Hanna Instruments HI 5421 Instruction Manual

Page 1
HI 5421
DO/BOD/OUR/SOUR/Temperature
Bench Meter
Instruction Manual
www.hannainst.com
Printed in ROMANIA
Hanna Instruments Inc.
Technical Support for Customers
Tel. (800) 426 6287 Fax (401) 765 7575 E-mail tech@hannainst.com www.hannainst.com
Local Sales and Customer Service Office
MAN5421 03/15
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TABLE OF CONTENTS
WARRANTY .............................................................................................................................................................. 2
PRELIMINARY EXAMINATION ..................................................................................................................................... 3
GENERAL DESCRIPTION ............................................................................................................................................. 3
FUNCTIONAL DESCRIPTION ....................................................................................................................................... 4
SPECIFICATIONS ....................................................................................................................................................... 6
OPERATIONAL GUIDE................................................................................................................................................ 7
DISPLAYING MODES ................................................................................................................................................. 8
SYSTEM SETUP ...................................................................................................................................................... 11
DO SETUP ............................................................................................................................................................. 17
BOD SETUP ........................................................................................................................................................... 31
OUR SETUP ........................................................................................................................................................... 32
SOUR SETUP ......................................................................................................................................................... 33
DO CALIBRATION ................................................................................................................................................... 34
PRESSURE CALIBRATION ......................................................................................................................................... 36
DO MEASUREMENT ................................................................................................................................................. 37
BOD MEASUREMENT ............................................................................................................................................... 41
OUR MEASUREMENT .............................................................................................................................................. 46
SOUR MEASUREMENT ............................................................................................................................................ 47
LOGGING ............................................................................................................................................................... 48
PC INTERFACE ........................................................................................................................................................ 52
PROBE CONDITIONING & MAINTENANCE .................................................................................................................. 53
TROUBLESHOOTING GUIDE ..................................................................................................................................... 54
ACCESSORIES ......................................................................................................................................................... 55
HI 5421 is warranted for two years against defects in workmanship and materials when used for their intended purpose and maintained according to instructions. The probe is guaranteed for six months. This warranty is limited to repair or replacement free of charge.
Damage due to accidents, misuse, tampering or lack of prescribed maintenance is not covered. If service is required, contact the dealer from whom you purchased the instrument. If under warranty, report the model number, date of purchase, serial number and the nature of the failure. If the repair is not covered by the warranty, you will be notified of the charges incurred. If the instrument is to be returned to Hanna Instruments, first obtain a Returned Goods Authorization number from the Technical Service Department and then send it with shipping costs prepaid. When shipping any instrument, make sure it is properly packed for complete protection. To validate your warranty, fill out and return the enclosed warranty card within 14 days from the date of purchase.
Dear Customer, Thank you for choosing a Hanna Instruments product. This manual will provide you with the necessary information for correct use of the instrument. Please read this instruction manual carefully before using the instrument. If you need additional technical information, do not hesitate to e-mail us at tech@hannainst.com or view our worldwide contact list at www.hannainst.com.
WARRANTY
All rights are reserved. Reproduction in whole or in part is prohibited without the written consent of the copyright owner.
RECOMMENDATIONS FOR USERS
Before using these products, make sure they are entirely suitable for the environment in which they are used. Operation of these instruments in residential areas could cause unacceptable interferences to radio and TV
equipment, requiring the operator to follow all necessary steps to correct interferences. The glass bulb at the end of the pH electrode is sensitive to electrostatic discharges. Avoid touching this glass
bulb at all times. Any variation introduced by the user to the supplied equipment may degrade the instruments’ EMC
performance. To avoid electrical shock, do not use these instruments when voltages at the measurement surface exceed
24 Vac or 60 Vdc. To avoid damage or burns, do not perform any measurement in microwave ovens.
Hanna Instruments reserves the right to modify the design, construction or appearance of it’s products without
advance notice.
ACCESSORIES
HI 7040M Zero Oxygen Solution, 230 mL HI 7040L Zero Oxygen Solution, 500 mL HI 7041S Refilling Electrolyte Solution, 30 mL
OTHER ACCESSORIES
HI 710005/8 Voltage adapter from 115 Vac / 12 Vdc 800 mA (USA plug) HI 710006/8 Voltage adapter from 230 Vac / 12 Vdc 800 mA (European plug) HI 76404W Electrode holder HI 76483 DO probe for laboratory use with built-in temperature sensor HI 76483A/P 5 spare membranes HI 92000 Windows
®
compatible software
HI 920013 USB cable
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Remove the instrument from the packing material and examine it carefully to make sure that no damage has occurred during shipping. If there is any damage, notify your dealer or the nearest Hanna Service Center. The meter is supplied complete with:
HI 76483 DO probe for laboratory use with built-in temperature sensor
HI 7041S Electrolyte solution (30 mL)
HI 76483A Membrane caps (2 pcs.)
HI 76404W Electrode Holder
• 12Vdc Power Adapter
• Instruction Manual
HI 5421-01 is supplied with 12 Vdc/115 Vac adapter. HI 5421-02 is supplied with 12 Vdc/230 Vac adapter.
Note: Save all packing material until you are sure that the instrument works properly. Any defective item
must be returned in the original packing with the supplied accessories.
HI 5421 is a professional bench meter with color graphic LCD for DO, BOD, OUR, SOUR and temperature measurements. The display viewing modes are: Basic information only, GLP information, Graph and Log History mode. The main features of the instruments are:
• Single input channel;
• Capacitive touch keypad;
• Dedicated Help key with contextual message
• Six measurement parameters: DO, BOD, OUR, SOUR, pressure and temperature;
• Automatic or user standard DO calibration;
• AutoHold feature to freeze the stable reading on the LCD (DO only);
• Two selectable alarm limits (for DO, BOD, OUR, SOUR);
• Three selectable logging modes: Automatic, Manual or AutoHold (DO only);
• Up to 100 logging lots for automatic or manual modes, up to 200 OUR and SOUR reports and up to 200 BOD method information entries;
• Selectable sampling period feature for automatic logging from 1 second to 180 minutes;
• GLP feature for DO;
• Online and offline graph;
• Large color backlight graphic LCD (240 x 320 pixels) with selectable color palette;
• PC interface via USB; download logged data to PC or use for Real time logging (HI 92000 PC application required);
• Profile feature: store up to ten different user setups.
PRELIMINARY EXAMINATION
GENERAL DESCRIPTION
54
TROUBLESHOOTING GUIDE
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For an accurate calibration, it is recommended to wait a minimum of 15 minutes to ensure conditioning of the probe. Keep the protective cap on during polarization and remove it for calibration and measurements. Follow the calibration procedure.
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HI 5421 DESCRIPTION
FRONT PANEL
REAR PANEL
1) Liquid Crystal Display (LCD)
2) Capacitive touch keypad
3) ON/OFF button
4) Power adapter socket
5) DO probe input
6) USB connector
FUNCTIONAL DESCRIPTION
53
PROBE CONDITIONING & MAINTENANCE
The DO probe body is made of PEI. Use the protective cap provided when the probe is not in use. To inspect or replace the membrane proceed as follows:
Inspection:
Inspect membrane surface to ensure it is in perfect condition. The semipermeable membrane isolates the sensor elements from the environment but allows oxygen to enter. If any dirt is observed on the membrane, rinse carefully with distilled or deionized water. If imperfections still exist, or any damage is evident (such as salt crystals, wrinkles or tears-holes), the membrane should be replaced. Verify no bubbles are trapped between the cathode and membrane.
