Hamilton Polilyte, EasyFerm Operating Instructions Manual

pH and ORP Arc sensors
Operating Instructions
TABLE OF CONTENTS
Table of Contents
TABLE OF CONTENTS
1.1 Intended Use .............................................................. 4
1.2 About this Operating Instruction ................................. 4
3.1 General Precautions ................................................... 5
3.2 Operation of pH/ORP Arc Sensor ............................... 5
3.3 Earthing ...................................................................... 6
3.4 Electrical Safety Precautions ...................................... 6
3.5 Chemical, Radioactive or Biological
Hazard Precautions .................................................... 7
4.1 General Description .................................................... 7
4.2 Hardware Description ................................................. 8
4.3 pH/ORP Arc Sensor with Micro-Transmitter inside ..... 9
5.1 Unpacking .................................................................. 9
5.2 Configuring the pH/ORP Arc sensor with ArcAir ......... 9
5.2.1 Installing ArcAir Basic on the Computer ......... 10
5.2.2 Connecting a pH /ORP Arc sensor
to ArcAir ......................................................... 10
5.2.3 Create User Accounts .................................... 10
5.2.4 Configuring the pH/ORP Arc Sensor
Parameters ......................................................11
5.2.5 Configuring the calibration settings .................11
5.2.6 Configuring the temperature settings
of SIP / CIP process ....................................... 12
5.2.7 Configuring the analog interface for
your process control system .......................... 12
5.2.8 Defining a measuring point name for
identification of the process ............................ 13
5.3 Install pH/ORP Arc Sensor in Your
Measuring Loop ....................................................... 13
5.3.1 Mechanical Process Connection .................... 13
5.3.2 VP 8 Pin Designation ...................................... 13
5.3.3 Controlling 4–20 mA current interface
signals by pulse-width modulation.................. 14
5.3.4 Electrical Connection for Analog
4–20 mA Connection ..................................... 15
5.3.5 Electrical connection for the
digital RS485 interface ................................... 16
6 Operation .............................................................. 18
7 Maintenance ......................................................... 18
7.1 Verify Sensor Status ................................................. 18
7.2 Calibration ................................................................ 19
7.2.1 One Point Calibration in pH or
ORP Buffer Solution ....................................... 20
7.2.2 Two Point Calibration in pH Buffer Solution .... 20
7.2.3 Product calibration ......................................... 21
7.3 Cleaning ................................................................... 21
8 Troubleshooting ................................................... 22
8.1 Sensor Self-Diagnostic ............................................. 22
8.1.1 Warnin g s ........................................................ 23
8.1. 2 Er ro r s ............................................................. 23
8.2 Getting Technical Support ........................................ 23
8.3 Returning Arc sensors for Repair .............................. 23
9 Disposal ................................................................ 24
10 Ordering Information ........................................... 24
10.1 pH/ORP Arc Sensors ............................................. 24
10.2 Parts and Accessories ........................................... 25
10.3 Arc Services ........................................................... 29
Hamilton Warranty
Please refer to the General Terms of Sales (GTS).
Important note
Copyright © 2018 Hamilton Bonaduz AG, Bonaduz Switzerland. All rights reserved. The reproduction of any part of this document in any form is forbidden without the express written agreement of Hamilton Bonaduz AG.
Contents of this manual can be modified without previous announcement. Technical modifications reserved. Greatest possible care was used on the correctness of the information in this manual. If errors should be discovered nevertheless, Hamilton Bonaduz AG is pleased to be in­formed about it. Regardless of this, Hamilton Bonaduz AG cannot assume liability for any errors in this manual or for their consequences.
3Operating Instructions pH/ORP Arc Sensors
GENERAL INFORMATION • LIABILITY SAFETY PRECAUTIONS AND HAZARDS

1 General Information

1.1 Intended Use

The EasyFerm and Polilyte Arc sensor families (pH/ORP Arc sensors) are intended for the measurement of pH and ORP (Oxidation Reduction Potential).
ATTENTION! pH/ORP Arc sensors are not intended
for hazardous atmospheres.
ATTENTION! The pH/ORP Arc sensors has a built-in temperature sensor (NTC 22 kOhm). This temperature sensor is to be used only for monitoring the sensor conditions, not for controlling the process temperature.
ATTENTION! The measurement values transmitted over wireless communication are not intended to be used for process control.

1.2 About this Operating Instruction

These Operating Instructions are designed to support the inte­gration, operation and qualification of the EasyFerm and Poliyte Arc sensor families. To achieve this, it will describe the features of EasyFerm and Poliyte Arc sensor families and its integration in Process Control Systems (PCS). Both the hardware and the communication between the pH/ORP Arc sensor and Process Control Systems are detailed in this manual. After reading this manual the user should be capable of installing and operating pH/ORP Arc sensors.
ATTENTION! Essential information for avoiding personal injury or damage to equipment.
NOTE: Important instructions or interesting information.
tenance and regular replacement of the sensors. In the case of critical sensor applications, Hamilton recommends using back-up measuring points in order to avoid consequential damages. The user is responsible for taking suitable precautions in the event of a sensor failure.
NOTE: The pH/ORP Arc sensor is not intended and specified as a safety device. A SIL (Safety Integrity Level) certification is not available. It is in the sole responsibility of the user to validate the pH/ORP Arc sensor according the safety requirements of his application.

3 Safety Precautions and Hazards

ATTENTION! Read the following safety instruc­tions carefully before installing and operating the pH/ORP Arc sensor.

