Instruction Manual
HI 99171
Portable Waterproof
Leather & Paper pH Meter
www.hannainst.com
WARRANTY
All Hanna Instruments meters are warranted
for two years against defects in workmanship
and materials when used for their intended purpose and maintained according to instructions.
The probes are warranted for a period of
six months.
This warranty is limited to repair or replacement
free of charge. Damage due to accidents, misuse,
tampering or lack of prescribed maintenance are
not covered.
If service is required, contact the dealer from
whom you purchased the instrument. If under
warranty, report the model number, date of purchase, serial number and the nature of the problem. If the repair is not covered by the warranty,
you will be notified of the charges incurred. If the
instrument is to be returned to Hanna Instruments,
first obtain a Returned Goods Authorization Number from the Customer Service department and
then send it with shipment costs prepaid. When
shipping any instrument, make sure it is properly
packaged for complete protection.
All rights are reserved. Reproduction in whole or in
part is prohibited without the written consent of the
copyright owner.
Dear Customer,
Thank you for choosing a Hanna Instruments
Product.
Please read this instruction manual carefully
before using the instrument.
If you need additional technical information,
do not hesitate to e-mail us at
tech@hannainst.com
This instrument is in compliance with the
directives.
PRELIMINARY EXAMINATION
Remove the instrument from the packing material and examine it carefully to make sure
that no damage has occurred during shipment. If noticeable damage is evident, notify
your dealer.
Note: Save all packing material until you
are sure that the instrument functions correctly. All defective items
must be returned in the original packing together with the supplied accessories.
GENERAL DESCRIPTION SPECIFICATIONS
HI 99171 is a portable and waterproof pH
meter supplied with the HI 1414D probe,
specifically designed with a flat tip sensor
for direct pH measurement on surfaces,
such as leather and paper.
Moreover, a built-in temperature sensor allows simultaneous pH and temperature
readings and a mini amplifier renders measurements impervious to noise and electrical interferences.
The meter is supplied in a rugged carrying
case, complete with:
• HI 1414D pH/temperature probe
• HI 70004 pH 4.01 buffer, 20 mL sachet
• HI 70007 pH 7.01 buffer, 20 mL sachet
• HI 700680 cleaning solution for cellulose
deposits, 20 mL sachet (2 pcs.)
• HI 70960 sample preparation solution, 30
mL dropper bottle
• batteries and instructions
LCD DESCRIPTION
1. Automatic Temperature Compensation
indicator
2. Stability indicator
3. Battery percentage
4. pH calibration indicator
5. Low battery indicator
6. Selectable temperature unit
7. Secondary display
8. Primary display
9. Measuring unit for primary display
Range -2.00 to 16.00 pH
-5.0 to 105.0°C / 23.0 to 221.0°F
Resolution 0.01 pH / 0.1°C / 0.1°F
Accuracy ±0.02 pH
(@20°C/68°F) ±0.5°C up to 60°C; ±1°C outside
±1°F up to 140°F; ±2°F outside
Typical EMC ±0.02 pH
Deviation ±0.2°C or ±0.4°F
Temp. Compensation Automatic
pH Calibration Automatic, 1 or 2 point
with 2 sets of standardized buffers
(4.01/7.01/10.01 or 4.01/6.86/9.18)
Probe
(included) HI 1414D
amplified pH/temperature probe
Battery Type 3 x 1.5V AA / IEC LR6
Battery Life Approx. 1500 hours
Auto-off After 8 minutes of non-use
Environment 0 to 50°C; RH 100%
Dimensions150 x 80 x 36 mm (5.9 x 3.2 x 1.4”)
Weight 210 g (7.4 oz.)
ACCESSORIES
HI 1414D Combination amplified flat-tip
pH electrode with built-in temperature sensor, DIN connector and 1 m (3.3') cable
HI 70004P pH 4.01 buffer solution, 20 mL
sachet (25 pcs.)
