JUMO tecLine CR-4P Operating Instructions Manual

JUMO tecLine CR-4P
Conductive 4-electrode conductivity sensor
Type 202930
B 202930.0
Operating Instructions
2012-04-05/00502496
WARNING:
Incorrect measurement values or failure of the instrument or a transmitter connected to it, could potentially cause dangerous, imprecise dosing or a system malfunction! Suitable preventive measures to stop this happening must be in place.
Note:
Please read these operating instructions before commissioning the instrument. Keep the manual in a place which is accessible to all users at all times.
If any difficulties should arise during startup, please do not tamper with the instrument in any way. By doing so, you could endanger your rights under the instrument warranty! Please contact your supplier.
Contents
1 Typographical conventions ...................................................... 5
1.1 Warning signs ..............................................................................................5
1.2 Reference signs ...........................................................................................5
2 Description ................................................................................ 6
3 Instrument identification .......................................................... 8
3.1 Nameplate ....................................................................................................8
3.2 Type description ..........................................................................................8
3.3 Accessories ..................................................................................................9
4 Mounting .................................................................................. 10
4.1 General .......................................................................................................10
4.2 JUMO PEKA process connection adapter .................................................11
4.3 Mounting suggestions ................................................................................11
5 Installation ............................................................................... 15
5.1 Electrical connection ..................................................................................15
5.2 Terminal assignment and wiring colors .....................................................15
5.3 CR-4P cable ...............................................................................................16
5.4 Connection example ..................................................................................17
6 Calibration ............................................................................... 19
6.1 Notes ..........................................................................................................19
6.2 General .......................................................................................................19
6.3 JUMO AQUIS 500 CR settings ..................................................................19
7 Maintenance/troubleshooting ............................................... 20
7.1 Cleaning the conductivity sensor ...............................................................20
7.2 Troubleshooting .........................................................................................21
8 Technical data ......................................................................... 22

1.1 Warning signs

Danger
This symbol is used when there may be danger to personnel if the instructions are ignored or not followed correctly!
Caution
This symbol is used when there may be damage to equipment or data if the instructions are ignored or not followed correctly!

1.2 Reference signs

Note This symbol is used to draw your special attention to a remark.

1 Typographical conventions

1
abc
Action instruction
Footnote
Footnotes are remarks that refer to specific points in the text. Footnotes consist of two parts:
A marker in the text and the footnote text. The markers in the text are arranged as consecutive superscript numbers.
This symbol indicates that an action to be performed is described. The individual steps are marked by this asterisk. Example: Connect the cable.
5