3.1 General Precautions

For safe and correct use of pH/ORP Arc sensor, it is essential that both operating and service personnel follow generally accepted safety procedures as well as the safety instructions given in this document, the pH/ORP Arc sensor operation instruction manual. The specification given in the «Specification Sheet» as regards temperature, pressure etc. may under no circumstances be ex­ceeded. Inappropriate use or misuse can be dangerous.
The lifetime of the pH/ORP Arc sensor highly depends on the specific conditions of the application. Temperature, pressure, chemicals used may accelerate the ageing of the pH/ORP Arc sensor. See chapter 7 for replacement conditions.
Cleaning, assembly and maintenance should be performed by personnel trained in such work. Before removing the sensor from the measuring setup, always make sure the no process medium can be accidentally spilled. When removing and cleaning the sensor, it is recommended to wear safety goggles and protective gloves. The sensor can not be repaired by the operator and has to be sent back to Hamilton for inspection.
Necessary precautions should be taken when transporting the sensors. For repair or shipment the sensor should be sent back in the original reusable packaging box. Every pH/ORP Arc sensor sent back for repair must be decontaminated.

2 Liability

The liability of Hamilton Bonaduz AG is detailed in the document «General Terms and Conditions of Sale and Delivery».
Hamilton is expressly not liable for direct or indirect losses arising from use of the sensors. It must in particular be insured in this conjunction that malfunctions can occur on account of the inher­ently limited useful life of sensors contingent upon their relevant applications. The user is responsible for the calibration, main-
If the conditions described in these operating instructions manual are not adhered to or if there is any inappropriate interference with the equipment, all of our manufacturer’s warranties become obsolete.

3.2 Operation of pH/ORP Arc Sensor

When using the pH/ORP sensors in process environment suit­able protective clothing, safety glasses and protective gloves
5Operating Instructions pH/ORP Arc Sensors
SAFETY PRECAUTIONS AND HAZARDS PRODUCT DESCRIPTION
must be worn, particularly when dealing with a malfunction where the risk of contamination from spilled liquids exists. Instal­lation and maintenance of sensors must be performed only by trained personnel. The mobile devices and sensors must be used for their intended applications, and in optimum safety and operational conditions.
Use only wired digital or analog connection for the process con­trol. The Arc wireless interface is designed for sensor monitoring, maintenance and service purposes.
Make sure that the PG13,5 thread and the O-ring are not dam­aged when screwing the sensor into the process. O-rings are consumable parts which must be exchanged regularly (at least once per year). Even when all required safety measures have been complied with, potential risks still exist with respect to leaks or mechanical damage to the armature. Wherever there are seals or screws, gases or liquids may leak out undetected. Always make sure that no process medium can be accidentally spilled before removing the sensor from its measurement setup. Make sure that no air or gas bubbles sticks to the sensitive part of the sensor. As a consequence, the measurement value could be un­stable. Do not put stress on the system by vibration, bending or torsion. Before use, verify that the sensor is properly configured for your application.
Failure to observe and carry out the maintenance procedures may impair the reliability and correct functioning of the measure­ment system.
The integrated 4–20 mA analog output has been configured according to factory defaults. You can find full details, including serial number and most important specifications, on the certifi­cate provided with each sensor. Before use, verify that the sensor is properly configured for your application.
parts. Carefully follow all the instructions in chapter 5.3 to avoid electrical damage to the sensor. The contacts must be clean and dry before sensor is connected to the cable.
ATTENTION! Switch off the power supply and unplug the connector before dismounting the pH/ORP Arc sensors.
ATTENTION! If the power supply (230VAC/24VDC) is switched off or disconnected the reading on the PCS is wrong.

3.5 Chemical, Radioactive or Biological Hazard Precautions

Selection of the appropriate safety level and implementation of the required safety measures for working with pH/ORP Arc sensor is the sole responsibility of the user.
If working with hazardous liquids observe and carry out the main­tenance procedures, paying particular attention to cleaning and decontamination. If pH/ORP Arc sensor becomes contaminated with biohazardous, radioactive or chemical material, it should be cleaned. Failure to observe and carry out the maintenance procedures may impair the reliability and correct functioning of the measuring module.
ATTENTION! To avoid dr ying out the diaphragm and a potential decrease in sensor performance, make sure the sensor is always stored with a cap containing Storage Solution (Ref 238931).

3.3 Earthing

The sensor has to be mounted at the mounting location with an electrostatically conductive of < 1MOhm. It is recommended to assign the VP 8 cable shield to earth (PE potential equalization) especially in electromagnetically noisy environments. This signifi­cantly improves noise immunity and signal quality.

3.4 Electrical Safety Precautions

Do not connect the sensor to a power source of any voltage be­yond the range stated in the power rating Technical Specifications (www.hamiltoncompany.com).
Always use Hamilton VP 8 cables for safe connection. Cables are available in a broad range of lengths (Chapter 10). Make sure the cable is intact and properly plugged to avoid any short circuit. Keep pH/ORP Arc sensor away from other equipment which emits electromagnetic radio frequency fields, and minimize static electricity in the immediate environment of the optical measuring

