HF scientific MicroTSCM Streaming Current Monitor User Manual

MicroTSCM
Streaming Current Monitor
HF scientific 3170 Metro Parkway Ft. Myers, FL 33916 Phone: 239-337-2116 Fax: 239-332-7643 EMail:HFinfo@Watts.com Website: www.hfscientific.com
21648 (07/09) REV 2.4

Table of Contents

Section Page
Specifications ................................................................................................... 1
1.0 Overview........................................................................................................... 2
1.1 Unpacking and Inspection of the Instrument and Accessories ....................2
2.0 Safety................................................................................................................ 2
2.1 Symbols Used In the MicroTSCM........................................................2
3.0 Theory of Operation........................................................................................ 3
3.1 Treatment of Water for Clarification..................................................... 4
3.2 Charge Analysis ....................................................................................5
4.0 Installation and Commissioning ................................................................... 6
4.1 Sample Point ........................................................................................ 6
4.2 Flow Rate .............................................................................................. 6
4.3 Sensor Mounting & Plumbing .............................................................. 7
4.4 Analyzer Mounting................................................................................ 8
4.5 Electrical Connections .......................................................................... 9
4.5.1 Power ........................................................................................ 9
4.5.2 Outputs – Voltage & Current .................................................. 9
4.5.3 Alarm Contacts........................................................................ 10
5.0 Operation ...................................................................................................... 11
5.1 The Sensor/Sampler ...........................................................................11
5.2 The Analyzer ....................................................................................... 11
5.3 The Graphing Screen........................................................................... 12
5.4 Menus ................................................................................................. 13
6.0 Calibration .................................................................................................... 14
6.1 Calibration Procedures ....................................................................... 14
6.2 EEPROM Programming Correction ................................................... 14
7.0 Automatic Control......................................................................................... 15
7.1 Optimization of Treatment Process..................................................... 15
7.2 PI Control Overview ........................................................................... 15
7.3 PI Control Procedure........................................................................... 16
7.3.1 Process Band Calculation........................................................ 16
7.3.2 Entering the Control Parameters ............................................ 17
7.3.3 Manual Control ....................................................................... 17
21648 (07/09) REV 2.4
Table of Contents (continued)
Section Page
8.0 Additional Features and Options ................................................................ 18
8.1 Sensor Gain Switch ............................................................................. 18
8.2 Remote Panel Meter ............................................................................ 18
8.3 Optional Flow Switch.......................................................................... 18
9.0 Routine Maintenance.................................................................................... 19
9.1 Preferred Method – Chemical Cleaning.............................................. 19
9.2 Manual Cleaning ................................................................................. 19
9.3 Analyzer Fuse ..................................................................................... 20
10.0 Troubleshooting............................................................................................. 21
10.1 Diagnostic Chart ................................................................................. 21
10.2 Technical & Customer Assistance ......................................................21
11.0 Accessories and Replacement Parts List .................................................... 22
12.0 Definitions ..................................................................................................... 23
13.0 Warranty........................................................................................................ 24
MICROTSCM (07/09) REV 2.4

