Hanna Instruments HI 3835 User Manual

Instruction Manual
SPECIFICATIONS
INSTRUCTIONS
HI 3835
Salinity Test Kit
www.hannainst.com
SPECIFICATIONS
Dear Customer, Thank you for choosing a Hanna Product. Please read the
instructions carefully before using the chemical test kit. It will provide you with the necessary information for correct use of the kit.
Each kit is supplied with:
• Diphenylcarbazone Indicator, 1 bottle with dropper (15 mL);
• Nitric Acid Solution, 1 bottle with dropper (30 mL);
• HI 3835-0 Reagent Titrant Solution, 1 bottle (120 mL);
• 1 plastic vial;
• 1 calibrated syringe (1 mL) with tip.
Note: Any damaged or defective item must be returned in
its original packing materials.
Range 0 to 40 g/kg (ppt) Analysis Method Titrametric Sample Size 1 mL Number of Tests 110 (average) Case Dimensions 200x120x60 mm (7.9x4.7x2.4") Shipping Weight 460 g (17.2 oz.)
SIGNIFICANCE AND USE
Salinity is defined as the total solids in water after all carbonates have been converted to oxides, all bromide and iodide have been replaced by chloride and all organic matter has been oxidized. The value is in g/kg or ppt (parts per thousand). The monitoring of salinity is essential for industrial waste and seawater. The Hanna Test Kit measures salinity using a fast and efficient titrametric method. The test requires only a few simple and safe steps to obtain a result. The components are contained in a compact case, which makes it perfect for on-site tests.
CHEMICAL REACTION
The salinity level in g/kg is determined by a mercuric nitrate titration method. The pH is lowered to approximately 3 by addition of nitric acid. Mercuric ions react with chloride ions to form mercuric chloride. When excessive mercuric ions are present, it complexes with diphenylcarbazone to form a purple solution. The color change from yellow to violet indicates the endpoint.
Hg(NO3)2+2Cl
ISTR3835R4 04/02 PRINTED IN ITALY
HgCl
+2NO
2
READ ALL THE INSTRUCTIONS BEFORE USING THE TEST KIT Note: Push and twist pipet tip onto tapered end of syringe
ensuring an air-tight fit.
Note: Use separate pipet tips for sampling and titration.
• Take the titration syringe and push plunger completely into the syringe. Insert tip into water sample and pull plunger out until the lower edge of the plunger seal is on the 0 mL mark of the syringe.
• Place syringe tip into the plastic vial and slowly add the titration solution drop by
• Add the sample in the syringe to the plastic vial.
• Add 1 drop of Diphenylcarbazone Indicator and cap the vial. Swirl the solution. The solution will become a violet color.
drop, swirling to mix after each drop. Continue adding titration solution until the solution in the vial changes from yellow to violet.
• Read off the milliliters of titration solution from the syringe scale, and multiply by 40 to obtain salinity in g/kg (ppt).
x 40
ACCESSORIES
• Remove the cap. While swirling the vial, add Nitric Acid Solution drop by drop until the solution turns yellow.
HI 3835-100 Spare reagents (100 tests)
REFERENCES
Standard Methods for the Examination of Water and Waste­water, 16th Edition, 1985.
3
HEALTH AND SAFETY
• Take the titration syringe and insert a new pipet tip. Push plunger completely into the syringe. Insert tip into HI 3835-0 Reagent Titrant Solution and pull plunger out until the lower edge of the plunger seal is on the 0 mL mark of the syringe.
The chemicals contained in this kit may be hazardous if improperly handled. Read Health and Safety Data Sheet before performing this test.
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