Hanna Instruments HI 991404-01 User Manual
Instruction Manual
(HI 991404 - HI 991405)
www.hannainst.com
WARRANTY
HI 991404 and HI 991405 are warranted for two years against
defects in workmanship and materials when used for their intended purpose
and maintained according to instructions. The probes are warranted for
six months. This warranty is limited to repair or replacement free of charge.
Damages due to accident, misuse, tampering or lack of prescribed maintenance are not covered.
If service is required, contact the dealer from whom you purchased the instrument. If under warranty, report the model number, date of purchase, serial
number and the nature of the failure. If the repair is not covered by the
warranty, you will be notified of the charges incurred. If the instrument is to be
returned to Hanna Instruments, first obtain a Returned Goods Authorization
Number from the Customer Service department and then send it with shipment costs prepaid. When shipping any instrument, make sure it is properly
packaged for complete protection.
All rights are reserved. Reproduction in whole or in part is prohibited without the written consent of the copyright owner.
Dear Customer,
Thank you for choosing a Hanna product.
This manual will provide you with the necessary information
for a correct operation.
If you need additional technical information, do not hesitate
to e-mail us at tech@hannainst.com.
These instruments are in compliance with the directives.
PRELIMINARY EXAMINATION
Remove the instrument from the packing material and examine it carefully. If any damage has occurred during shipment,
notify your dealer or the nearest Hanna Service Center.
The meters are supplied with:
• HI 1293D pH electrode and HI 7630 fixed EC probe
• pH 4.01 and 7.01 buffer solutions (20 mL each)
• 1413 µS/cm calibration solution (20 mL), for HI 991404
• 12.88 mS/cm calibration solution (20 mL), for HI 991405
• 12 Vdc power adapter and instructions
Note: Conserve all packing material until the instrument has
been observed to function correctly. Any defective item
must be returned in its original packing.
GENERAL DESCRIPTION
HI 991404 and HI 991405 have been designed for continuous, high accuracy pH, EC/TDS and temperature measurements.
These indicators continuously monitor the three most important nutrient parameters in hydroponics, greenhouses and
horticultural applications with a single instrument.
These micro-processor based meters feature a large, dual level,
backlit LCD to give instantaneous readings of pH, EC or TDS
and temperature, even from a distance.
Calibration and temperature compensation are automatic,
while the TDS conversion factor and temperature coefficient are
user adjustable for application-specific measurements.
The HI 1293D advanced, non-clogging double-junction pH
electrode and the rugged conductivity probe will withstand
even the most aggressive environments.
The instruments are powered by a 12 Vdc transformer and
are easy to install and use.
FUNCTIONAL DESCRIPTION SPECIFICATIONS
Range
0.0 to 14.0 pH / 0.0 to 60.0°C / 32.0 to 122.0°F
0 to 3999 µS/cm / 0 to 2000 ppm (HI 991404)
0.00 to 20.00 mS/cm / 0.00 to 10.00 ppt (HI 991405)
Resolution 0.1 pH / 0.1°C / 0.1°F
1 µS/cm / 1 ppm (HI 991404)
0.01 mS/cm / 0.01 ppt (HI 991405)
Accuracy (@20ºC/68ºF)
±0.1 pH / ±0.5°C / ±1°F / ±2% FS for EC/TDS
Typical EMC Deviation
±0.1 pH / ±1°C / ±2°F / ±2.5 FS for EC/TDS
Temperature Compensation
with β adjustable from 0.0 to 2.4%/ºC for EC/TDS
TDS Factor Adjustable form 0.45 to 1.00 (CONV)
Probes HI 1293D pH electrode (included)
HI 7630 conductivity probe (fixed)
pH Calibration Automatic, 1 or 2 point
with auto-buffer recognition
EC/TDS Calibration Automatic, 1 point
Power Supply 12 Vdc power adapter (included)
Environment 0 to 50ºC (32 to 122ºF);
RH max 95% non-condensing
Dimensions / Weight
160 x 105 x 31 mm (6.2x4.1x1.2’’) / 190 g (6.7 oz.)
