Hioki SM9001, SM9002 Instruction Manual

Introduction
SM9001
SURFACE/VOLUME RESISTANCE
MEASUREMENT ELECTRODE
SM9002
VERIFICATION FIXTURE FOR
SURFACE RESISTANCE MEASUREMENT
Instruction Manual
May 2019 Revised edition 3 SM9001A981-03 19-05H
EN
Protective stand
SM9001
Counter-elec­trode with inte­grated stand
SM9002 Verification Fixture for Surface Resis­tance Measure­ment (Option)
Cables
 (D2+D1) Surface resistivity: s = × (Measured value)
D2D1
D12 (Measured value)
Volume resistivity: v = × 4t 10
s : Surface resistivity (Ω)v : Volume resistivity (mm)  : Circular constant = 3.14
D1 : Diameter of the main electrode (mm) D2 : Diameter of the ring electrode (mm)
t : Thickness of sample (mm)
D2 D1
t
Ring electrode
Main electrode
Counter electrode
Object to be measured
Thank you for purchasing the HIOKI Model SM9001 Surface/Volume Resis­tance Measurement Electrode and the HIOKI Model SM9002 Verification Fix­ture for Surface Resistance Measurement . To obtain maximum performance from the device, please read this manual first, and keep it handy for future ref­erence.
Initial Inspection
When you receive the device, inspect it carefully to ensure that no damage oc­curred during shipping. If damage is evident, or if it fails to operate according to the specifications, contact your dealer or Hioki representative.
Overview
The SM9001, an electrode for measuring the surface resistance and volume re­sistance of flat samples, is an optional product designed for use with Hioki Super Megohm Meters and Digital Super Megohm Meters/Micro-ammeters. It com­plies with JIS C 2170 (IEC 61340-2-3) and is capable of reliable measurement in applications ranging from evaluation of electrostatic countermeasures to high-resistance measurement in materials development and other fields.
Safety Information
This manual contains information and warnings essential for safe operation of the device and for maintaining it in safe operating condition. Before using it, be sure to carefully read the following safety precautions.
Mishandling this device during use could result in injury or death, as well as damage to the device. Be certain that you understand the instructions and precautions in the manual before use. We disclaim any responsibility for accidents or injuries not resulting directly from device defects.
Safety Symbols
Indicates cautions and hazards. When the symbol is printed on the instru­ment, refer to a corresponding topic in the Instruction Manual.
Indicates DC (Direct Current).
The following symbols in this manual indicate the relative importance of cautions and warnings.
Indicates an imminently hazardous situation that will result in death or serious injury to the operator.
Indicates a potentially hazardous situation that may result in death or serious injury to the operator.
Indicates a potentially hazardous situation that may result in minor or moderate injury to the operator or damage to the device or malfunction.
Usage Notes
Follow these precautions to ensure safe operation and to obtain the full benefits of the various functions.
• Before using the device, make sure that the insulation on the cable is undamaged and that no bare conductors are improp­erly exposed. Using the device in such conditions could cause an electric shock, so contact your dealer or Hioki repre­sentative for repair.
• The maximum rated voltage between input terminals and ground is 1000 VDC. Attempting to measure voltages exceed­ing 450V with respect to ground could damage the device and result in personal injury.
• To avoid shock and short circuits, turn off all power before connecting the device.
• Do not allow the device to get wet, and do not take measure­ments with wet hands. This may cause an electric shock.
• Do not use the device where it may be exposed to oil, chemi­cals, or solvents. Contact with these substances may cause cracking in the device, resulting in damage or electric shock.
• Do not slant the device or place it on top of an uneven sur­face. Dropping or knocking down the device can cause injury or damage to the device.
• This device is not designed to be entirely water- or dust-proof. Do not use it in an especially dusty environment, nor where it might be splashed with liquid. This may cause damage.
• Do not store or use the device where it could be exposed to di­rect sunlight, high temperature or humidity, or condensation. Under such conditions, the device may be damaged and insu­lation may deteriorate so that it no longer meets specifications.
• To avoid damage to the device, protect it from physical shock when transporting and handling. Be especially careful to avoid physical shock from dropping.
• To prevent an electric shock accident, confirm that the white or red portion (insulation layer) inside the cable is not exposed. If a color inside the cable is exposed, do not use the cable.
Instrument Installation
Avoid the following locations that could cause an accident or damage to the device.
Exposed to direct sunlight Exposed to high tempera­ture
In the presence of corro­sive or explosive gases
Electrode struc­ture
Dimensions
Mass Approx. 2.5 kg (88.2 oz.)
