Hanna Instruments HI 933301 Instruction Manual

Page 1
Instruction Manual
HI933300 HI933301
Portable Microprocessor
Printing and Logging
Multi-Range
Conductivity Meters
http://www.hannainst.com
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ISO 9000 Certified Company since 1992
Dear Customer, Thank you for choosing a Hanna Instruments Product. Please read this instruction manual carefully before using the instrument. This manual will provide you with all the neces­sary information for the correct use of the instrument, as well as a precise idea of its versatility in a wide range of applications. These instruments are in compliance with directives EN 50081-1 and 50082-1.
TABLE OF CONTENTS
Preliminary Examination............................. 1
General Description ................................... 1
LCD Display Functional Description .......... 3
Functional Description HI 76302W
Conductivity Probe ..................................... 3
Functional Description HI 933300 .............. 4
Functional Description HI 933301 .............. 5
Specifications ............................................. 6
Operational Guide ...................................... 7
Conductivity Calibration............................ 18
Conductivity Versus Temperature Chart.. 26
Temperature Calibration........................... 27
Printing/Recording with HI933301............ 30
Printing/Logging with HI933300 ............... 33
Data Transfer to PC................................. 42
Fault Functions......................................... 44
Memory Organization (HI933300)............ 45
Printer Maintenance ................................. 46
Probe Maintenance .................................. 48
Battery Replacement................................ 49
Accessories.............................................. 50
Warranty................................................... 52
CE Declaration of Conforminty ................ 53
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GENERAL DESCRIPTION
The HI933300 and HI933301 are multirange conductivity meters equipped with printer and datalogger (HI933300 only).
The measurement interval is user-selectable from 1 to 180 minutes, and the temperature coefficient β can vary from 0.0 to 3.0%/°C.
These microprocessor-based meters provide automatic calibration with 5 memorized val­ues:
0 µS/cm (µmhoS/cm)
84 µS/cm (µmhoS/cm)
1413 µS/cm (µmhoS/cm)
12880 µS/cm (µmhoS/cm)
80000 µS/cm (µmhoS/cm).
This makes the calibration procedure ex­tremely simple.
HI933300 can also log and directly print the conductivity and temperature measurements.
PRELIMINARY EXAMINATION
Remove the instrument from the packing ma­terial and examine it to make sure that no damage has occurred during shipping. If there is any damage, notify your Dealer.
Each printing/logging conductivity meter is sup­plied complete with:
• HI 76302W Conductivity Probe with 1 m (3.3') screened cable
AA size Alkaline Batteries (4 pcs)
• Paper roll (10 pcs)
Rugged carrying case
Note: Save all packing materials until you are
sure that the instrument functions cor­rectly. All defective items must be re­turned in the original packaging together with the supplied accessories.
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2
The stored data can be retrieved at a later time for printing or can be transferred to a computer through an optional HI9200 infrared transmitter. The HI933300 will transfer the data in seconds through the infrared lights with no need for a cable between the trans­mitter and the meter.
The internal software allocates memory space to store up to 8,000 readings.
The meters provide automatic temperature compensation with the supplied HI76302W 4-ring probe with integrated temperature sen­sor. The sensors in the meter's probe utilize the latest technology in conductivity mea­surement.
The four-ring potentiometric method incorpo­rated into the probe has been proven to pro­vide higher accuracy than the more common amperometric method.
HI933300 and HI933301 have a range of 0 to 199900 µS/cm and can be used in any sample from deionized water to brine.
The probe's stainless steel rings have a large surface for better response and ease of clean­ing.
The meters are equipped with an automatic shut-off system and a 12VDC socket for maxi­mum versatility in both laboratory and field use.
Other features include: on-board time and date, calibration factors stored in Eprom, au­tomatic low battery alert system.
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LCD DISPLAY FUNCTIONAL DESCRIPTION
1
2
LO BAT
mS
LOG
INTV
1. Primary Display
2. Secondary Display
FUNCTIONAL DESCRIPTION HI 76302W
CONDUCTIVITY PROBE
2
1
3
4
1. Watertight Shielded Screened Cable
2. Air-Release Holes
3. PVC Protective Sleeve
4. 4 Stainless Steel Rings.
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4
FUNCTIONAL DESCRIPTION HI 933300
2
MICROPROCESSOR LOGGING CONDUCTIVITY METER
PRINT
PAPER
ALT
CAL
CFM
RANGE
TIME
LOG
3
4 5
6 7
9 8
10
11
HI 933300
1
mS
LOG
1. Power adapter plug
2. Conductivity probe socket
3. LCD display
4. PAPER key, to pull the paper and to reset the printer
5. PRINT key, to obtain a printout
6. ALT key, Alternate Function key
7. RANGE key, to display the conductivity or the temperature
8. LOG key, to enter the logging mode
9. TIME key, to display present time and printing interval
10. CFM key, to confirm calibration data
11. CAL key, to enter or exit the calibration mode.
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FUNCTIONAL DESCRIPTION HI 933301