Membrane Cap Installation:
For a new probe, remove the protective shipping tube by gently twisting and pulling it off the body of the probe (see fig.1). If a membrane cap was previously installed, unscrew the membrane cap by turning it clockwise (see fig.2).
The new membrane cap should be rinsed with electrolyte solution prior to use. Fill the cap with clean electrolyte solution. Gently tap the sides of the membrane cap to ensure that no air bubbles remain trapped. Do not tap the bottom directly, as this will damage the membrane. Make sure that the O-ring is seated properly inside the membrane cap (see figure). With the sensor facing down, slowly screw the membrane cap counterclockwise. Some electrolyte will overflow. When totally screwed on, verify no bubbles are found trapped in the electrolyte.
Cathode Inspection:
The platinum cathode should always be bright and untarnished. Inspect this when the cap is removed. If it is tarnished or stained, the cathode should be cleaned. Use extreme caution when handling the probe tip as the cathode insulator is glass. Inspect that the insulator has not been cracked. Use a clean lint-free cardboard or cloth. Rub the cathode very gently side to side 4-5 times. This will be enough to polish and remove any stains without damaging the platinum tip. Afterwards, rinse the probe with deionized or distilled water and install a new membrane cap using fresh electrolyte and directions above.
Conditioning:
Before proceeding with the calibration make sure the probe is ready for measurements. Reinstall the plastic protective cap over membrane end. Reconnect probe to meter and allow probe to polarize.
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KEYBOARD DESCRIPTION
FUNCTION KEYS
VIRTUAL KEYS
The upper row keys are assigned to the virtual keys placed on the bottom of the LCD, which allow you to perform the displayed function, depending on the current menu (e.g.
and
in Measure
mode).
LCD GENERAL DESCRIPTION
To enter / exit calibration mode.
To select the desired measurement mode: DO, BOD, OUR, SOUR.
To enter Setup (System Setup, DO Setup, BOD Setup , OUR Setup or SOUR Setup) and to access Log Recall function.
To obtain general informations about the selected option / operation.
52
PC INTERFACE
Data transmission from the instrument to the PC can be done with the HI 92000 Windows® compatible software (optional). HI 92000 also offers graphing and on-line help features.
Data logged on the HI 5421 meter can be exported to the most popular spreadsheet applications for further analysis. The instrument has an USB interface.
Use a standard USB cable to connect your instrument to the PC. Make sure that the instrument and the HI 92000 software have the same baud rate and the appropriate
communication port. The PC software may also be used for real time logging.
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SPECIFICATIONS
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51
To delete lots:
• Press
while in
Log Recall
mode.
• Press
or to access delete or delete all
mode. Otherwise, press
to return to
Log Recall
view
mode.
• After selecting one of the Delete keys, use
or
to select one lot and then press or
to delete the selected lot or all lots. The “Please wait...” message will be displayed on the LCD until the selected lot or all lots are deleted.
• Press
and then press to exit deleting mode
and return to
Log Recall
view mode.
• Press
to exit
Log Recall
mode and return to
Measure
mode.
Note: Logged lots should also be deleted whenever “Limited Automatic Logging Space” or “Automatic Log
Is Full” message appears on the LCD, in the Reminder messages area.
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POWER CONNECTION
Plug the 12 Vdc adapter into the power supply socket.
Note: This instrument use non volatile memory to retain the meter settings, even when unplugged.
PROBE CONNECTION
For DO, BOD, OUR or SOUR measurements connect a DO probe to the DIN connector located on the rear panel of the instrument.
INSTRUMENT START UP
• Please ensure that the capacitive keypad is not covered by hand or other objects at the meter power on.
• Turn the instrument on from the power button located on the rear panel of the instrument.
• Please wait until the instrument finishes the initialization process.
Note: It is normal for the loading process to take a few seconds. If the instrument doesn’t display the next
screen, restart the meter using the power button. If the problem persists, contact your dealer.
OPERATIONAL GUIDE
50
• Press , or to select the desired Log Report type. All logged lots for the selected Log Report type will be displayed on the LCD.
• To filter the displayed lots, press
and then the desired parameter. Only the selected measurement parameter lots will be displayed on the LCD.
• Select the desired lot with
or and press
to display the logged data from the highlighted lot.
The “Please wait...” message will be displayed on the LCD for one second. The selected Logging Data Configuration options will be displayed on the LCD, together with GLP information (last calibration date and calibrated standards) if a calibration has been performed on the selected mode and the logged values (measured value, temperature value, temperature compensation mode and the logging time).
Note: For automatic logging only, it is possible to view the
plotted graph.
• Press
to display the graph.
• By pressing
it is possible to move the graph along
the X or Y axis with the arrow keys.
• If pressing
while the graph is displayed, the zoom
menu for the X and Y axes will be accessed. Press
,
or
to switch between the active zooming axes and then zoom in or out on the selected axis by pressing the appropriate virtual key.
• Press
to return to the previous menu at any time.
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DISPLAYING MODES
For each measurement mode (DO, BOD, OUR or SOUR) the following display configurations are available: Basic, Graph and Log History. GLP is available for DO measurements.
Basic
Accessing this option, the measured value and its units are displayed on the LCD, along with the temperature value, temperature compensation mode, pressure value, pressure compensation mode and minimal GLP data. To choose the Basic displaying mode:
• Press while in
Measure
mode. The “Choose
Display Configuration” message will be displayed in the Reminder messages area.
• Press
. The instrument will display the basic
information for the selected measurement mode.
GLP
Accessing this option for DO measurement, a detailed GLP data will be displayed on the LCD: Last Calibration Date and Time, Sample ID, Calibration Standards, Barometric Pressure, Salinity, Temperature Values, the current Date and Time.
To access the GLP displaying mode:
• Press
while in
Measure
mode. The “Choose
Display Configuration” message will be displayed in the Reminder messages area.
• Press
. The instrument will display the detailed GLP
data.
49
3) Direct/AutoHold Reading Mode and Automatic Log
Press
and then keys must be pressed on front
display to initiate this function. Real time continuous measurements are on display with “AutoHold” flashing and real time continuous logging into meter memory, until the meter reaches the stability criteria to go into Auto Hold mode. The stored sample logs will be marked with an “H” to indicate the Auto Hold mode. The virtual
key
returns operation to real time continuous measurements
and
stops the logging session.
4) Direct/AutoHold Reading Mode and Manual Log
Press
in order to add one new record in the log report.
The manual log is working even if it is in Auto Hold or Continuous reading mode. Press
to initiate
the Auto Hold event. “AutoHold” will flash until the stability criteria is reached and then the screen freezes in Auto Hold mode, the data is marked with an “H”.