Specifications

Measurement Range Accuracy Repeatability Linearity Resolution Response Time Analyzer Display Alarms Analog Output Communications Port Flow Rate Flow Alarm Operating Temperature Storage Temperature Wetted Materials
± 10.0 SCU or ICu
±1 % of Full Scale
1%
±1%
0.01 SCU or ICu
1 second
Backlit Graphical LCD with trending
Two Programmable, One Sensor, 120-240VAC 2A Form C Relay
Powered 4-20 mA, 1000 Ω drive
Optional RS-232 or RS-485
6.0 – 9.5.0 L/min. (1.5 -2.5 gpm)
Optional Float Switch
0°C – 50°C (32°F – 122°F)
-20°C – 60°C (-4°F – 140°F)
HDPE, PTFE, Stainless Steel, Neoprene, ABS
Standard Cable Length Max. Sensor to Analyzer Power Source SCM Sensor Case Analyzer Regulatory
Compliance And Certifications
Shipping Weight
Shipping Dimensions
Warranty
7.62m (25 feet)
76.25 m (250 feet) Consult factory for lengths over 50 feet
120 or 240 VAC, 50/ 60 Hz, 40VA
Designed to meet IP 66 /NEMA 4X
CE Approved, ETL listed to UL 3111-1 &
ETL Certified to CSA 22.2 No. 1010-1-92
Instrument: 9.5 kg (21 lbs.)
Calibration kit: 5.5 kg (12 lbs.)
Instrument: 61 cm X 46 cm X 35cm (24“ X 18 “ X 14”)
Calibration kit: 41cm X 41 cm X 38 cm (16” X 16” X 15”)
1 Year from date of shipment
MICROTSCM (07/09) Page 1 REV 2.4

1.0 Overview

The SCM–Streaming Current Monitor allows for optimizing and control of dosing coagulants used for clarification of water. Although the analyzer is capable of displaying the units in either SCU’s or ICu, this manual will always refer to SCU.
1.1 Unpacking and Inspection of the Instrument and Accessories
The table below indicates the items in the shipment.
Item Quantity
MicroTSCM Analyzer 1
SCM Sensor 1
Sample Chamber 1
Calibration Kit 1
Instruction Manual 1
Remove the instrument from the packing carton. Carefully inspect all items to ensure that no visible damage has occurred during shipment. If the items received do not match the order, please immediately contact the local distributor or the HF scientific Customer Service Department.

2.0 Safety

This manual contains basic instructions that must be followed during the commissioning, operation, care and maintenance of the instrument. The safety protection provided by this
equipment may be impaired if it is commissioned and/or used in a manner not described in this manual. Consequently, all responsible personnel must read this manual prior to
working with this instrument.
In certain instances “Notes”, or helpful hints, have been highlighted to give further
clarification to the instructions. Refer to the Table of Contents to easily find specific topics and to learn about unfamiliar terms.
2.1 Symbols Used In the MicroTSCM
Standard IEC symbols are used on the high voltage cover.
ISO 3864, No. B.3.6 Caution, risk of electric shock.
cover
This symbol indicates that hazardous voltages may be present under this
ISO 3864, No.B3.1 Caution refers to accompanying documents. This symbol is a reminder to read the sections in the manual referring to the electrical connections, and potential hazards.
MICROTSCM (07/09) Page 2 REV 2.4

3.0 Theory of Operation

In a liquid form, water molecules move around each other at a fast rate. One affect of this fast movement is the ability to suspend matter. This phenomenon is called “Brownian Motion”. It occurs when microscopic particles are maintained dispersed in suspension due to their random bombardment by the fast movement of water molecules. Typical particles found in raw water entering WTP have finely divided clay particles and organic matter collectively called silt.
A second phenomenon which stabilizes the suspension is the surface charge of the suspended matter. When a salt such as sodium chloride is place in water, complete dissolution occurs. This system reaches a stable energy level when the individual sodium and chloride ions (Na+ and Cl-) are separated in the water phase by being surrounded by water molecules.
In the case of large pseudo salts, e.g. Aluminosilicates (clay), only partial dissolution takes place due to incomplete breakdown of the crystal to individual ions. The structure of these clays is similar to silica or sand except that random silicon atoms in the crystal are replaced by aluminum atoms in the cage structure, causing the clay to swell and crack between adjacent aluminum atoms in the crystal. Thus a clay particle is formed with a size of less than 1 micron with a negative charge. This particle is small enough to be maintained in suspension by Brownian Motion. The particles in the suspension repel each other due to their surface charge, preventing them from coming together and agglomerating, or flocking to form a larger particle, which would settle out. The result is an energetically stable system and is the reason why the particles remain dispersed.
The counter ions (say sodium for the sake of argument) are separated from the large cage structure because they are dissolved in the water. Clay particles have a negative charge associated with it, while the counter ions, typically cat-ions (or positively charged ions) are dispersed in the water phase.
In the case of most naturally occurring substances, the larger ion, when in suspension, has a negative net charge (anionic). The smaller, counter ion is positive (cationic). The residual charge of the larger particles is negative, which causes them to repel each other, preventing them from forming agglomerates. The size of the particles never becomes large enough to settle out, so they remain dispersed in suspension.
This phenomenon creates an energetically stable system. In order to cause the suspended particles to agglomerate and settle out, the energy of the system must be upset. There are numerous mechanical means to accomplish this, but the addition of chemical flocking agents to the suspension, drastically reduces the time and is far more efficient.
Chemical additives perform two functions, charge neutralization & bridging. Both of these techniques allow the small particles to floc and grow sufficiently that Brownian motion can no longer support them. Due to the high density of the particle, flocs will form and settle as fine sludge.
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Additive Chemicals
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Contaminant Particles
1. Charge Neutralization 2. Bridging
Figure 1: Effects of Chemicals

