Labconco CentriVap Concentrators and Cold Traps User Manual
Uss
U
Concentrators and Cold Traps
Models
78100 Series
78110 Series
74600 Series
73850 Series
79820 Series
79830 Series
79840 Series
74750 Series
CentriVap®Centrifugal
err’’ss
e
M
M
a
a
n
n
u
u
all
a
To receive important product updates,
complete your product registration card
online at register.labconco.com
Labconco Corporation
8811 Prospect Avenue
Kansas City, MO 64132-2696
800-821-5525, 816-333-8811
FAX 816-363-0130
E-MAIL labconco@labconco.com
HOME PAGE www.labconco.com
Please read the User’s Manual before operating equipment.
Copyright © 2005, 2007, 2010 Labconco Corporation. All rights reserved.
The information contained in this manual and the accompanying products are copyrighted and all rights
reserved by Labconco Corporation. Labconco Corporation reserves the right to make periodic design
changes without obligation to notify any person or entity of such change.
Warranty
Labconco provides a warranty on all parts and factory workmanship. The warranty includes areas of
defective material and workmanship, provided such defect results from normal and proper use of the
equipment.
The warranty for all Labconco products will expire one year from date of installation or two years
from date of shipment from Labconco, whichever is sooner, except the following;
• Purifier® Logic® Biological Safety Cabinets and PuriCare® Lab Animal Research Stations
carry a three-year warranty from date of installation or four years from date of shipment from
Labconco, whichever is sooner.
• SteamScrubber® & FlaskScrubber® Glassware Washers carry a two-year warranty from date
of installation or three years from date of shipment from Labconco, whichever is sooner.
• Blood Drawing Chairs carry a ten year warranty.
• Carts carry a lifetime warranty.
• Glassware is not warranted from breakage when dropped or mishandled.
This limited warranty covers parts and labor, but not transportation and insurance charges. In the
event of a warranty claim, contact Labconco Corporation or the dealer who sold you the product. If
the cause is determined to be a manufacturing fault, the dealer or Labconco Corporation will repair or
replace all defective parts to restore the unit to operation. Under no circumstances shall Labconco
Corporation be liable for indirect, consequential, or special damages of any kind. This statement may
be altered by a specific published amendment. No individual has authorization to alter the provisions
of this warranty policy or its amendments. Lamps and filters are not covered by this warranty.
Damage due to corrosion or accidental breakage is not covered.
Returned or Damaged Goods
Do not return goods without the prior authorization from Labconco. Unauthorized returns will not be
accepted. If your shipment was damaged in transit, you must file a claim directly with the freight carrier.
Labconco Corporation and its dealers are not responsible for shipping damages.
The United States Interstate Commerce Commission rules require that claims be filed with the delivery
carrier within fifteen (15) days of delivery.
Limitation of Liability
The disposal and/or emission of substances used in connection with this equipment may be governed by
various federal, state, or local regulations. All users of this equipment are required to become familiar with
any regulations that apply in the user’s area concerning the dumping of waste materials in or upon water,
land, or air and to comply with such regulations. Labconco Corporation is held harmless with respect to
user’s compliance with such regulations.
Contacting Labconco Corporation
If you have questions that are not addressed in this manual, or if you need technical assistance, contact
Labconco’s Customer Service Department or Labconco’s Product Service Department at 1-800-821-5525
or 1-816-333-8811, between the hours of 7:00 a.m. and 6:00 p.m., Central Standard Time.
Part #7539800, Rev. F
ECO F695
T
AABBLLEE
T
CHAPTER 1: INTRODUCTION 1
Safety Symbols 2
CHAPTER 2: PREREQUISITES 3
Electrical Requirements 4
Location and Exhaust Requirements 4
Vacuum Pump Requirements 5
Vacuum Line Traps 5
Space Requirements 5
CHAPTER 3: GETTING STARTED 6
Unpacking Your CentriVap 7
CentriVap Components 7
Emergency Access Into the Chamber 10
Component Orientation & Hose Connections 10
Electrical Connection 12
Rotor Installation 12
Ground Wire 12
Chemical Resistance of CentriVap Components 12
Chemical Resistance Chart 13
Solvent Safety Precautions 14
CHAPTER 4: USING YOUR CENTRIVAP 16
Planning 16
Glassware Selection 16
Loading Glassware Into the CentriVap 17
Temperature Setting Guidelines 17
Time Setting Guidelines 17
Heat Boost Operation 17
CentriVap Controls 18
Operating the CentriVap Controls 18
Operating The CentriVap 20
Operational Notes 21
Cycle Interruption 21
Safety Precautions 21
O
O
FF
C
C
OONNTTEENNTTSS
CHAPTER 5: MAINTAINING YOUR CENTRIVAP 22
CHAPTER 6: ACCESSORIES FOR YOUR CENTRIVAP 24
Installing a Glass Lid 27
Installing a Secondary Chemical Trap 27
Installing a Vacuum Gauge 28
Installing a CentriZap Strobe Light 29
Installing a Glass Trap in the Cold Trap 30
CHAPTER 7: TROUBLESHOOTING 31
APPENDIX A: CENTRIVAP COMPONENTS 34
APPENDIX B: CENTRIVAP DIMENSIONS 42
APPENDIX C: CENTRIVAP SPECIFICATIONS 46
Electrical Specifications 46
Environmental Conditions 47
Evaporation Rates 48
DECLARATION OF CONFORMITY 49
CChhaapptteerr 11::
IInnttrroodduuccttiioonn
Congratulations on your purchase of a Labconco CentriVap Concentrator System.
