FreeZone® Triad® Benchtop Freeze Dryers
The considerate freeze dryer.
Your samples are our motivation. Because we know
how much freeze drying matters. Tissue research.
Drug discoveries. Vaccine development. Lives saved.
Your freeze dried samples may need to be stoppered
in vials under vacuum. Or you may have a variety of
samples on trays and in asks. If so, consider the
FreeZone® Triad®.
Triad makes selecting the right freeze dryer system easy.
How? By combining a benchtop lyophilizer with a built-in
stoppering tray dryer for vials and four port manifold for
asks. Its -85° C collector can handle either aqueous or
dilute acetonitrile samples. Add a vacuum pump and
you’re ready to go. Ready to start your work.
As we’ve done since 1974, we build each FreeZone by
hand. With care. And the highest quality materials. Your
Triad will last and last.
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We considered everything. All in one system. Versatile
sample handling. Durability. Triad.
Lyo-Works™ Operating System
Features & Benets
Programs
Lets you create, edit,
view and initiate programs.
Stores up to 30 programs
with up to 16 steps each. Each
step may include ramp rate,
shelf temperature, hold time
and vacuum.
Home
Get at-a-glance collector
temperature, vacuum
pressure, shelf and sample
temperature, program step
and data logging mode.
Program Button
Opens the Programs screen.
Data Logging
Starts/stops logging. View the
data in table or graph form.
Manual Button
Manually starts/stops the collector and shelf temperature control.
Select from three modes: shelf to Max Cold, freeze dr y asks only,
and maintain shelf temperature to set point.
Settings
Select language, security
code, sensor calibration,
time/date/time zone, alert
emails and more.
Sensors
Displays temperature
values for collector, vacuum,
shelf and sample sensors.
Help
Access diagnostic tools.
Vacuum Button
Manually starts/stops
the vacuum pump or change
the vacuum set point.
Defrost Button
Manually starts/stops defrost.
Automatically turns off when
collector reaches +60° C or
after two hours of defrost.
Lyo-Works is more than a large touch screen display.
It’s a set of powerful controls and useful insights
about
your freeze drying process. You’ll experience peace of
mind about the integrity of your samples throughout
lyophilization, even when you’re not in the lab.
Lyo-Works lets you monitor, record and store the
condition of your samples.
• Real time on-screen tables and graphs to
immediately show sample status so you can make
adjustments if needed
See how Lyo-Works works at labconco.com/lyo-works.
• Data and program storage for repeatability
of protocols
• Data transfer via Ethernet or USB port
(no additional recorders or computers needed)
Your samples and time are valuable. Find out how your
samples are doing every step of the way from your
smartphone—at work or away.
• Get email updates on your samples’ status
• Get email notications when your freeze dryer’s
set points are outside of normal range
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FreeZone® Triad® Benchtop Freeze Dryers
Features & Benets
❉
Pneumatic mechanism stoppers containers on shelf
Containers are stoppered while chamber is under vacuum and
without the use of compressed gas. Atmospheric pressure causes
the diaphragm to expand. The pressurized diaphragm forces
the plate down, pushing the stoppers into the containers.
❉
Environmentally-safe
refrigeration
Two compressors cool the
collector coil to -85° C
(-121° F), ideal for samples with
low eutectic points including
ones containing dilute
acetonitrile. Refrigeration and
heat alter the temperature of
uid circulating through
channels in the shelf. Shelf
may be set to pre-freeze and
then to lyophilize. Safe
refrigerant is non-ammable
and does not contain
hydrochlorouorocarbons
(HCFCs) or chlorouorocarbons
(CFCs) that can damage
the ozone.
❉
Collector drain pan and hose
Stainless steel drain pan
catches defrosted condensate.
Remove the pan for cleaning.
Four valve ports
Versatile Triad lets you freeze
dry samples in asks and on
the shelf at the same time.
Pre-freeze samples to save
money and time
Samples may be frozen on the
shelf at a controlled rate,
eliminating the need for a
separate freezer and
product transfer.
