filter.
3. Blower Switch provides convenient ON/OFF control.
4. Hood Canopy maximizes the work area and visibility.
5. Carbon Filter is designed to remove small amounts of fumes and
chemicals. (See Chapter 6 for carbon types and estimated filter life.)
Safety Precautions
1. Although the enclosure has been engineered to maintain optimum operator
safety, caution should always be used while working inside the enclosure. Prior to using, check to make sure that the exhaust blower is operating and air is entering the enclosure at its specified face velocity.
2. Use good housekeeping in the enclosure at all times. Clean spills
immediately. Periodically clean the enclosure interior with mild soap and water.
3. Do not store containers or supplies against the rear baffle, as this will affect
airflow. Blocking large portions of the rear baffle will change the airflow pattern in the enclosure causing turbulence.
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Chapter 4: Performance Features and Safety Precautions
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4. Always work with your hands as far back into the enclosure as possible.
5. Do not work in this enclosure without the exhaust system running.
6. General acid use, as well as perchloric acid use in this enclosure is prohibited.
7. High-level radioisotope materials are prohibited in this enclosure. Consult
your Safety Officer.
8. Avoid cross drafts and limit traffic in front of the enclosure. Air
disturbances created may draw chemical vapors out of the enclosure.
9. The use of safety goggles, protective clothing, gloves and any other personal
protective equipment recommended by your safety officer should be used.
10. Care must be taken to ensure that the concentration of gases or vapors do
not reach flammable or explosive limits. Use of an open flame must be avoided in the enclosure.
11. Applications that generate gases or vapors from toxic chemicals must be
evaluated carefully so that buildup to levels above the TWA of the chemical does not occur. Do not work with chemicals having a TWA below 100 ppm.
12. Ensure that the enclosure is connected to electrical service in accordance
with local and national electrical codes. Failure to do so may create a fire or electrical hazard. Do not remove or service any electrical components without first disconnecting the enclosure from electrical service.
13. Dispose of carbon filters as hazardous waste. The user is responsible for
recording the chemicals adsorbed or treated by the filters and disposing properly.
14. Ensure only trained operators use the enclosure. New users should review
the User’s Manual and become familiar with the operation of the enclosure.
15. If the enclosure is to be used in a confined space, make sure the space is
well ventilated and the concentration of chemical vapors cannot accumulate greater than the TWA.
16. Only chemicals that can be safely adsorbed and treated with specific
carbon-based filters are appropriate for use in this enclosure. Contact Labconco for chemical assessment.
17. The warning properties (i.e., odor, taste) of the volatile organic compounds
or other material being used in the enclosure must be adequate to provide an early indication that the carbon filters may be saturated or inadequate. Contact Labconco for help with chemical assessment.
18. Use the smallest possible quantity of chemical(s) within the enclosure and
never exceed the amount that can be effectively adsorbed by the carbon filters before breakthrough. Consult Chapter 6 for filter life estimates.
19. Leave the blower on for at least one minute after work in the enclosure has
been completed.
20. If a chemical is spilled on the work surface, DO NOT switch off the
blower until all traces have been removed.
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Chapter 4: Performance Features & Safety Precautions
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21. Tag the enclosure with appropriate warning if filters have been removed for
service.
22. If the blower fails during use, processes should cease and the area should
be vacated and ventilated.
23. Always refer to the NIOSH Pocket Guide to Chemical Hazards to
understand the chemical’s properties and health risks. (See Chapter 5). For
additional help with filter and chemical selection contact Labconco at 1­800-821-5525 or 1-816-333-8811.
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CHAPTER 5
APPROPRIATE APPLICATIONS
FOR YOUR ENCLOSURE
Now that the installation of your enclosure is completed, you are ready to use your Fume Adsorber. Read this chapter to learn about:
1. Routine Daily Work Procedures.
2. Suitable Applications.
3. Appropriate Chemicals for Carbon Filters.
4. Definition of Terms.
5. Hazardous Misapplications for Carbon Filters.
6. Chemical Carcinogen use with Carbon Filters.
7. Prohibited Acid Use.
Start-up
Turn on exhaust system blower with the ON/OFF switch. Check the baffle air slots for obstructions. Wear a long sleeved lab coat and rubber gloves. Use protective eyewear.
Wear a protective mask if appropriate. Consult your Safety Officer for additional personal protective equipment recommendations.