4 Product Description

4.1 General Description

pH/ORP Arc sensors are critical measurement and control pa­rameters for many liquid processes. Hamilton offers a wide selec­tion of sensors for use in all bioprocesses, as well as many other industries that require high accuracy and reliability from their sen­sors. Hamilton is one of the few manufacturers to have multiple pH membrane glass options and reference designs to tailor the sensor for the specific application. With their micro transmitter, pH/ORP Arc sensors enable direct communication to the process control system via 4–20 mA standard signal or digital Modbus. Wireless communication with the Arc Wireless Adapter may be used for monitoring, configuration and calibration, and saves time without compromising the quality of the wired connection. The sensor features furthermore an integrated Bluetooth 4.0, enabling in this way wireless data exchange with smartphones and tablets.
With the transmitter integrated, Arc sensors provide more reli­able measurements directly to your process control system. The μ-transmitter located in the sensor head stores all relevant sensor data, including calibration and diagnostic information, simplify­ing calibration and maintenance. The integrated quality indicator predicts the remaining sensor and cap life time.
Key benefits include:
• Multiple pH membrane glass options for different application
7Operating Instructions pH/ORP Arc Sensors
PRODUCT DESCRIPTION INSTALLATION
• No separate transmitter needed
• Easy to install
• Direct digital Modbus or analog communication to the
process control system via 4–20 mA standard signal.
• Full online wireless option via Bluetooth 4.0 for easy
monitoring, configuration and calibration

4.2 Hardware Description

The pH/ORP sensor consists of a sensor head with integrated electronic and a sensor pH sensitive glass membrane in contact with the measured medium. The pH glass shaft is terminated by the sensitive glass membrane and diaphragm with the reference measurement system. During development, special attention was paid to an optimum sanitary design. All materials in contact with the solution meet the FDA requirement.
VP 8 Connector

4.3 pH/ORP Arc Sensor with Micro-Transmitter inside

With the micro-transmitter integrated, pH/ORP Arc sensors offer fully compensated signal directly to the process control system. Communication protocols include standard analog 4–20 mA. The micro transmitter located in the sensor head stores all relevant sensor data, including calibration and diagnostic information, simplifying calibration and maintenance.

5 Installation

5.1 Unpacking

1) Unpack carefully the pH or ORP Arc sensor. Enclosed you will find the pH/ORPArc sensor, the Declaration of Quality, the Instruction Manual, and Material certifications.
2) Inspect the sensor for shipping damages or missing parts.
Sensor Head with μ-transmitter
Process connection PG13,5
O-ring
Figure 2: pH/ORP Arc sensor deliver y package.
5.2 Configuring the pH/ORP Arc sensor
with ArcAir
Arc sensors require application specific configuration. Following parts are required to configure and calibrate Arc sensors:
• Arc View Mobile or ArcAir computer Software Solution
• External Power supply with Arc USB Power Cable (Ref 243490-xx)
To configure and set up the Arc sensors at least ArcAir Basic is required. Below in this table you will find the different ArcAir licenses and its functionality:
Sensitive Glas Membrane
Figure 1: Sensor description
ArcAir Read Calibrate Configure Documentation
Free
Basic
Advanced
– –
9Operating Instructions pH/ORP Arc Sensors
INSTALLATIONINSTALLATION
Arc Wire less
Conver ter BT
ArcAir
Figure 3: Arc pH/ORP Sensor configuration with ArcAir.
Arc Wi 1G/2G
Adapter BT
Arc pH/ORP Sensor
Arc USB Power Cable

5.2.1 Installing ArcAir Basic on the Computer

1) Download the Zip file «ArcAir» from the Hamilton webpage www.hamiltoncompany.com (search for ArcAir).
2) Unpack the ZIP-File.
3) Do not plug in the Wireless Converter before the installation of ArcAir is completed.
4) Install «ArcAir» by double clicking «ArcAir.exe» and follow the instructions on the screen.
5.2.2 Connecting a pH /ORP Arc sensor
to ArcAir
1) Connect a sensors with the power supply, e.g. Arc USB Power Cable Ref 243490-xx
2) Switch on the mobile’s Bluetooth connection or connect a Wireless Converter BT to USB Port of your computer (only for wireless connection)
3) The ArcAir application recognizes and displays the connected sensors automatically
NOTE: Initial operation of ArcAir is in the laboratory mode as long as no user account is created. Laboratory mode does not require a login password and enable all features in the installed license version.
5.2.4 Configuring the pH/ORP Arc Sensor Parameters
1) Start the ArcAir application
2) Select the desired sensor
3) Open the drawer «Settings» (make sure you have the «Sensor Settings» user right)
4) Configure the sensor
A description of the available settings is given below:
Parameter Default Name Description Value Configuration Location
Meas. Unit These are the pH Required Settings/ measurement mV Measurement physical units
T unit These are the K Required Settings/ temperature °F Measurement physical units °C
*Moving The sensor ORP/ average uses a moving Temp.: 2 default Values average over R the measuring points
*In calibration mode the sensor will automatically switch to 3 sec sampling rate after the first calibration.
Recommended
: 16 parameter Measurement
Glass
Settings/
ATTENTION! For automatic sensor login a unique and global Operator Level S password for all intelli­gent sensors is required. Please make sure you have added the same Operator Level S Password for all Arc sensors in the ArcAir application under Backstage/Settings/Operator Level S Password.