2 Description

General
Conductive conductivity sensors are used in conjunction with suitable transmitters in industrial analysis measurement technology to determine the electrolytic conductivity of liquids.
The JUMO tecLine CR-4P fills the gap between conductive conductivity measurement with two-electrode measuring sensors, and inductive conductivity measurement.
Four-pin technology makes it possible to cover a very wide measuring range from about 1 µS/cm to 600 mS/cm, with just one measuring sensor.
The hygienic design of the sensor and the EHEDG-certified system for process connection (JUMO PEKA), mean that it can be used in pharmaceutical and food technology without difficulty. JUMO PEKA is an adapter system that combines the measuring sensor with the process connection. All the materials are physiologically safe, and meet FDA standards.
Stainless steel electrodes are inserted into a circular, plastic body. The process seal provided as standard is an EPDM O-ring. A fast-response temperature probe delivers information about the process temperature to the measurement amplifier. Electrical connection is made via an M12 connector.
The measuring sensor is available in three fitting lengths, for optimum installation in different pipe diameters. The measuring sensor can also be installed in container walls. No incident flow is required to make it work, but is recommended for fast, stable measurement values and to prevent the accumulation of deposits.
Operative range
Note
Key features
A certificate of quality is included among the items supplied (exact cell constant, FDA approval for the material, typical surface roughness, etc.).
Their vast measuring range of 1 µS/cm to 600 mS/cm, allows the sensors to be used in washing processes in food and drink applications, pharmaceuticals and biotechnology, where the different conductivities have to be safely recorded by a measuring system (e.g. CIP/SIP applications, reverse processes in ion exchangers, phase separation, bottle cleaning plants, process water).
Used in combination with the JUMO AQUIS 500 CR transmitter/controller, as per data sheet 202565 and JUMO PEKA process connection adapters as per data sheet 409711.
• Vast measuring range
• EHEDG-certified process connections (clamp, Varivent
• CIP/SIP capability
• Design complies with EHEDG and FDA standards
• Certificate of quality included
®
, aseptic NKS)
6
Function
voltage/current
voltage
current/voltage
control
voltage measurement
(1) (4)
(2)
(3)
(2)
(3)
(4)
(4)
(1)
(4)
(1)
(1)
(5)
2 Description
The measuring sensors have two pairs of electrodes. The transmitter applies alternating current at the outer pair of electrodes. A voltage is released at the inner electrodes - subject to the conductivity of the measuring material. The transmitter acquires the voltage and uses it to calculate the electrolytic conductivity value. Functionally, excitation and measurement are kept separate. This has some advantages compared to 2-electrode measuring sensors, as the effects of polarization recede into the background. To a large extent, incoming resistances are automatically compensated. Measurement errors as a result of contamination or deposits, are reduced.
Measuring sensors
(1) Current supply, outer electrode 1 6 (2) Voltage tap, inner electrode 1 7 (3) Voltage tap, inner electrode 2 3 (4) Current supply, outer electrode 2 4 (5) Pt1000 temperature probe 1, 2 and 5
Description M12 connector pin
7

3 Instrument identification

JUMO GmbH & Co. KG
Fulda, Germany www.jumo.net
Typ: 202930/10-1005-997-83/000 VARTN: 20/00123456 F-Nr.: 01234567 01 0 0942 0002 Cell M: 0,30 1/cm

3.1 Nameplate

On the measuring sensor
The date of manufacture is encoded in "F-Nr." (serial number): 0942 means year of manufacture 2009/calendar week 42.

3.2 Type description

(1) Basic type
202930 JUMO tecLine CR-4P
(2) Basic type extension
10 Short design 20 Medium design 30 Long design
(3) Temperature compensation
1005 Pt1000
(4) Electrode material
31 Stainless steel 1.4435 (316L)
(5) Process connection
997 JUMO PEKA
(6) Electrical connection
83 M12 connector
(7) Extra codes
000 none
1
Process connection adadpters (see "Accessories") must be ordered separa­tely.
2
The CR-4P cable is required for electrical connection (see "Accessories")!
Conductive 4-electrode conductivity sensor
1
2
Order code /- ---/ Sample order 202930 / 10 - 1005 - 31 - 997 - 83 / 000
8
(1) (2) (3) (4) (5) (6) (7)

3.3 Accessories

Designation Sales No.
CR-4P cable, 5 m, made up, with M12 connector 00528699 CR-4P cable, 10 m, made up, with M12 connector 00528700
3 Instrument identification
JUMO PEKA process connection adapter for
Varivent DN 40-125 Stainless steel 1.4435/316L 00445046 Varivent DN 40-125 Stainless steel 1.4435/316L;
Clamp DN 25/32/40 Stainless steel 1.4435/316L 00445047 Clamp DN25/32/40 Stainless steel 1.4435/316L;
Clamp DN 50 Stainless steel 1.4435/316L 00445037 Clamp DN 50 Stainless steel 1.4435/316L;
Aseptic DN 40 Stainless steel 1.4435/316L 00446458 Aseptic DN 40 Stainless steel 1.4435/316L;
Aseptic DN 50 Stainless steel 1.4435/316L 00445035 Aseptic DN 50 Stainless steel 1.4435/316L;
Aseptic NKS DN 40 Stainless steel 1.4435/316L 00447555 Aseptic NKS DN 40 Stainless steel 1.4435/316L;
Material Sales No.
00577961 Ra < 0,8 µ with certificate EN 10204-3.1
00577998 Ra < 0,8 µ with certificate EN 10204-3.1
00577997 Ra < 0,8 µ with certificate EN 10204-3.1
00577995 Ra < 0,8 µ with certificate EN 10204-3.1
00577979 Ra < 0,8 µ with certificate EN 10204-3.1
00577999 Ra < 0,8 µ with certificate EN 10204-3.1
9