Models are available for operation on 115V or 230V.
The CentriVap Concentrator, when combined with the CentriVap Cold Trap, uses
centrifugal force with heat and vacuum to rapidly evaporate and condense
solvents from biological and analytical samples. Centrifugation eliminates
bumping and foaming as vacuum is applied and also concentrates the solute in the
bottom of the vial. This allows recovery of solutes from sample volumes as small
as a few microliters. The concentrator is equipped with a 300 watt heater to speed
evaporation by warming the chamber during processing. A timed outlet for the
vacuum pump connection delays the start of the pump until the rotor reaches
operating speed. A safety switch prevents the concentrator from starting when the
lid is in the open position and a latch prevents the lid from being opened while the
rotor is turning. The compact, low profile design allows the concentrator to be
placed on a benchtop or other laboratory work surface.
The microprocessor, which controls the operation of the heater and the motor,
provides excellent regulation and reproducibility of protocols. The end of the run
can be signaled by a manually preset timer. Nine different protocols can be stored
in memory so exact test parameters can be easily repeated.
As the companion to the Concentrator, the CentriVap Cold Trap protects the
vacuum pump by trapping moisture, vapors and corrosive fumes as they evaporate
from the samples. The stainless steel trap is used for aqueous and organic
applications. For corrosive applications, the optional Glass Trap insert should be
used. The 230V 50Hz models comply with CE regulations.
Product Service 1-800-522-7658
1
Chapter 1: Introduction
Safety Symbols
Your CentriVap Concentrator was designed with safety in mind, however
conditions may exist that could be hazardous.
Throughout this manual potentially hazardous conditions are identified using the
following words and symbols.
It is important that you understand the warnings listed throughout this manual
before you operate the CentriVap Concentrator.
2
Product Service 1-800-522-7658
CChhaapptteerr 22::
PPrreerreeqquuiissiitteess
Before you install your CentriVap, you need to prepare your site for installation.
You must be certain that the area is level and of solid construction. In addition, a
means to exhaust the vacuum pump must be provided. An electrical source must
be located near the installation site.
Carefully read this chapter to learn:
• The electrical supply requirements.
• The exhaust requirements.
• The vacuum pump requirements.
Refer to Appendix C: CentriVap Specifications for complete electrical and
environmental conditions, specifications and requirements.
Product Service 1-800-522-7658
3
Chapter 2: Prerequisites
Electrical Requirements
The CentriVap Concentrator requires a dedicated grounded electrical outlet. This
outlet requires a 15 Amp circuit breaker or fuse for models rated at 115V (60 Hz).
An 8 Amp circuit breaker or fuse is required for models rated at 230V (50/60 Hz).
If the power cord supplied with the Concentrator does not match the available
receptacle, replace it with an approved power cord of the suitable style. See
CentriVap Components in Chapter 3 for power cord specifications.
The CentriVap Cold Trap requires a dedicated electrical outlet. 115V (-50°C &
-85°C) Models require a 15 Amp circuit breaker or fuse rated at 115V (60 Hz).
115V (-105°C) Models require a 20 Amp circuit breaker or fuse rated at 115V (60
Hz). 230V Models require an 8 Amp circuit breaker or fuse rated at 230V (50/60
Hz). If the power cord supplied with the Cold Trap does not match the available
receptacle, replace it with an approved power cord of the suitable style. See
CentriVap Components in Chapter 3 for power cord specifications.
Location and Exhaust Requirements
The CentriVap Concentrator should be located on a surface that is stable, flat and
level.