2
MICROPROCESSOR PRINTING CONDUCTIVITY METER
ON/OFF
PAPER
ALT
CAL
CFM
RANGE
PRINT
RECORD
3
4 5
6 7
9 8
10
11
HI 933301
1
mS
LOG
1. Power adapter plug
2. Conductivity probe socket
3. LCD display
4. PAPER key, to pull the paper and to reset the printer
5. ON/OFF key, to turn the meter on or off
6. ALT key, Alternate Function key
7. RANGE key, to display the conductivity or the temperature
8. RECORD key, to enter the recording mode
9. PRINT key, to obtain a printout
10. CFM key, to confirm calibration data
11. CAL key, to enter or exit the calibration mode.
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SPECIFICATIONS
HI 933300 & HI933301
0.0 to 150.0
150 to 1500
1.50 to 15.00
15.0 to 199.9
0.0 to 60.0
0.1 µS/cm, 1 µS/cm
0.01 mS/cm, 0.1 mS/cm, 0.1°C ±1% full scale; ±0.5°C
excluding probe error
±1% F.S
±0.5°C
Automatic 1, 2, 3, 4 or 5 points at 0, 84, 1413, 12880, 80000 µS/cm
Automatic from 0 to 60 °C (32 to 140°F) with variable ß from 0.0 to 3.0%
HI76302W (included) detach- able with 4 stainless steel AISI 316 rings and incorporated tem­perature sensor. Probe length is 120mm (4.8"), diameter is 20mm (0.8"); screened cable length is 1 meter (3.3')
Low-power impact type-belt, 14 characters per line using 38 mm plain paper
Selectable from 1, 2, 5, 10, 15, 30, 60, 120, 180 minutes
4 x 1.5 volt AA size.
500 hours with 60' printing
interval. Power socket for
12VDC adapter
0 to 50°C (32 to 122°F), 95 %RH
196 x 80 x 57 mm
(7.7 x 3.1x 2.2")
425 g (15 oz.) instrument only
Measurement Range µS/cm
µS/cm mS/cm mS/cm
°C
Resolution
Accuracy (@20°C/68°F)
Typical EMC Deviation
Calibration
Temperature Compensation
Probe
Printer
Printing/Logging interval
Battery Type
Life
Environment
Dimensions
Weight
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OPERATIONAL GUIDE
INITIAL PREPARATION
Each meter is supplied com­plete with batteries. Remove the back cover, unwrap the batteries and install them while paying attention to their po­larity.
To prepare the instrument for use, connect the probe to the meter securely by aligning the pins with the socket located on the top of the instrument, pushing the plug in and tight­ening the threaded ring.
Make sure that the sleeve is properly inserted on the probe, with the holes towards the top of the probe (the end nearest to the cable).
To turn the HI933300 on, press the RANGE key.
To turn the HI933301 on, press the ON/OFF key.
The meter will display the clock time as 0:00 and a default sampling interval of 1 minute.
-
-
+
+
1.5V
1.5V
-
-
+
+
1.5V
1.5V
SCREW
POTS
RANGE
ON/OFF
TIME
INTV
7
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8
ON/OFF
RANGE
TIME
ALT
RANGE
CAL
TIME
DATE
DATE
To maximize battery life, the display is auto­matically switched off after 5 minutes of non­use.
The meter continues to moni­tor (if in the logging or record­ing mode) conductivity and temperature even when the display is off.
To revive the display, press either the ON/OFF or the RANGE key.
SETTING DATE/TIME/PRINTING INTERVAL (for HI933300 only)
Press the ALT and the TIME keys simulta­neously. The display will show the date set­ting. At the bottom of the display the year will start blinking.
Use the UP or DOWN arrow key to select the year.
When the correct year is selected, press the TIME key once. The month will start blinking.
CAL CFM
or
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9
Select the month by using the UP or DOWN arrow key.
Press the TIME key. The day will start blink­ing.
Use the UP or DOWN arrow key to select the correct day.
Press the ALT and the TIME keys simulta­neously. The display will now show the time and the printing interval will start blinking.
The interval can be selected from 1, 2, 5, 10, 15, 30, 60, 120 or 180 minutes by using the UP and DOWN arrow keys.
TIME
ALT
RANGE
CAL
TIME
INTV
CAL CFM
or
TIME
DATE
CAL CFM
or
CAL CFM
or
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Once the desired interval is selected press the TIME key once to set it. The hour will start blinking.
To select the hour press the UP or DOWN arrow key (24 hour clock).
Press the TIME key once. The minutes will start blinking.
Use the UP or DOWN arrow key to select the minute.
Press the ALT and the TIME keys to leave this mode.
The meter's time, date and interval are now set and stored in the memory even when the display is switched off.
TIME
CAL CFM
or
TIME
TIME
INTV
TIME
INTV
CAL CFM
or
TIME
ALT
RANGE
CAL
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VIEWING TIME / DATE / CONDUCTIVITY / TEMPERATURE (for HI933300 only)
To view the time press the TIME key. This also displays the selected interval time.
To view the date, press the UP arrow key when the LCD is displaying the time.
To view the conductivity and temperature press the RANGE key. Conductivity will be dis­played on the primary display and tempera­ture on the secondary (without decimal point).
To view the temperature press the RANGE key again. The temperature will be displayed on the primary display with a decimal point.
TIME
DATE
CAL
TIME
INTV
RANGE
mS
RANGE
°C
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SETTING DATE/TIME/PRINTING INTERVAL (for HI933301 only)
Press the ALT and the RANGE keys twice simultaneously. The display will show the date setting. At the bottom of the display the year will start blinking.
Use the UP or DOWN arrow key to select the year.
When the correct year is selected, press the TIME key once. The month will start blinking.
Select the month by using the UP or DOWN arrow key.
Press the RANGE key. The day will start blinking.
DATE
CAL CFM
or
ALT
RANGE
RANGE
DATE
RANGE
DATE
CAL CFM
or
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Use the UP or DOWN arrow key to select the correct day.
Press the ALT and the RANGE keys simulta­neously. The display will now show the time and the printing interval will start blinking.
The interval can be selected from 1, 2, 5, 10, 15, 30, 60, 120 or 180 minutes by using the UP and DOWN arrow keys.