5.2.3 Create User Accounts

1) Start ArcAir application on computer
2) Click on «Backstage» left upper corner
3) Select «User Management»
4) Click the «Add» Button for opening the user editor
5) Type in the user details and password
6) Select the specific rights for the user
ATTENTION! First user is the administrator and all user rights are assigned as default.
5.2.5 Configuring the calibration settings
Parameter Default Name Description Value Configuration Location
Drift Higher drift will 1%/Min Recommend Calibration/ pH/ORP interrupt the default Calibration calibration parameter Settings process. Warning comes up «drif t pH/ORP»
Drift T Higher drift will 0.5 K/min Recommend Calibration/ interrupt the default Calibration calibration parameter Settings process. Warning comes up «drift temperature»
11Operating Instructions pH/ORP Arc Sensors
INSTALLATION INSTALLATION
5.2.6 Configuring the temperature settings of SIP / CIP process
Parameter Default Name Description Value Configuration Location
SIP process User defines Temp. min: Recommend Status / denition conditions 120°C default SIP / CIP for the SIP Temp. max. parameter counter 130°C Time: 20 min
CIP process Use r defines Temp. min: Recommend Status / denition conditions 80°C default SIP / CIP for the CIP Temp. max. parameter cou nte r 10 0°C Time: 20 min
5.2.7 Configuring the analog interface for your process control system
Parameter Default Name Description Value Configuration Location
Interface The output of 4-20 mA Recommended Interface/ Mode the 4-20 mA linear default Analog can be parameter configure linear, bilinear or with a fix value
Value at Defined 1 µS/cm / Required Interface/ 4 mA measurement 0 °C Analog value for 4 mA Output output
Value at Defined 10001 Required Interface/ 20 mA measurement µS/cm / Analog value for 20 mA 40°C Output 20 mA output
Mode in Current output No output Recommended Inter face/ event of mode in case default Analog warning of warnings parameter Output
Mode in Current output Continuous Recommended Interface/ event of mode in case output default Analog errors of errors parameter Output
Output in Current output 3.5 mA Recommended Interface/ event of in case of default Analog warning warnings parameter Output
Output in Current output 3.5 mA Recommended Interface/ event of in case of default Analog errors errors parameter Output
Output for T Current output 3.5 mA Recommended Interface/ out of limit in case of default Analog temperature parameter Output out of limit
5.2.8 Defining a measuring point name for identification of the process
Parameter Configu­Name Description Default Value ration Location
Measuring User can 243605-1234 Optional Information / point define a Info sensor name Userspace for better identification of the mea­ suring point

5.3 Install pH/ORP Arc Sensor in Your Measuring Loop

5.3.1 Mechanical Process Connection

The mechanical design of the pH/ORP Arc sensor is compatible with all Hamilton process housings, including FlexiFit, Retractex, RetractoFit and Hygienic Sockets.
Before installing the armatures, you should test that the seal is tight and the parts are all in working order. Ensure that there is no damage to the sensor or the armature. Check whether all O-rings are in place in the appropriate grooves and are free of damage. To avoid any mechanical damage to O-rings on assembly, they should be slightly greased.
Please note that O-rings are wetted parts and greasy compounds must comply to your FDA application needs.

5.3.2 VP 8 Pin Designation

Always use Hamilton Sensor Data Cable VP 8 for safe connec­tion, which are available in different lengths (Chapter 10).
A
B
C D
E
F
G
Shield
H
Figure 4: Pin description for electrical connection of pH/ORP Arc sensors
13Operating Instructions pH/ORP Arc Sensors
INSTALLATION INSTALLATION
VP pin Function Color*
A 4-20 mA interface # 2 Yellow
B 4-20 mA interface # 1 Green
C Power supply: + 24 VDC (7 to 30 VDC) Red
D Power supply: Ground Blue
E Not used Brown
F Not used White
G RS485 (A) Gray
H RS485 (B) Pink
Shaft Shield Green/Yellow
*Sensor D ata Cable VP 8
Figure 6: Progress of a rectangular signal with a period T and a pulse duration t2 for the generation of an analog signal with the value y
.
2

5.3.3 Controlling 4–20 mA current interface signals by pulse-width modulation

Hamilton pH/ORP Arc sensors use the method of pulse-width modulation (PWM) to adjust the DC currents of the 4–20 mA interfaces corresponding to the measured values. In principle, the pulse width (ti) of a rectangular signal with a constant fre­quency, the pulse duty factor (ti/T), is modulated and afterwards demodulated by a low-pass filter to generate continuous analog DC signals. The resulting value yi corresponds to the average of the PWM signal (see Figures 5 and 6). The PWM-loads of the Sensors have low-pass filters which are not able to eliminate all AC fractions of the used PWM frequency of 3.5 kHz due to tech­nical impossibilities. Therefore, the current signals of the 4–20 mA interfaces are still overlaid by a certain AC which should be masked by lag smearing or input filters of the current input card of the process control system (PCS). Recommended PCS set­tings are a sampling rate below 3.5 kHz, an averaging over more than 1 s, and the use of galvanically separated inputs to avoid oscillations.
It is also possible to use mathematical functions or isolating amplifiers for signal processing filtering if necessary. For detailed technical advice about suitable isolating amplifiers, please contact Hamilton technical support.
ATTENTION! The pH/ORP Arc sensor gener­ates the 4-20 mA signals by pulse width modulation (PWM) which is not compatible to all PCS systems. Also a galvanic separation between the power sup­ply and the PCS is necessary for correct sensor functionality when used in 4-20 mA setups. Figure 10 illustrates a solution for the problem.
Analog interface 1 and 2
Galvanically not isolated, pulse width modulation with 3.5 kHz, recommended PCS settings:
• Use galvanically separated inputs
• Sampling rate < 3 kHz and ≠ n * 3.5 kHz
• Average over > 1 s