5) Direct/AutoHold Reading Mode and Auto Hold Log
Press
and then keys to initiate and automate the capture of stable data which is stored in the Recall Manual Log file. During the process, “AutoHold” will flash until the stability criteria is reached and then the screen freezes in Auto Hold mode, the data is logged and marked with an “H”. The virtual key
returns operation to Real time continuous measurement. Press again to log a second stable
data point. The lot ID along with the record index will appear for short time on the top/left corner on the selected channel window, every time a record will be added to the lot.
LOG RECALL
This feature allows the user to view all stored data. If no data were logged, the “No records were found.” message will be displayed on the LCD in the Log Recall screen. Otherwise, the instrument will display all the memorized lots in accordance with the selected option: Automatic Log, Manual Log or OUR/ SOUR Reports. To view the memorized data:
• Press
while in
Measure
mode.
• Press
and then select the log report type.
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Graph
The online graph with real time logging (DO, BOD, OUR or SOUR vs. Seconds) will be displayed when this option is selected. If there is no active log, the previously logged data for the selected parameter will be shown.
Notes: • If no data is being logged, the graph will be empty.
• If no automatic log is saved, the offline graph will be empty.
To access the offline / online graph:
• Press
while in
Measure
mode. The “Choose Display
Configuration” message will be displayed in the Reminder messages area.
• Press
.
• Press
to begin online graph.
To Zoom Graph
• Press
then . and will appear in virtual keys.
•Use
and to move along the X (Time) axis of the graph.
• Press
to access the zoom menu for Y axis. Use or for zooming Y (parameter)
axis.
• Press
to return to the main menu.
When the off-line graph is displayed:
• Use the arrow keys to move along the X (Time) and Y (parameter) axes of the graph.
• Press
to access the zoom menu for X and Y axes. Use or to switch between the
active zooming axes. Press
or to zoom the selected axis.
Note: While in zoom graph menu the
key is not accessible.
• Press
to return to the main menu.
48
LOGGING
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There are 5 ways the Reading Mode and Log may be configured together. The table below shows the combinations and indicates where the completed log will be stored.
2) Direct Reading Mode and Manual Log:
Real time continuous measurements are on display and snapshots of measurement data are stored in the Manual log when the user
presses . Subsequent snapshots will be added to the same Manual Lot every time the
is depressed unless
New Lot is selected under
Log
options.
Note: When the
is pressed the lot ID along with the current record number will appear for short time on the selected channel window on the top/left corner (e.g. L001_DO 14 - this means lot ID L001_DO and recod number 14).
1) Direct Reading Mode and Automatic Log:
Real time continuous measurements are on display and continuous logs to meter memory. These are sometimes referred as interval
logs. Press .
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Log History
The measurement, along with LOG History, will be visible when this option is selected:
1) The last stored logged data (Not actively logging) or
2) The last data logged from an active logging lot or
3) An empty display - NO LOTS saved, Not currently logging the log history list also contains the main measured value, the temperature, as well as a record time stamp. To access the Log History displaying mode:
• Press
while in
Measure
mode. The “Choose
Display Configuration” message will be displayed in the Reminder messages area.
• Press
. The instrument will display the log history
regarding the selected
Measure
mode.
Notes: • When an alarm condition is active, the logged records will have an exclamation mark “!”.
• If logged in Auto Hold, logged records will have an “H”.
• If another
Measure
mode is selected, the Log History will reset.
• If the temperature unit is changed, all logged temperature values will be automatically displayed
in the new temperature unit.
•“A” denotes automatic temperature compensation.
•“M” denotes manual temperature compensation.
47
s
The Specific Oxygen Uptake Rate (SOUR), also known as the oxygen consumption or respiration rate, is defined as the milligram of oxygen consumed per gram of volatile suspended solids (VSS) per hour. This quick measurement has many advantages: rapid measure of influent organic load and biodegradability, indication of the presence of toxic or inhibitory wastes, degree of stability and condition of a sample, and calculation of oxygen demand rates at various points in the aeration basin. The following equation is used for SOUR determination:
SOUR = OUR / Solids Weight
where:
OUR is the Oxygen Uptake Rate Solids Weight is the
Total solids
or the
Volatile suspended solids
weight in g/L
Temperature correction:
The SOUR value is corrected to 20 °C (68 °F) according to the Farrel and Bhide equation:
SOUR
20
= SOURT x Θ
(20 - T)
Where T is the measured temperature in °C and Θ is a temperature dependent variable:
Θ= 1.05 for T above 20 °C
Θ= 1.07 for T below 20 °C
This calculation is valid only for temperature values in the range 10 to 30 °C. Temperature correction is performed only if the option SOUR @20°C is enabled (see
Method Configuration
in
SOUR Setup
).
Before starting a SOUR measurement remember to set the SOUR configuration from the setup menu and make sure the has been calibrated in DO mode.
To measure the SOUR of a sample:
• Press and then to select SOUR measure mode.
• Place calibrated probe into sample.
• Press
to start taking the measurement.
• At the end of the measurement the meter will display the computed SOUR value, the duration of the measurement and the pressure and temperature values.
SOUR MEASUREMENT
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SYSTEM SETUP
The System Setup menu allows the user to customize the user interface, view meter information, set the external serial communication interface and to restore the manufacturer settings.
Accessing System Setup
• Press
while in
Measure
mode.
• Press
. The system setup options will be displayed on
the LCD.
To access a System Setup option:
• Use
or to highlight the desired option.
• Press
to access the selected option.
The following is a detailed description of the System Setup option screen.
Beeper
This option allows the user to turn an acoustic warning signal on or off. This function can be used to signal 4 different events: a stable signal, an alarm state, when every key is pressed or when an incorect key is pressed. Enable (or disable) the Beeper for these events. Disabling the Beeper will stop audible signals.
46
The OUR is used to determine the oxygen consumption or respiration rate. It is defined as the mg/L of oxygen consumed per hour.
The following equation is used for OUR determination:
where: DO
START
= Dissolved oxygen level at start of test
DO
END
= Dissolved oxygen level at end of test
t
ELAPSED
= Elapsed time of test in seconds
total volume/sample volume = Dilution factor of sample
Before starting an OUR measurement remember to set the OUR configuration from the OUR setup menu and make sure the instrument has been calibrated in DO mode.
To measure the OUR of a sample:
• Press
and then to select OUR measure mode.
• Place calibrated probe into sample.
• Press
to start taking the measurement.
• At the end of the measurement the meter will display the computed OUR value, the duration of the measurement and the pressure and temperature values.
OUR MEASUREMENT
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12
Saving Confirmation
Enable this option to force verification of a change made to a “GLP Data Option field” or a Sample ID name. If Saving Confirmation is enabled, the user will have to accept the change with a key stroke. If Saving Confirmation is disabled, the changes made to these fields change automatically without verification.
GLP Data
Use this option to customize log GLP information with specific identification data. When enabled, these ID tags will be included in the GLP section of all data logs. Each data field can use up to 10 characters. The five available fields are:
Operator ID
: used to add the name of the operator
Instrument ID
: used to name an instrument with a discrete name, location or number
Company Name
: used to include the Company ID to the GLP data field.
Additional Info
: Two data fields are available for general notes or notations.
To add the GLP Data:
• Press
while in
Measure
mode.
• Press
.
• Use
or to select the GLP Data option.
• Press
and use or to highlight the
desired option.
• Press
to edit the desired information. The Text Editor
menu will be displayed on the LCD.