Load only the materials required for the procedure. Do not overload the
enclosure.
Work Techniques
Keep all materials inside the enclosure and perform all contaminated
operations as far to the rear of the work area as possible.
Avoid using techniques or procedures that disrupt the airflow patterns of
the enclosure.
Final Purging
Upon completion of work, the enclosure should be allowed to operate for
two to three minutes undisturbed, to purge airborne contaminants from the work area before shutting off the blower.
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Chapter 5: Appropriate Applications for Your Enclosure
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!
Shutdown
Turn off the exhaust system blower with the ON/OFF switch.
Suitable Applications
NIOSH (National Institute for Occupational Safety and Health, USA) has established guidelines for chemical cartridge and HEPA filtered respirators. Suitable applications for the carbon filtered enclosures are based on guidelines below. As with respirators, chemical contaminants are adsorbed or treated by carbon.
Release of low concentrations of vapors effectively adsorbed or treated in
carbon based filters. Recommended for use with chemicals with a TWA of
100 or greater unless chemical can be filtered with the use of an impregnated specialized filter; impregnated filters such as formaldehyde, formalin, ammonia, and amines are examples of specialized filters.
Treatment of low-level carcinogens or suspected carcinogens. (See Chemical
Carcinogens in Chapter 5)
Procedures that may have traditionally been done on the open bench (low
levels only).
Odoriferous chemicals that are an unpleasant nuisance.
Other applications, not fitting the above guidelines, would be better suited with the exhaust ducted to the outside by using some other containment enclosure offered by Labconco.
REFERENCES TO NIOSH OR OSHA GUIDELINES AND REGULATIONS APPLY TO ANY WORK PLACE UNDER THE JURISDICTION OF THE U.S. DEPARTMENT OF LABOR. OTHER COUNTRIES OUTSIDE THE U.S. HAVE ESTABLISHED STANDARDS, WHICH MAY DIFFER SLIGHTLY FROM THOSE USED AS GUIDELINES FOR THIS
PRODUCT. IT IS THE USER’S RESPONSIBILITY TO
BECOME AWARE OF LOCAL REGULATIONS GOVERNING THE SAFE USE AND DISPOSAL OF CHEMICALS AND CARBON FILTERS. KNOWLEDGE OF ESTABLISHED SAFE EXPOSURE LEVELS IS IMPERATIVE TO THE PROPER USE OF CARBON FILTERED ENCLOSURES.
Appropriate Chemicals for Carbon Filters
Below is a general set of rules to determine appropriateness of chemical usage.
Selected organic chemicals considered to be occupational carcinogens by NIOSH can only be used in the filtered enclosure with carbon filters under rigid restrictions. See separate discussion on next page on carcinogens for special instructions.
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Chapter 5: Appropriate Applications for Your Enclosure
16
Organics must have time weighted exposure limits (TWA) of 100 PPM or greater. Chemicals must have a detectable odor at concentrations below the TWA for the
chemical. Chemicals must be designated by NIOSH guidelines as acceptable for use with
chemical cartridge-type respirators (the exception is formaldehyde and ammonia/amines, which used impregnated carbon). Chemicals not listed by NIOSH in the Pocket Guide must be approved by Labconco Product Specialist (or Engineering).
Inlet concentration must never exceed the IDLH (Immediately Dangerous to Life and Health) concentrations.
Chemicals having a recommendation by NIOSH of at least “Escape GMFOV”
(Gas Mask Full-Face Respirator). When evaporating a mixture of chemicals, the chemical having the lowest TWA
will be used to determine if the mixture meets the guidelines. Call a Labconco Product Specialist at 1-800-821-5525 for assistance in
determining chemical appropriateness.
Definition of Terms
NIOSH National Institute for Occupational Safety and Health/Mine Safety and Health Administration. (U.S.A.)
TWA Recommended Exposure Limits expressed as a Time Weighted Average. The exposure limit for that chemical for up to a 10-hour workday, 40 hours a week. Expressed in units of parts per million or milligrams per cubic meter.
Odor Threshold The value in parts per million or milligrams per cubic meter for
which one might expect to smell a chemical’s presence in the air. This value is very
subjective and detection will vary with the sensitivity of one’s nose. The period of
time until the odor threshold is reached in the exhaust stream can be estimated from
Labconco’s exclusive chemical assessment program. Contact Labconco on
estimates for carbon filter life for specific applications. See Chapter 6.