Once the desired interval is selected press the RANGE key once to set it. The hour will start blinking.
To select the hour press the UP or DOWN arrow key (24 hour clock).
CAL CFM
or
ALT
RANGE
TIME
INTV
CAL CFM
or
RANGE
TIME
INTV
CAL CFM
or
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Press the RANGE key once. The minutes will start blinking.
Use the UP or DOWN arrow key to select the minute.
Press the ALT and the RANGE keys simulta­neously to leave this mode.
The meter's time, date and interval are now set and stored in memory even when the display is switched off.
VIEWING TIME / DATE / CONDUCTIVITY / TEMPERATURE (for HI933301 only)
To view the time press the ALT and RANGE keys simultaneously. This also displays the selected interval time.
RANGE
CAL CFM
or
TIME
INTV
ALT
RANGE
TIME
INTV
ALT
RANGE
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To view the date, press the UP arrow key when the LCD is displaying the time.
To view the conductivity and temperature press the RANGE key. Conductivity will be dis­played on the primary display and tempera­ture on the secondary (without decimal point).
To view the temperature press the RANGE key again. The temperature will be displayed on the primary display with a decimal point.
SETTING THE TEMPERATURE COEFFICIENT
Press the RANGE key until the display shows the temperature coefficient setting.
This value is adjustable from 0.0 to 3.0%/°C.
DATE
CAL
RANGE
mS
RANGE
°C
RANGE
%
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Use the UP and the DOWN arrow key to change the setting.
TAKING CONDUCTIVITY MEASUREMENTS
Make sure that the meter has been cali­brated before taking any measurements (see page 18).
To take a measurement, place the probe into the solution with the holes completely sub­merged. Tap and stir the probe to remove all air bubbles that may be trapped inside the PVC sleeve.
HI933300 and HI933301 are auto-ranging conductivity meters, and the reading automatically switches from one resolution to the next, from pure water @
0.1µS/cm up to 199900µS/cm. If the LCD displays four
dashes, the meter is out of range.
HI76302W conductivity probe has a built-in temperature sensor and automatically com­pensates for any temperature variation.
Wait for a few minutes for the temperature sensor to attain thermal equilibrium with the test solution before taking the measurement.
If the temperature of the conductivity probe and the solution is of considerable difference, a longer time should be allowed before taking readings.
CAL CFM
or
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mS
Once the reading stabilizes the measurement is complete.
If further measurements are desired, rinse the probe with tap water and test the next sample.
Note: The probe body and sleeve are made
of PVC and are very susceptible to damage due to temperatures exceed­ing 50°C (122°F).
If the probe is exposed to high tem­perature, the bond between the rings and the probe body may become im­paired and the probe will not function properly, in which case it has to be replaced.
TAKING TEMPERATURE MEASUREMENTS
Taking temperature measurement with HI933300 and HI933301 is very easy.
Press the RANGE key until the display shows the °C mode.
Simply immerse the probe into the sample and allow the reading to stabilize.
AFTER MEASUREMENTS
When all measurements are completed fol­low the probe maintenance procedure de­scribed at page 48.
RANGE
°C
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CONDUCTIVITY CALIBRATION
It is recommended that HI933300 and HI933301 are calibrated frequently for great-
est accuracy, especially when used often or in samples with widely differing conductivity values. For best results choose conductivity solutions that are closest in value to the sample to be measured.
For accurate calibra­tion, use two bea­kers for each solu­tion: the first one for rinsing the probe, the second one for calibration. In this way cross contamination is minimized.
If possible, to minimize any EMC interfer­ences, use plastic beakers for the solutions.
These meters can also be calibrated in air at
0.0µS/cm. For example if your measurements are in the
2 to 20 mS/cm range you should use HI7030 or HI 8030 (12880µS/cm=12.88 mS/cm) con­ductivity calibration solution.
A complete list of all the Hanna Instruments calibration solution is given in the Accesso­ries section (see page 50).
Press the RANGE key to se­lect the conductivity measure­ment mode.
Ensure that the probe is con­nected to the meter securely.
Insert the probe into the PVC sleeve with the holes towards the top (the end nearest to the cable) of the probe.
RINSE CALIBRATION
RANGE
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PROCEDURE FOR OFFSET CALIBRATION (at 0.0 µS/cm)
To perform the Offset calibration, dry the con­ductivity probe and leave it in air.
Press the ALT and the CAL keys simulta­neously. The primary LCD display will blink "0.0 µS" for about 10 seconds.
When "0.0 µS" stops blinking, the cali- bration can be confirmed. Press the CFM key to confirm the offset value.
If the input reading is out of the offset range, an error message will show on the secondary display "E0". Press the CAL key to re-calibrate the value.
If everything is satisfactory the LCD will blink "84.0 µS", expecting the first calibration solution.
Press the CAL key to exit the calibration mode now.
CAL
ALT
µS
µS
CFM
CAL
CAL
µS
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PROCEDURE FOR SINGLE POINT CALIBRATION WITH BUFFER SOLUTION
HI933300 and HI933301 have auto-buffer rec-
ognition: you can simply place the probe into the type of buffer solution that you need to calibrate and perform the single point calibra­tion very quickly as described below.
Choose one of the following calibration solu­tions:
84.0 µS/cm (cal. solution HI7033/HI8033) 1413 µS/cm (cal. solution HI7031/HI8031)
12.88mS/cm(cal. solution HI7030/HI8030)
80.0 mS/cm(cal. solution HI7034/HI8034)
Fill a beaker with conduc­tivity calibration solution (e.g. HI7030 or HI8030,
12.88mS/cm).
Press the RANGE key to select the conductivity measurement mode.
