Hanna Instruments HI 3854 User Manual

Instruction Manual
HI 3854
Zinc Test Kit
SPECIFICATIONSSPECIFICATIONS
SPECIFICATIONS
SPECIFICATIONSSPECIFICATIONS
Range 0 to 3.0 mg/L (ppm) as Zinc Smallest Increment 0.6 ppm Analysis Method Colorimetric Sample Size 20 mL Number of Tests 100 Case Dimensions 230x59x70 mm (9.0x2.3x2.8") Shipping Weight 250 g (8.8 oz.)
SIGNIFICANCE AND USESIGNIFICANCE AND USE
SIGNIFICANCE AND USE
SIGNIFICANCE AND USESIGNIFICANCE AND USE
INSTRUCTIONSINSTRUCTIONS
INSTRUCTIONS
INSTRUCTIONSINSTRUCTIONS
READ THE ENTIRE INSTRUCTIONS BEFORE USING THE KIT
• Fill the plastic vessel with 20 mL of the sample, up to the mark.
• Add 1 packet of reagent HI 3854A-0 and mix, using the plastic spoon, until the powder is completely dis­solved.
• Wait 3 minutes and 30 sec­onds to allow color to develop. Fill the color com­parator cube with 5 mL of the reacted sample.
• Determine which color best matches the solution in the cube and record the result as mg/L (ppm) of zinc.
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Dear Customer, Thank you for choosing a Hanna Product. Please read the instructions carefully before using the
chemical test kit. It will provide you with the necessary information for correct use of the kit.
Remove the chemical test kit from the packing material and examine it carefully to make sure that no damage has occurred during shipping. If there is any noticeable dam­age, notify your Dealer or the nearest Hanna office immediately.
Each kit is supplied with:
HI 3854A-0 Reagent, packets (100 pcs);
• HI 93731B-0 Zinc Reagent B (Cyclohexanone), 2
• bottles (60 mL);
1 color comparator cube;
• 1 glass cuvet (10 mL) with HDPE plastic stopper ;
• 1 syringe (1 mL);
• 1 calibrated plastic vessel (20 mL);
• 1 plastic spoon.
Note: Any damaged or defective item must be returned in
its original packing materials.
Zinc is widely used in alloys (brass, bronze, and dye-casting alloys), in galvanizing iron and other metals, also as a fungicide. It is also an essential growth element in human diet. But with concentrations higher than 5 mg/L, it gives a bitter taste to water and opalescence to alkaline water. Zinc can enter the domestic water supply from the deterio­ration of galvanized iron and dezincification of brass.
Note:
mg/L is equivalent to ppm (parts per million).
CHEMICAL REACTIONCHEMICAL REACTION
CHEMICAL REACTION
CHEMICAL REACTIONCHEMICAL REACTION
Zinc reacts with the zincon reagent to form a brownish­green to blue complex in a solution buffered at alkaline pH. Since other metals can form colored complexes with zincon, cyanide is added to complex zinc and any other heavy metal present. Then, cyclohexanone is added to selectively free zinc from its cyanide complex so that it can react with zincon to form the final blue colored product. The amount of color developed is proportional to the concentration of zinc present in the aqueous sample.
ISTR3854 12/99 PRINTED IN ITALY
• Pour 10 mL of the so­lution from the vessel into the glass cuvet, up to the mark.
• Add 0.5 mL of HI 93731B-0 reagent by means of the syringe. Close the cuvet with the HDPE plastic stopper and mix for 15 seconds.
• It is better to match the color with a white sheet at about 10 cm behind the comparator.
REFERENCESREFERENCES
REFERENCES
REFERENCESREFERENCES
Standard Methods for the Examination of Water and Waste-
th
water, 18
Edition, 1992
APHA/AWWA/WEF.
HEALTH AND SAFETYHEALTH AND SAFETY
HEALTH AND SAFETY
HEALTH AND SAFETYHEALTH AND SAFETY
The chemicals contained in this kit may be hazardous if improperly handled. Read Health and Safety Data Sheet before performing this test.
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