Accessories
Electrodes
Option
Product warranty period
Main electrode : Floating structure
Ring electrode : Fixed to enclosure Approx. 100×223H mm (including handle and barrier)
Approx. 3.94” × 8.78”H Connection Cable length: Approx. 1 m
Instruction manual ..................................... 1
Counter-electrode with integrated stand.... 1
Dimensions: Approx. 154W×155D×25H mm
Mass: Approx. 1.2 kg (42.3 oz.)
Electrode dimensions: Approx. 100 mm×100 mm
Protective stand ......................................... 1
Carrying case (with lock) ........................... 1
Short bar .................................................... 1
Counter-electrode connection cable .......... 1
Cable length : Approx. 700 mm (27.56”)
Mass : Approx. 27.0 g (1.0 oz.)
Electrode rubber
Material: Conductive rubber
Profile : Main electrode ; 30.5 mm (D1),
Model SM9002 Verification Fixture for Surface Resistance
Temperature and humidity range during inspection
18°C to 28°C (64.4°F to 82.4°F),
60% RH or less. (non-condensing) 3 years (The electrode rubbers, which are consumables, are not covered by the warranty.)
(isolated from ring electrode)
: Ring electrode ; 57.0 mm (inner diameter)(D2),
Measurement
Measurement functionality
Reference stan­dards
Measurement items
Measurement ranges
Electrode internal resistance
Maximum rated voltage to earth
Resistance when shorted
IEC61340-2-3:2000 JIS C2170:2004
Surface resistance measurement [Rs]
The surface resistance of the sample is measured after placing
the electrode at roughly the center of the sample or at least 10
mm from the edge of the sample.
Volume resistance measurement [Rv]
The volume resistance of the sample is measured after placing
the sample on the counter-electrode with integrated stand and
then placing the electrode at roughly the center of the sample or
at least 10 mm from the edge of the sample. *Switch measurement targets by switching terminal connections.
Resistance measurement range: 1×103 to 1×1013
The minimum resistance measurement is determined by the speci­fications of DSM series and SM series Super Megohm Meters.
Between main electrode and ring electrode
1000 V DC
Between main electrode and ring electrode
: 1×10
: 1×10
14
or more
3
or less
(6.06”W × 6.10”D × 0.98”H),
Thickness: 3 mm
63.0 mm (outer diameter), Thickness: 3 mm
Indicates advisory items related to performance or correct operation of the device.
Stowing the electrode in its carrying case
Exposed to water, oil, oth­er chemicals, or solvents Exposed to high humidity or condensation
Exposed to high levels of particulate dust
Subject to vibration
Specifications
General Specifications
Operating envi­ronment Operating tem­perature and hu­midity
Storage tempera­ture and humidity
Dielectric strength
Indoors, altitude up to 2000 m (6562 feet), Pollution degree 2
0°C to 40°C (32°F to 104°F), 80%RH or less. (non-condensing)
-10°C to 50°C (14°F to 122°F), 80%RH or less. (non-condensing)
Between input terminals (together) and SM9001 enclosure: 7504 V DC, for 15 seconds
Exposed to strong electro­magnetic fields Near electromagnetic radiators
Near induction heating sys­tems. (e.g., high-frequency induction heating systems and IH cooking utensils)
Supported models Conversion to resistivity (JIS C2170:2004/ IEC 61340-2-3:2000)
Super Megohm Meter SM series, DSM series
Names of Parts
Short bar
Handle
Input cable
Output cable
Protective stand
Counter-electrode terminal
SM9001
Counter-elec­trode with inte­grated stand
Counter-electrode surface
Stand surface
Main electrode rubber
Ring electrode
rubber
Bottom of SM9001
Top of SM9001
Guard terminal
(Blue)
Common terminal (gray)
Output terminal
(Red)
Barrier
1. Connect the short bar to the surface resistance measurement [Rs] terminals
(common terminal [gray] and output terminal [red]).
2. Place the sample on the stand surface of the counter-electrode with integrat-
ed stand and gently place the SM9001 on top of the sample at least 10 mm from the edge, lowering it from directly above.
3. Verify that no voltage is being output from the Super Megohm Meter. Con-
nect the input cable to the Super Megohm Meter's input terminal and the out­put cable to the Super Megohm Meter's output terminal.
4. Operate the Super Megohm Meter to start measurement.
For more information about measurement, see the Super Megohm Meter's instruction manual.
1. Connect the short bar to the volume re-
sistance measurement [Rv] terminals (common terminal [gray] and guard ter­minal [blue]).