Dip the probe into the sample. The level of solu­tion must be higher than the holes on the PVC sleeve. Tap the probe re­peatedly on the bottom of the beaker and stir it to ensure that no air bubbles are trapped inside the sleeve.
Press the CAL key and the buffer value will be blinking on the display (e.g.
12.88 mS/cm).
8 cm
(3¼")
RANGE
CAL
mS
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When the buffer value stops blinking, indi­cating that the probe has stabilized, press the CFM key to confirm the value.
Press the CAL key to exit the calibration mode now.
PROCEDURE FOR A COMPLETE CALIBRATION WITH 5 BUFFERS
HI933300 and HI933301 have 5 memorized
calibration values:
0.0 µS/cm (probe in air)
84.0 µS/cm (cal. solution HI 7033/HI8033)
1413 µS/cm (cal. solution HI 7031/HI8031)
12.88mS/cm(cal. solution HI7030/HI8030)
80.0 mS/cm(cal. solution HI 7034/HI8034)
These meters can be calibrated at all the above five points as described below.
To perform the Offset cali­bration, dry the conductiv­ity probe and leave it in air.
Press the ALT and the CAL keys simulta­neously. The primary LCD display will blink "0.0 µS" for about 10 seconds.
mS
CFM
CAL
CAL
ALT
µS
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22
When "0.0 µS" stops blinking, the cali- bration can be confirmed. Press the CFM key to confirm the offset value.
If the input reading is out of the offset range, "E0" as error message will appear on the secondary display . Press the CAL key to re-calibrate the value.
If everything is satisfac­tory the LCD will blink "84.0 µS", expecting the next calibration so­lution (HI7033 or HI8033).
Fill a beaker with HI7033 or HI8033 conductivity
calibration solution.
Immerse the probe into the calibration solution. The level of solution must be higher than the holes on the PVC sleeve. Tap the probe repeatedly on the bottom of the beaker and stir it to ensure that no air bubbles are trapped inside the sleeve.
When the "84.0 µS" stops blinking, indi- cating that the measurement has stabi­lized, press the CFM key again to confirm the second point calibration.
µS
CFM
CAL
µS
8 cm
(3¼")
H
I 7
0
3
3
CFM
µS
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23
If the value is out of the slope range, an "E1" error message will appear on the secondary display. Press the CAL key to re-calibrate the value.
If everything is satisfac­tory the LCD will blink "1413 µS", expecting the next calibration so­lution (HI7031 or HI8031).
Wait for 1 minute, then immerse the probe into the HI7031/HI8031 cali­bration solution. The level of solution must be higher than the holes on the PVC sleeve. Tap the probe repeatedly on the bottom of the beaker and stir it to ensure that no air bubbles are trapped inside the sleeve.
When the "1413 µS" stops blinking, indi- cating that the measurement has stabi­lized, press the CFM key again to confirm the third calibration point.
If the value is out of the slope range, an "E2" error message will appear on the secondary display. Press the CAL key to re-calibrate the value.
CAL
µS
8 cm
(3¼")
HI 7031
CFM
µS
CAL
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If everything is satisfac­tory the LCD will blink "12.88 mS", expecting the next calibration so­lution (HI7030 or HI8030).
Wait for 1 minute, then immerse the probe into the HI7030/HI8030 cali­bration solution. The level of solution must be higher than the holes on the PVC sleeve. Tap the probe repeatedly on the bottom of the beaker and stir it to ensure that no air bubbles are trapped inside the sleeve.
When the "12.88 mS" stops blinking, indicating that the measurement has sta­bilized, press the CFM key again to con­firm the fourth calibration point.
If the value is out of the slope range, an "E3" error message will appear on the secondary display. Press the CAL key to re-calibrate the value.
If everything is satisfac­tory the LCD will blink "80.0 mS", expecting the next calibration solu­tion (HI7034 or HI8034)
Wait for 1 minute, then immerse the probe into the HI7034/HI7034 cali­bration solution. The level of solution must be higher
mS
8 cm
(3¼")
HI 7030
CFM
mS
CAL
mS
8 cm
(3¼")
H
I 7
0
3
4
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than the holes on the PVC sleeve. Tap the
probe repeatedly on the bottom of the beaker and stir it to ensure that no air bubbles are trapped inside the sleeve.
When the "80.0 mS" stops blinking, indicating that the measurement has sta­bilized, press the CFM key again to con­firm the fifth calibration point.
If the value is out of the slope range, an "E4" error message will appear on the secondary display. Press the CAL key to re-calibrate the value.
If everything is satisfactory the calibration ends and the meter will return to the nor­mal operational mode.
Note:
If the instrument will not calibrate refer to the Probe Maintenance and Clean­ing section (see page 48).
It is always possible to quit the cali­bration mode by pressing the CAL key.
mS
CFM
CAL
CAL
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CONDUCTIVITY VERSUS
TEMPERATURE CHART
As shown in the chart below, temperature has an effect on conductivity.