WARNING: The CentriVap System should be located within a fume hood if
hazardous or flammable solvents are used. Heating of materials could lead
to the liberation of hazardous gases. In all cases, regardless of the solvent
used, it is strongly recommended that the vacuum pump is vented in a fume
hood. An accessory secondary trap is available to minimize the exhausting of
solvents into the atmosphere. This does not, however, negate the need to
exhaust the vacuum pump into a fume hood. Failure to properly vent the
CentriVap will expose personnel to potentially harmful chemicals.
The CentriVap has not been evaluated by an approval agency for the use of
biological, radio toxins or flammable liquids or materials.
4
Product Service 1-800-522-7658
Chapter 2: Prerequisites
Vacuum Pump Requirements
A vacuum pump must be provided by the user. A vacuum pump with a free air
flow rate of 82 liters per minute and < 2 mBar ultimate pressure is adequate for
aqueous samples. More volatile samples can be satisfactorily processed using a
diaphragm pump with a free airflow of 42 liters per minute and 200 mBar
vacuum. The inlet fitting on the vacuum pump must be suitable for 0.50 ID hose.
Vacuum pumps used with 115V models should be equipped with a 115V, 15 Amp
NEMA 5-15P plug. Vacuum pumps used with 230V models should be equipped
with a “reverse” IEC 320 plug. This will allow the vacuum pump to be plugged
into the receptacle on the back of the CentriVap.
IMPORTANT NOTE: To ensure that aggressive samples used in the
CentriVap do not damage the vacuum pump, it is recommended that all
internal wetted parts are Teflon®* or Teflon coated.
When selecting the vacuum pump it is very important to consider the
flammability of the solvent that will be used. If the solvents are flammable,
an explosion-proof vacuum pump or one suitable for the solvents to be
processed is recommended. See Chapter 3 Solvent Safety Precautions for
solvents suitable for use in the CentriVap.
Vacuum Line Traps
When using a mechanical pump that is not corrosion resistant, the CentriVap Cold
Trap or equivalent trap must be used in the vacuum line to prevent damage from
solvent vapors. When evaporating acids, it is advisable to include a soda lime
acid secondary trap in the vacuum line. This adds additional protection for the
pump.
NOTE: Several components within the CentriVap are made from stainless
steel or aluminum and can be degraded if exposed to acids. Contact
Labconco before evaporating acids.
A moisture trap, solvent trap and radioisotope trap are also available. Refer to
Chapter 6: Accessories for Your CentriVap for ordering information.
Space Requirements
Refer to Appendix C: CentriVap Specifications for dimensional drawings of the
CentriVap.
No person or any hazardous material should be within 12 inches of the CentriVap
Concentrator while it is operating.
*Teflon® is a registered trademark of DuPont
Product Service 1-800-522-7658
5
CChhaapptteerr 33::
GGeettttiinngg SSttaarrtteedd
Now that the site for your CentriVap is properly prepared, you are ready to
unpack, inspect, install, and test your CentriVap. Read this chapter to learn how
to:
• Unpack and move your CentriVap.
• Set up your CentriVap.
• Connect the electrical supply source to your CentriVap.
• Properly exhaust your CentriVap.
• Safely use solvents with your CentriVap.
CAUTION: The CentriVap Concentrator weighs over 42 lbs. (19 Kg). The
carton allows for lifting with a mechanical lift truck or hand truck. If you
must lift the CentriVap manually, use at least two (2) persons and follow safe
lifting guidelines.
The CentriVap Cold Trap weighs over 70 lbs. (33 Kg). The carton allows for
lifting with a mechanical lift truck or hand truck. If you must lift the Cold
Trap manually, use at least two (2) persons and follow safe lifting guidelines.
6
Product Service 1-800-522-7658
Chapter 3: Getting Started
Unpacking Your CentriVap
Carefully unpack your CentriVap and inspect it for damage that may have
occurred in transit. If your CentriVap is damaged, notify the delivery carrier
immediately and retain the entire shipment intact for inspection by the carrier.
The United States Interstate Commerce Commission rules require that claims be
filed with the delivery carrier within fifteen (15) days of delivery.
Do not discard the carton or packing material for your CentriVap until you have
checked all of the components and installed and tested the CentriVap.
NOTE: Do not return goods without the prior authorization of Labconco.
Unauthorized returns will not be accepted. If your CentriVap was damaged
in transit, you must file a claim directly with the freight carrier. Labconco
Corporation and its dealers are not responsible for shipping damage.
CentriVap Components
Locate the model of CentriVap you received in the following tables. Verify that
the components listed are present.