2. Place the sample on the counter-elec-
trode surface of the counter-electrode with integrated stand and gently place the SM9001 on top of the sample at least 10 mm from the edge, lowering it from di­rectly above so that it does not extend beyond the counter-electrode surface.
3. Connect the included counter-electrode
connection cable to the output terminal (red) and the counter-electrode terminal.
4. Verify that no voltage is being output
from the Super Megohm Meter. Connect the input cable to the Super Megohm Meter's input terminal and the output ca­ble to the Super Megohm Meter's output terminal.
5. Operate the Super Megohm Meter to
start measurement. For more information about measure­ment, see the Super Megohm Meter's in­struction manual.
3
Counter-electrode connection cable
1
4
2
High-resistance test surface Low-resistance test surface
Flip over
1. Connect the short bar to the surface resistance measurement [Rs] terminals
(common terminal [gray] and output terminal [red]).
2. Gently place the SM9001 on the SM9002's low-resistance test surface, low-
ering it from directly above.
3. Apply 10 V and read the resistance value after 15 sec.
4. Stop applying the voltage. Lift up the SM9001 and rotate the SM9002 90°.
5. Repeat steps (3) and (4) until the SM9002 has been rotated through 360°.
1. Connect the short bar to the surface resistance measurement [Rs] terminals
(common terminal [gray] and output terminal [red]).
2. Gently place the SM9001 on the SM9002's high-resistance test surface, low-
ering it from directly above.
3. Apply 100 V and verify that a stable resistance value of 1 T±5% is obtained.
• To avoid breaking the cable, do not bend or pull it.
• Avoid stepping on or pinching cables, which could damage the cable insulation.
• The cable is hardened under the 0 degree or colder environ­ment. Do not bend or pull it to avoid tearing its shield or cut­ting cable.
• Keep the cables well away from heat sources, as bare con­ductors could be exposed if the insulation melts.
• When placing the SM9001 in contact with the sample, do so gently and from directly above the sample.
• Check the surface of the electrode rubber for dirt, foreign matter, scratches, or other impediments to proper operation.
• Place the measurement target (or when measuring volume resistance, the counter-electrode) on a level surface.
• While performing measurement, avoid contact with the SM9001. Avoid sub­jecting the SM9001 to excessive force by pulling on or twisting cables.
• Do not subject the electrode rubber to twisting (friction) or mechanical shock.
• If unable to obtain stable measurement results, clean the surface of the SM9001's electrode rubber with industrial-use ethanol (use a concentration of at least 95%). If cleaning fails to yield improvement, remove the SM9001's electrode rubber and clean the entire unit with industrial-strength ethanol (use a concentration of at least 95%). For more information, see "Removing and reattaching the electrode rubber."
• To protect the electrode rubber, place the SM9001 on its protective stand when not using it to measure samples and avoid sitting it directly on the bot­tom surface. When placing the SM9001 on the protective stand, do so care­fully and avoid subjecting the stand to excessive force.
Measuring surface resistance
Maintenance and Service
• If damage is suspected, check the "Before Returning for Repair" section before contacting your dealer or Hioki representative.
• Use the original packing materials when transporting the device, if possible.
Cleaning
To clean the device, wipe it gently with a soft cloth moistened with water or mild detergent. Never use solvents such as benzene, acetone, ether, ketones, thin­ners or gasoline, as they can deform and discolor the case. Clean the electrode rubber with industrial-use ethanol (use a concentration of at least 95%).
About electrode rubber
Removing and reattaching the electrode rubber
• The electrode rubber can be removed by gripping it carefully so as not to scratch it and pulling it off.
• The electrode rubber has a top and a bottom. Check for proper orientation before reattaching it. The surface that makes contact with the measurement target is thinner, while the surface that makes contact with the metal portion of the SM9001 is thicker.
• Gently insert the electrode rubber and then fit it tightly against the metallic surface by pushing it against a level base such as the counter-electrode.
Contact your dealer or Hioki representative if:
• The electrode rubber no longer covers the adjacent metal
• The electrode rubber exhibits visible damage
• The electrode rubber is excessively dirty and efforts at cleaning prove to be ineffective
Before Returning for Repair
If abnormal operation occurs, check the following items.
Symptom Check Items Solution
Are the terminals con­nected properly?
Connect the terminals securely.
Measurement functionality
Low-resistance measurement
Resistance measurement electrodes connected to a measuring instrument are secured to the inspection fixture, and a judgment is made concerning whether the system is functioning properly. (Test voltage: 10 V DC) Verification consists of a series of repeated measurements
Measurement items
Circuit design
Maximum rated volt­age to earth
while varying the phase position of the fixture and electrodes by 90°.