❉ Labconco exclusive feature
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FreeZone® Triad® Benchtop Freeze Dryers
Specications
Application suitability:
• Small sample loads or numerous sample batches containing
water or acetonitrile
• Stoppering vials or serum bottles under vacuum
• Limited oor space
All models feature:
❉ Stainless steel collector coil capable of removing 1.84 L of water
in 24 hours and holding 2.5 L of ice before defrosting*
❉ Two 1/3 hp HCFC/CFC-free refrigeration compressors cool the
collector to -85° C (-121° F) and work in concert with a 1000-watt
heater to cool and heat uid medium circulating through channels
in the shelf. Not for use with samples containing methanol or
ethanol
• Processing shelf, 12.4" w x 14.5" d (31.5 x 36.8 cm). Spacing
between shelf and top of chamber accommodates containers
with stoppers up to 148 mm maximum height
• One probe for monitoring temperature of sample in chamber
• Pirani vacuum sensor
• Temperature ramp and hold programming from -55° C to +50° C
(-67° F to +122° F) and -75° C (-103° F) during pre-freezing.
Controls temperature to ±1° C of set point. Memory to store 30
programs with 16 segments each including number of steps,
ramp rate, shelf temperature, hold time and vacuum level
❉ Full color, 5" capacitive touch screen with Lyo-Works OS:
– Real time display of collector temperature and vacuum level
– Creation and storage for up to 30 programs with up to 16
steps each. Ability to set ramp rate, shelf temperature, shelf
temperature time and vacuum set point per step
– Manual start-up buttons for collector and shelf temperature
control and vacuum pull down
– Alerts, diagnostic tests, user manual and defrost control
– Data logging stores and displays data in table or graph format,
and may be exported via USB or Ethernet
– Settings include language (English, Spanish, French,
German, or Italian), time, temperature (° C or ° F) and vacuum
(mBar, Torr or Pa)
– Alerts can be emailed to user-entered addresses via
Ethernet connection
– Vacuum pump maintenance alert
– Security lock-out
❉ Pneumatic stoppering mechanism with diaphragm and plate.
No compressed gas is required
• Stoppering control knob, vacuum release control knob and 1/8"
OD user-supplied sterile/inert gas backll port
• Four left side-mounted neoprene valves with molded plastic
knobs and ttings that accommodate 1/2" and 3/4" ask adapters
❉ USB port and Ethernet connection
• Electrical receptacle for vacuum pump
• Hot gas defrost with stainless steel drain pan, silicone drain
hose and auto shut off at +60° C (+140° F)
• Vacuum control valve
❉ Vacuum break valve
• Stainless steel and powder-coated steel exterior
• Clear acrylic door, 1" thick, with silicon gasket and latch
• 3/4" OD vacuum connection. 36" long, 3/4" ID vacuum hose with
two clamps
Models conform to the following standards:
• UL Standard 61010-1 (115/230V, 60 Hz models)
• CAN/CSA C22.2 No. 61010-1 (115/230V, 60 Hz models)
• CE Conformity marking (230V, 50 Hz models)
྇California WARNING: Cancer - P65Warnings.ca.gov
Options include:
• Region-specic electrical plug congurations
All models require (not included):
• Vacuum pump with a displacement of at least 98 L/min,
0.002 mBar ultimate pressure and tting for 3/4" ID vacuum
hose. See page 7
• Freeze dry glassware if not bulk freeze drying
Serum Bottle Capacity
Catalog Number 7575010 7575210 7575310 7573210 75 73410 7573 610 757 3810 7 574 010 7 574210
Volume 2 ml 3 ml 5 ml 10 ml 20 ml 30 ml 50 ml 100 ml 125 ml
Shelf Capacity 400 441 233 196 121 86 64 42 36
* Freeze drying rate will be l ower for samples other than plain water. For optimum performance, room te mperature should be 21° C (70° F) or colder.
❉ Labconco exclusive feature
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FreeZone® Triad® Benchtop Freeze Dryers
Ordering Information
Catalog Number Congurator:
Use this key to congure the nine digit catalog number to order
your FreeZone Triad Benchtop Freeze Dryer.