°C °F HI7030 HI7031 HI7033 HI7034 HI7035 HI7039
HI8030 HI8031 HI8033 HI8034 HI8035 HI8039
S/cm) S/cm) S/cm) S/cm) S/cm) S/cm)
0 32 7150 776 64 48300 65400 2760 5 41 8220 896 65 53500 74100 3180 10 50 9330 1020 67 59600 83200 3615 15 59 10480 1147 68 65400 92500 4063 16 60.8 10720 1173 70 67200 94400 4155 17 62.6 10950 1199 71 68500 96300 4245 18 64.4 11190 1225 73 69800 98200 4337 19 66.2 11430 1251 74 71300 100200 4429 20 68 11670 1278 76 72400 102100 4523 21 69.8 11910 1305 78 74000 104000 4617 22 71.6 12150 1332 79 75200 105900 4711 23 73.4 12390 1359 81 76500 107900 4805 24 75.2 12640 1386 82 78300 109800 4902 25 77 12880 1413 84 80000 111800 5000 26 78.8 13130 1440 86 81300 113800 5096 27 80.6 13370 1467 87 83000 115700 5190 28 82.4 13620 1494 89 84900 117700 5286 29 84.2 13870 1521 90 86300 119700 5383 30 86 14120 1548 92 88200 121800 5479 31 87.8 14370 1575 94 90000 123900 5575
HI933300 and HI933301 will always display the value of the buffers at 25°C (77°F), e.g. "1413 µS" using HI7031 or HI8031 as cali­bration solution.
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27
TEMPERATURE CALIBRATION
(for Technical Personnel only)
INITIAL PREPARATION
Prepare a container of ice and water and another container with hot water (at a tem­perature of at least 50°C/122°F). Place insu­lation material around the containers to mini­mize temperature changes.
Use a ChecktempC or a calibrated thermom­eter with a resolution of 0.1° as reference thermometer.
Note: After performing the following calibra-
tion, conductivity must be recalibrated.
PROCEDURE
Press the RANGE key to select the tem­perature measurement mode (just tem­perature measurement on the primary dis­play).
Ensure that the probe is connected to the meter securely by aligning the pins with the socket, pushing the plug in and tight­ening the threaded ring. Insert the probe
0 °C
(32 °F)
°C
50 °C
(122 °F)
°C
RANGE
°C
Page 30
28
into the PVC sleeve with the holes towards
the top (the end nearest to the cable) of the probe.
Place the probe into the container with ice and wa­ter (0.0°C/32°F).
Press the CAL key. The secondary (lower) display will blink "0" for about 30 sec­onds.
When "0" stops blinking, the calibration can be confirmed. Press the CFM key to confirm the first value.
If the value is out of the offset range, an error message will show on the secondary display "E1". Press the CAL key to re­calibrate the value.
CAL
CFM
CAL
0 °C
(32 °F)
°
C
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29
If everything is satisfactory the LCD will blink "50" expecting the second buffer (50°C/122°F).
Note: if a single point cali-
bration is required, press the CAL key to leave the calibra­tion mode now.
Place the probe into the second container with hot water (50°C/122°F).
When "50" stops blinking, press the CFM key again to confirm the second calibra­tion point.
If the value is out of the slope range, an error message will show on the secondary display "E2". Press the CAL key to re­calibrate the value.
If everything is satisfactory the tempera­ture calibration is complete and the meter will return to the normal operational mode.
CAL
CFM
CAL
°C
50 °C
(122 °F)
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30
PRINT
PRINTING/RECORDING WITH HI933301
To print the measured values press the PRINT key.
The printout provides the fol­lowing information:
a- Running log number b- Date (DD-MM-YY) c - Time (HH-MM) d- Conductivity value in µS/cm or mS/cm e- Temperature in degrees Centigrade.
RECORDING MODE (PROGRAMMED PRINTOUTS)
Set the appropriate printing interval (see Op­erational Guide section on page 12).
Press the ALT and the RECORD keys simulta­neously to enter the record­ing mode.
The log number will appear for a few seconds on the display to indicate the cor­rect operational mode.
The meter will print the measurement taken at that moment and will continue to print according to the set interval until the record­ing function is stopped (see below).
29-03-96
--01-­*15.01
147.6 µS
25.1 ° C
a b
c d e
PRINT RECORDRANGE
ALT CAL CFM
LOG INTV
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31
Each printout provides the following informa­tion:
a- Running log number. b- Running sample number in that particular
log. c- Date (DD-MM-YY) d- Printing interval indicator in minutes e- Time (HH-MM) f - Conductivity value in µS/cm or mS/cm g- Temperature in degrees Centigrade.
When the meter is in the re­cording mode "LOG" is dis­played on the bottom left cor­ner of the LCD.
If no keys are pressed, the meter goes to standby mode to prolong the battery life. To reactivate the display press any key.
Notes:
It is recommended to use the voltage
adapter (HI710005 or HI710006) dur­ing recording, especially when many printouts are going to be taken.
Before starting to record, make sure
that there is enough paper for your measurements. When the paper is finished the meter will not advise the operator and the printouts could be lost.
29-03-96
--01-- 0001M 0015 *16.59
5137 µS
25.9 ° C
<>
a b
c d e f g
LOG INTV
TIME
Page 34
32
It is possible to insert a new paper roll during the recording mode (see page 46).
Once in the logging mode, the interval cannot be changed.
Exit the logging mode (pressing the ALT and the RECORD keys si­multaneously) before setting the new inter­val (see page 12).
If the PRINT key is pressed while still in recording mode, an ad­ditional printout is pro­duced without affecting the running sample number.
SAMPLE NUMBER
During recording it is possible to know the running sample number. Press the RECORD key and the display will show the number of values that have been printed until now.
TO STOP RECORDING
In order to quit the recording mode, press the ALT and the RECORD keys simultaneously. This will generate a recording exit status printout.
The running log number can be reset by simply removing the batteries.
PRINT RECORDRANGE
ALT CAL CFM
PRINT
RECORD
<>
PRINT RECORDRANGE
ALT CAL CFM
29-03-96
--01-- 0001M 0055 *17.39
Page 35
33
PRINTING/LOGGING WITH HI933300
To print the measured values shown on display, press the PRINT key once.
This function can be activated in normal op­eration mode as well as during logging and scanning data on display (see below).