Saturation Level or Time There is a limit to the amount of chemical that can be adsorbed by activated carbon or neutralized by chemically-treated carbon. Once the capacity of the carbon is reached, it is considered to be saturated and will adsorb (or neutralize) no further material; the outlet concentration of the chemical will equal the inlet concentration from that point until the filter is replaced. (Note that the capacity of activated carbon is not a constant, but varies with the inlet concentration). Labconco Product Specialists can determine the estimated saturation time for a particular chemical.
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Chapter 5: Appropriate Applications for Your Enclosure
17
!
Carbon
IDLH (Immediately Dangerous to Life and Health). An atmosphere that poses an immediate hazard to life or produces immediate irreversible health effects. IDLH concentrations should not be approached in the enclosure.
Hazardous Misapplications for Carbon Filters with Volatile Chemicals
There is one scenario where the accessory carbon filter misapplication would be a part of a hazardous condition. If the user continues to operate the enclosure with any of the following conditions present a potentially hazardous condition will exist:
1. The inlet concentration of vapors is greater than the TWA.
2. The carbon filter becomes saturated.
3. The ventilation of the room is insufficient to dilute the exhaust of the
enclosure to below the TWA for the chemical.
When the inlet concentration is greater than the TWA, extra measures must be taken to monitor the filter and number of room air exchanges.
Chemical Carcinogen Use with Carbon Filters
Selected carcinogens can only be used with carbon filters in the Fume Adsorber under strict guidance from your Safety Officer.
The use of a vented fume hood or ventilated enclosure with ducting to the outside is always the preferred method when working with carcinogens.
Prohibited Acid Use
The Fume Adsorber with integral blower motorized impeller cannot be exposed to acids. Where applications require the use of acids, a vented fume hood or vented enclosure should be used with a remote blower and ducted to the outside. Consult Labconco for other small enclosures used with a remote blower suitable for acid work. No exceptions are permitted, as the impeller life span will be limited with acid use. Consult Labconco for other enclosures suitable for acid work.
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CHAPTER 6 MAINTAINING YOUR ENCLOSURE
Monitoring airflow and changing the carbon filters (if equipped) is the primary maintenance required.
Review this chapter on maintenance for the following:
1. Routine Maintenance.
2. Determination of when to replace carbon filters and how to replace.
3. Calculating carbon filter life.
Routine Maintenance Schedule
Weekly
Wipe down the interior and exterior surfaces of the enclosure with a mild
soap, depending upon the usage of the unit, and allow to dry.
Operate the exhaust system, noting the airflow velocity through the
enclosure using a source of visible smoke.
Monthly (or more often as required)
Determine the actual face velocity through the sash opening of the
enclosure where the average reading should be at the specified velocity of 35±10 fpm. (Use calibrated thermal anemometer or other approved apparatus).
While the enclosure is filled with the contaminant, test filter condition on
carbon filters using the appropriate gas detector tube at intervals of 20% of the total estimated time. There is a 5/16" diameter hole on the upper right side for inserting the detector tube. The exception to the 20%
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Chapter 6: Maintaining Your Enclosure
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Catalog #
Filter Size
Pounds of Carbon
Carbon Type
For use with
Adsorption weight
Adsorption Volume
6961300
9x26x1.38
6.0
Organic Vapor
Organic Vapors
Varies, see chemical chart
Varies, see chemical guide and chapter 6
6961301
9x26x1.38
7.5
Impregnated Formasorb
Formaldehyde
10%, 0.75lbs
851 ml of 37% Formalin
6961302
9x26x1.38
8.8
Impregnated Ammonasorb
Ammonia and Amines
10%, 0.88lbs
800 ml of 37% Formalin
recommendation is formaldehyde or any carcinogen or suspected carcinogen. These hazardous chemicals must be checked at least every 10% of the total estimated time. Gas detector tubes for the specific chemicals that are being used in the enclosure can be obtained from your laboratory supply dealer.
Replace carbon filters when chemical breakthrough is indicated by odor,
time, detector tube, or for some chemicals, analytical instrumentation. See “Replacing Carbon Filters” section of this manual in Chapter 6.
Determination of When to Replace Carbon Filters and How to Replace
Carbon filter(s) MUST be replaced when any one of the following two conditions are met:
1. The filtered enclosure outlet (exhaust) concentration approaches the inlet
concentration, indicating filter saturation.