7940010
Select the ELECTRICAL CONFIGURATION and
PLUG TYPE of your freeze dryer. These are the eighth
and ninth digits of your catalog number.
10 = 230V, 60 Hz, 12A with plug for North America
15 = 230V, 60 Hz, 12A with plug for Saudi Arabia
30 = 230V, 50 Hz, 12A with Schuko plug
40 = 230V, 50 Hz, 12A with plug for China/Australia
50 = 230V, 50 Hz, 12A with plug for Great Britain (UK)
70 = 230V, 50 Hz, 12A with plug for India
Plug Congurations
230V, 60 H z
for North America
230V, 50 H z
for China/Australia
230V, 60 H z
for Sa udi Ara bia
230V, 50 H z
for Gr eat Brit ain (UK )
230V, 50 H z
Schuko
230V, 50 H z
for India
Actual Dimensions & Shipping Weight
Overall Dimensions ( w x d x h) Shipping Weight
28.3" x 29.5" x 27.7" (71.9 x 74.9 x 70.4 cm) 440 lbs. (200 kg)
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Vacuum Pumps
Selection Guide & Ordering Information
The Rotary Vane, Combination and Scroll Vacuum Pumps
provide the deep vacuum needed for good freeze drying results.
Sample Contains Pump Type Recommend Pump (≥98 lpm )* Recommended Pump (≥163 lpm)
Water Rotary Vane 7739402 7739403
Acids & Solvents
Combination 7584002 —
Scroll — 7587002
Rotary Vane Combination
General Purpose Rotary Vane Vacuum Pumps
For use with aqueous samples. Ultimate vacuum (total pressure)
-3
2 x 10
mBar (1.5 micron). With cast aluminum casing, rubber feet,
lifting bracket, on/off switch, two inlet adapters (1/2" and 3/4" OD).
Two position selector: High Vacuum and High Throughput. Three
position gas ballast: Closed, Low Flow and High Flow. Single
phase direct drive motor, totally enclosed and fan cooled, with
thermal overload protection. Isolation valve seals the inlet to
prevent oil and air contamination of the system in the event of
power failure. Include 230V reverse IEC plug, four each one liter
bottles of vacuum pump oil and one exhaust lter with oil mist and
odor lter elements.
Find the recommended Rotary Vane, Combination and/or Scroll
Vacuum Pump for your Triad based on your sample type.
Scroll
as HPLC-prepared and peptide puried materials. Two-stage rotary
vane pump and two-stage, chemical-resistant diaphragm pump.
Diaphragm pump removes the condensible vapors in the rotary
vane pump before they can contaminate the oil, to extend oil and
pump life. Pump oil lasts up to 10 times longer than in conventional
rotary vane pumps. Ultimate vacuum (partial pressure) 2 x 10
mBar (1.5 micron). Pressure control valve compensates for the
different volumes displaced by the two pumps. Glass separator
captures downstream condensate vapors. Includes 230V reverse
IEC plug, lifting handle, 3/4" OD inlet adapter, one liter bottle of
vacuum pump oil, power switch, power cord and plug. 115 (98)
L/min displacement at 60 Hz (50 Hz). Operates on 230V, 50/60 Hz,
2.7A. Shipping weight 66 lbs. (30 kg)
-3
Catalog
Number
7739402
7739403
7584002—VACUUBRAND HYBRID** Combination
Vacuum Pump
For use with acids and other harsh chemicals including TFA, TFA
by-products, acetonitrile, HBe and HNO
*Faster f reeze drying rates may be achieved by using pump s with larger displac ement capacities.
**VACUUBRAND HYBRID
Electrical
Conguration
230V, 50/60
Hz, 2.4A
230V, 50/60
Hz, 4.0A
™
is a trade mark of VACUUBRAND GMBH + CO KG.
Displacement
at 60 Hz
(50 Hz) L/min
117 (98)
L/min
195 (163)
L/min
present in samples such
3
Shipping
Weight
62 lbs.