5.3.4 Electrical Connection for Analog 4–20 mA Connection

The 4–20 mA interface enables direct connection of the pH/ORP Arc sensor to a data recorder, indicator, control unit or PCS with analog I/O. The pH/ORP Arc sensor works as a current sink sensor and is passive. Connect the sensor according to the pin designations (Chapter 5.3.2). The 4–20 mA interface of the pH/ ORP Arc sensor is pre-configured with default values for the 4–20 mA range, and measurement unit. Configure the 4–20 mA interface according to your requirements for proper measurement (Chapter 5.2.7).
Figure 5: Progress of a rectangular signal with a period T and a pulse duration t
for the generation of an analog signal with the value y1.
1
Examples of circuit arrangement
Sensor
VP pin A /B
4–20 mA regulation
Sensor power
VP Pin C
VP pin D
Figure 7: Three-wire loop wiring diagram for the 4–20 mA inter face.
U (7–30 VDC) Po wer Supply S ensor
Yellow/Green
4–20 mA c urrent
Red
Blue
PCS
0 VDC; GND1
+
+ 24 VDC
0 VDC; GND2
u
Analog Input
15Operating Instructions pH/ORP Arc Sensors
INSTALLATION INSTALLATION
Sensor
VP pin A /B
4–20 mA regulation
Sensor power
VP Pin C
VP pin D
Yellow/Green
4–20 mA c urrent
U (7–30 VDC) Po wer Supply S ensor
-
input
+
Red
Blue
+
-
output
PCS
+
-
0 VDC; GND
+ 24 VDC
0 VDC; GND
u
Analog Input
Figure 8: The safest form of wiring, using an external isolation amplifier. (For detailed technical advice, please contact the technical support at Hamilton)

5.3.5 Electrical connection for the digital RS485 interface

The digital RS485 interface enables communication with pH/ORP Arc sensor for performing measurements, for calibrating and changing the configuration parameters. pH/ORP Arc sensors are always connected to digital controlling devices as a Modbus slave. To function, they require a power supply (VP 8 pins C and D, see below). The section in chapter 5.2 describes configuration in digital mode.
Additional information:
In an electromagnetically noisy environment, it is advisable to connect the VP cable shield to the earth. This significantly im­proves noise immunity and signal quality.
Example of circuit arrangement
Sensor
VP pin C
VP pin D
VP pin G
VP pin H
Figure 9: Wiring diagram for the RS485 interface.
Master device Distributors
SDA(-)
SDB(+)
RDA(-)
RDB(+)
+ 24 VDC
Common
120 Ohm
line termination
(option)
#1
A/A'
B/B'
+ 24 VDC
Common
#2
A/A'
B/B'
+ 24 VDC
Common
#3
A/A'
B/B'
+ 24 VDC
Common
Power supply
+24 VDC
+
-
0 VDC; G round
PCS
A
RS 485
B
Ground
#n
n≤31
A/A'
B/B'
+ 24 VDC
Common
line termination
120 Ohm
(option)
The Modbus RTU communication protocol corresponds to the Modbus-IDA standard (see www.modbus.org). pH/ORP Arc sen­sor uses an open register set developed by Hamilton. Additional information about the register content and structure can be found in the programmers manual under www.hamiltoncompany.com. The Modbus physical layer is described in detail with require­ments on cabling and line termination in the «Modbus Serial
>
line Protocol and Implementation Guide» www.modbus.org Technical Resources / Modbus Specifications / Modbus Serial line Protocol and Implementation Guide.
ATTENTION! Because all sensors are delivered with factory-default settings, each sensor must be configured for its specific application before first use (see the section entitled «Configuring pH/ORP Arc sensor» chapter 5.2).
The pins for digital the RS485 interface have the following desig­nation with respect to VP cable conductor colors:
VP pin Function Color
C Power supply: + 24 VDC Red (7 to 30 VDC)
D Power supply: Ground Blue
G RS485 (A) Gray
H RS485 (B) Pink
Shaft Shield Green/Yellow
Figure 10: Multi-drop bus wiring for the Modbus two-wire mode. Each sensor functions as a Modbus slave.
NOTE: In order to avoid signal reflection on the lines the use of line termination resistors (120 Ohm each) is recom­mended. The effect of signal reflections becomes more relevant with long cable length and/or high baud rates.
NOTE: In the connection scheme shown above, each sensor must have the unique Modbus device address for proper communication.
The serial Modbus connection between the RS485 port of the master and the corresponding interfaces of the sensors has to be ensured according to the EIA/TIA RS485 standard. Only one sensor can communicate with the master at any time.
17Operating Instructions pH/ORP Arc Sensors
OPERATION • MAINTENANCE MAINTENANCE

6 Operation

ATTENTION! Only use the sensor within the speci­fications (see www.hamiltoncompany.com). Failure to do so may lead to damages or measurement failure.
1) Remove the watering caps from the pH/ORP Arc tip, and yellow cap from the VP 8 sensor head
2) Check the O-ring on the sensor shaft and verify for shipping damages or missing parts.
3) Verify the functionality of the sensor (Chapter 7.1)
4) Calibrate the sensor (Chapter 7.2)
5) Connect the sensor to the process control system (Chapter 5.3)
6) Verify the measurement in standard solution and on your control system
7) Mount the sensor to the armature or process connection (Chapter 5.3)
NOTE: No analog reading is performed at a tempera­ture higher than 110°C to protect the analog electronics and enhanced the sensor lifetime.
The sensor is performing correctly. No errors or warnings have been registered.
At least an error or a warning has been registered. Verify the sensor errors and warnings in Sensor Status.
No communication between the sensor and ArcAir. This may be due to a hardware failure.
Figure 11: Description of the traffic lights on ArcAir.

