Hanna Instruments HI 4321 User Manual
Instruction Manual
HI 4321
Conductivity/Resistivity/TDS/Salinity/
Temperature
Bench Meter
www.hannainst.com
1
Dear Customer,
Thank you for choosing a Hanna Instruments product. This manual will provide you with the necessary
information for correct use of the instrument.
Please read this instruction manual carefully before using the instrument.
If you need additional technical information, do not hesitate to e-mail us at tech@hannainst.com or see the
back side of this manual for our worldwide sales and technical service contacts.
These instruments are in compliance with
HI 4321 is warranted for two years against defects in workmanship and materials when used for their
intended purpose and maintained according to instructions. The probe is guaranteed for six months. This
warranty is limited to repair or replacement free of charge.
Damage due to accidents, misuse, tampering or lack of prescribed maintenance is not covered.
If service is required, contact the dealer from whom you purchased the instrument. If under warranty, report
the model number, date of purchase, serial number and the nature of the failure. If the repair is not covered
by the warranty, you will be notified of the charges incurred. If the instrument is to be returned to Hanna
Instruments, first obtain a Returned Goods Authorization number from the Technical Service Department and
then send it with shipping costs prepaid. When shipping any instrument, make sure it is properly packed for
complete protection.
To validate your warranty, fill out and return the enclosed warranty card within 14 days from the date of
purchase.
directives.
WARRANTYWARRANTY
WARRANTY
WARRANTYWARRANTY
2
TABLE OF CONTENTSTABLE OF CONTENTS
TABLE OF CONTENTS
TABLE OF CONTENTSTABLE OF CONTENTS
WARRANTY ...................................................................................................................................... 2
PRELIMINARY EXAMINATION .............................................................................................................. 4
GENERAL DESCRIPTION ...................................................................................................................... 4
FUNCTIONAL DESCRIPTION ................................................................................................................ 5
SPECIFICATIONS ................................................................................................................................ 7
OPERATIONAL GUIDE ....................................................................................................................... 9
DISPLAYING MODES ......................................................................................................................... 10
SYSTEM SETUP ............................................................................................................................... 13
CONDUCTIVITY SETUP ......................................................................................................................... 19
RESISTIVITY SETUP ............................................................................................................................. 34
TDS SETUP .............................................................................................................. 36
SALINITY SETUP .............................................................................................................. 38
CONDUCTIVITY CALIBRATION.................................................................................. 40
CONDUCTIVITY MEASUREMENT.................................................................................. 42
RESISTIVITY MEASUREMENT .................................................................................. 45
TDS MEASUREMENT ............................................................................................... 46
SALINITY CALIBRATION .................................................................................. 47
SALINITY MEASUREMENT .................................................................................. 48
TEMPERATURE CALIBRATION .................................................................................. 50
LOGGING ....................................................................................................................................... 51
PC INTERFACE .................................................................................................................................... 56
PROBE CONDITIONING & MAINTENANCE ..................................................................................... 56
TROUBLESHOOTING GUIDE .............................................................................................................. 57
ACCESSORIES .................................................................................................................................. 58
3
PRELIMINARY EXAMINATIONPRELIMINARY EXAMINATION
PRELIMINARY EXAMINATION
PRELIMINARY EXAMINATIONPRELIMINARY EXAMINATION
Remove the instrument from the packing material and examine it carefully to make sure that no damage has
occurred during shipping. If there is any damage, notify your dealer or the nearest Hanna Service Center.
The meter is supplied complete with:
• HI 76312 Four-ring Conductivity Probe with built-in temperature sensor and ID
• HI 76404N Electrode Holder
• 12Vdc Power Adapter
• Instruction Manual
HI 4321 is supplied with 12 Vdc/230 Vac adapter.
HI 4321-01 is supplied with 12 Vdc/115 Vac adapter.
Note: Save all packing material until you are sure that the instrument works properly. Any defective item
must be returned in the original packing with the supplied accessories.
GENERAL DESCRIPTIONGENERAL DESCRIPTION
GENERAL DESCRIPTION
GENERAL DESCRIPTIONGENERAL DESCRIPTION
HI 4321 is a professional bench meter with color graphic LCD for conductivity, resistivity, TDS, salinity and
temperature measurements.