1. Liquid Crystal Display
2. ON/OFF/MODE button
3. Power supply connector
4. 12 VDC power adapter
5. HI 1293D pH-electrode with differential input, pipe
thread 1/2’’ NPT
6. EC/TDS/Temperature probe, pipe thread 1/2’’ NPT
(works also as matching pin for pH-electrode)
7. DIN connector
8. SET/HOLD button
Recommendations for Users
Before using this product, make sure that it is entirely suitable for the
environment in which it is used.
Operation of this instrument in residential areas could cause unacceptable
interferences to radio and TV equipment.
The glass bulb at the end of the electrode is sensitive to electrostatic discharges. Avoid touching this glass bulb at all times. During operation, ESD wrist
straps should be worn to avoid possible damage to the electrode by electrostatic discharges.
Any variation introduced by the user to the supplied equipment may degrade
the instrument’s EMC performance.
To avoid electrical shock, do not use this instrument when voltages at the
measurement surface exceed 24 Vac or 60 Vdc.
To avoid damages or burns, do not perform any measurement in microwave
ovens.
Automatic,
Hanna Instruments reserves the right to modify the design, construction and
appearance of its products without advance notice.
IST991404R2 07/05
OPERATIONAL GUIDE CALIBRATION
Preliminary operations
Connect the pH electrode to the meter.
Connect the 12 Vdc adapter to the meter and to the mains;
the display will lit. Press and hold the MODE button for 2-3
seconds. All the used segments on the LCD will be visible for a
few seconds.
To change the temperature unit
To change the temperature unit (from °C to °F), from
measurement mode, press and hold the MODE button until
“TEMP” and the current temperature unit are displayed on
the lower LCD (E.g. TEMP °C).
Use the SET/HOLD button to change the temperature unit,
and then press MODE button twice to return to normal
measurement mode.
To freeze the display
Press and hold the SET/HOLD button for 2-3 seconds, until
“HOLD” appears on the secondary display.
Press either button to return to normal mode.
Taking measurements
Select the pH, EC or TDS mode with the SET/HOLD button.
Immerse the probes in the solution to
be tested. In order to ensure better
accuracy, probes should not touch or
stand close to the walls or bottom of
the sample vessel.
The pH, EC or TDS value automatically
compensated for temperature is shown
on the primary LCD while the secondary LCD shows the temperature of the
sample.
Measurements should be taken when the stability symbol on
the top left of the LCD disappears.
IMPORTANT NOTE
Measurements have to be taken with both pH electrode and conductivity/temperature probe (also
working as matching pin) immersed in the same
vessel.
To change the TDS conversion factor (CONV) and the
temperature compensation coefficient β (BETA)
• From measurement mode, press and hold the MODE
button until “TEMP” and the current temperature unit are
displayed on the lower LCD (E.g. TEMP °C).
• Press the MODE button again to show the current conversion factor (E.g. 0.50 CONV).
• Use the SET/HOLD button to change the conversion factor.
• Press the MODE button to show the current temperature
coefficient (E.g. 2.1 BETA).
• Use the SET/HOLD button to change the value.
• Press MODE to return to normal measuring mode.
To turn the meter off
Press the MODE button while in normal measurement mode.
“OFF” will appear on the lower part of the display. Release
the button. The display still lits, until the power supply is
connected.
Notes:
• Before taking any measurement make sure the meter has
been calibrated.
• To clear a previous calibration, press the MODE button
after entering the calibration mode. The lower LCD will
display “ESC” for 1 second and the meter will return to
normal measurement mode. The “CAL” symbol on the LCD
will disappear. The meter will be reset to the default
calibration.
• If measurements are taken in different samples successively,
rinse the probes thoroughly to eliminate cross-contamination; and after cleaning, rinse the probes with some of the
sample to be measured.
pH ELECTRODE MAINTENANCE
• When not in use, rinse the electrode with water and store
it with a few drops of HI 70300 storage solution in the
protective cap.
NEVER USE DISTILLED OR DEIONIZED WATER FOR STORAGE
PURPOSES.
• If the electrode has been left dry, soak in a storage or pH
7 solution for at least one hour to reactivate it.