7.2 Calibration

The pH/ORP Arc sensors provide two kinds of sensor calibra­tion: automatic standard calibration, and product calibration. The automatic standard calibration and the product calibration may be performed using ArcAir (see chapter 5.2).
pH/ORP Arc sensors can be calibrated automatically with buffer solution defined in sensor configuration profile.
NOTE: For greater measurement accuracy ensure that temperature difference between calibration medium and process medium is minimal.
Six sets of the pH calibration standards are provided with each Arc pH sensor:

7 Maintenance

Periodic maintenance routines need to be run in order to ensure safe and reliable operation and measurement of sensor and the accessories.
ATTENTION! Avoid any contact of the equipment
with corrosive media.

7.1 Verify Sensor Status

1) Power the sensor with the Sensor Power Cable and connect the sensor to ArcAir.
2) Control the traffic lights (Figure 11).
3) Refer to the troubleshooting (Chapter 8) for the next steps if the traffic light is not green.
4) Control the quality of the sensor in Sensor Status / Quality Counter and Temperature / Quality Indicator.
• Hamilton
• Merck Titrisol
• DIN 19267
• NIST Standard
• METTLER TOLEDO
• Radiometer
The pH Arc sensors are pre-calibrated at the factory using two Hamilton standards: pH 4 (Calibration point 1), and pH 7 (Calibra­tion point 2) at room temperature. The following buffers within Hamilton standards set are defined as factory default for calibra­tion with automatic buffer recognition: pH 4.01, pH 7.00 and pH
10.01. The use of the same buffer to both calibration points will yield an error and reject this calibration.
NOTE: The concept behind Arc pH sensors enables calibration and configuration in the lab before use in the process control. Another calibration for the installation in the process setup is not required.
NOTE: ORP Arc sensors utilize a one-point calibration procedure with automatic standard recognition. The ORP values and temperature dependence data for a number of predefined redox buffers are stored in the sensor. Therefore the sensor recognizes a standard, examines the accuracy and stability of the ORP and temperature signals, and performs the calibration.
®
19Operating Instructions pH/ORP Arc Sensors
MAINTENANCE MAINTENANCE
One set of Hamilton redox calibration standards is provided with each Arc ORP sensor:
• Hamilton
• METTLER TOLEDO
• Reagecon

7.2.1 One Point Calibration in pH or ORP Buffer Solution

1) Power the pH/ORP Arc sensor and connect to ArcAir via the Arc Wireless Converter BT or Arc USB Power Cable.
pH4
Figure 12: Calibration setup
2) Install the sensor into the buffer solution bottle and connected
3) Select the sensor in the sensor list.

7.2.3 Product calibration

The product calibration is an in-process calibration procedure in order to adjust the measurement to specific process condi­tions, or in case the sensor cannot be removed for the standard calibration. Product calibration adapts the calibration point 2 to the process conditions in force at the time of product calibration. In order to restore the original calibration point 2, the product calibration can be deleted at any time. A new standard calibration deletes the product calibration as well.
NOTE: The difference between initial measurement and laboratory values for pH sensors can not be greater than two pH units and for ORP sensors it can not be greater than 400 mV.
Product calibration of Arc pH Sensor
4) Open the Calibration tab.
5) Select Calibration Point 1
6) Immerse the sensor into buffer solution (default pH 4.0 or 475mV) (Figure 19)
7) Click Start to start the calibration wizard.
8) Follow the instructions on the screen.
7.2.2 Two Point Calibration in pH Buffer
Solution
1) Power the pH/ORP Arc sensor and connect to ArcAir via the Arc Wireless Converter BT or Arc USB Power Cable.
pH7
Figure 13: Calibration setup
2) Install the sensor into the buffer solution bottle and connected
Figure 14: Effect of product calibration (CP6) on an existing standard calibration function based on the one point calibration (CP1).
A product calibration is performed as follows:
1) Connect one of the pH/ORP Arc sensor with the power supply, e.g. USB Power Cable Ref 243490-xx and install a Wireless Converter BT.
2) Select the desired sensor from the sensor list
3) Go to «Process Settings»
4) Click «Start» to start the product calibration wizard
5) Follow the instruction on the screen
NOTE: Alternatively, the product calibration may be
performed with a field device on side the measuring point.
3) Select the sensor in the sensor list.
4) Open the Calibration tab.
5) Select Calibration Point 1
6) Immerse the sensor into buffer solution (default pH 7.0) (Figure 20)
7) Click Start to start the calibration wizard.
8) Follow the instructions on the screen.

7.3 Cleaning

In general, acids, alkalis and other common solvents can be used for brief periods to clean sensors. Rinse with water immediately afterwards. Sensors exhibit sluggish response times for some time after cleaning, so place them in storage solution for 15 min. before using them again.
21Operating Instructions pH/ORP Arc Sensors
TROUBLESHOOTING TROUBLESHOOTING
Ceramic diaphragms: In the event of protein contamination, immerse the sensor’s electrode for several hours in 0.4% HCl + 5 g/l pepsin or Hamilton’s Cleaning Solution Set Ref 238290. If blackening of the diaphragm is noted (due to silver compounds), immerse the electrode in 0.4% HCl + 76 g/l thiourea.
ATTENTION! Cleaning, assembly and mainte-
nance should be performed by personnel trained in such work. Do not use any abrasive tissues or clean­ing materials and do not use any cleaning chemicals other then described above. Before removing the sensor from the measuring setup, always make sure that the setup is pressure-less and cold and that no process medium can be accidentally spilled. When removing and cleaning the sensor, it is recommend­ed to wear safety glasses and protective gloves.