4 Mounting

M28x1.5
ø22.5
GL
EL
(1) (2)
(3)

4.1 General

Mounting location
Installation position
Incident flow
Find a location that ensures easy accessibility for the later calibration. The fastening must be secure and must ensure low vibration for the instrument. The operating conditions (temperature, pressure, chemical composition of the
measuring material, etc.,) must not be allowed to damage the measuring sensor. The measuring sensor must not be modified mechanically (e.g. shortened,
drilled, ground). A minimum distance of at least two meters must be maintained when
installing several JUMO tecLine CR-4P type conductivity sensors.
The conductivity sensor can be mounted in any position. But it is essential to make sure that the measuring sensor electrodes are fully immersed in the measuring material.
No incident flow is required to make the conductivity sensor work, but is recommended for fast, stable measurement values and to prevent the accumulation of deposits. Structural measures must be taken to prevent flow separation or gas bubbles in the measuring material.
Immersion length
The immersion length (EL) of the conductivity sensor must be in keeping with the installation situation.
(1) Width across flats 27 (2) JUMO PEKA process connection
A suitable process connection adapter is an essential requirement of installation, see below.
(3) 21 × 2.5 O-ring (EPDM)
10
Immersion length EL Total length GL Type
18 126 202930/10 38 146 202930/20 48 156 202930/30

4.2 JUMO PEKA process connection adapter

øD
ø68
L
18
21.5
(2)
(1)
(1)
(3)
(3)
The EHEDG-certified system for process connection – JUMO PEKA – allows it to be used in pharmaceutical and food technology without difficulty. JUMO PEKA is an adapter system that combines the measuring sensor with the process connection. All the materials are physiologically safe, and meet FDA standards.

4.3 Mounting suggestions

4 Mounting
Varivent
®
(1) JUMO PEKA process connection adapter
Varivent (2) JUMO tecLine CR-4P conductivity sensor. (3) The Varivent
is not supplied by JUMO and must be provided by the customer!
®
DN 40-125, sales no.: 00445046
®
housing DN xx
Varivent housing DN Diameter D L Type 40 38 3 202930/10 50 50 9 65 66 18 80 81 24.5 100 100 34
11
4 Mounting
21.5
ø50.5
øD1
øD
L
21.5
ø64
(2)
(1a)
(1)
(3)
(1b)
(4)
Clamp
(1) JUMO PEKA process connection adapter
(1a) Clamp DN 25/32/40, sales no.: 00445046
(1b) Clamp DN 50, sales no.: 00445037 (2) JUMO tecLine CR-4P conductivity sensor. (3) The DN xx clamp adapter, DIN 32676
is not supplied by JUMO and must be provided by the customer! (4) The clamp DN xx T-piece, DIN short, similar to DIN 11852
is not supplied by JUMO and must be provided by the customer!
Clamp adapter DN
25 32-25 32 26 5 202930/20
50 65-50 66 50 15
T-pieceDNDiamter
D
40-25 38 0 202930/30 50-25 50 7 65-25 66 15 80-25 81 20 100-25 100 30
80-50 81 20 100-50 100 30
Diamter D1
LType
12
Aseptic
øD
L
25
25
ø67
ø55
øD1
(2)
(1a)
(1)
(4)
(1b)
(3)
4 Mounting
(1) JUMO PEKA process connection adapter
(1a) Aseptic DN 40, sales no.: 00446458
(1b) Aseptic DN 50, sales no.: 00445035 (2) JUMO tecLine CR-4P conductivity sensor. (3) The DN xx threaded adapter, DIN 11864
is not supplied by JUMO and must be provided by the customer! (4) The DN xx T-piece
is not supplied by JUMO and must be provided by the customer!
Threaded adapter
40 50-40 50 38 10 202930/30
50 65-50 66 50 18
T-pieceDNDiameter
D
65-40 66 18 80-40 81 27 100-40 100 37
80-50 81 27 100-50 100 37
Diameter D1
LType
13
4 Mounting
25
øD1
øD
ø64
L
(2)
(1)
(1)
(4)
(3)
Aseptic NKS
(1) JUMO PEKA process connection adapter
Aseptic NKS DN 40, sales no.: 00447555 (2) JUMO tecLine CR-4P conductivity sensor. (3) Collar clamp adapter NKS DN 40, Form A, DIN 11864-3
is not supplied by JUMO and must be provided by the customer! (4) The DN xx T-piece
is not supplied by JUMO and must be provided by the customer!
Collar clamp adapter
NKS DN 40 Form A
T-pieceDNDiameter
D
50-40 50 38 10 202930/30 65-40 66 18 80-40 81 27 100-40 100 37
Diameter D1
LType
14