When in measurement mode, the printout pro­vides the following information:
a- Running log number b- Date (DD-MM-YY) c - Time (HH-MM) d- Conductivity value in µS/cm or mS/cm e- Temperature in degrees Centigrade.
LOGGING MODE
This function is suggested when remote mea­surements have to be taken automatically without the necessity of an operator and for a long period of time. In this mode data will be stored directly into memory.
Set the appropriate logging interval (see Op­erational Guide section on page 8).
Press the ALT and the LOG keys simulta­neously to enter the logging mode. The log number and page number will appear for a few seconds on the display to indicate the correct operational mode. The printer will print a complete set of data and the "LOG" sym
PRINT
29-03-96
--01-­*18.01
1455 µS
25.9 ° C
a b
c d e
Page 36
34
bol will appear on the bottom left corner of the LCD.
Press the ALT and the PAPER keys at the same time and the "LOG" symbol on the display will start to blink.
After approximately 5 minutes the display will switch off but the logging function remains active.
To reactivate the display press any key ex­cept the ALT key.
Notes:
Once in the logging mode, the interval can­not be changed. Exit the logging mode (pressing the ALT and the LOG keys simul­taneously) before set­ting the new interval (see page 8).
CFM
TIME LOG
RANGE
ALT CAL
LOG
29-03-96
--01-- 0001M 0001 *18.05
1455 µS
25.9 ° C
<>
PRINT
PAPER
ALT CAL
LOG
CFM
TIME LOG
RANGE
ALT CAL
Page 37
35
If the PRINT key is pressed while in log­ging mode, a printout is produced without af­fecting the running sample number.
SAMPLE NUMBER
During logging it is possible to know the running sample number.
Reactivate the display if the meter is in standby mode by pressing any key (except the ALT key).
Press the LOG key twice and the display will show the number of values that have been taken until now in the current log.
LOGGING MODE WITH PRINTING
This function is suggested when an immedi­ate report of the measurement is required in addition to the recording of data into memory.
Press the ALT and the LOG key simulta­neously to enter the logging mode. The log number and page number will appear for a few seconds on the display to indicate the correct operational mode.
The meter will print a complete set of data and the "LOG" symbol will appear on the bottom left corner of the display.
PRINT
LOG
CFM
TIME LOG
RANGE
ALT CAL
LOG
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36
29-03-96
--01-- 0001M 0004 *16.10
5815 µS
25.6 ° C
29-03-96
--01-- 0001M 0005 *16.11
5829 µS
25.6 ° C
<>
<>
a b
c d e f g
During logging with print­ing, the display shows the time, interval and the LOG symbol.
To display the conductivity value, press the RANGE key.
If no key is pressed, the display goes blank after about 5 minutes. To reactivate the dis­play press any key except the ALT key.
Each printout provides the following informa­tion: a- Running log number. b- Running sample number in that particular
log c - Date (DD-MM-YY) d- Logging interval indicator in minutes e- Time (HH-MM) f - Conductivity value in µS/cm or mS/cm g- Temperature in degrees Centigrade.
29-03-96
--01-- 0001M 0001 *16.07
5897 µS
25.9 ° C
<>
LOG INTV
TIME
RANGE
µS
Page 39
37
It is always possible to switch from the log­ging with printing function to the logging func­tion only. Press the ALT and the PAPER keys at the same time and the "LOG" sym­bol will start to blink, indicating that the data are only stored in memory and not printed.
Notes:
It is recommended to use the voltage adapter (HI710005 or HI710006) dur­ing logging with printing mode, espe­cially when many printouts are going to be performed.
Before proceeding with logging with printing, make sure there is enough paper for your measurements. When the paper is finished the meter will not advise the operator and the printouts could be lost. If this happens, data will continue to be stored into memory, and it is always possible to print it at different time (see below).
It is possible to insert a new paper roll during logging session (see page 46).
Once in the logging mode, the interval cannot be changed. Exit the logging mode first (pressing the ALT and the LOG keys si­multaneously) before setting the new interval (see page 8).
If the PRINT key is pressed while in log­ging mode, a printout is produced without af­fecting the running sample number.
CFM
TIME LOG
RANGE
ALT CAL
PRINT
PRINT
PAPER
ALT CAL
LOG
Page 40
38
TO STOP LOGGING
Press the ALT and the LOG keys simultaneously, this will generate a log exit status print out.
TO SCAN STORED DATA ON DISPLAY
Press the LOG key. The display will show the log number and the page number of the next log.
While pressing the ALT key, press the CFM key until the desired log number appears on the secondary display. The primary display will show the number of samples in that particular log.
Press the DOWN arrow key to reverse the sequence.
CFM
TIME LOG
RANGE
ALT CAL
29-03-96
--01-- 0001M 0009 *16.15
5814 µS
25.6 ° C
29-03-96
--01-- 0001M 0009 *16.15
<>
<>
Date
Printing Interval
Ending
Time
Log #
Total Sample #
LOG
CFM
TIME LOG
RANGE
ALT CAL
Page 41
39
Press the ALT and the RANGE keys simulta­neously. This now shows the date in which logging has commenced.
Press the UP arrow key and the time will be displayed.
Press the UP arrow key and the temperature will be displayed.
Press the UP arrow key and the conductivity value will be displayed.
Continue pressing the UP arrow key to display one by one all the memorized data of the same log in the above sequence, i.e. time, tem­perature, conductivity value.
ALT
RANGE
DATE
TIME
CAL
°C
CAL
CAL
mS
CAL
Page 42
40
To exit from the recall mode press the LOG key.