8 Troubleshooting

8.1 Sensor Self-Diagnostic

pH/ORP Arc sensors provide a self-diagnostic functionality to detect and identify the most common sensor malfunctions. Both interfaces, analog 4–20 mA or digital Modbus, may provide warn­ing and error messages. The analog 4–20 mA interface can be configured according to the NAMUR recommendations to indi­cate an abnormal event (See Chapter 5.2.3). Use ArcAir for moni­toring the sensor status and for troubleshooting. The following types of messages are provided by the self-diagnosis function.

8.1.1 W a r n i n g s

Warning Cause / Solution
pH calibration Perform a calibration in order to ensure recommended reliable measurement (Chapter 7.2)
pH last calibration Start a new calibration and ensure that not successful always use new calibration solutions (Chapter 7.2)

8.1.2 E r ro r s

Errors (failures) Cause / Solution
pH reading failure At least one error is active
Glass resistance too high Make sure the pH glass membrane is not damaged. Perform a cleaning procedure (Chapter 7.3)
Glass resistance too low Make sure the pH glass membrane has not a crack
Reference electrode Diaphragm is clogged, perform a resistance too high cleaning procedure (Chapter 7.3)
Reference electrode Short circuit at the reference resistance too low electrode, please contact our Technical Support.
Temperature sensor Temp. sensor defective, please defective contact our Technical Support.
Sensor failure Sensor quality value < 15% Perform new calibration
Internal communication No internal communication, error please call our Technical Support
NOTE: Errors cannot be ignored and corrective action
is immediately necessary.
NOTE: Warnings can be ignored but the warning will be displayed continuously until the corrective action is successfully completed.
NOTE: For additional information about the sensor status and the diagnostics features refer to the sensor operation instruction manual or the programmer`s manual.

8.2 Getting Technical Support

If a problem persists even after you have attempted to correct it, contact Hamilton`s Customer Support: Please refer to the contact information at the back of this operating instruction.

8.3 Returning Arc sensors for Repair

Before returning a pH/ORP Arc sensor to Hamilton for repair, contact our Customer Service (see Chapter 8.2) and request a Returned Goods Authorization (RGA) number.
Do not return a pH/ORP Arc sensor to Hamilton without an RGA number. This number assures proper tracking of your sensor. pH/ORP Arc sensors that are returned without an RGA number will be sent back to the customer without being repaired.
Decontaminate the Arc sensor and remove health hazards, such as radiation, hazardous chemicals, infectious agents etc. Pro­vide complete description of any hazardous materials that have been in contact with the sensor.
23Operating Instructions pH/ORP Arc Sensors
DISPOSAL • ORDERING INFORMATION ORDERING INFORMATION

9 Disposal

The design of Hamilton sensors optimally consid­ers environmental compatibility. In accordance with the EC guideline 2012/19/EU Hamilton sensors that
are worn out or no longer required must be sent to a dedicated collection point for electrical and electronic devices, alternatively, must be sent to Hamilton for disposal. Sensors must not be sent to an unsorted waste disposal point.
有害物質表,請參閱www.hamiltoncompany.com,
章節過程分析,符合性聲明

10 Ordering Information

Parts below may only be replaced by original spare parts.

10.1 pH/ORP Arc Sensors

Ref Description
242428-4313 Polilyte Plus PHI Arc 120
242428-4323 Polily te Plus PHI Arc 225
242428-4333 Polily te Plus PHI Arc 325
242428-4353 Polily te Plus PHI Arc 425
242428-1313 Polilyte Plus H Arc 120
242428-1323 Polilyte Plus H Arc 225
242428-1333 Polilyte Plus H Arc 325
242428-1353 Polilyte Plus H Arc 425
242428-3313 Polilyte Plus HF Arc 120
242428-3323 Polily te Plus HF Arc 225
242428-3333 Polily te Plus HF Arc 325
242428-3353 Polily te Plus HF Arc 425
243060 Polilyte Plus ORP Arc 120
243061 Polilyte Plus ORP Arc 225
243062 Polilyte Plus ORP Arc 325
243063 Polilyte Plus ORP Arc 425

