Hanna Instruments HI 99171 User Manual

Instruction Manual
HI 99171
Portable Waterproof
Leather & Paper pH Meter
www.hannainst.com
WARRANTY
All Hanna Instruments meters are warranted for two years against defects in workmanship
and materials when used for their intended pur­pose and maintained according to instructions.
The probes are warranted for a period of six months.
This warranty is limited to repair or replacement free of charge. Damage due to accidents, misuse, tampering or lack of prescribed maintenance are not covered.
If service is required, contact the dealer from whom you purchased the instrument. If under warranty, report the model number, date of pur­chase, serial number and the nature of the prob­lem. If the repair is not covered by the warranty, you will be notified of the charges incurred. If the instrument is to be returned to Hanna Instruments, first obtain a Returned Goods Authorization Num­ber from the Customer Service department and then send it with shipment costs prepaid. When shipping any instrument, make sure it is properly packaged for complete protection.
All rights are reserved. Reproduction in whole or in part is prohibited without the written consent of the copyright owner.
Dear Customer, Thank you for choosing a Hanna Instruments Product. Please read this instruction manual carefully before using the instrument. If you need additional technical information, do not hesitate to e-mail us at
tech@hannainst.com
This instrument is in compliance with the directives.
PRELIMINARY EXAMINATION
Remove the instrument from the packing ma­terial and examine it carefully to make sure that no damage has occurred during ship­ment. If noticeable damage is evident, notify your dealer.
Note: Save all packing material until you
are sure that the instrument func­tions correctly. All defective items must be returned in the original pack­ing together with the supplied ac­cessories.
GENERAL DESCRIPTION SPECIFICATIONS
HI 99171 is a portable and waterproof pH
meter supplied with the HI 1414D probe, specifically designed with a flat tip sensor for direct pH measurement on surfaces, such as leather and paper.
Moreover, a built-in temperature sensor al­lows simultaneous pH and temperature readings and a mini amplifier renders mea­surements impervious to noise and electri­cal interferences.
The meter is supplied in a rugged carrying case, complete with:
HI 1414D pH/temperature probe
HI 70004 pH 4.01 buffer, 20 mL sachet
HI 70007 pH 7.01 buffer, 20 mL sachet
HI 700680 cleaning solution for cellulose
deposits, 20 mL sachet (2 pcs.)
HI 70960 sample preparation solution, 30
mL dropper bottle
batteries and instructions
LCD DESCRIPTION
1. Automatic Temperature Compensation indicator
2. Stability indicator
3. Battery percentage
4. pH calibration indicator
5. Low battery indicator
6. Selectable temperature unit
7. Secondary display
8. Primary display
9. Measuring unit for primary display
Range -2.00 to 16.00 pH
-5.0 to 105.0°C / 23.0 to 221.0°F
Resolution 0.01 pH / 0.1°C / 0.1°F Accuracy ±0.02 pH
(@20°C/68°F) ±0.5°C up to 60°C; ±1°C outside
±1°F up to 140°F; ±2°F outside
Typical EMC ±0.02 pH Deviation ±0.2°C or ±0.4°F
Temp. Compensation Automatic pH Calibration Automatic, 1 or 2 point
with 2 sets of standardized buffers
(4.01/7.01/10.01 or 4.01/6.86/9.18)
Probe
(included) HI 1414D
amplified pH/temperature probe
Battery Type 3 x 1.5V AA / IEC LR6 Battery Life Approx. 1500 hours Auto-off After 8 minutes of non-use Environment 0 to 50°C; RH 100% Dimensions150 x 80 x 36 mm (5.9 x 3.2 x 1.4”) Weight 210 g (7.4 oz.)
ACCESSORIES
HI 1414D Combination amplified flat-tip
pH electrode with built-in tem­perature sensor, DIN connec­tor and 1 m (3.3') cable
HI 70004P pH 4.01 buffer solution, 20 mL
sachet (25 pcs.)