The display viewing modes are: Basic information only, GLP information, Graph and Log History mode.
The main features of the instruments are:
• One input channel;
• Five measurement parameters: conductivity, resistivity, TDS, salinity and temperature;
• Pure water checking using the USP <645> standard;
• Automatic or custom standard conductivity calibration in up to four points, probe offset calibration;
• One fixed point salinity calibration (Percent Scale only);
• AutoHold feature to freeze the stable reading on the LCD;
• Two selectable alarm limits (for conductivity, resistivity, TDS, salinity);
• Three selectable logging modes: Automatic logging, Log on demand (manual logging) and AutoHold logging
mode;
• Up to 100 logging lots for automatic or manual modes and up to 200 USP reports;
• Selectable area and settable sampling period feature for automatic logging;
• GLP feature;
• Online and offline graph;
• User-friendly interface on large color graphic LCD (240x320 pixels);
• Opto-isolated PC interface via RS232 respectively USB.
4
HI 4321 DESCRIPTION
FRONT PANEL
REAR PANEL
FUNCTIONAL DESCRIPTIONFUNCTIONAL DESCRIPTION
FUNCTIONAL DESCRIPTION
FUNCTIONAL DESCRIPTIONFUNCTIONAL DESCRIPTION
1) Liquid Crystal Display (LCD)
2) Main Keyboard
3) USB connector
4) ON/OFF switch
5) Power adapter socket
6) RS232 serial communication connector
7) Conductivity probe input
5
KEYBOARD DESCRIPTION
FUNCTION KEYS
To enter / exit calibration mode.
To select the desired measurement mode: Conductivity, Resistivity, TDS, Salinity.
To enter Setup (System Setup, Conductivity Setup, Resistivity Setup , TDS Setup or Salinity
Setup) and to access Log Recall function.
To obtain general informations about the selected option / operation.
VIRTUAL KEYS
The upper row keys are assigned to the virtual keys placed on the bottom of the LCD, which allow you to
,
perform the displayed function, depending on the current menu (e.g.
Measure
mode).
and in
LCD GENERAL DESCRIPTION
6
SPECIFICATIONSSPECIFICATIONS
SPECIFICATIONS
SPECIFICATIONSSPECIFICATIONS
1234IH
mc/Sµ999.9ot000.0
egnaR
noituloseR
ycaruccA)mc/Sµ10.0±(gnidaerfo%1±
ytivitcudnoC
ytivitsiseR
SDT
tnatsnoclleC00.002ot0050.0
epytlleCsllec4,2
stniop/epytnoitarbilaC
rednimernoitarbilaCseY
noitasnepmocerutarepmeTdelbasiD/)retawlarutan(raenilnoN/raeniL
tneiciffeocerutarepmeTC°/%00.01ot00.0
erutarepmetecnerefeRC°0.03otC°0.51
seliforP01otpU
tnailpmocPSUseY
egnaR
noituloseR
ycaruccA)mcxmhO1±(gnidaerfo%2±
egnaR
noituloseR
ycaruccA)mpp10.0±(gnidaerfo%1±
mc/Sµ99.99ot00.01
mc/Sµ9.999ot0.001
mc/Sm999.9ot000.1
mc/Sm99.99ot00.01
mc/Sm0.0001ot0.001
mc/Sµ100.0
mc/Sµ10.0
mc/Sµ1.0
mc/Sm100.0
mc/Sm10.0
mc/Sm1.0
dradnatsresU,noitingocerdradnatsotuA
noitarbilactnioPitluM/tnioPelgniS
mcxsmhO9.99ot0.1
mcxsmhO999ot001
mcxsmhOK99.9ot00.1
mcxsmhOK9.99ot0.01
mcxsmhOK999ot001
mcxsmhOM99.9ot00.1
mcxsmhOM0.001ot0.01
mcxsmhO1.0
mcxsmhO1
mcxsmhOK10.0
mcxsmhOK1.0
mcxsmhOK1
mcxsmhOM10.0
mcxsmhOM1.0
mpp999.9ot000.0
mpp99.99ot00.01
mpp9.999ot0.001
tpp999.9ot000.1
tpp99.99ot00.01
tpp0.004ot0.001
mpp100.0
mpp10.0
mpp1.0