10.2 Parts and Accessories

Ref Description
238633-1313 EasyFerm Plus PHI Arc 120
238633-1323 EasyFerm Plus PHI Arc 160
238633-1333 EasyFerm Plus PHI Arc 200
238633-1343 EasyFerm Plus PHI Arc 225
238633-1353 EasyFerm Plus PHI Arc 325
238633-1373 EasyFerm Plus PHI Arc 425
243632-1313 EasyFerm Bio PHI Arc 120
243632-1323 EasyFerm Bio PHI Arc 160
243632-1333 EasyFerm Bio PHI Arc 200
243632-1343 EasyFerm Bio PHI Arc 225
243632-1353 EasyFerm Bio PHI Arc 325
243632-1373 EasyFerm Bio PHI Arc 425
243632-2313 EasyFerm Bio HB Arc 120
243632-2323 EasyFerm Bio HB Arc 160
243632-2333 EasyFerm Bio HB Arc 200
243632-2343 EasyFerm Bio HB Arc 225
243632-2353 EasyFerm Bio HB Arc 325
243632-2373 EasyFerm Bio HB Arc 425
243050 EasyFerm Plus ORP Arc 120
243051 EasyFerm Plus ORP Arc 225
243052 EasyFerm Plus ORP Arc 325
243053 EasyFerm Plus ORP Arc 425
242428-2313 Polilyte Plus HB Arc 120
242428-2323 Polilyte Plus HB Arc 225
242428-2333 Polilyte Plus HB Arc 325
242428-2353 Polilyte Plus HB Arc 425
Ref Product Name Length Interface
355263 Sensor Data Cable VP 8 1 m
355264 Sensor Data Cable VP 8 3 m 4-20 mA/Modbus
355265 Sensor Data Cable VP 8 5 m 4-20 mA/Modbus
355266 Sensor Data Cable VP 8 10 m 4-20 mA/Modbus
355267 Sensor Data Cable VP 8 15 m 4-20 mA/Modbus
355268 Sensor Data Cable VP 8 20 m 4-20 mA/Modbus
Description: The Sensor Data Cable VP 8 – open end is designed for connection to a data recorder, indicator, control unit or PCS (Process Control System) with analog I/O.
4-20 mA/Modbus
25Operating Instructions pH/ORP Arc Sensors
ORDERING INFORMATION ORDERING INFORMATION
Ref Product Name
243460 Arc Wi 1G Adapter BT
Ref Product Name Connection to
243490-01 Arc USB Power Cable Arc Sensor VP 8 Arc Wi 1G Adapter BT
243490-02 Arc USB Power Cable Arc Wi 2G Adapter BT M12 - 8
242176 Arc Sensor Cable VP 8
355339 Arc Wi 2G BT Service Cable 2m
355289 Arc Wi 2G Service Cable 2m
Description: The Arc USB Power Cable provides power supply via USB port for Arc sensors and digital communication to Hamilton’s PC software for monitoring, configuration, calibration and firmware updates.
Description: The Arc Wi 1G Adapter BT provides the wireless communication between the Arc sensors and mobile devices via Bluetooth 4.0.
Ref Product Name
243499 Arc Wireless Converter BT
Description: Designed for wireless communication between ArcAir PC version and Arc Sensors.
Ref Product Name
242333 Arc Wireless Converter Advanced
Description: Designed for wireless communication between ArcAir and Arc Sensors. The advanced version enables ArcAir Advanced in the computer version.
Ref Product Name
243470 Arc Wi 2G Adapter BT
Description: The Arc Wi 2G Adapter BT not only provides wireless communication via Bluetooth 4.0, but also simplifies analog connection of Arc sensors to the process control system (PCS).
27Operating Instructions pH/ORP Arc Sensors
ORDERING INFORMATION
Ref Product Name
10071111 Arc View Mobile Basic
Description: The pre-configured Arc View Mobile, Hamilton`s mobile solution for monitoring measurement values, calibrating Arc sensors and configuring various parameters with the unified user interface for pH, DO, Conductivity and ORP. The Arc View Mobile is based on the Samsung Galaxy Tab Active tablet and comes pre-configured with the ArcAir basic, app blocker application, power supply cable, instruction manual and Hamilton quick guide.
Ref Product Name
100071113 Arc View Mobile Advanced
Description: The pre-configured Arc View Mobile, Hamilton`s mobile solution for monitoring measurement values, calibrating Arc sensors and configuring various parameters with the unified user interface for pH, DO, Conductivity and ORP. The Arc View Mobile is based on the Samsung Galax y Tab Active tablet and comes pre­configured with the ArcAir advanced application, including features for CFR 21 Part 11 and Eudralex Volume 4 Annex 11 compliance, app blocker application, power supply cable, instruction manual and Hamilton quick guide.
ORDERING INFORMATION

10.3 Arc Services

Hamilton service engineers are available in Europe and China in order to provide customers with on-site services. Hamilton offers a wide range of services from technical support to initial opera­tion, qualification and maintenance of the sensors.
Various tailored services are offered especially for the BioPharma, ChemPharma and brewery industries. Experienced service engi­neers ensure an optimal and professional service.
Overview of service offers
Online service
Technical support
Initial Operation/Calibration
Qualification (IQ/OQ)
Service packages
Maintenance
ArcAir Application
Download the ArcAir application from the AppStore and PlayStore.
AppStore > PlayStore >
Training
29Operating Instructions pH/ORP Arc Sensors
NOTES NOTES
31Operating Instructions pH/ORP Arc Sensors
Windows is a registered trademark or trademark of Microsoft Corporation in the United States and/or other countries.
© 2018 Hamilton Bonaduz AG. All rights reserved.
624263/05 — 12/2 018
Web: www.hamiltoncompany.com USA: 800-648-5950
Europe: +41-58-610-10-10
Hamilton Americas & Pacific Rim
4970 Energy Way Reno, Nevada 89502 USA Tel: +1-775-858-3000 Fax: +1-775-856-7259 sales@hamiltoncompany.com
Hamilton Europe, Asia & Africa
Via Crusch 8 CH-7402 Bonaduz, Switzerland Tel: +41-5 8- 610-10 -10 Fax: +41-58- 610-00-10 contact.pa.ch@hamilton.ch
To find a representative in your area, please visit www.hamiltoncompany.com.
This guide may be available in other languages. Visit www.hamiltoncompany.com for more information.
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