Note: this mode will not alter
data in memory.
TO PRINT STORED DATA
Having selected a log number by using ALT and CFM keys, as detailed in the chapter "TO SCAN STORED DATA ON DISPLAY" you can print all or part of that log section by using the ALT and PRINT keys.
The printer will then start to print the logged section be­ginning with the selected sample number without alter­ing the content of the memory.
Note: It is always possible to
print only the sample shown on the display by pressing the PRINT key.
For example if 10 samples are stored in a particular log, use the DOWN arrow key to display sample No. 5.
Sample 5 can be printed on its own using the PRINT key.
Samples 5, 6, 7, 8, 9 and 10 can be printed by pressing ALT and PRINT keys.
If you wish to stop the printer during the download session press "ALT" and
CFM
LOG
PRINT
CFM
PRINT
CFM
TIME LOG
RANGE
ALT CAL
PRINT
PAPER
ALT CAL
Page 43
41
"PAPER" simultaneously and the printer will immediately stop.
Note: Before proceeding with
printing, make sure there is enough paper for the data to be printed.
When the paper is fin­ished the meter will not advise the operator and the printouts could be lost.
If this happens, stop the printer by pressing ALT and PAPER key simulta­neously. Data will be kept in memory.
Insert a new paper roll and repeat the above instructions starting from the last printed sample number (see chapter "PRINTER MAINTENANCE" on page 46 for chang­ing paper roll).
PRINT
PAPER
ALT CAL
PRINT
PAPER
ALT CAL
PRINT
PAPER
ALT CAL
Page 44
42
Windows® is registered Trademark of "Microsoft Co."
TIME
DATA TRANSFER TO PC
HI933300 contains infrared emitting circuitry.
Set the meter to TIME mode and simply place your datalogger on a HI 9200 Infra­red Transmitter (ensuring that the two infrared LEDs are placed on top of each other) and the contents of the memory can then be down­loaded to your PC through the HI9200's RS 232 port.
During the data transfer the instrument displays the mes­sage "r 232".
Using the HI9200 Infrared Transmitter, all recorded data can be fed to your Personal Computer for easy reproduction, storage or elaboration without the interference of cables or cords between the meter and the transmit­ter.
Data transmission from the instrument to the PC is now much easier with new HI92000 Windows® compatible application software of­fered by Hanna Instruments.
Page 45
43
HI 92000 allows you to use the powerful means of the most widely used spread sheet programs available (e.g.Excel©, Lotus 1-2-3©).
Simply open your file downloaded by HI 92000 from your spread sheet program and then it is possible to make any elaboration available with your software (e.g. graphics, statistic analysis).
User friendly, HI 92000 offers a variety of fea­tures and has on line help to support you throughout any situation.
To install HI 92000 you need a 3.5" drive and a few minutes to follow the instructions con­veniently printed on the disk label.
Excel© Copyright "Microsoft Co."
Lotus 1-2-3© Copyright "Lotus Co."
Page 46
44
HI933300 and HI933301 are factory pro­grammed to automatically diagnose a fault. This is displayed with error codes on the LCD.
Error codes: PEr 0, PEr 1, PEr 2 = Short
circuit on the system, the meter should be returned for repair (see Warranty sec­tion).
PEr3 = Printer mechanism
fault - repair needed (see Warranty sec­tion).
PEr4 =Printer clutch
jammed - reset the printer (see page 47).
PEr 9 = Printer jammed - re-
set the printer (see page 47).
FAULT FUNCTIONS
Page 47
45
Capacity: 8000 data samples which are di­vided into 16 pages.
Each time a new logging period starts, it automatically starts from a new page.
If the logging function is still on, and the available page is 0 the meter will overwrite the first lot of data in the existing memory. During logging the meter automatically re­turns to the oldest page in memory and if it contains data, it will overwrite. In this case the first log will not correspond to the oldest set of data
It is recommended to periodically clean the memory. Save data with PC if you need to keep a record and then disconnect the bat­teries for about 1 minute. If you do this, remember to set the date and time, once the batteries have been reconnected.
ATTENTION:
Data is stored into memory until the batteries are removed.
If battery replacement is required and data is not to be lost, plug the adapter in and pro­ceed with battery replacement (see page 49). Only once the batteries have been replaced it is possible to unplug the adapter without loosing the stored data.
MEMORY ORGANIZATION (HI933300)
Page 48
46
TO CHANGE THE INK CARTRIDGE
When printouts become faint, it might be neces­sary to change the ink cartridge. Contact your Hanna authorized center.
TO INSERT THE PAPER ROLL
The HI933300 and HI933301 use plain paper rolls 38 mm width. To insert a new roll is very easy.
Open the paper cover pulling it gently.
Take the carton cylinder away.
Insert the paper edge in the printer slot and feed the printer by pressing the PAPER key.
PAPER
PRINTER MAINTENANCE
Page 49
47
Allow about 5 cm (2") to exit from the printer and replace the paper cover.
TO RESET PRINTER
Investigate the cause of the printer jam (e.g. the paper caught under the cover that has prevented printer from advancing paper feed).
Press the PAPER key to reset the printer.
PAPER
Page 50
48
Rinse the probe with tap water after every series of measure­ments. If a more thor­ough cleaning is re­quired, remove the PVC sleeve and clean the probe with a cloth or a nonabra­sive detergent. When reinserting the sleeve onto the probe, be sure that the sleeve is in the right direc­tion with the four holes towards the cable end. After cleaning the probe, re-calibrate the instrument.
The probe body is in PVC and for this rea­son must never come into close contact with sources of heat. If the probe is ex­posed to high tem­peratures, detach­ment of the rings might occur, resulting in a serious impairment of probe function. In such cases, the probe has to be replaced.