5.1 Electrical connection

ϑ
1
2
5
1
7
6
5
2
8
3
4
• Lay the input, output, and supply lines so they are physically separated
from each other and are not parallel
• If possible, use the CR-4P cable (see Accessories) to connect the
conductivity sensor; do not lay the connecting cable close to components or lines through which current is flowing
• The cables must have an uninterrupted run (do not route them via terminal
blocks or similar arrangements)
• No other consumers can be connected to the power terminals of the
instrument
• The conductivity sensor is not suitable for installation in areas with an
explosion hazard
• It is essential to comply with the electrical connection instructions in the
operating manual of the transmitter that is being used
• Apart from faulty installation, incorrect settings on the transmitter may also
affect the proper functioning of the subsequent process or lead to damage; you should therefore always provide safety equipment that is independent and it should only be possible for qualified personnel to make settings

5 Installation

5.2 Terminal assignment and wiring colors

Incorrect connection of the conductivity sensor will produce inaccurate measurement results!
Connection for M12 connector CR-4P cable
Pin Assignment Color
Pt1000 temperature probe for temperature compensation
Voltage tap inner electrode 2 3 PK Current entry outer electrode 2 4 BL Current entry outer electrode 1 6 RD Voltage tap inner electrode 1 7 GR NC Warning: The shielding of the cable has to be connected to the transmitter only – not to the
sensor!
1 2 5
GN YE BN
15
5 Installation
YE
ø7.5
GN
BN
WH
BL
GR
PK
RD

5.3 CR-4P cable

Use only the CR-4P cable for conductivity sensor connection:
• CR-4P cable, 5 m, made up, with M12 connector
Sales no.: 00528699
• CR-4P cable, 10 m, made up, with M12 connector
Sales no.: 00528700
M12 cable socket: metal, 8-pin Cable diameter: 7.5 mm Cable material: PUR, blue Ambient temperature: -30 to +80 °C Cable length: 5 m or 10 m
For metrological reasons, the maximum cable length is limited to 10 m!
16