• Enter the desired information by accepting the highlighted character which is added to the text bar, using
. The
and keys help the user select the desired character. It is also possible to delete the last
character by positioning the cursor on the Backspace character (
) and pressing .
• Press
to return to the GLP Data options. If the Saving Confirmation is enabled, press to
accept the modified option,
to escape without saving or to return to the editing mode.
Otherwise, the modified options are saved automatically.
45
• If all samples/seeds were moved to the lower box, the will appear.
• Otherwise, if some of the samples/seeds were selected, press to change soft keys. will appear. Use
/ arrows to select sample, then press
.
• The BOD Results with SEED correction will be displayed.
Press
to save and replace the previous sample report
with this bottle ID or press
to keep the previous
sample BOD with no seed correction.
To print a copy of the BOD analysis with seed correction:
• Use HI 92000 software and connect the HI 5421 meter.
• Select the BOD sample from the available BOD reports.
• Press
to print a paper copy of the analysis.
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13
Date & Time
Set the current date & time and the format in which they appear. These parameters will be displayed on the
Measure
screens and also when storing measured data.
Set Date and Time
This option allows you to set the current date (year/month/day) and time (hour/minute/second). Notes: • Only years starting with 2000 are accepted.
• The time is set using the selected time format. For 12 Hour time format only, the AM/PM can also be selected with
or .
Set Time Format
Choose between 12-Hour (AM/PM) time format or 24-Hour time format.
Set Date Format
Choose the desired date format from 7 available options: DD/MM/YYYY; MM/DD/YYYY; YYYY/MM/DD; YYYY-MM-DD; Mon DD,YYYY; DD-Mon-YYYY or YYYY-Mon-DD.
To set the Date & Time:
• Press
while in
Measure
mode.
• Press
.
• Use
or to select the Date & Time option.
• Press
and use or to highlight the Set
Date and Time.
• Press
to confirm your selection. Use /
to select next/previous entry to be edit. Press and use
or to set the desired value, then press
to save the modified value (for Set Date and Time option).
• For the other two options press
to confirm your selection and select one of the displayed options.
• Press
to return to previous menu. If the Saving Confirmation is enabled, press to accept the
modified option,
to escape without saving or to return to the editing mode. Otherwise, the
modified option is saved automatically.
Note: If the time is changed with more than one hour before last calibration, a pop-up warning will appear
on the LCD, notifying the user that a date/time conflict has occured and some time-dependent modes could work improperly (e.g.
Measure
, GLP, Log).
44
SEED CORRECTION
To apply seed corrections to the sample data follow the following procedure:
• Press
then to select BOD mode.
• Press
and to view samples.
Note: This list contains bottles with initial data, with 5 day BOD
determinations and 5 day BOD determinations with seed corrections. The dates reflect the last date the sample was evaluated.
• Press
then to select the sample and seed
bottles.
• If more than one Seed Bottle is used, the average value of the seeds will be used for Seed correction.
• Press
to move samples into the lower box. These
bottles will be corrected with the selected seed values.
Page 14
14
LCD Setup
This option allows the user to set the Contrast, the Backlight of the LCD and the Backlight Saver. The Contrast parameter can be adjusted within 7 steps, while the Backlight parameter within 8 steps. The Backlight Saver can be set from 1 to 60 minutes or it can be OFF (disabled). All the changes are visible on the LCD for each parameter.
Note: If the instrument backlight turnes off after the time period set, press any key to turn it back on. To set the LCD Setup:
• Press
while in
Measure
mode.
• Press
.
• Use
or to select the LCD Setup option.
• Press
and use key to highlight the desired
parameter.
• Use
or to adjust the contrast / backlight or to
set the desired backlight saver time.
• Press
to confirm the modified options and return to the
System Setup menu.
Color Palette
This option allows the user to choose a desired color palette. To select the Color Palette:
• Press while in
Measure
mode.
• Press
.
• Use
or to select the Color Palette option.
• Press
and use or to highlight the desired color.
• Press
to confirm your selection and return to the System Setup menu or press
to return to the
System Setup menu without changing.
1roloCtxeteulbdnuorgkcabetihW
2roloCtxetetihwdnuorgkcabeulB
3roloCtxetkcalbdnuorgkcabetihW
4roloCtxetetihwdn
uorgkcabkcalB
43
• The Current dissolved oxygen measurement of the incubated sample will be made.
• Press
to apply dilution corrections and calculate BOD.
• The message ”Please wait until DO reading is stable” may appear.
Note: If
appears instead of , the incubation period was less than 24 hours and calculation will not be possible. After pressing the
the message “Repeat Initial
Reading.” appears. If replacing Initial BOD is required then press
otherwise press .
• Remove probe from sample and rinse with purified water. Press to analyze another prepared sample or seed.
The list will reflect the 5 day analysis.
Note: No Seed correction is made in these calculations at this step. This may be made manually by subtracting
the seed concentration from the samples, or made automatically with the meter (see SEED CORRECTION section).
To print a copy of the BOD analysis of the sample:
• Use HI 92000 software to connect the HI 5421 meter.
• Select BOD sample fom available BOD samples.
• Press
to have a paper copy of analysis.
Page 15
15
Language
This option allows the user to choose the desired language in which all informations will be displayed. To select the Language:
• Press
while in
Measure
mode.
• Press
.
• Use
or to select the Language option.
• Press
and use or to highlight the
desired language.
• Press
to confirm your selection and return to the System
Setup menu or press
to return to the System Setup
menu without changing.
Serial Communication
This option allows the user to set the desired speed for the serial communication (baud rate) in bps. The meter and the PC program must have the same baud rate.
To set the Serial Communication:
• Press while in
Measure
mode.
• Press
.
• Use
or to select the Serial Communication
option.
• Press
and use or to highlight the
desired baud rate.
• Press
to confirm your selection and return to the System
Setup menu or press
to return to the System Setup
menu without changing.
Meter Information
This option provides general information about the instrument serial number (each instrument has an unique identification serial number), the software version and the factory calibration date and time.
Note: All instruments are factory calibrated for DO, pressure and temperature. One year after factory calibration,
the warning message “Factory Calibration Expired” will be displayed when powering up the instrument. The instrument will still function, however, it should be taken to the nearest Hanna Customer Service for factory calibration.
42
• With the probe measuring the sample press . The initial DO measurement will be saved.
• Remove probe from sample and fill and cover to prepare bottle for incubation.
• Rinse probe off with purified water. If desired, move probe to next sample. Press
and repeat this procedure on
additional samples and Seed samples.
• At the conclusion of Day 0 the probe should be cleanned and stored and all samples should be incubated following Operational Procedures.
DAY 5 (Final DO)
• Remove samples and Seed samples from the incubator for analysis.
• Press
then select . Calibrate the DO probe.
• Press
then select .
• Press
.
• Press
to access the list of the samples and seeds
available. The seed records will have the symbol “*” displayed before the bottle ID.
• Select the first sample to analyze.
• Press
. The Day 0 analysis of the sample will appear.
• Place the cleaned and calibrated DO probe into the sample selected. The exact technique should follow standard operating procedures.
• Press
. The dissolved oxygen value of the sample
measured is displayed.
