IBM 6300 User Manual

MODEL 6300

VISIBLE RANGE

SPECTROPHOTOMETER

OPERATING MANUAL

630 026

SAFETY

Please read this information carefully prior to installing or using this equipment.

1. The unit described in this manual is designed to be operated only by trained personnel. Any
adjustments, maintenance and repair must be carried out as defined in this manual, by a person
qualified to be aware of the hazards involved.

2. It is essential that both operating and service personnel employ a safe system of work, in addition
to the detailed instructions specified in this manual.

3. The covers on the unit should only be removed by personnel who have been trained to avoid the
risk of shock.

4. References should always be made to the Health and Safety data supplied with any chemicals
used. Generally accepted laboratory procedures for safe handling of chemicals should be employed.

5. If it is suspected that safety protection has been impaired in any way, the unit must be made
inoperative and secured against any intended operation. The fault condition should immediately be
reported to the appropriate servicing authority.

6300/REV B/12-96

6300 SPECTROPHOTOMETER

OPERATING MANUAL

CONTENTS

SECTION 1 INTRODUCTION

Instrument Description 1.1
Instrument Specification 1.2

SECTION 2 INSTALLATION

Unpacking 2.1
Installation 2.2
Displays 2.3
Controls 2.4
Outputs 2.5

SECTION 3 OPERATION

Initial Set-Up 3.1
Sample Measurement 3.2
Good Practice Guidelines 3.3

SECTION 4 MAINTENANCE

General 4.1
Light Source Replacement 4.2

SECTION 5 OPTIONAL ACCESSORIES

Optional Accessories 5.1
Spares 5.2

SECTION 6 INTERFACING

Analogue 6.1
RS232 6.2

6300/REV B/12-96

SECTION 1

INTRODUCTION

1.1 INSTRUMENT DESCRIPTION

The Model 6300 is a microprocessor controlled Visible Range Spectrophotometer covering the wave­length range of 320 to 950nm with a 10nm bandwidth. The monochromator is of a modified Czerny Turner
design, incorporating a stepper motor driven 1200 lines/mm holographic diffraction grating and featuring
automatic second order response suppression. The 6300 has full interfacing capability for Analogue output
and serial (RS232) interfacing. The optical system is independantly housed and isolated with lenses to give
maximum protection from environmental contamination. Combined with a mechanically rigid structure, the
6300 provides a system with fast warm-up, low drift and high reliability.

1.2 INSTRUMENT SPECIFICATIONS

Wavelength:

Range 320 - 950nm
Resolution 1nm
Accuracy ±2nm
Bandwidth 10nm

Transmittance:

Range 0 to 199.9%
Resolution 0.1%
Stray Light <0.5%
Photometric Accuracy ±2%

Absorbance:

Range -0.300 to 1.999A
Resolution 0.001A

Concentration:

Range -300 to 1999 Concentration
Resolution 0.1/1
Units ppm, mg/l-1, g/l-1, M, blank

Factor 0 to 199.9, 1000 to 9999
Photometric Noise Levels: <1%
Photometric Stability: 1%/Hr after warm-up
Readout: Custom LCD Graphics display
Outputs: Analogue (0 - 1.999V d.c.) / RS232 serial port
Light Source: Tungsten Halogen 20W 12V
Input Voltage: 115/230Vac -20% + 10%
Input Power: <50W
Size: 365 (w) x 272 (d) x 160 (h)mm
Weight: 6Kgs

1

6300/REV B/12-96

SECTION 2

INSTALLATION

2.1 UNPACKING

Remove the Model 6300 from the packaging and ensure the following items are present:

1. Model 6300 Spectrophotometer

2. Mains Cable

3. Pack 100 disposable Cuvettes (060 084)

4. Optional Accessories (as ordered)

Any shortages or damage should be reported immediately to the Manufacturer or your local
Distributor.

2.2 INSTALLATION

MAINS SUPPLY

The 6300 is designed to operate on 115/230V a.c. supplies (-20%+10%) 50/60Hz.
The standard 2 metre mains cable supplied with the unit is fitted with an IEC type connector which can be
plugged directly into the POWER IN socket on the rear panel.
The mains fuse is housed within the POWER IN socket. When replacing the fuse the unit should be
disconnected from the mains supply.
In the event of the fuse failing after replacement it is advisable to consult with the Manufacturer or your
local Distributor before proceeding further.

Fuse Rating: 2A 'F' (fast blow type)

NOTE: The unit should be positioned within 1.5 metres of an earthed mains supply.

VOLTAGE SELECT

NOTE: When changing the voltage select switch position always ensure the fuse rating

is correct.

Before attempting to change the voltage select disconnect the instrument from the mains supply. Withdraw
the fuse holder from the power input socket and remove the fuse. Extract the grey fuse retainer and rotate
so that the correct voltage is visible through the aperture in the fuse holder. Replace the fuse retainer in its
holder, fit the correct fuse and push assembly back into the power input socket.

MAINS CONNECTIONS

A suitable plug should be connected to the 3 wires on the mains lead. These are colour coded to conform
to the internationally recognised standard such that:

BROWN LIVE
BLUE NEUTRAL
GREEN/YELLOW EARTH

IMPORTANT: THE UNIT MUST BE EARTHED.

The Green/Yellow wire in the a.c. supply cable must be connected to a properly grounded terminal.

2

6300/REV B/12-96

2.3 DISPLAYS

1. Primary display area - Transmission, Absorbance, Concentration

2. Primary display adjust annunciator

3. Secondary display area - Wavelength, Factor

4. Primary display units

5. Secondary display adjust annunciator

6. Operation with PC

7. Menu options - %T ABS CONC FACTOR UNITS

8. Menu pointers (for 7)

3

6300/REV B/12-96