2. The odor in the work area becomes intolerable or the concentration of the
chemical in the work area is greater than the TWA.
There are four means of determining when its time to change the carbon filters (not shown in the order of preference).
Odor - A person’s sensitivity to odor, tolerance of odor and their comfort level
under odoriferous conditions vary with the individual. While odor is an indicator that chemicals are passing through the carbon filter, several points need to be understood:
Odor within the room is not necessarily an indication of saturation or
hazardous exposure concentrations.
Odor can be used as a prompt to sample the chemical concentration on the exit
side of the carbon filter.
Organic chemicals approved for use in the filtered enclosure have odors that
are detectable before reaching the time weighted exposure limits.
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Chapter 6: Maintaining Your Enclosure
20
!
Detection Tubes - Color change indicators can be used to measure the concentration of the chemical at the exit side of the carbon filter or in the outlet exhaust. A kit including syringe pump and flexible tubing can be purchased as an accessory from Labconco (Catalog # 6924900). Labconco Customer Service Representatives are supplied with detector tube catalog numbers, as well as telephone numbers to direct you to where to purchase these items. For Organic, Formaldehyde and Ammonia, chemical specific detector tubes should be purchased when installing fresh filters. Each kit contains instructions on how many strokes of the syringe are required to obtain the stated sensitivity. The sampling syringe is connected to the filtered enclosure exhaust. There is a 5/16" diameter hole on the upper right side for inserting the detector tube. Connect the syringe to the detector tube while the system is running and pull the air through the tube with the syringe. Each stroke of the syringe represents a 100-ml sample and corresponds to the number of strokes necessary to give the indicated color changes.
Due to the wide variety of organics and varying TWA’s, it is recommended that
specific detector tubes be purchased directly from Sensidyne, Draeger or your laboratory supply dealer. Alternate detector pumps can also be purchased from your laboratory supply dealers. The vast majority of detector tubes available start measuring at the TWA. When a user observes a color change in the tube, they should replace the filter immediately. If no detector tube for your specific chemical is available, other means of detection must be used.
Time - For applications that have very consistent inlet concentrations and
operating time, “Time” can be used to anticipate saturation or TWA levels based
on prior experience. However, this does not replace the need for sampling. Consult Labconco technical specialist for an estimate of carbon filter life based on chemical usage. Detector tubes, or analytical instrumentation should always be used to determine concentrations in the carbon filter. It is recommended that the carbon filters be checked with detector tubes or other means at intervals of 20% of the total estimated filter life. The exception to the 20% recommendation is formaldehyde and any carcinogen or suspected carcinogen. These more hazardous chemicals must be checked at least every 10% of the total estimated time.
Analytical Instrumentation - This is the most accurate means of measuring concentrations of any chemical. It is the method of choice when no detector tubes are available or the tubes are not sensitive enough to measure at the TWA concentration for the chemical. This method is also to be used to determine saturation when the chemical concentration is below the measurement range of detector tubes.
Carbon Filter Replacement Procedure See Figure(s) A-2 and A-3 in Appendix A for Carbon Filter Replacement.
Do NOT contact blower wheel while still in motion.
NE PAS être en contact avec la roué du ventilateur tant qu’il est en marche.
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Chapter 6: Maintaining Your Enclosure
21
= 4.4 weeks before filter saturation
= .17 ml/min
1. The carbon filter(s) are replaced by first removing the rear perforated
baffle.
2. Remove the upper support bracket for the filter. Then loosen the lower
support bracket.
3. Carefully remove the carbon filter. For 60" wide units there are two carbon
filter(s)
4. Replace the new carbon filter(s) with the gasket on the downstream side
facing the blower. Replace the filter support brackets and tighten.
5. Replace the perforated baffle; replace and tighten the screws.
Calculating Carbon Filter Life
Labconco developed a modeling program to estimate the filter life for typical carbon filters. Since filter life is dependent on the chemical used, the airflow, filter size, and the dwell time, refer to the Chemical Guide for the Paramount® Filtered Enclosure. The estimated life for carbon filters for the Fume Adsorbers with integral impeller is conservatively calculated at 10% of the published values for the Paramount in the Chemical Guide. Consult with a Labconco Technical Specialist for further information on filter life. For example, if you use p-Xylene in your process and evaporate approximately 100 ml per week during 2 hours of use per day then follow these steps to calculate the concentration in parts per million (ppm).