HI 7004L pH 4.01 buffer solution, 500 mL
bottle
HI 70006P pH 6.86 buffer solution, 20 mL
sachet (25 pcs.)
HI 7006L pH 6.86 buffer solution, 500 mL
bottle
HI 70007P pH 7.01 buffer solution, 20 mL
sachet (25 pcs.)
HI 7007L pH 7.01 buffer solution, 500 mL
bottle
HI 70300M Storage solution, 230 mL bottle HI 70300L Storage solution, 500 mL bottle HI 7061M General purpose cleaning so-
lution, 230 mL bottle
HI 7061L General purpose cleaning so-
lution, 500 mL bottle
HI 70632M Cleaning & disinfection sol. for
blood products, 230 mL bottle
HI 70632L Cleaning & disinfection sol. for
blood products, 500 mL bottle
HI 700680P Cleaning sol. for cellulose de-
posits, 20 mL sachet (25 pcs.)
HI 70680M Cleaning solution for cellulose
deposits, 230 mL bottle
HI 70680L Cleaning solution for cellulose
deposits, 500 mL bottle
HI 70960 Electrolyte solution for sample
preparation, 30 mL bottle
HI 710007 Blue shockproof rubber boot HI 710008 Orange shockproof rubber boot HI 721312 Hard carrying case
Hanna Instruments reserves the right to
modify the design, construction and appear-
ance of its products without advance notice.
IST99171R1 05/05
OPERATIONAL GUIDE
To connect the probe
With the meter turned off, connect the HI 1414D probe to the DIN socket on the top of the meter by aligning the pins and pushing in the plug. Tighten the nut to ensure a good connection. Remove the protective cap from the probe before taking any measurements.
To turn the meter ON and check the battery status
Press the ON/OFF/MODE button until the display lights up. At start-up, all the LCD segments are displayed for 1 second, then the percent indica­tion of the remaining battery life is shown for an­other second (E.g. % 100 BATT). The meter then enters the normal measuring mode.
Note: If the display needs to be checked, keep the
ON button pressed while turning the meter on. The meter will display all segments as long as the button is pressed.
To freeze the display
While in measurement mode, press the SET/ HOLD button, HOLD appears on the secondary display and the reading will be frozen on the LCD (E.g. pH 5.73 HOLD). Press any button to return to normal mode.
To turn the meter OFF
While in normal measurement mode, press the ON/OFF/MODE button. OFF will appear on the secondary display. Release the button.
Note: The meter is provided with an acoustic sig-
nal feature, which can be disabled using the switch located in the battery compartment.
Note: When the meter detects the absence of a
temperature probe at its input, the Automatic Temperature Compensation is turned off, and the meter uses a default value of 25°C (77°F) for the temperature measurement and com­pensation. In this condition, the secondary LCD shows 25.0°C (77.0°F) blinking. When a probe is connected, the meter automatically returns to the ATC mode, the A TC t ag is turned on, and the temperature is shown on the secondary display.
Note: To clean the meter, do not use aggressive
detergents. It is recommended to use water.
pH MEASUREMENT & CALIBRATION
• Make sure the meter has been calibrated be­fore use.
• If the probe is dry, soak it in HI 70300 storage solution for one hour to reactivate it.
• Place the tip of the probe on the sample to be tested and wait until the symbol on the top left of the LCD is turned off.
• The LCD shows the pH value (automatically compensated for temperature) on the primary LCD, while the secondary LCD shows the tem­perature of the solution.
• After each measurement, it is recommended to perform a complete cleaning of the probe: use the suitable Cleaning solutions (see "Ac­cessories" section) and clean the probe tip thoroughly to eliminate dirtiness and avoid cross-contamination.
• When not in use, switch the meter OFF and clean the probe with the specific Cleaning so- lutions (see "Accessories" section) before stor­ing it.
pH calibration
For better accuracy, frequent calibration of the instrument is recommended. In addition, the instrument must be recalibrated whenever:
a) The pH electrode is replaced. b) After testing aggressive chemicals. c) Where high accuracy is required. d) At least once a month.