tpp100.0
tpp10.0
tpp1.0
)rotcaf00.1htiw(SDTlautca
7
1234IH
elacSytinilaSlacitcarP
usp00.24ot00.0
egnaR
ytinilaS
noituloseR
ycaruccAgnidaerfo%1±
noitarbilaC
egnaR
erutarepmeT
draobyeK)syeklautriv4(syek8
PLG
dloH-otuAseY
erutaefgniggoL
DCLslexip023x042DCLcihparGroloC
thgilkcaB)revasthgilkcabelbatteshtiw(seY
stupnINIDnip8
stuptuOBSU,232SR
rewoPretpadacdV21
snoisnemiD)"7.3x1.9x3.6(mm49x132x061
thgieW)bl6.2(gK2.1
seirosseccA
noituloseRK1.0/F°1.0/C°1.0
ycaruccA
noitarbilacresUnoitarbilacstniop3
noitacilppaCPseY
selpmasdroceRtol/sdrocer00001htiwstol001
lavretnigniggoLemitgolxamdnas1neewtebelbatteS
epyTdloHotuA,dnamednogoL,citamotuA
noitazinitalpeRseY
sdradnatsdetnemelpmI3,2,1egatsPSU
noitingocereborPseY
noitulosnoitarbilacCE
retaW
elacSretaWaeSlarutaN
tpp00.08ot00.0
elacStnecreP
%0.004ot0.0
aeSlarutaN/elacSytinilaSlacitcarProf10.0
elacStnecreProf%1.0
tniop1-elacStnecreP
)reffub7307IHhtiw(
C°0.021ot0.02-
F°0.842ot0.4-
K51.393ot51.352
K2.0±/F°4.0±/C°2.0±
)eborptuohtiw(
,tneiciffeoc/.pmet.fer,tnatsnoclleC
tesffoeborp,pmatsemit.lac,stniopnoitarbilac
,mc/Sm00.5,mc/Sµ3141,mc/Sµ0.48
mc/Sm8.111,mc/Sm0.08,mc/Sm88.21
)Sµ005ot0,tsnocllec1.0(eborpllec2
)egnarediwtnatsnocllec0.1(eborpllec4
)gnikcehcegnarwolroftesrotsiser,llecwolf(tikPSU
8
OPERATIONAL GUIDEOPERATIONAL GUIDE
OPERATIONAL GUIDE
OPERATIONAL GUIDEOPERATIONAL GUIDE
POWER CONNECTION
Plug the 12 Vdc adapter into the power supply socket.
Note: These instruments use non volatile memory to retain the meter settings, even when unplugged.
PROBE CONNECTION
For conductivity, resistivity, TDS or salinity measurements connect a conductivity probe to the DIN connector
located on the rear panel of the instrument.
INSTRUMENT START UP
• Turn the instrument on from the power switch located on the rear panel of the instrument.
• Please wait until the instrument finishes the initialization process.
Note: It is normal for the loading process to take a few seconds. If the instrument doesn’t display the next
screen, restart the meter using the power switch. If the problem persists, contact your dealer.
9
DISPLAYING MODESDISPLAYING MODES
DISPLAYING MODES
DISPLAYING MODESDISPLAYING MODES
For each measurement mode (Conductivity, Resistivity, TDS or Salinity) the following display configurations
are available: Basic, Good Laboratory Practice (GLP), Graph and Log History.
Basic
Accessing this option, the measured value and its units are displayed on the LCD, along with the temperature value, temperature
compensation mode, and minimal GLP data.
To choose the Basic displaying mode:
• Press
Configuration” message will be displayed in the Reminder
messages area.
• Press
tion for the selected measurement mode.
GLP
Accessing this option, a detailed GLP data will be displayed on the
LCD for conductivity and salinity (Percent Scale only)
modes: Last Calibration Date and Time, Cell Constant, Probe
Offset, Reference Temperature, Compensation Coefficient, Temperature Compensation.
To access the GLP displaying mode:
• Press
Configuration” message will be displayed in the Reminder
messages area.