(28 kg)
65 lbs.
(30 kg)
7587002—Scroll Vacuum Pump
For use with acids below 20% concentration and solvents
including acetonitrile. Low maintenance, longer lasting. Does not
require oil for lower lifetime operation costs, less maintenance is
needed compared to oil pumps. Lubrication-free, hermetically-free
environment for totally clean and dry vacuum. Two spiral scrolls
compress air and vapors to move them toward the exhaust.
Ultimate vacuum (partial pressure) 2 x 10
Quiet operationof <52 dB(A). Glass separator captures
downstream condensate vapors. Includes 3/4" inlet adapter,
power switch, power cord and plug. 195 (189) L/min displacement
at 60 Hz (50 Hz). Operates on 230V, 50/60 Hz, 2.7A. Shipping
weight 59 lbs. (26 kg)
-3
mBar (5.3 micron).
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Vacuum Pumps
Accessories
1472200—Inlet Filter. For Rotary Vane Pumps 7739402 and
7739403. Prevents oil back streaming and prevents submicron
particle damage. Includes lter assembly and one lter cartridge.
Life is approximately 1000 hours at 1.33 x 10
vacuum. Shipping weight 1.0 lb. (0.5 kg)
1473400—Replacement Exhaust Filter. For Rotary Vane Pumps
7739402 and 7739403. Removes oil mist and odor from exhaust.
Includes lter assembly, one oil mist lter cartridge and one odor
lter cartridge. Oil mist lter life approximately one year and odor
lter cartridge life approximately six months at 1.33 x 10
(10 microns) vacuum. Shipping weight 1.0 lb. (0.5 kg)
7584300—VACUUBRAND* B-Oil. One liter. Replacement oil for
Combination Vacuum Pumps 7584000 and 7584002. Shipping
weight 2.0 lbs. (0.9 kg)
7541300—Vacuum Pump Oil. One gallon (3.8 L) synthetic
hydrocarbon oil. Shipping weight 12 lbs. (5 kg)
Vacuum Pump Oil. Hydro-treated parafnic hydrocarbon oil.
Replacement oil for Rotary Vane Pumps 7739402 and 7739403.
Catalog Number Volume Shipping Weight
1988000 One liter 2.0 lbs. (0.9 kg)
1988001 One gallon (3.8 L) 12 lbs. (5 kg)
-2
mBar (10 microns)
-2
mBar
1473500—Oil Return Kit. Allows extended operation of the
pump with the ballast open and helps to keep oil purged of
contaminants. When excess oil collects in the lter, it is directed
back to the pump to conserve oil. Stainless steel cylinder and
tubing with clamp. Shipping weight 0.5 lb. (0.2 kg)
7587300—Pump Silencer. For Scroll Pump 7587002. Filters
exhaust and silence exhaust pump noise. Includes lter, centering
ring and exhaust outlet clamp. Shipping weight 2.0 lbs. (0.9 kg)
7587200—Tip Seal Replacement Kit. For Scroll Pump 7587002.
Includes two tip seals, two o-rings, exhaust valve and spring and
other small components. Shipping weight 2.0 lbs. (0.9 kg)
7587500—Bearing Replacement Service Kit. For Scroll Pump
7587002. Includes contact bearings, shaft end cap, washers,
screws, plugs and o-rings. Shipping weight 2.0 lbs. (0.9 kg)
7373436—Wire-Reinforced PVC Tubing. 3/4" ID. 3' length.
Shipping weight 5.0 lbs. (2.3 kg)
Visit labconco.com for ordering information on serum
bottles, vials, asks, carts and other accessories.
*VACUUBRAND™ is a trade mark of VACUUBRAND GMBH + CO KG.
LABCONCO CORPORATION
8811 Prospect Avenue
Kansas City, MO 64132
(800) 821-5525 | (816) 333-8811
labconco.com
Made in the U.S.A.
©2018 LABCONCO CORPORATION
Printed in the U.S.A.
Product design subject to change
without notice.
3-35-06/19/18
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