HF scientific Micro1000 User Manual

OWNER’S MANUAL
HF scientific– Micro 1000 Laboratory
Turbidimeter 0-10,000 NTU
HF scientific
3170 Metro Parkway Ft. Myers, FL 33916 Phone: (239) 337-2116 Fax: (239) 332-7643 Toll free: 888-203-7248 Email: HF info@Watts.com
Website: www.hfscientific.com
Catalog No. 22615 (1/11) Rev 3.2

DECLARATION OF CONFORMITY

Application of Council Directive: 73/23/EEC
Standard to which Conformity is Declared:
Product Safety Immunity & EMI UL3101-1 EN61326-1: 2006 CSA-C22.2 No. 1010-1-92 EN61010-1: 1993 + A2: 1995
Manufacture’s Name: HF scientific, inc.
Manufacture’s Address: 3170 Metro Parkway, Fort Myers, Florida 33916-7597
Importer’s Name:
Importer’s Address:
Type of Equipment: Laboratory Turbidimeter
Model No.: Micro 1000 Catalog Numbers: 20014 Micro 1000 IR 20016
I, the undersigned, hereby declare that the equipment specified above conforms to the above Directive and Standard.
Place: Fort Myers, Florida USA (Signature)
Rowan T. Connelly, General Manager
Rev. 3.2 i
1. SPECIFICATIONS..........................................................................................................................1
2. Overview..........................................................................................................................................2
2.1. Unpacking and Inspection of the Instrument and Accessories................................................................................2
2.2. User Interface..............................................................................................................................................................3
3. Safety ...............................................................................................................................................4
4. Routine Operation............................................................................................................................5
4.1. Measurement Principle & Methodology...................................................................................................................5
4.2. Grab Sample Measurement (Routine Measurement).............................................................................................. 6
4.3. Pour Through Sample Measurement (Optional Accessory)....................................................................................7
4.4. Flow Through Sample Measurement (Optional Accessory)....................................................................................7
4.5. Dry Air Purge System.................................................................................................................................................8
4.6. Using the Security Access Feature (Good Manufacturing Practice [GMP])..........................................................8
5. Calibration Procedures.....................................................................................................................8
5.1. Calibration Standards.................................................................................................................................................9
5.2. Indexing the Calibration Standard(s)........................................................................................................................9
5.3. Calibrating the Instrument.......................................................................................................................................10
6. Instrument Configuration (SETUP) Mode.....................................................................................13
6.1. Setting the Scale.........................................................................................................................................................13
6.2. Setting the Ratio Mode..............................................................................................................................................13
6.3. Selecting Display Resolution.....................................................................................................................................14
6.4. Configuring the Security Code.................................................................................................................................14
6.5. Setting up the RS232 Port (Printing Function).......................................................................................................15
6.6. Setting the Calibration Interval...............................................................................................................................16
6.7. Setting the Date (Year, Month and Day).................................................................................................................17
6.8. Setting the Time (Hours and Minutes)....................................................................................................................18
6.9. Exiting the setup mode..............................................................................................................................................18
7. Troubleshooting .............................................................................................................................20
7.1. System Warning Message(s).....................................................................................................................................20
7.2. System Error Message(s)..........................................................................................................................................23
7.3. Factory Default Parameters.....................................................................................................................................23
8. Routine Maintenance .....................................................................................................................23
8.1. Cuvette Cleaning and Care......................................................................................................................................24
8.2. Lamp Replacement ...................................................................................................................................................24
9. Contacting the HF scientific, inc. Technical Service Department.................................................25
Rev. 3.2 ii
10. Accessories and Replacement Parts List........................................................................................25
11. Glossary .........................................................................................................................................26
12. Warranty ........................................................................................................................................27
Rev. 3.2 iii
1.