Cold Traps
Description Power Cords Accessories
1334500
1336100
1332600
1332700
1338000
1336400
1336500
1332601
1332701
1342100
7828606
1488800
7464600
Catalog #
7811020 -50˚C 115 60 X X X X X
7811030 -50˚C 230 50 X X X X X
7811035 -50˚C 230 50 X X X X X
7811037 -50˚C 230 50 X X X X X
7811040 -50˚C 230 60 X X X X X
7460020 -85˚C 115 60 X X X X X
7460030 -85˚C 230 50 X X X X X
7460035 -85˚C 230 50 X X X X X
7460037 -85˚C 230 50 X X X X X
7460040 -85˚C 230 60 X X X X X
7385020 -105˚C 115 60 X X X X X
7385030 -105˚C 230 50 X X X X X
7385035 -105˚C 230 50 X X X X X
7385037 -105˚C 230 50 X X X X X
7385040 -105˚C23060 XXXXX
Temperature
Rating
Plug: CEE 7/7
Voltage (V)
Plug: NEMA 5-15
Connector: IEC C13
Frequency (Hz)
Plug: BS 1363
Plug: CH1-10P
Connector: IEC C13
Connector: IEC C13
Plug: NEMA 6-15
Connector: IEC C13
Connector: IEC C13
Plug: CEE 7/7
Plug: BS 1363
Plug: NEMA 5-20
Connector: IEC C19
Connector: IEC C19
Plug: CH2-16P
Connector: IEC C19
Connector: IEC C19
Tubing
Plug: NEMA 6-20
Connector: IEC C19
clamps (2)
Wire Assembly
7539800
User's Manual
Product Service 1-800-522-7658
7
Chapter 3: Getting Started
Description Power Cords Accessories
Concentrators
1334500
1336100
1332600
1332700
1338000
7828606
1488800
7397601
7396206
7539800
Connector: IEC C13
Plug: NEMA 6-15
Tubing
clamps (2)
Coupling Insert (Std.)
Coupling Insert (AR)
Catalog #
Options
Voltage (V)
Frequency (Hz)
Connector: IEC C13
Plug: NEMA 5-15
Connector: IEC C13
Plug: CEE 7/7
Connector: IEC C13
Plug: BS 1363
Connector: IEC C13
Plug: CH1-10P
7810010 standard 115 60 X X X X X
7810011 standard 230 60 XXXX X
7810012 heat boost 115 60 X X X X X
7810013 heat boost 230 60 XXXX X
7810014 glass lid 115 60 X X X X X
7810015 glass lid 230 60 XXXX X
7810016 acid resistant 115 60 X X X X X
7810017 acid resistant 230 60 X X X X X
7810030 standard 230 50 X X X X X
7810031 heat boost 230 50 X X X X X
7810032 glass lid 230 50 X X X X X
7810033 acid resistant 230 50 X X X X X
7810034 standard 230 50 X X X X X
7810035 heat boost 230 50 X X X X X
7810036 glass lid 230 50 X X X X X
7810037 acid resistant 230 50 X X X X X
7810038 standard 230 50 X X X X X
7810039 heat boost 230 50 X X X X X
7810040 glass lid 230 50 X X X X X
7810041 acid resistant 230 50 X X X X X
User's Manual
8
Product Service 1-800-522-7658
Chapter 3: Getting Started
Accessories
1486000
1488800
7474001
7828606
1553800
7397605
7455101
7455100
7815200
7814800
7814900
7460900
Clamps (2) .48 - .78"
Clamps (2) .56 - 1.25"
Valve Assembly
Tubing 1/2" ID
Tubing 1/4" ID
Glass Trap
12-13mm (Teflon)
Rotor Assembly
12-13mm
Rotor Assembly
Solvent Insert
Acid Insert
Moisture Insert
Clear Cannister
4330150
Gel Dryers
Concentrator Systems
4330100
7811040
7811037
7811035
7811030
7811020
7810041
7810040
7810038
7810037
7810036
7810034
7810033
7810032
7810030
7810017
7810016
7810015
7810014
7810011
7810010
Frequency (Hz)
Voltage (V)
System Type
Description Concentrators Cold Traps
Catalog #
7982010 Aqueous 115 60 X X X X X
7982011 Aqueous 230 50 X X X X X
Product Service 1-800-522-7658
7982012 Aqueous 230 60 X XXXX
7982035 Aqueous 230 50 X X X X X
7982037 Aqueous 230 50 X X X X X
7983013 Acid 115 60 X X X X X X
7983014 Acid 230 50 X X X X X X
7983015 Acid 230 60 X X X X X X
7983035 Acid 230 50 X X X X X X
7983037 Acid 230 50 X X X X X X
7984010 Solvent 115 60 X X X X X
7984011 Solvent 230 50 X X X X X
7984012 Solvent 230 60 X X X X X
7984035 Solvent 230 50 X X X X X
7984037 Solvent 230 50 X X X X X
7475010 Gel Drying 115 60 X X X X XXXXX
7475011 Gel Drying 230 50 X X X X XXXXX
7475012 Gel Drying 230 60 X X X X XXXXX
9
Chapter 3: Getting Started
If you do not receive one or more of the components listed for your CentriVap,
contact Labconco Corporation immediately for further instructions.