HI 7004L pH 4.01 buffer solution, 500 mL
bottle
HI 70006P pH 6.86 buffer solution, 20 mL
sachet (25 pcs.)
HI 7006L pH 6.86 buffer solution, 500 mL
bottle
HI 70007P pH 7.01 buffer solution, 20 mL
sachet (25 pcs.)
HI 7007L pH 7.01 buffer solution, 500 mL
bottle
HI 70300M Storage solution, 230 mL bottle
HI 70300L Storage solution, 500 mL bottle
HI 7061M General purpose cleaning so-
lution, 230 mL bottle
HI 7061L General purpose cleaning so-
lution, 500 mL bottle
HI 70632M Cleaning & disinfection sol. for
blood products, 230 mL bottle
HI 70632L Cleaning & disinfection sol. for
blood products, 500 mL bottle
HI 700680P Cleaning sol. for cellulose de-
posits, 20 mL sachet (25 pcs.)
HI 70680M Cleaning solution for cellulose
deposits, 230 mL bottle
HI 70680L Cleaning solution for cellulose
deposits, 500 mL bottle
HI 70960 Electrolyte solution for sample
preparation, 30 mL bottle
HI 710007 Blue shockproof rubber boot
HI 710008 Orange shockproof rubber boot
HI 721312 Hard carrying case
Hanna Instruments reserves the right to
modify the design, construction and appear-
ance of its products without advance notice.
IST99171R1 05/05
OPERATIONAL GUIDE
To connect the probe
With the meter turned off, connect the HI 1414D
probe to the DIN socket on the top of the meter by
aligning the pins and pushing in the plug. Tighten
the nut to ensure a good connection. Remove
the protective cap from the probe before taking
any measurements.
To turn the meter ON and check the battery
status
Press the ON/OFF/MODE button until the display
lights up. At start-up, all the LCD segments are
displayed for 1 second, then the percent indication of the remaining battery life is shown for another second (E.g. % 100 BATT). The meter then
enters the normal measuring mode.
Note: If the display needs to be checked, keep the
ON button pressed while turning the meter on.
The meter will display all segments as long as
the button is pressed.
To freeze the display
While in measurement mode, press the SET/
HOLD button, HOLD appears on the secondary
display and the reading will be frozen on the LCD
(E.g. pH 5.73 HOLD). Press any button to return
to normal mode.
To turn the meter OFF
While in normal measurement mode, press the
ON/OFF/MODE button. OFF will appear on the
secondary display. Release the button.
Note: The meter is provided with an acoustic sig-
nal feature, which can be disabled using the
switch located in the battery compartment.
Note: When the meter detects the absence of a
temperature probe at its input, the Automatic
Temperature Compensation is turned off, and
the meter uses a default value of 25°C (77°F)
for the temperature measurement and compensation. In this condition, the secondary LCD
shows 25.0°C (77.0°F) blinking. When a probe
is connected, the meter automatically returns
to the ATC mode, the A TC t ag is turned on, and
the temperature is shown on the secondary
display.
Note: To clean the meter, do not use aggressive
detergents. It is recommended to use water.
pH MEASUREMENT & CALIBRATION
• Make sure the meter has been calibrated before use.
• If the probe is dry, soak it in HI 70300 storage
solution for one hour to reactivate it.
• Place the tip of the probe on the sample to be
tested and wait until the symbol on the top
left of the LCD is turned off.
• The LCD shows the pH value (automatically
compensated for temperature) on the primary
LCD, while the secondary LCD shows the temperature of the solution.
• After each measurement, it is recommended
to perform a complete cleaning of the probe:
use the suitable Cleaning solutions (see "Accessories" section) and clean the probe tip
thoroughly to eliminate dirtiness and avoid
cross-contamination.
• When not in use, switch the meter OFF and
clean the probe with the specific Cleaning so-
lutions (see "Accessories" section) before storing it.
pH calibration
For better accuracy, frequent calibration of the
instrument is recommended. In addition, the
instrument must be recalibrated whenever:
a) The pH electrode is replaced.
b) After testing aggressive chemicals.
c) Where high accuracy is required.
d) At least once a month.