• Press
data.
while in
. The instrument will display the basic informa-
while in
. The instrument will display the detailed GLP
Measure
mode. The “Choose Display
Measure
mode. The “Choose Display
measure
10
Graph
Accessing this option, the online graph with currently logged
values (Conductivity, Resistivity, TDS or Salinity vs. Seconds)
could be displayed.
If there is no active log, the previously logged data for the
selected parameter will be plotted.
Notes: • If no data were logged, the graph displaying mode
will not be accessible.
• If no automatic log is saved, the offline graph will not
be available.
To access the offline / online graph:
• Press
Configuration” message will be displayed in the Reminder
messages area.
• Press
When the online graph is displayed:
• Use and to move the graph along the horizontal (
• Press to access the zoom menu for the vertical (
vertical axis zooming.
• Press
When the offline graph is displayed:
• Use the arrow keys to move the graph along the horizontal and vertical axes.
• Press
to zoom the selected axis.
Note: While in zoom graph menu the
• Press
while in
.
Measure
mode. The “Choose Display
Time
Parameter
to return to the main menu.
to access the zoom menu for the horizontal and vertical axes. Use or /
/ / to switch between the active zooming axes. Press or
key is not accessible.
to return to the main menu.
) axis. Use or for
) axis.
11
Log History
Accessing this option, last logged records will be displayed on the LCD.
The log history list also contains the appropriate conductivity /
resistivity / TDS / salinity values, the logged temperature, the
temperature source, as well as the records time stamp.
To access the Log History displaying mode:
• Press
Configuration” message will be displayed in the Reminder
messages area.
• Press
regarding the selected measure mode.
Notes: • When an alarm condition is active, the logged records will have an exclamation mark (!).
• When a meter is in auto-hold, the logged records will have an “H” symbol.
• If another measure mode is selected, the Log History will be cleared.
• If the temperature unit is changed, all logged temperature values will be automatically displayed
while in
in the new temperature unit.
Measure
mode. The “Choose Display
. The instrument will display the log history
12
SYSTEM SETUPSYSTEM SETUP
SYSTEM SETUP
SYSTEM SETUPSYSTEM SETUP
The System Setup menu allows the user to customize the user interface, consult the meter information, set the
external serial communication interface and to restore the manufacturer settings.
Accessing System Setup
• Press
while in
Measure
mode.
• Press
on the LCD.
To access a System Setup option:
• Use
• Press
The following is a detailed description of the System Setup option screen.
Beeper
This option allows the user to enable or disable the beeper. When the beeper is enabled, a specific beep will
be heard when the reading becomes stable, when an alarm condition is reached,
a wrong key is pressed.
. The system setup options will be displayed
or to highlight the desired option.
to access the selected option.
when pressing a key or if
Stability Indicator
When the reading becomes stable, the instrument delivers a medium beep only if this option is activated, along
with the “Stable” indicator on the LCD.
Alarm
If this option is activated, a continuous double beep will be heard each time the set limits in
exceeded, along with the “Alarm” indicator on the LCD.
Key Pressed
If this option is activated, a short beep will be heard each time a valid key is pressed.
Wrong Key
If this option is activated, a long beep will be heard when an incorrect key is pressed.
13
Measure
mode are
To set the Beeper:
• Use
or to select the
Beeper
option.
• Press
desired beeper associated event you want to modify.
• Press
beeper status option.
• Press
menu or press
Saving Confirmation
When enabling this option, a prompt will appear on the LCD alerting
the user to save the modified values by pressing
without saving by pressing
and return to the editing mode by pressing
modified values will be saved automatically.
To enabled /disabled the saving confirmation:
• Use
• Press and use or to choose enabled
/ disabled.
• Press
cancel operation.
and use or to highlight the
and use or to highlight the
to confirm your selection and return to the
to return without changing.
or canceling the saving operation
or to select the
to confirm your selection or press
Saving Confirmation
Beeper
, exiting
. If disabled, the
option.
to
GLP Data
This option allows the user to set general information which will appear in the log reports. The edited text can have
max 10 characters.
Operator ID
Instrument ID
Company Name
Additional Info 1 & Additional Info 2
– edit the operator’s name.
– edit an identification name / number for the instrument.