3.1 Treatment of Water for Clarification

Most water treatment chemicals consist of a cationic (positively charged) chemical e.g. aluminum salts, ferric salts, polyamines or cationic polyacrylamides, some of which have the cationic part tagged on to a long polymer chain. As stated earlier, raw water entering the WTP is an energetically stable system of suspended particles with a net negative charge. Cationic chemicals are added to bring the charge to neutral.
Before the development of Streaming Current technology, the best way to determine the optimum dosage has been the jar test method. The jar test involves taking a representative sample of the water being treated and placing it in several jars. Different amounts of clarifying chemicals are added to each jar; stirred and comparing the clarity of the water in the different jars. Jar tests are time consuming and it is difficult to reproduce the conditions of the WTP in a jar. The tests can take several hours rendering them useless when plant personnel are really responding to rapid changes in water quality. A typical curve of Turbidity vs. Chemical dosage is shown in Figure 3. Some considerations when treating the water are the rate of floc formation, the size of the floc formed, how fast the floc settles, and the clarity of the final settled and filtered water.
Other techniques exist, such as a dosing curve, which indicates a recommended dosage for a given water turbidity. This is generally built up over years of dosing experience with the water, but has the disadvantage that turbidity caused by extremely small particles requires a higher dosage than that caused by larger particles, and therefore can only be adapted for use with known type turbidity on any given water.
MICROTSCM (07/09) Page 4 REV 2.4
TURBIDITY
CHEMICAL DOSAGE ppm
Figure 3: Turbidity vs Dosage

3.2 Charge Analysis

Charge analysis is the measurement of the electro kinetic charge of a solution due to the presence of charged particles. The electro kinetic charge can be measured by a number of different methods.
1. Applied electric field
Measurement: The relative mobility of the solid or liquid phase.
This is the first method developed for calculating the Zeta Potential. The motion of charged particles under the influence of an electric field was observed and the potential required to achieve a certain amount of particle mobility was measured.
A cell consisting of two flat plates separated by approximately 0.1 mm and having an electrode at each end of the cell is filled with water containing suspended matter. When an electrical potential is applied to the electrodes, the particles can be observed to drift toward one of the electrodes. The Zeta Potential is calculated from the measured speed of particle drift.
2. Induced Electrical Potential
Measurement: The potential developed as the result of forced movement of particles in the solution. This is the method used by the MicroTSCM. Continuous sample water is directed into an annulus, inside which a displacement piston oscillates vertically at a fixed frequency. This action causes the liquid to move between the two stainless steel electrodes. The suspended particles are absorbed onto the walls under the action of Van der Waal’s and electrostatic forces. As the sample is moved rapidly back and forth, mobile counter ions surrounding the colloids are sheared near the surface of the walls and moved past the electrodes. The resultant A.C. signal or Streaming Current, proportional to charge density, is electronically processed and displayed.
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