Page 16
16
To view the Meter Information:
• Press
while in
Measure
mode.
• Press
.
• Use
or to select the Meter Information option.
• Press
to acces the Meter Information menu.
• Press
to return to the System Setup menu.
Restore Factory Settings
This option allows the user to erase all user settings and reset the instrument to the default factory settings. To restore the Factory Settings:
• Press
while in
Measure
mode.
• Press
.
• Use
or to select the Restore Factory Settings
option.
• Press
to confirm your selection. A pop-up menu will be
displayed, asking for confirmation.
• Press
to confirm your selection and return to the System
Setup or press
to return to the System Setup menu
without restoring defaults.
• Press
to return to
Measure
mode.
Software update
This function allows the user to update instrument software. In order to start the PC upgrade application, you need to select the proper baud rate, the software update package and start the update.
41
Biochemical oxygen demand (BOD) is an indicator for the concentration of biodegradable organic matter present in a sample of water. It can be used to determine the general quality of the water and its degree of pollution. BOD measures the rate of oxygen uptake by microorganisms in a sample of water at a fixed temperature and over a given period of time. To ensure that all other conditions are equal, a very small amount of microorganism seed is added to each sample being tested. This seed is typically generated by diluting activated sludge with deionized water. The samples are kept at 20 °C in the dark and tested for dissolved oxygen (DO) after five days. The loss of dissolved oxygen in the sample, once corrections have been made for the degree of dilution and seed addition, is called the BOD5.
Before running a BOD measurement remember to set the BOD method configuration from the BOD setup menu and make sure the probe has been calibrated in DO mode. Before starting the BOD procedure, calibrate the DO probe (see DO Calibration section).
• Press and then to select BOD measure mode.
• Press
and then
.
• Use or to select
Method Configuration
option.
• Enter the operation limits for this method.
DAY 0 (Initial DO)
• Press
and then followed by
to access the BOD management screen.
Note: The last sample analyzed will appear on the display.
• Press
to add and measure a new sample or
to add and measure a new seed sample.
• Press
then press .
• A field will appear to add ID, a description, bottle volume, seed volume and sample volume.
• Place the DO probe in the sample bottle. Sample should be well mixed. Follow all standard operating procedures.
• Press
.
BOD MEASUREMENT
Page 17
17
DO SETUP
The
DO Setup
menu allows the user to set the parameters related to the DO measurement and calibration.
Accessing DO Setup
• Press
while in
Measure
mode and then to
select the
DO
measure mode.
• Press
and then to access
DO Setup
menu.
To access a DO setup options:
• Use
or to highlight the desired option.
• Press
to access the selected option or to exit
setup.
The following is a detailed description of the
DO Setup
option
screens.
Profile
This option opens the Profile manager. Enabling Profile allows the user to Save, Load or Delete an application Profile. The Profile option allows the user to store up to ten separate profile applications. Each Profile can be named and recalled at a moment’s notice. A profile is a sensor setup complete with measurement units, logging and display preferences, calibration standards, setup of the Display screen for measurement (i.e. graphing, GLP) and any other sensor configuration. Once saved, the exact same profile can be used at another time. This is a handy feature if the meter is used occasionally for additional applications because it saves time in the setup of the meter and ensures the same procedure will be used.
To save the measurement configuration for DO mode:
• Press
then and use or to highlight
Profile
option.
• Press
/ to enable / disable this feature.
The available options are:
Profile Feature:
enable or disable the profile feature.
Save Profile:
save the current profile.
Save Profile As...:
save current profile using a specific name.
Load Profile:
load from available profiles.
Delete Profile:
delete a profile.
40
The meter contains a built-in barometer, and it is able to automatically compensate for changes in barometric pressure. If another pressure value than the barometer’s reading is to be used, then the manual pressure feature must be enabled (See
DO Setup
).
The table below contains a conversion altitude (m) to pressure (mmHg) for the altitude values from the previous table.
edutitlA
)m(
000300600900210051008100120042007200030033006300930004
erusserP
)gHmm(
067237507976456036706485365245225305484764164
Page 18
18
Save Profile
To save a profile:
• Press
while in DO mode.
• Press
.
• Use
or to highlight
Profile
option.
• Press
and then use or to highlight
Save Profile
.
• Press
. The existing configuration will be saved in current
profile.
Save Profile As...
To create a new profile:
• Press
while in DO mode.
• Press
.
• Use
or to highlight
Profile
option.
• Press
and then use or to highlight
Save Profile As...
.
• Press
. The
Text Editor
box will be displayed on the LCD.
• Enter the desired profile name by using
and to highlight the desired character and then
press
to add it to the text bar. It is also possible to delete the last character by positioning the cursor
on the Backspace character (
) and pressing .
• Press
to return to the previous menu. If the
Saving Confirmation
is enabled, press to accept
the modified option,
to escape without saving or to return to the editing mode. Otherwise,
the modified option is saved automatically.
Note: The saved profile will automatically become the current profile.
Load Profile
To load one profile:
• Press
while in DO mode.
• Press
.
• Use
or to highlight the
Profile
option.
• Press
and then use or to highlight
the
Load Profile
option.
39
BAROMETRIC PRESSURE COMPENSATION
The dissolved oxygen saturation value varies with pressure, so it is important to compensate the effect that pressure has on DO measurements.
leveLaeSevobasreteM,edutitlA
0m003m006m009m0021m0051m0081m0012m0042m0072m0003m0033m0063m0093m0004
m
06.411.416.311.316.211.217.112.118.014.010.017.93.90.99.80.23
28.313.318.214.219.115.110.116.012.019.95.92.98.85.84.86.53
41.316.212.217.113
.119.015.011.017.93.90.97.84.80.89.72.93
64.210.215.111.117.013.019.96.92.99.86.82.89.76.75.78.24
88.114.110.116.012.018.95.91.98.84.81.88.75.73
.72.74.64
013.119.015.011.017.94.90.97.84.81.88.75.72.79.68.60.05
218.014.010.016.93.99.86.83.80.87.74.71.79.66.65.66.35
413.019.96.92.99.85.82.89
.76.74.71.78.66.63.62.62.75
619.95.92.98.85.82.89.76.73.70.78.65.63.61.60.68.06
815.91.98.85.81.88.76.73.70.78.65.63.60.68.57.54.46
021.98.84.81.88.75
.73.70.77.65.62.60.68.56.55.50.86
227.84.81.88.75.72.70.77.65.62.60.68.56.54.53.56.17
424.81.88.75.72.70.77.65.62.60.68.56.54.52.51.52.57
523.80.87.74
.71.78.66.64.61.69.57.55.53.51.50.50.77
621.88.75.72.70.77.65.62.60.68.56.54.52.50.59.48.87
828.75.73.70.77.65.62.60.68.56.54.52.50.58.47.44.28
036.73
.70.78.65.63.60.68.56.54.52.50.58.46.46.40.68
233.70.78.65.63.61.68.56.54.52.50.58.47.45.44.46.98
431.78.66.63.61.69.56.54.52.50.59.47.45.43.43.42.39
638.66.63.61.69.57.55.53.51.59.47.45.44.42.41.48.69
836.64.61.69.57.55.53.51.59.47.45.44.42.41.40.44.001
044.62.69.57.55.53.51.59.47.46.44.42.41.49.39
.34.401
242.60.68.56.53.52.50.58.46.44.43.41.40.48.38.36.701
440.68.56.54.52.50.58.46.45.43.41.40.48.37.37.32.111
648.56.54.52.50.58.47.45.43.42.40.