• From normal mode, press and hold the ON/
OFF/MODE button until OFF on the secondary
display is replaced by CAL. Release the button.
• The LCD enters the calibration mode, displaying “pH 7.01 USE” (or “pH 6.86 USE” if the
NIST buffer set was selected). After 1 second
the meter activates the automatic buffer recognition feature. If a valid buffer is detected, then
its value is shown on the primary display, and
REC appears on the secondary LCD. If no valid
buffer is detected, the meter keeps the USE
indication active for 12 seconds, and then replaces it with WRNG , indicating that the sample
being measured is not a valid buffer.
• For a
Note: It is always recommended to carry out a
• For a
Note: When the calibration procedure is com-
single-point calibration
4.01, 9.18 or 10.01, the meter automatically
accepts the calibration when the reading is
stable; the meter will show on the primary display the accepted buffer , with the message “OK
1” on the secondary display, and an audible
signal is produced. After 1 second the meter
automatically returns to the normal measuring mode.
If a single-point calibration with buffers pH 7.01
or 6.86 is desired, then after the calibration point
has been accepted the ON/OFF/MODE button
must be pressed in order to return to the normal measuring mode. After the button is
pressed, the meter shows "7.01" (or "6.86") "OK 1", and an audible signal is produced. After 1 second, the meter automatically returns
to the normal measuring mode.
two-point calibration for better accuracy.
two-point calibration
pH 7.01 (or pH 6.86) buffer . After the calibration
point has been accepted, the “pH 4.01 USE”
message appears. The message is held for
12 seconds, unless a valid buffer is recognized. If no valid buffer is recognized, then the
WRNG message is shown. If a valid buffer (pH
4.01, pH 10.01 or pH 9.18) is detected, then
the meter completes the calibration procedure.
When the buffer is accepted, the LCD shows
the accepted value with the “OK 2” message
on the secondary display. The meter then returns to the normal measuring mode.
pleted, the CAL tag is turned on.
with buffers pH
, place the probe in
To quit calibration and to reset to the default values
• After entering the calibration mode and before
the first point is accepted, it is possible to quit
the procedure and return to the last calibration
data by pressing the ON/OFF/MODE button.
The secondary LCD displays ESC for 1 second and the meter returns to normal mode.
• T o reset to the default values and clear a previous calibration, press the SET/HOLD button
after entering the calibration mode and before
the first point is accepted.
The secondary LCD displays CLR for 1 second, the meter resets to the default calibration
and the “CAL” tag on the LCD disappears.
METER SETUP
Setup mode allows the selection of the temperature unit and of the pH buffer set.
T o enter the Setup mode, press and hold the ON/
OFF/MODE button until CAL on the secondary
display is replaced by TEMP and the current temperature unit (E.g. TEMP °C). Then:
•
for °C/°F selection
After the temperature unit has been selected,
press ON/OFF/MODE to enter the buffer set
selection mode; press ON/OFF/MODE twice
to return to the normal measuring mode.
•
to change the calibration buffer set
ting the temperature unit, the meter will show
the current buffer set: “pH 7.01 BUFF” (for 4.01/
7.01/10.01) or “pH 6.86 BUFF” (for 4.01/6.86/
9.18). Change the set with the SET/HOLD button, then press ON/OFF/MODE to return to normal mode.
, use the SET/HOLD button.
, after set-
BATTERY REPLACEMENT
The meter displays the remaining battery percentage when turned on. When the level is
below 5%, the symbol on the bottom left
of the LCD blinks to indicate a low battery
condition. If the battery level is low enough to
cause erroneous readings, the Battery Error
Prevention System (BEPS) turns the meter
off.
Unscrew the 4 screws located on the back of
the meter and carefully replace the 3 AA batteries located in the battery compartment,
while paying attention to their polarity. Reattach the back making sure that the gasket is
in place and tighten the 4 screws to ensure a
watertight seal.