5.4 Connection example

(1)
(2)
(3)
This example is only valid for connecting the JUMO tecLine CR­4P conductivity sensor to a JUMO AQUIS 500 CR transmitter/ controller for conductivity!
Cable routing in he transmitter
5 Installation
Run the connecting cables through the JUMO AQUIS 500 CR cable glands.Locate the measuring lead as shown in the diagram.
Fasten the measuring lead to the screen with the clip (3).
Connect the wires, as shown below.Connect the pluggable screw terminals of row 1 (1) and row 2 (2) to the
instrument slots.
17
5 Installation
ϑ
Resistance thermometer
SC = shield
Row 1
Row 2
Conductivity sensor
1
2
3
4
1
2
3
4
5
6
7
8
6
7
8
9
10
9
10
11
12
4
L1(L+)
5
6
8
9
11
12
13
15
16
17
N(L-)
11
12
13
14
15
(a)
(b)(c)
(1)
(3)
(2)
Measuring sensor connection
Terminal assignment
Ter m ina l 1 - R D Ter m ina l 2 - G R Ter m ina l 3 - P K Ter m ina l 4 - B L Ter m ina l 8 - Y E Ter m ina l 9 - G N Ter m ina l 10 - BN
Connection of JUMO dTRANS CR 02
(1) Row 1 (a) Option 1 (b) Option 2 (c) Option 3 (2) Row 2 Main input board
(conductivity/resistance/temperature/standard signal)
(3) Row 3 PSU board
(power supply/2× relays)
18

6.1 Notes

6.2 General

6 Calibration

Ageing and contamination (deposits) can cause the cell constant of the conductivity sensor to change.
The transmitter should therefore be calibrated to the connected conductivity sensor at regular intervals (subject to the measuring material and the operating conditions)!
JUMO tecLine CR-4P conductivity sensors are exactly gaged at the factory. The cell constant of every measuring sensor is documented both on the cell stem and on the calibration certificate that is also supplied.
This cell constant should be entered directly into the connected transmitter (e. g. JUMO AQUIS 500 CR).
In combination with the JUMO AQUIS 500 CR, measuring accuracy in the 20 µS/cm to 600 mS/cm range is better than 5 %. To achieve far greater measuring accuracy, calibrate the transmitter close to its later working point.
To monitor and increase the quality of measurement, the conductivity measurement chain (conductivity sensor + connecting cable + transmitter) should be regularly calibrated.
Reference solutions
It is advisable to use one of the following reference solutions for calibration:
• ASTM D 1125, reference solution B: 0.1 N KCl with 12856 µS/cm
• DIN 38404, Part 8, Section 8.3: 0.1 mol/l KCl with 12.95x10 However, any calibration solution in the medium conductivity range can also
be used.

6.3 JUMO AQUIS 500 CR settings

It is essential to comply with the JUMO AQUIS 500 CR operating instructions (B 202565.0)!
The following settings are the minimum that have to be made:
• Cell type (type of connection): 4-electrode or 4-wire
• Nominal cell constant 1.0 1/cm
• Relative cell constant as % (see sensor nameplate or
certificate)Einstellungen am JUMO dTRANS CR 02
3
µS/cm
19

7 Maintenance/troubleshooting

7.1 Cleaning the conductivity sensor

Conductive conductivity sensors are not authorized for use in highly adherent, oily or glutinous media - we recommend using our inductive conductivity measuring instruments here!
After cleaning the conductivity sensor, always rinse it with water!
The conductive conductivity sensor electrodes are in direct contact with the measurement medium. Regular cleaning must
therefore be performed, relative to the contamination susceptibility of the measuring material!
Abrasive cleaners have limited suitability! The measurement electrodes must not be damaged!
• Light contamination can be wiped off with a soft, cleansing tissue, or similar
• Wash off sticky contamination or greasy and oily contamination with a hot
rinsing agent solution and a soft cloth or soft brush; Ethanol can also be used to clean the sensor, if necessary
• Diluted hydrochloric acid (3 % by weight) can also be used to dissolve the
contamination in the event of calciferous coatings or precipitated metal hydroxides or metal oxides
• If none of the methods mentioned above remove the contamination, other
solvents, acids or caustic solutions may be used, with the aid of ultrasonic baths where required; in this case, it is necessary to ensure that the conductivity sensor components are resistant to the cleaning agents being used, see section 8 "Technical data"
20
7 Maintenance/troubleshooting