49.37.36.35.38.411
847.55.53.51.59.47.45.44.42.40.49.37.36.35.34.34.811
055.53.51.59.47.46.44.42.41.49.38.36.35.34.33.30.221
Page 19
19
Delete Profile
To delete one of the existing profiles:
• Use
or to highlight the
Profile
option.
• Press
and then use or to highlight
the
Delete Profile
option.
• Press
.
A list with all customised profiles will appear on
the screen.
• Use
or to select the desired profile and press
.
• Press
to return to previous menu.
Reading Mode
This option allows the user to select between
Direct or Direct/AutoHold
DO reading modes.
To set the reading mode:
• Press while in DO mode.
• Press
.
• Use
or to highlight the
Reading Mode
option.
• Press
or as desired.
• Press
to return to previous menu.
• Press
.
A list with all customized profiles will be displayed on the screen.
• Use
or to select the desired profile and press
to
confirm or
to exit without
selecting.
38
SALINITY COMPENSATION
If the sample contains significant concentration of salinity, the read out values must be corrected, taking into account the lower degree of oxygen solubility in this situation. Before taking any DO measurements remember to set the salinity value from the DO setup menu. The salinity affects the DO concentration, decreasing its value. The table below shows the maximum oxygen solubility at various temperatures and salinity levels.
leveLaeSta)l/g(ytinilaS
l/g0l/g01l/g02l/g03l/g53
006.4146.3147.2109.1105.110.23
218.3119.2170.2192.1119.015.63
490.3152.2174.1137.0183.012.93
644.2156.111
9.0122.0198.98.24
838.1190.1104.0157.944.94.64
0182.1185.0139.923.930.90.05
2177.0111.0105.929.856.86.35
4192.0186.901.955.803.82.75
6168.982.937.812.879.78.06
8154.909.893.809.766.74.46
0280.965.870.806.783.70.86
2237.832.877.733.721.76.17
4204.839.794.770.778.62.57
5
242.897.763.759.657.60.77
6290.856.732.738.646.68.87
8218.783.789.616.624.64.28
0345.741.757.693.622.60.68
2392.709.645.691.630.66.98
435
0.786.633.610.658.52.39
6328.674.641.638.586.58.69
8316.682.669.566.515.54.001
0414.690.697.505.563.50.401
2422.639.536.553.522.56.701
4440.677.584.512.590.52.111
6478.516.533.570.579.48.411
8407.574.502.559.458.44.811
0545.533.570.538.457.40.221
Note: The relationship between salinity and chlorinity for sea water is given by the equation below:
Salinity (g/l) = 1.80655 Chlorinity (g/l)
Page 20
20
Temperature Unit
The user can choose from
Celsius, Fahrenheit
or
Kelvin
temperature units.
To set the
Temperature Unit
:
• Press
while in DO mode.
• Press
.
• Press
and then use or to highlight
the
Temperature Unit
option.
• Press
and then use or to select
Celsius, Fahrenheit
or
Kelvin
unit.
• Press
to confirm your selection or press to
cancel operation.
Calibration
This selection allows configuration of options pertaining to calibration.
Standard Recognition
The user can choose between
Automatic
recognition (using 2 standards) or
User Standard
(a single point
calibration).
• Press
while in DO mode.
• Press
.
• Use
or to highlight the
Standard Recognition
option.
• Press
or as desired
.
• Press to return to previous menu.
37
Make sure the instrument has been calibrated before taking DO measurements.
DIRECT MEASUREMENT
To measure the DO of a sample using the Direct reading mode:
• Press
and then to select DO measure
mode.
• Select the
Direct
reading mode (see DO
Setup
).
• Submerge the DO probe and allow time for the reading to stabilize.
• The measured DO value will be displayed together with the temperature and pressure values.
Notes: • For accurate DO measurements, a water movement of
0.3 m/s is required. This is to ensure that the oxygen-depleted membrane surface is constantly replenished. A moving stream will provide adequate circulation.
• If the reading is out of range, “-----” will be displayed.
DIRECT/AUTOHOLD MEASUREMENT
To measure DO of a sample using the Direct/AutoHold reading mode:
• Select the
Direct/AutoHold
reading mode (see DO
Setup
).
• If pressing
, the “AutoHold” indicator will start
blinking on the display until the stability criterion is reached. The DO value will be frozen on the display, along with “AutoHold” indicator.
• To return to normal measure mode press
.
DO MEASUREMENT
Page 21
21
Calibration Reminder
This option allows the user to set the calibration reminder as
Daily, Periodic
or
Disabled
.
To set the calibration reminder:
• Press
while in DO mode.
• Press
.
• Use
or to highlight the
Calibration
option.
• Use
or to highlight the
Calibration
reminder
option.
• Press
to confirm your selection and then use
or to choose the desired option
.
• Press to confirm your selection or press to cancel operation.
Set Reminder Period
Daily
reminder - the user can set the time from the day when the reminder is to appear.
Periodic
reminder - the user can set the time from the last calibration (days, hours and minutes) after which the
reminder appears.
To set the reminder period:
• Press
while in DO mode.
• Press
.
• Use
or to highlight the
Calibration
option.
• Use
or to highlight the
Set Reminder Period
option.
• Press
and use / to select next /
previous entry to be edited.
• Press
and use or to set the desired
value, then press
to save the modified value or press
to cancel operation.
• Press
to return to previous menu.
36
PRESSURE CALIBRATION
If
Automatic
pressure source is chosen from the
Pressure Source
menu (see
DO Setup
), a pressure calibration at
one point can be performed. To perform pressure calibration:
• Press to clear the current calibration;
• Use
or to modify the pressure value;
• Press
to finish the calibration or to exit
calibration.
Note: Use a reference pressure measurement if calibrating meter’s
sensor.
When the user standard is selected:
• The calibration can be performed at one value.
• Edit the desired standard value by using and then .
• Press
again to finish the calibration or to exit calibration.
Page 22
22
Measurement Unit
The user can select the desired measurement unit. The available options are:
% Sat, mg/L
or
ppm
. % Saturation is correct for any solvent measurement of dissolved oxygen. mg/L and ppm are used for concentration measurement in water only.
• Press
while in DO mode.
• Press
.
• Use
or to highlight the
Measurement Unit
option.
• Press
.
• Use
or to select
% Sat
or
mg/L
or
ppm
.
• Press
to confirm your selection or press to
cancel operation.
Clear Calibration
Accessing this option, the existent DO calibration can be cleared. If the calibration is cleared a default meter calibration is used. Another sensor calibration should be performed. To clear calibration:
• Press while in DO mode.
• Press
.
• Use
or to highlight the
Calibration
option.
• Use
or to highlight the
Clear Calibration
option.
• Press
. A pop-up menu will be displayed asking for confirmation (if calibration is available).
• Press
to confirm or press to escape without saving and return to the
Calibration
options.
35
Note: When not in use and during polarization, use the protective transparent cap.