SPECIFICATIONS

MICRO 1000 MICRO 1000IR
Instrument Conformance
Light Source Tungsten Filament Lamp Infrared LED Measurement Options and Ranges
NTU FNU EBC NEPHELO FAU Signal Averaging Yes Yes Auto Ranging Yes Yes Accuracy † 0 – 1000 NTU 1000 – 4000 NTU 4000 – 10,000 NTU Repeatability ± 1% of reading or ± 0.01 NTU
Resolution 0.0001 NTU below 10 NTU 0.0001 NTU below 10 NTU Response Time Less than 6 seconds Less than 6 seconds Serial Input/Output RS-232 Directional RS-232 Directional
Certifications CE, ETL (UL & CSA ) CE, ETL (UL & CSA) Power Supply 15 V DC Wall Mount 15 V DC Wall Mount Display Backlit Multi-Line LCD Backlit Multi-Line LCD Miscellaneous Specifications Operating Temperature Range Sample Flow Rate Through The Flow Cell Air Purge 0.1 SCFM at 10 PSIG 0.1 SCFM at 10 PSIG Shipping Dimensions 12” x 14” x 12”
Shipping Weight 7 lb (3.18 kg) 7 lb (3.18 kg) Warranty 1 - Year 1 - Year
§ The specifications found in EPA method 180.1 are essentially the same as the specifications set out in method
2130B of the Standard Methods for the Examination of Water and Wastewater 19th edition and the specifications set out in ASTM Standard Method D1889-94. This turbidimeter meets, or exceeds, the specifications set forth in these methods.
Instrumental accuracy measured under controlled laboratory conditions at 25°C (77°F)
Conforms to specifications set forth in EPA method 180.1 (Nephelometric Method)
Ratio on or Ratio off
0 – 10,000
-------­0 - 2,450 0 – 67,000
--------
± 2% of reading + 0.01 NTU ± 5% of Reading ± 10% of Reading
whichever is greater
1 - Built in Diagnostics 2 - Security Access Code 0° C – 50° C (32 ° F - 122° F) 0° C – 50° C (32 ° F - 122° F)
0.5 – 1.5 gpm (2-6 L/min) 60 psi max pressure (414 kPa)
(35.6cm x 30.5cm x 30.5cm)
§
Conforms to specifications set forth in ISO 7027: Water Quality –Determination of Turbidity
Ratio on or Ratio off
0 – 10,000 0 – 10,000 0 – 2,450
-------­0 – 10,000
± 2% of reading + 0.01 NTU ± 5% of Reading ± 10% of Reading ± 1% of reading or ± 0.01 NTU whichever is greater
1- Built in Diagnostics 2- Security Access Code
0.5 – 1.5 gpm (2-6 L/min) 60 psi max pressure (414 kPa)
12” x 14” x 12” (35.6cm x 30.5cm x 30.5cm)
Rev. 3.2 1

2. Overview

The Micro 1000 process turbidimeter allows you to measure the turbidity of your process water. The White Light Micro 1000 has been designed to meet the design criteria specified by the US EPA on turbidity measurement. The Infra-Red Micro 1000 (Micro 1000 IR) was designed to meet the design criteria specified in ISO 7027 and DIN 27027 for the measurement of the turbidity of a sample.

2.1.Unpacking and Inspection of the Instrument and Accessories

The table below indicates the items that you should find in your turbidimeter shipment.
Remove the Calibration Kit (Cardboard box), the Package of 3 Cuvettes and the instrument from the packing carton. Carefully inspect all items to ensure that no visible damage has occurred during shipment. If the items you received do not match your order, please contact your local distributor or the HF scientific, inc. Customer Service department immediately.
ITEM Quantity
Laboratory Turbidimeter 1
Calibration Kit for the MICRO 1000 1
3 Pack of Cuvettes 1
MICRO 1000 Instruction Manual 1
Power Supply 1
Note: Extra care should be taken when unpacking, opening, and handling the calibration standards
and sample cuvettes in the Accessory Kit; surface scratches or finger smudges on the cuvette surface may cause measurement errors. Handle these items by the top area of the cuvette only.
Rev. 3.2 2

2.2.User Interface

The user interface of the instrument is designed with a 6 key touch pad and a single user display. The six keys of the touch pad and their functionality are described below. Figures 1a and 1b are depictions of the front and rear views of the instrument.
Optical Well
Display
Lamp Module
Touch Pad
Figure 1a - Front view of the Instrument
Optical Well
Lamp Module
15VDC
Air Purge In
RS-232
Air Purge Out
Figure 1b – Rear view of the Instrument
Rev. 3.2 3
The ON/OFF key ( ) key is used to turn the instrument ON or OFF. The enter key ( ) is used to accept information. The up and down arrow keys (SandT) are used to set and reset numerical values and to change instrument modes. The left and right arrow keys (◄and►) are used to scroll through lists. In addition, the rear panel of the instrument is designed to provide ready access to the power plug connector, the RS-232 serial port and the dry air purge connector.
Figure 2 illustrates all the items that can appear on the display. The upper row of the display (1) is used for reporting the turbidity levels and to provide user guidance in the customer setting routine. The lower row of the display (2) is used to communicate error messages and user guidance. The display has several status indicators (3) that distinguish the operation of the instrument. In addition there are several indicators that display the different scales (4) that the instrument will report. Other indicators (5) provide guidance when the setup and calibration routines are being used.

3. Safety

This manual contains basic instructions that you must follow during the commissioning, operation, care and maintenance of the instrument. The safety protection provided by this equipment may be impaired if it is commissioned and/or used in a manner not described in this manual. Consequently, all responsible personnel must read this manual prior to working with this instrument.
Figure 2 – Display used in the instrument. All items that
are used on the display are shown in this figure
The instrument has a time-out feature that automatically returns the system operation to the normal operation mode from any other mode after a five (5) minute period of inactivity.
Ensure that the instrument has been turned off prior to removing power from the instrument.
In certain instances WARNINGS, Notes, or helpful hints, have been highlighted to give further
clarification to the instructions. Refer to the Table of Contents to easily find specific topics and to learn about unfamiliar terms.
Rev. 3.2 4
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