Steps for Calculating PPM and Filter Life
1. Determine the amount of the proposed chemical lost to evaporation over a
given amount of time. For example, if you use p-Xylene and lose approximately 100 ml per week during 2 hours of use per day.
2. Convert the amount lost into ml/min. For this example:
100 ml X 1 week X 10 hours = 100 ml lost week 10 hours use 600 minutes 600 minutes
3. Convert ml/min to PPM by multiplying ml/min by the conversion factor
found in the second to the last column on the right of the Paramount Chemical Guide. For p-Xylene .17 x 25 = 4.2 PPM.
4. Find the PPM value on the chart that comes closest to the value you just
calculated in step #3. In this example, round up to 5 PPM, which is close to the calculated 4.2. We may approximate the filter life to be around 437 hours of actual use, but use 10% of this for the Fume Adsorber filter or 44 hours.
5. Insert the estimated filter life to determine how long filters will last.
44 hours filter life 10 hours per week use
6. This value is for one organic vapor filter. So, 4.4 weeks is approximately
one month before filter saturation.
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Chapter 6: Maintaining Your Enclosure
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Number of
Filters
Filter Size
Pounds of
Formasorb
Carbon
Adsorbed weight of
Formaldehyde
Adsorption Volume of
Formalin
1
26x9x1.38
7.50
0.75 lbs./340 g
851 ml
Number of
Filters
Filter Size
Pounds of
Ammonasorb
II Carbon
Adsorbed weight of
Ammonia
Adsorbed Volume of
50% Ammonia Solution
1
26x9x1.38
8.75
.88 lbs./ 400 g
800 ml
Formaldehyde only
For formaldehyde, use 10% of the impregnated carbon weight. Formalin is 37% formaldehyde by weight. The density of formalin is 1.08 g/ml. These values are for one filter.
Ammonia only
For ammonia, use 10% of the impregnated carbon weight. Assume use of a 50% solution of ammonia for these calculations. These values are for one filter.
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PROBLEM
CAUSE
CORRECTIVE ACTION
Contaminants outside of enclosure.
Improper user techniques for the enclosure.
See Chapter 3 and Chapter 4 sections in the manual. (Ref. Appendix D).
Restriction of the baffle air slots or blockage of the exhaust outlet.
Remove obstruction to ensure that all air slots and the exhaust outlet are unobstructed.
External factors are disrupting the enclosure airflow patterns or acting as a source of contamination.
See “Location Requirements” Chapter 2, “Certifying the Enclosure” Chapter
3, and “Safety Precautions” Chapter 4
sections of this manual. (Ref. Appendix D).
Enclosure has improper face velocity.
Have the enclosure’s exhaust system
checked. Check carbon filters for loading. Enclosure should have an average face velocity of 35 fpm.
Filtered exhausted.
Change and replace the carbon filter.
CHAPTER 7
TROUBLESHOOTING
Refer to the following table if your Fume Adsorber fails to operate properly. If the suggested corrective actions do not solve your problem, contact Labconco for additional assistance.
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Chapter 7: Troubleshooting
24
PROBLEM
CAUSE
CORRECTIVE ACTION
Blower won’t
operate.
Unit not plugged into outlet.
Plug the enclosure into appropriate electrical service.
Circuit breaker(s) or Ground Fault Interrupter.
Reset circuit breaker. Blower wiring is disconnected.
Inspect blower wiring and re-connect.
Blower switch is defective.
Replace switch.
Motorized impeller or blower is defective.
Replace motorized impeller or blower.
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Item
Qty.
Part Number
Description
1A 1 6961000
Canopy Hood, Plastic 30"
1B 1 6961001
Canopy Hood, Plastic 60"
2A 1 6961500
Baffle, 30" Perforated
2B 1 6961501
Baffle, 60" Perforated
2C
4 or 8
1887808
Screw, Machine #10-24 x .50 PH Phil
3
2 or 4
6962500
Bracket, Filter Clamp
4
4 or 8
1896810
Screw, Machine #10-24 x .62 Phil PH/W
5A
1 or 2
6962000
Motorized, Impeller, 115V
5B
1 or 2
6962001
Motorized, Impeller, 230V
6A 1 1307000
Switch, Rocker-DPST
6B 1 6962600
Wire Harness 115/230V
7A 1 1327205
Circuit Breaker 2 Amp (115V)
7B 2 1327206
Circuit Breaker 1 Amp (115V)
8A 1 1334500
Power Cord, 115V
8B 1 1334100
Power Cord, 230V
9A
1 or 2
6961300
Filter, Disposable Organic Vapor
9B
1 or 2
6961301
Filter, Disposable Formaldehyde
9C
1 or 2
6961302
Filter, Disposable Ammonia
APPENDIX A ENCLOSURE COMPONENTS AND REPLACEMENT PARTS
The components that are available for your Fume Adsorber are listed. The parts shown are the most commonly requested. If other parts are required, please contact Product Service.