To calibrate the DO probe with meter: When the automatic standard recognition is selected:
• Use HI 7040 Zero Oxygen solution for 0% calibration
(freshly prepared).
• Rinse polarized DO probe with clean water. Dry tip and allow measurement to stabilize on meter.
Procedure:
• Suspend probe with membrane just over beaker of water for calibration in 100% Saturation.
• Press
and wait for “Stable“ to appear on display.
Display will be in % Saturated for calibration.
•“% Sat 100” should appear on display.
• Press .
• Place probe in beaker of HI 7040 Zero Oxygen solution. “% Sat 0.0” will appear on display. Wait until “Stable“ appears.
• Press
.
Note: A single point calibration can also be made. Press after first standard.
Page 23
23
Barometer
This parameter allows configuration of parameters related to barometric pressure. This parameter is only needed when measuring in concentration units of mg/L or ppm. From the
Barometer
menu the user can choose the pressure source and units, as well as the pressure.
To access a
Barometer
option:
• Press
while in DO mode.
• Press
.
• Use
or to highlight the
Barometer
option from the
DO Setup
menu.
• Press
to access the
Barometer
option.
Pressure Source
The user can choose between
Manual
and
Automatic
pressure source.
If using
Automatic
, the meter uses a pressure sensor located inside the meter. To set the
pressure source:
• Select
or using virtual key.
• Press
to confirm selection. Note: If
Manual
pressure source is chosen, the pressure value used
to compute is set manually. If
Automatic
pressure source is chosen, the meter uses a measurement from the pressure sensor located in the meter. This sensor can be calibrated (see
Pressure Calibration
).
Pressure
Use to set Manual pressure value or calibrate the interrnal pressure sensor used when Automatic is selected under
Pressure Source
.
Note: Select
Pressure unit
first (see on the next page).
To set the pressure:
• Press while in DO mode.
• Press
.
• Use
or to highlight the
Barometer
option
from the
DO Setup
menu.
• Use
or to highlight the
Pressure
option.
• Press
and then use
or to increase /
decrease the value.
• Press
to save or press
then
to remove
previous calibration.
34
DO CALIBRATION
It is recommended to calibrate the probe frequently, especially if high accuracy is required. The DO probe should be recalibrated:
• Whenever the DO probe is replaced.
• At least once a week.
• Before BOD, OUR, SOUR measurements.
• When calibration reminder is activated (“DO Cal Expired”).
• If the readings are far from the calibration point.
Note: BOD, OUR and SOUR readings are automatically derived from the DO readings. Calibrate in DO mode.
The following options are available for the Dissolved Oxygen calibration:
• Two point calibration at 100 and 0% Saturation.
• Single point at 0% Saturation.
• Single point at 100% Saturation.
• Single point user calibration using a standard value set by the user in % saturation, mg/L or ppm. When automatic calibration is performed it is assumed that the standard value is 100% water saturated air and 0% Saturated solution. When a user calibration is performed it is assumed that the standard value is the DO value at the current pressure, temperature and salinity.
Initial preparation
Make sure the probe is ready for measurements, i.e. the membrane is filled with electrolyte and the probe is connected to the meter and polarized. For an accurate calibration, it is recommended to wait for at least 15 minutes to ensure precise conditioning of the probe. Remove the protective cap from the DO probe. Make sure the salinity value has been set to the salinity of the standard if user concentration standard is employed.
Probe conditioning
The probe is polarized with a fixed voltage of approximately 800 mV between the cathode and anode. Probe polarization is essential for stable measurements. With the probe properly polarized, oxygen is continually consumed as it passes through gas permeable PTFE membrane. If polarization is interrupted, the electrolyte solution continues to be enriched with oxygen until it reaches an equilibrium with the surrounding solution. Whenever measurements are taken with a non-polarized probe, the measurement will be drifty and inaccurate. The measurement will jump when the probe is moved.
Page 24
24
Pressure Units
The user can choose from six pressure units:
mmHg, mbar, kPa
,
inHg, psi
or
atm
.
To set the Pressure Unit:
• Press
while in DO mode.
• Press
.
• Use
or to highlight the
Barometer
option
from the
DO Setup
menu.
• Use
or to highlight the
Pressure Units
option.
• Press
and then use or to select the
desired units
.
• Press to confirm your selection or press to cancel operation.
Salinity
This parameter permits selection of measurement unit and value. Salinity Compensation is used when using DO concentration measurements (mg/L or ppm). Oxygen solubility decreases when water contains salt.
Note: Select salinity unit before setting
Sample Value
.
To edit the Sample
Salinity
:
• Press
while in DO mode.
• Press
.
• Use
or to highlight the
Salinity
option from
the
DO Setup
menu.
• Use
or to highlight
Salinity
.
• Press
and then use
or to increase /
decrease the value.
• Press
to save or press
to cancel operation.
To select
Salinity Unit
:
The user may select from three units:
%, g/L
or
PSU
.
• Use
or to highlight the
Salinity
option from
the
DO Setup
menu.
33
Barometer - see
DO Setup
section.
Salinity - see
DO Setup
section.
Sample ID - see
DO Setup
section.
Log - see
DO Setup
section.
Alarm - see
DO Setup
section.
The SOUR Setup menu allows the user to set the parameters related to SOUR measurement.
Accessing SOUR Setup
• Press while in
Measure
mode and then to select
SOUR
mode.
• A pop up message appears to remind user to set method configuration. Press
to continue.
• Press
and then
to access
SOUR Setup
menu.
To access a
SOUR Setup
option:
• Use
or to highlight the desired option.
• Press
to access the selected option.
The following is a description of the
SOUR Setup
options.
Profile - see
DO Setup
section.
Temperature - see
DO Setup
section.
Measurement Unit - only concentration units are available (
mg/L
or
ppm
). See
DO Setup
section.
Method Configuration
This option allows the user to edit the SOUR method configuration. To edit the options:
• Highlight the
Method Configuration
option and then press
.
• Use or to select the parameter and then press
.
• Use
or to increase / decrease the parameter
value, then press
to save the change. Use or
to move to each parameter. When finished editing
select
and all changes will be saved.
SOUR SETUP
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• Use or to highlight the
Salinity Unit
option.
• Press
and then use or to select the desired units
.
• Press to confirm your selection or press to cancel operation.
Edit Sample ID
This option allows the user to enter a ten character sample ID. If ID increment is
None
, a Text Editor screen is
displayed. If ID increment is
Automatic
, a Numeric Editable screen is displayed.
To access the Edit Sample ID:
• Press
while in DO mode.
• Press
.
• Use
or to highlight
Edit Sample ID
.
Note: ID increment is None.
• Press
and use or to highlight the
Edit
Sample ID
option.
• Press
. The Text Editor appears.
Sample ID
This option allows the user to assign an identification number/name to sample logs. Two
Sample ID
parameters
are available:
ID Increment
mode and
Edit Sample ID
.
ID Increment
Choose
None
to identify a sample with a text tag.
Choose
Automatic
to identify a sample with a numeric tag. This number will be incremented by one for each new lot log but it can also be altered manually here. This number does not increment for each manual log sample. This will be automatically incremented when a New Lot is selected. To select the ID increment mode:
• Press
while in DO mode.