Emergency Access into the Chamber
The CentriVap is designed to prevent access to the chamber in the event of a
power disruption. If it is necessary to open the lid when there is no electrical
power connected to the CentriVap, insert a small screwdriver or similar
instrument into the small round hole on the left side of the case near the top
behind the control panel. This will unlock the lid latch mechanism. While
holding the screwdriver in place, raise the lid with the other hand.
CAUTION: Never attempt to defeat the latch or open the lid while the
CentriVap is running. Personnel injury can result from moving parts and
chemicals.
Component Orientation & Hose Connections
The relative position of the CentriVap Concentrator, Cold Trap and the vacuum
pump may be as shown or may be reversed. The refrigeration system in the Cold
Trap draws air in through the right side of the cabinet and exhausts air through the
left side of the cabinet. A minimum of 3" should be allowed between the sides of
the Cold Trap and the adjacent wall surfaces. Restriction of the airflow through
the cabinet during operation could adversely affect performance.
10
Product Service 1-800-522-7658
Chapter 3: Getting Started
After positioning the components, it is necessary to join the system together using
the hoses provided. Attach one hose to the tube that extends out the back of the
Concentrator. Attach the other end of this hose to one of the barb fittings on the
Cold Trap Cover Assembly. Secure the hoses with the clamps supplied. Attach
another hose to the remaining barb fitting on the Cold Trap Cover and clamp
securely. If the accessory Secondary Trap is not used, attach the other end of the
hose to the inlet port on the vacuum pump. If the accessory Secondary Trap is
used, install the Secondary Trap as explained in Chapter 6: Accessories for Your
CentriVap. Then attach the hose from the Cold Trap Cover to the “out” connector
on the Secondary Trap and clamp securely. Attach another hose from the
remaining connector on the Secondary Trap to the inlet port on the vacuum pump
and clamp securely.
WARNING: It is recommended that the vacuum pump be located inside a
fume hood or other laboratory ventilation device if hazardous solvents are
used in the CentriVap. If this is not possible, the vacuum pump should have a
hose attached to the exhaust port and the other end of the hose should be
positioned inside the fume hood or ventilation device.
Product Service 1-800-522-7658
11
Chapter 3: Getting Started
Electrical Connection
Plug the power cord into the receptacle on the back of the CentriVap Concentrator
and plug the other end into a suitable power receptacle. Plug the power cord into
the receptacle on the back of the CentriVap Cold Trap and plug the other end into
a suitable power receptacle. Plug the power cord from the vacuum pump into the
receptacle on the back of the Concentrator. If the vacuum pump has an off/on
switch, turn the switch ON. The vacuum pump will be controlled by the
Concentrator.
Rotor Installation
Place the rotor onto the shaft of the Concentrator. Rotate the rotor slightly to
engage the drive pin in the shaft with the slots in the rotor hub. The top of the
shaft should be in line with the top of the rotor hub.
INPORTANT NOTE: Do not use a rotor if it shows any signs of damage.
Failure of a spinning rotor could damage the CentriVap or cause samples to
be lost.
Ground Wire
Attach one end of the included ground wire to the stainless steel elbow on the
drain tubing on the right or left side (depending on model) of the Cold Trap.
CAUTION: When draining the CentriVap Cold Trap always attach the
other end of the grounding clip to the solvent catch pot to eliminate the risk
of electrostatic spark ignition.
Chemical Resistance of CentriVap Components
Your CentriVap Centrifugal Concentrator and Cold Trap are designed to be
chemical resistant to most compounds that are commonly used in concentration
processes. However, by necessity, the CentriVap is comprised of a number of
different materials, some of which may be attacked and degraded by corrosive
chemicals. The degree of degradation is obviously dependent on the concentration
and duration of exposure. Some major components of the CentriVap that are
susceptible to degradation are as follows:
12
Product Service 1-800-522-7658
Loading...