High-resistance measurement
Resistance measurement electrodes connected to a measuring instrument are secured to the inspection fixture, and a judgment is made concerning whether the system is functioning properly.
(Test voltage: 100 V DC)
Low-resistance measurement
The circuit consists of contact electrodes arranged in a radial pattern at the center and ring measurement electrode positions and twenty 10 M±1% resistors placed at an even interval. The circuit forms a 500 k±1% parallel connection.
High-resistance measurement
The circuit consists of contact electrodes placed at the center and ring measurement electrode positions and one 1 TΩ±5% resistor.
100 V DC
Appearance
Using the fixture
The following describes how the fixture is used in a typical application. Custom­ers needing to perform a rigorous verification process that complies with JIS C 2170:2004 should be sure to check the actual JIS document.
Low-resistance measurement
Pre-Operation Inspection
Before using the device, check it and verify that it operates properly to make sure that it suffered no damage during storage or transportation.
Check the following before using the device.
Check Items Diagnose and Solution
Is the insulation of the cable to be used damaged, or is bare metal exposed?
Is there a break in a cable?
• Between the main electrode rubber and the input cable's inner wire
• Between the guard terminal (blue) and the input cable's outer wire
• Between the output terminal (red) and the output cable
Is the electrode's internal resistance at least
14
1×10
• Place the SM9001 in a horizontal orientation and take a measurement while the main electrode and ring electrode are not in contact with any­thing. (Applied voltage: 100 V/1 min.)
?
Measurement Procedures
When measuring insulation resistance, a dangerous voltage will be applied to the electrodes in the START, MEASURE, and CHARGE states. To avoid electric shock, do not touch the elec­trodes.
Do not use a damaged cable doing so may result in electric shock.
Have the SM9001 repaired if there is a break in a cable.
Remove dirt and other foreign matter from between the main elec­trode and ring elec­trode.
Measuring volume resistance
Connect the short bar to
The resistance value is abnormal.
Has the short bar been connected properly?
Is the electrode rubber dirty?
the proper pair of termi­nals for the type of mea­surement you intend to perform.
Clean the electrode rub­ber.
SM9002 Verification Fixture for Surface Resistance Measurement
The SM9002 Verification Fixture for Surface Resistance Measurement is a sys­tem verification fixture for use in measuring surface resistance as required by Section 8.4 of JIS C 2170:2004 (IEC 61340-2-3:2000). The SM9002 is an option designed specifically for use with the SM9001 and cannot be used for system verification of other devices.
Specifications
General Specifications
Operating environ­ment
Operating tempera­ture and humidity
Storage tempera­ture and humidity
Dielectric strength
Electrode structure
Dimensions Approx. 100×56H mm (3.94” × 2.20”H)
Mass Approx. 300 g (10.6 oz.)
Product warranty period
Indoors, altitude up to 2000 m (6562 feet), Pollution degree 2
18°C to 28°C (64.4°F to 82.4°F), 60% RH or less. (non-condensing)
-10°C to 50°C (14°F to 122°F), 80% RH or less. (non-condensing)
Between electrodes (together) and SM9002 enclosure: 1120 V DC, for 15 seconds
High-resistance : Chrome-plated metal (brass) Low-resistance : Gold-plated copper cladding formed on
PC board
3 years
If the acquired resistance values are both within 5% of 500 k, then the system is operating properly.
High-resistance measurement
• Some Super Megohm Meter models are capable of generating a terminal­to-ground voltage of 1,000 V, but the SM9002 is rated for a maximum ter­minal-to-ground voltage of 100 V.
• Check the SM9002 test surface and the SM9001 electrode rubber for dirt, foreign matter, scratches, or other impediments to proper operation.
• While performing measurement, avoid contact with the SM9001. Avoid subjecting the SM9001 to excessive force by pulling on or twisting cables.
• Due to the delicate nature of the contact with the SM9001, you may obtain out-of-range measured values even if the product is operating properly if the SM9001 has not been placed on the surface from directly above. Remove and then reposition the SM9001 if the value is out of range.
• If unable to obtain stable measurement results, clean the surface of the SM9001's electrode rubber and the SM9002 test surface with industrial­use ethanol (use a concentration of at least 95%). If cleaning fails to yield improvement, remove the SM9001's electrode rubber and clean the entire unit with industrial-strength ethanol (use a concentration of at least 95%). For more information, see "Removing and reattaching the electrode rub­ber."
• Place the SM9002 on a level surface.
• The SM9002 should be stored in a pouch inside the SM9001's included carrying case.
• Do not touch the test surface or get it dirty.
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