• Press
.
• Use
or to highlight the
Sample ID
option.
Press
.
• Use or to highlight the
ID Increment
option.
• Press
or
as desired.
• Press
to return to previous menu.
32
Barometer - see
DO Setup
section.
Salinity - see
DO Setup
section.
Sample ID - see
DO Setup
section.
Log - see
DO Setup
section.
Alarm - see
DO Setup
section.
OUR SETUP
The OUR Setup menu allows the user to set the parameters related to the OUR measurement.
Accessing OUR Setup
• Press
while in
Measure
mode and then to
select OUR mode.
• A pop up message will appear to remind user to configure the method configuration. Press
to continue.
• Press
and then
to access
OUR Setup
menu.
To access a OUR Setup option:
• Use
or to highlight the desired option.
• Press
to access the selected option.
The following is a description of the OUR Setup option screens. Profile - see
DO Setup
section.
Temperature Unit - see
DO Setup
section.
Measurement Unit - only concentration units are available (
mg/L
or
ppm
). See
DO Setup
section.
Method Configuration
This option allows the user to edit the OUR method configuration that will be used for calculation. To edit the options:
• Highlight the
Method Configuration
option and then press
.
• Use or to select the parameter and then press
.
• Use
or to increase / decrease the parameter
value, then press
to save the change. Use or
to move to each parameter. When finished editing
select
and all changes will be saved.
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26
• For text editing use and to highlight the desired character and then press
to add it to the text bar. It is also possible to delete the last character by positioning the cursor on the Backspace character (
) and pressing .
• Press
to return to
Sample ID
option. If the
Saving
Confirmation
is enabled, press to accept the modified
option,
to escape without saving, or to return to the editing mode. Otherwise, the modified options are saved automatically.
• For numeric editing (ID Increment Automatic) use
or
keys.
• Press
to save the current value or press
to cancel operation.
Stability criteria
This parameter permits the user to select a signal stability criteria for the measurement. (Stable tag appears on display.)
-
Fast
- permits quicker less accurate results, the measurement may still be changing.
-
Medium
-
Accurate
- may take longer for the Stability tag to appear but it will produce the greatest accuracy.
To select the Stability Criteria mode:
• Press
while in DO mode.
• Press
.
• Use
or to highlight
Stability Criteria
.
• Press
and use or to highlight the
desired option.
• Press
to save the current value or press
to
cancel operation.
31
Barometer - see
DO Setup
section.
Salinity - see
DO Setup
section.
Sample ID - see
DO Setup
section.
Log - see
DO Setup
section.
Alarm - see
DO Setup
section.
The BOD Setup menu allows the user to set the parameters related to the BOD measurements.
Accessing BOD Setup
A pop up message appears to remind user to set method configuration. Press
to continue.
• Press
while in
Measure
mode and then to select
BOD
mode.
• Press
and then to access
BOD Setup
menu.
To access a
BOD Setup
option:
• Use
or to select the desired option.
• Press
to confirm your selection.
The following is a description of the BOD Setup option screens. Profile - see
DO Setup
section.
Temperature Unit - see
DO Setup
section.
Measurement Unit - only concentration units (mg/L or ppm) are available. See
DO Setup
section.
Method Configuration
This option allows the user to edit the BOD method configuration. To edit the options:
• Press
and then to access
BOD Setup
menu.
• Highlight the
Method Configuration
option and then press
.
• Use or to select the parameter and then press .
• Use
or to increase / decrease the parameter
value then
to save.
• Press
to return to the previous screen.
BOD SETUP
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27
Logging Data Configuration
This option allows the user to select which parameters will accompany a log File:
Date/Time, Calibration
Data, Sample ID, Instrument ID, Operator ID, Company Name, Additional Info 1 and Additional Info 2
.
To set the Logging Data Configuration:
Log
Note: See Logging section for available types of logging. This option allows the user to edit the log settings:
Logging Type, Logging Data Configuration, Sampling Period
and
New Lot
.
Logging Type
Three logging types are available:
Automatic, Manual
and
Auto Hold
.
Automatic
- the measurement data is logged automatically at constant time intervals.
Manual
- a snapshot of the displayed measurement data is logged with time stamp when the user manually depresses Log.
Auto Hold
- this is configured along with the
Direct/AutoHold
reading mode to take a snapshot of stable
measurement data. Press
to initiate a logging session. Press to initiate an Auto Hold event. The log occurs automatically once measurement stability is reached. This type log removes subjective data, as it only captures stable measurements.
To set the Logging Type:
• Press
while in DO mode.
• Press .
• Use
or to highlight the
Log
option.
• Press
and use or to highlight the
Logging Type
option.
• Press
and use or to highlight the
desired option.
• Press
to confirm your selection or press to
cancel operation.
30
Alarm Limits
This option allows the user to set the alarm limits for the measured value. Note: The Alarm High value can not be lower than the Alarm Low value.
• Press
while in DO mode.
• Press
.
• Use
or to select the
Alarm
option.
• Press
and use or highlight the
Alarm
Limits
option.
• Press
and then use or to set the
desired value, then press
to save the modified value or
press
to cancel operation.
• Press
return to the
Alarm
options.
• Press
and use or highlight the
Alarm State
option.
• Press
and use or to highlight the desired option.
• Press
to confirm your selection or press
to cancel operation.
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• Press while in DO mode.
• Press .
• Use
or to highlight the
Log
option.
• Press
and use or to highlight the
Logging Data Configuration
option.
• Press
and use or to highlight the
desired parameter to be logged in file.
• Press
to enable the parameter or to disable it.
• Press
to return to previous menu.
Sampling Period
This option allows the user to select the desired sampling period for automatic logs. To set the Sampling Period:
• Press while in DO mode.
• Press
.
• Use
or to highlight the
Log
option.
• Press
and use or to highlight the
Sampling Period
option.
• Press
and use or to select the desired option.
• Press
to confirm your selection or press to
cancel operation.
29
New Lot
This option is used to create a new lot when manual logging is used. Note: If
New Lot
option is accessed and the
Logging Type
is
Automatic
, a warning message appears on the LCD informing
the user that a new lot can be created only if the
Logging
Type
is set as
Manual
.
To generate a New Lot:
• Press
while in DO mode.
• Press
.
• Use
or to select the
Log
option.
• Press
and use or to highlight the
New Lot
option.
• Press
to generate a new manual lot. A pop-up menu
will be displayed asking for confirmation.
• Press
to confirm or press to escape without saving and return to the
Log
options.
Alarm
This option allows the user to select the alarm settings:
Alarm State
and
Alarm Limits
. If the
Alarm
option
is enabled, a continuous double beep will be heard, along with the “Alarm” indicator blinking on the LCD, each time the set limits in
Measure
mode are exceeded.
Note: Alarm Beeper must be set On for audible beep to be heard. See:
System Setup
Beeper
Alarm
.
Alarm State
Three settings are available for the Alarm State option:
Disabled
- the alarm will be disabled.
Inside Limits
- the alarm state will trigger when the measured
value is inside the set limits.
Outside Limits
- the alarm state will trigger when the measured value is outside the set limits.
To set the Alarm State:
• Press while in DO mode.
• Press
.
• Use
or to select the
Alarm
option.
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