– edit the company name.
– for general purpose notations.
14
To set the GLP data:
• Use
or to select the
GLP Data
option.
• Press
desired option.
• Press to edit the desired information. The Text Editor menu
will be displayed on the LCD.
• Enter the desired information by using
highlight the desired character. It is also possible to delete the last
character by positioning the cursor on the Backspace character (
and pressing
• Press
Confirmation
option,
options are saved automatically.
Date & Time
This option allows the user to set the current date & time and the format in which they appear. These parameters
will be displayed on the
Set Date and Time
This option allows you to set the current date (year / month / day) and time (hour / minute / second).
Notes: • Only years starting with 2000 are accepted.
• The time is set using the selected time format. For 12 Hour time format only, the AM / PM can
and use or to highlight the
and to
)
.
to return to the
is enabled, press to accept the modified
to escape without saving or to return to the editing mode. Otherwise, the modified
Measure
also be selected with
GLP Data
menu. If the
screens and also when storing measured data.
or .
Saving
Set Time Format
This option allows you to choose between 12 Hour (AM / PM) time format and 24 Hour time format from the
displayed pop-up box.
Set Date Format
This option allows you to choose the desired date format from the available formats: DD/MM/YYYY; MM/DD/YYYY;
YYYY/MM/DD; Mon DD, YYYY; DD-MM-YYYY and YYYY-Mon-DD.
15
To set the Date & Time:
• Use
or to select the
Date & Time
option.
• Press
desired option you want to modify.
• Press to confirm your selection. Use and
other two options press
select one of the displayed formats with
• Press to confirm your selection and return to the
& Time
• Press
Note: If the time is changed with more than one hour before last measure parameters user calibration, a pop-up
warning will appear on the LCD, notifying the user that a date/time conflict has occured and some timedependent features could work improperly (e.g.
LCD Setup
This option allows the user to set the
parameter can be adjusted within 7 steps, while the
be set from 1 to 60 minutes or it can be disabled (OFF). All the changes are visible on the LCD for each parameter.
and use or to highlight the
and then use to modify the value with
or (for
options.
to return to the previous mode.
Set Date and Time
to confirm your selection and
option). For the
or .
GLP, Log
Contrast
, the
Backlight
Backlight
Date
).
of the LCD and the
parameter within 4 steps. The
Backlight Saver
. The
Contrast
Backlight Saver
can
Note: If the instrument backlight is turned off after the set period of
time, press any key to turn it back on.
To set the LCD:
• Use or to select the
• Press
parameter;
• Use
• Press return to the
and use key to highlight the desired
or to adjust the selected parameter;
System Setup
LCD Setup
option;
menu with saving.
16
Language
This option allows the user to choose the desired language for the user
interface.
To select the Language:
• Use
• Press and use or to highlight the
desired language.
• Press
or to select the Language option.
to confirm your selection and return to the
System
menu or press
Setup
without changing.
Serial Communication
This option allows the user to set the desired speed for the serial
communication (baud rate) between the instrument and PC from
1200, 2400, 4800 or 9600
To set the serial communication:
• Use
option.
• Press
desired baud rate.
• Press
System Setup
Note: The meter and the PC application must have the same baud rate.
or to select the
and use or to highlight the
to confirm your selection and return to the
menu or press
to return to the
.
System Setup
Serial Communication
to return without changing.
menu
17
Meter Information
This option provides general information about the instrument serial
number (each instrument has an unique identification serial number),
the software version and the factory calibration date and time (for
conductivity and temperature).
Note: All the instruments are factory calibrated for conductivity and
temperature. After one year from last factory calibration, the
warning will appear at meter startup to inform the user that
a new factory calibration is required.
To view the meter information:
• Use
or to select the
Meter Information
option.
• Press
press
Restore Factory Settings
This option allows the user to reset the instrument to the default
factory settings.
To restore the factory settings:
• Use
option.
• Press
displayed, asking for confirmation.
• Press
to confirm and to view the meter information or
to return to the
or to select the
to confirm your selection. A pop-up box will be
to confirm and return to the
to return without restoring defaults.
System Setup
Restore Factory Settings
System Setup
menu.
or press
18
Loading...