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Appendix A: Enclosure Components & Replacement Parts
26
Figure A-2
30" Wide Exploded View
Figure A-1
Replacement Parts Isometric
6
2
1
4
3
4
9
7, 8 Not Shown
6
2
4
3
5
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Appendix A: Enclosure Components & Replacement Parts
27
Figure A-3
60" Wide Exploded View
4
3
9
6
7, 8 Not Shown
5
5 3 9
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APPENDIX B DIMENSIONS
See the following dimensions below for all Fume Adsorbers.
Figure B-1
Dimensions for 30" & 60" Wide Fume Adsorber
(Dimensions are in inches)
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APPENDIX C FUME ADSORBER
SPECIFICATIONS
This Appendix contains technical information about all the Fume Adsorber enclosures including electrical specifications and environmental operating conditions.
Electrical Specifications
2 Amps, 115V, 50/60 Hz 1 Amp, 230V, 50/60 Hz
Environmental Conditions
Indoor use only. Maximum altitude: 6562 feet (2000 meters). Ambient temperature range: 41° to 104°F (5° to 40°C). Maximum relative humidity: 80% for temperatures up to 88°F (31°C),
decreasing linearly to 50% relative humidity at 104°F (40°C).
Main supply voltage fluctuations not to exceed ±10% of the nominal
voltage.
Transient over-voltages according to Installation Categories II (Over-
voltage Categories per IEC 1010). Temporary voltage spikes on the AC input line that may be as high as 1500V for 115V models and 2500V for 230V models are allowed.
Used in an environment of Pollution degrees 2 (i.e., where normally only
non-conductive atmospheres are present). Occasionally, however, a temporary conductivity caused by condensation must be expected, in accordance with IEC 664.
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Model Size
30"
60"
Height from Work Surface (inches)
13.50
13.50
Total Open Area with Bypass (sq. ft.)
2.75
5.55
Exhaust Airflow Volume at 35 fpm (CFM)
100
200
*Motor Horsepower (HP)
0.05
0.10
APPENDIX D QUICK CHART FOR THE FUME
ADSORBERS
To determine the actual face velocity at the sash opening, airflow velocity readings
will need to be taken across the opening. The “average face velocity” is achieved
by taking readings in two rows across the enclosure with the readings 6" from the ends and evenly spaced every 12"; the first row is 3" down from the upper plastic hood canopy and the second row is 3" up from the work surface.
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APPENDIX E REFERENCES
Many excellent reference texts and booklets are currently available. The following is a brief listing:
Applicable Standards
UL 61010-1 Standard for Safety Electrical Equipment for Measurement, Control and Laboratory Use; Part 1: General Requirements
Specifies the general safety requirements for electrical equipment.
Based on International Electrotechincal Commission (IEC) Publication
61010-1 with differences noted for U.S. use.
Tests for protection against electrical shock, mechanical hazards, spread of
fire, radiation, liberated gases, explosions and implosion.
Tests for resistance to shock, vibration, impact, heat, moisture and liquids.
Underwriters Laboratories Inc. 333 Pfingsten Road Northbrook, IL 60062 (847) 272-8800
www.ul.com
NIOSH Pocket Guide to Chemical Hazards
NIOSH Publications Mail Stop C-12 4676 Columbia Parkway Cincinnati, OH 45226-1998 Fax (513) 533-8573
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Appendix C: Fume Adsorber Specifications
32
General References
American Conference of Governmental Industrial Hygienists. Industrial Ventilation, A Manual of Recommended Practice, Cincinnati, OH
Department of Labor, Occupational Safety and Health Administration, 29 CFR Part 1910, Occupational Exposures to Hazardous Chemicals in Laboratories, Final Rule. Vol. 55,
No. 21. Washington D.C.:1990
NIH Guidelines for the Laboratory Use of Chemical Carcinogens. NIH Publication No. 81-2385.
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