7.2 Troubleshooting

Troubleshooting must always consider all the components of the conductivity measurement chain! The transmitter and the connecting cable must also be tested, as well as the conductivity sensor.
Error Possible cause Remedy
Measurement value is too high or too low
The transmitter does not display conductivity (e.g. display shows "0")
Conductivity sensor is dirty
Broken lead or incorrect electrical connection
Clean the conductivity sensor
Check the electrical connection
Conductivity displayed by transmitter is too high or too low
The transmitter does not display temperature
Display value unstable, fluctuating
The conductivity sensor can also be tested for short-circuits or internal contact problems, see section 2 "Description", part "Measuring sensors" and section 5.2 "Terminal assignment and wiring colors". A continuity tester (such as the diode tester of a multimeter) is needed for this.
Measuring sensor exposed to air (not fully immersed)
The measuring sensor electrical connection is incorrect: poles are inverted or "right - left" assignment is incorrect
Broken lead or incorrect electrical connection
Malfunction caused by incorrectly/insufficiently shielded connecting cable
Malfunction caused by gas bubbles
Check the measuring sensor installation location.
Is measuring material present? Check the electrical connection
Check the electrical connection
Use CR-4P cables for connection
Check cable connection and cable routing
Check installation location and position of the measuring sensor
21

8 Technical data

Typical measuring range Cell constant
2
1
1 µS/cm to approx. 600 mS/cm typically, K = 0.3-0.4cm
-1
Operating temperature -10 to +120 °C, briefly +140 °C (sterilization) Maximum pressure 16 bar at 25 °C
6 bar at -10°C and +140 °C Temperature measurement With Pt1000, DIN EN 60751 Class A Electrical connection
3
M12 connector Protection IP65 Fitting length 18 mm
38 mm
48 mm (see Dimensions) Materials in contact with the
measuring medium
• Cell housing
•Electrodes
• Probe pocket
• Seal Process connection JUMO PEKA
FDA compliant
PEEK
Stainless steel 1.4435 (316L)
Stainless steel 1.4435 (316L)
EPDM (other material on request)
4
(EHEDG-certified)
Available process connection adapters:
• Varivent DN 40-125, stainless steel 1.4435 (316L)
• Clamp DN 25/32/40 and DN 50, stainless steel 1.4435 (316L)
• Aseptic DN 40 and DN 50, stainless steel 1.4435 (316L)
• Aseptic NKS DN 40, stainless steel 1.4435 (316L)
Measuring sensor installation Only possible in conjunction with JUMO PEKA process
connection adapters!
c
Surface quality (roughness) Stainless steel components ≤ 0.6 µm
Plastic components ≤ 0.8 µm
1
Measuring ranges are also dependent on the transmitter being used.
2
The measured cell constant is recorded on the stem of the conductivity sensor. A cell constant deviation can be adjusted at the transmitter.
3
The CR-4P cable is required for connection (see section 5.3 "CR-4P cable")
4
See 4.2 "JUMO PEKA process connection adapter" and data sheet 409711.
22
JUMO GmbH & Co. KG JUMO Instrument Co. Ltd. JUMO Process Control, Inc.
Street address: Moritz-Juchheim-Straße 1 36039 Fulda, Germany Delivery address: Mackenrodtstraße 14 36039 Fulda, Germany Postal address: 36035 Fulda, Germany Phone: +49 661 6003-0 Fax: +49 661 6003-607 E-mail: mail@jumo.net Internet: www.jumo.net
JUMO House Temple Bank, Riverway Harlow - Essex CM20 2DY, UK Phone: +44 1279 63 55 33 Fax: +44 1279 63 52 62 E-mail: sales@jumo.co.uk Internet: www.jumo.co.uk
6733 Myers Road East Syracuse, NY 13057, USA Phone: 315-437-5866
1-800-554-5866 Fax: 315-437-5860 E-mail: info.us@jumo.net Internet: www.jumousa.com
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