• To prolong the life of the pH electrode, it is recommended
to clean it monthly by immersing it in the HI 7061
cleaning solution for half an hour. Afterwards, rinse it
thoroughly with tap water and recalibrate the meter.
pH calibration buffer set
• From pH measurement mode, press and hold the MODE
button until “TEMP” and the current temperature unit are
displayed on the lower LCD (E.g. TEMP °C).
• Press the MODE button again to show the current buffer
set: “pH 7.01 BUFF” for standard set (for pH 4.01/7.01/
10.01) or “pH 6.86 BUFF” for NIST buffer (pH 4.01/
6.86/9.18).
• Press the SET/HOLD button to change the buffer value.
• Press MODE to return to normal measuring mode.
pH calibration procedure
From pH measurement mode, press and hold the MODE
button until “CAL” is displayed on the lower LCD. Release the
button. The LCD will display “pH 7.01 USE” (or “pH 6.86
USE” if you have selected the NIST buffer set). The CAL tag
blinks on the LCD.
• For a single-point pH calibration, place the electrode and
the probe in any buffer from the selected buffer set (e.g.
pH 7.01, pH 4.01 or pH 10.01). The meter will recognize
the buffer value automatically.
If using pH 4.01 or pH 10.01, the meter will display “OK”
for 1 second and then return to measurement mode.
If using pH 7.01, after recognition of the buffer the meter
will ask for pH 4.01 as second calibration point. Press the
MODE button to return to measurement mode or, if
desired, proceed with the 2 point calibration as explained
below.
Note: For better accuracy it is always recommended to carry
out a two-point calibration.
• For a two-point pH calibration, place the electrode and
the probe in pH 7.01 (or 6.86 if you have selected the
NIST buffer set). The meter will recognize the buffer value
and then display pH 4.01 USE.
Rinse the electrode thoroughly and immerse it in the
second buffer solution (pH 4.01 or 10.01, or, if using
NIST, pH 4.01 or 9.18). When the second buffer is
recognized, the LCD will display “OK” for 1 second and the
meter will return to normal measurement mode.
Note: For storing calibration data in the non-volatile memory,
turn the meter OFF and then ON again through the
MODE button.
The CAL symbol on the LCD means that the meter is calibrated.
EC calibration procedure
• From EC measurement mode, press and hold the MODE
button until “CAL” is displayed on the lower LCD.
• Release the button and immerse the probe in the proper
calibration solution: HI 70031 (1413 µS/cm) for HI 991404
and HI 70030 (12.88 mS/cm) for HI 991405.
• Once the calibration has been automatically performed,
the LCD will display “OK” for 1 second and the meter will
return to normal measurement mode.
• Since there is a known relationship between EC and
TDS readings, it is not necessary to calibrate the TDS
range.
Note: For storing calibration data in the non-volatile memory,
turn the meter OFF and then ON again through the
MODE button.
The CAL symbol on the LCD means that the meter is calibrated.
ACCESSORIES
HI 1293D Spare pH electrode with differential input & DIN
HI 7630 (*) Conductivity probe with built-in temperature sen-
sor (also working as matching pin)
HI 7004M pH 4.01 solution, 230 mL bottle
HI 7006M pH 6.86 solution, 230 mL bottle
HI 7007M pH 7.01 solution, 230 mL bottle
HI 7009M pH 9.18 solution, 230 mL bottle
HI 7010M pH 10.01 solution, 230 mL bottle
HI 7030M 12.88 mS/cm solution, 230 mL bottle
HI 7031M 1413 µS/cm solution, 230 mL bottle
HI 7032M 1382 ppm solution, 230 mL bottle
HI 7038M 6.44 ppt solution, 230 mL bottle
HI 70442M 1500 ppm solution, 230 mL bottle
HI 7061M Electrode cleaning solution, 230 mL bottle
HI 70300M Electrode storage solution, 230 mL bottle
HI 710005 115 Vac/12 Vdc power adapter, US plug
HI 710006 230 Vac/12 Vdc power adapter, European plug
(*) To be replaced by authorized technical personnel only.
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