• From normal mode, press and hold the ON/ OFF/MODE button until OFF on the secondary display is replaced by CAL. Release the but­ton.
• The LCD enters the calibration mode, display­ing “pH 7.01 USE” (or “pH 6.86 USE” if the NIST buffer set was selected). After 1 second the meter activates the automatic buffer recog­nition feature. If a valid buffer is detected, then its value is shown on the primary display, and REC appears on the secondary LCD. If no valid buffer is detected, the meter keeps the USE indication active for 12 seconds, and then re­places it with WRNG , indicating that the sample being measured is not a valid buffer.
• For a
Note: It is always recommended to carry out a
• For a
Note: When the calibration procedure is com-
single-point calibration
4.01, 9.18 or 10.01, the meter automatically accepts the calibration when the reading is stable; the meter will show on the primary dis­play the accepted buffer , with the message “OK 1” on the secondary display, and an audible signal is produced. After 1 second the meter automatically returns to the normal measur­ing mode. If a single-point calibration with buffers pH 7.01 or 6.86 is desired, then after the calibration point has been accepted the ON/OFF/MODE button must be pressed in order to return to the nor­mal measuring mode. After the button is pressed, the meter shows "7.01" (or "6.86") ­"OK 1", and an audible signal is produced. Af­ter 1 second, the meter automatically returns to the normal measuring mode.
two-point calibration for better accuracy.
two-point calibration
pH 7.01 (or pH 6.86) buffer . After the calibration point has been accepted, the “pH 4.01 USE” message appears. The message is held for 12 seconds, unless a valid buffer is recog­nized. If no valid buffer is recognized, then the WRNG message is shown. If a valid buffer (pH
4.01, pH 10.01 or pH 9.18) is detected, then the meter completes the calibration procedure. When the buffer is accepted, the LCD shows the accepted value with the “OK 2” message on the secondary display. The meter then re­turns to the normal measuring mode.
pleted, the CAL tag is turned on.
with buffers pH
, place the probe in
To quit calibration and to reset to the de­fault values
• After entering the calibration mode and before the first point is accepted, it is possible to quit the procedure and return to the last calibration data by pressing the ON/OFF/MODE button. The secondary LCD displays ESC for 1 sec­ond and the meter returns to normal mode.
• T o reset to the default values and clear a previ­ous calibration, press the SET/HOLD button after entering the calibration mode and before the first point is accepted.
The secondary LCD displays CLR for 1 sec­ond, the meter resets to the default calibration and the “CAL” tag on the LCD disappears.
METER SETUP
Setup mode allows the selection of the tempera­ture unit and of the pH buffer set. T o enter the Setup mode, press and hold the ON/ OFF/MODE button until CAL on the secondary display is replaced by TEMP and the current tem­perature unit (E.g. TEMP °C). Then:
for °C/°F selection
After the temperature unit has been selected, press ON/OFF/MODE to enter the buffer set selection mode; press ON/OFF/MODE twice to return to the normal measuring mode.
to change the calibration buffer set
ting the temperature unit, the meter will show the current buffer set: “pH 7.01 BUFF” (for 4.01/
7.01/10.01) or “pH 6.86 BUFF” (for 4.01/6.86/
9.18). Change the set with the SET/HOLD but­ton, then press ON/OFF/MODE to return to nor­mal mode.
, use the SET/HOLD button.
, after set-
BATTERY REPLACEMENT
The meter displays the remaining battery per­centage when turned on. When the level is below 5%, the  symbol on the bottom left of the LCD blinks to indicate a low battery condition. If the battery level is low enough to cause erroneous readings, the Battery Error Prevention System (BEPS) turns the meter off. Unscrew the 4 screws located on the back of the meter and carefully replace the 3 AA bat­teries located in the battery compartment, while paying attention to their polarity. Reat­tach the back making sure that the gasket is in place and tighten the 4 screws to ensure a watertight seal.
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