PROBE MAINTENANCE
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49
BATTERY REPLACEMENT
When the batteries are run down "LOBAT" is displayed on the Liquid Crystal Display to warn the user.
Battery replacement must only take place in a non hazardous area using 1.5V alkaline AA type batteries.
In order to replace run down batteries, simply remove the two screws on the rear cover of the instrument and replace the four 1.5V AA bat­teries with new ones, paying attention to the correct polarity.
A 12VDC power source can also be used to power the unit (see the Accessories section page 51).
Note: The instrument uses the following con-
figuration.
It is recommendable to purchase the Hanna HI 710005 and HI 710006 voltage adapters that use the proper polarity configuration. Anyway, HI 933300 and HI 9333001 can be used with other adapters. In this case, re­member to check the correct polarity of your adapter before connecting it to the meter.
LO BAT
-
-
+
+
1.5V
1.5V
-
-
+
+
1.5V
1.5V
SCREW
POTS
+
-
Page 52
50
ACCESSORIES
CONDUCTIVITY CALIBRATION SOLUTIONS
HI 7030L 12880 µS/cm (µmho/cm), 460 mL HI 7030M 12880 µS/cm (µmho/cm), 230mL HI 7031L 1413 µS/cm (µmho/cm), 460 mL HI 7031M 1413 µS/cm (µmho/cm), 230 mL HI 7033L 84 µS/cm (µmho/cm), 460 mL HI 7033M 84 µS/cm (µmho/cm), 230 mL HI 7034L 80000 µS/cm (µmho/cm), 460 mL HI 7034M 80000 µS/cm (µmho/cm), 230 mL HI 7035L 111800 µS/cm (µmho/cm), 460 mL HI 7035M 111800 µS/cm (µmho/cm), 230 mL HI 7039L 5000 µS/cm (µmho/cm), 460mL HI 7039M 5000 µS/cm (µmho/cm), 230 mL
CONDUCTIVITY CALIBRATION SOLUTIONS IN FDA APPROVED BOTTLES
HI 8030L 12880 µS/cm (µmho/cm), 460 mL HI 8031L 1413 µS/cm (µmho/cm), 460 mL HI 8033L 84 µS/cm (µmho/cm), 460 mL HI 8034L 80000 µS/cm (µmho/cm), 460 mL HI 8035L 111800 µS/cm (µmho/cm), 460mL HI 8039L 5000 µS/cm (µmho/cm), 460 mL
Page 53
51
POWER UNITS
HI710005 Voltage adapter from 115 VAC
to 12 VDC
HI710006 Voltage adapter from 230 VAC
to 12 VDC
OTHER ACCESSORIES
CHECKTEMPC Electronic thermometer (range
-50.0 to 150.0°C)
HI 710031 Hard carrying case HI 710034 Plain Paper Spare Rolls (10 pcs) HI 710035 Spare Ink Cartridge (1pc) HI 721308 1.5V AA alkaline battery (10
pcs)
HI 76302W 4-ring probe with temperature
sensor with 1 meter (3.3') cable
HI 9200 Infrared Transmitter (for
HI933300 only)
HI 92000/16 Windows® 3.11 software for data
transfer to PC (for HI933300 only)
HI 92000/32 Windows® 95 software for data
transfer to PC (for HI933300 only)
MANCNPRNR1 Instruction manual
Windows® is registered Trademark of "Microsoft Co."
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52
WARRANTY
All Hanna Instruments meters are warranted for two years against defects in workman-
ship and materials when used for their in­tended purpose and maintained according to the instructions.
The probes are warranted for a period of six months.
Damages due to accident, misuse, tamper­ing or lack of prescribed maintenance are not covered. This warranty is limited to repair or replacement free of charge.
If service is required, contact the dealer from whom you purchased the instrument. If under warranty, report the model number, date of purchase, serial number and the nature of the failure. If the repair is not covered by the warranty, you will be notified of the charge for repair or replacement. If the instrument is to be returned to Hanna Instruments, obtain a Return Goods Authorization from the Cus­tomer Service Department first and then send it with shipment cost prepaid. When shipping any instrument, make sure it is properly pack­aged for complete protection.
To validate your warranty, fill out and return the enclosed warranty card within 14 days from the date of purchase.
All rights are reserved. Reproduction in whole or in part is prohibited without the written consent of the copyright owner.
Hanna Instruments reserves the right to modify the design, construction and ap­pearance of its products without advance notice.
Page 55
CE DECLARATION OF CONFORMITY
53
DECLARATION OF CONFORMITY
We
Hanna Instruments Srl V.le delle industrie 12 35010 Ronchi di Villafranca (PD) ITALY
herewith certify that the conductivity meters
have been tested and found to be in compliance with the following regulations:
IEC 801-2 Electrostatic Discharge IEC 801-3 RF Radiated IEC 801-4 Fast Transient EN 55022 Radiated, Class B
Date of Issue: 15-03-1996
D.Volpato - Engineering Manager
On behalf of
Hanna Instruments S.r.l.
HI 933300 HI 933301
Recommendations for Users
Before using these products, make sure that they are entirely suitable for the environment in which they are used.
Operation of these instruments in residential area could cause unacceptable interferences to radio and TV equipments, requiring the operator to take all necessary steps to correct interferences.
Any variation introduced by the user to the supplied equipment may degrade the instruments' EMC performance.
To avoid electrical shock, do not use these instruments when voltages at the measurement surface exceed 24VAC or 60VDC.
To avoid damages or burns, do not perform any measurement in microwave ovens.
Page 56
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