Hach-Lange SI794 P User Manual

DOC023.52.90115
si794 P
pH
4-Wire Transmitters
USER MANUAL
October 2008, Edition 1
© HACH LANGE GmbH, 2008. All rights reserved. Printed in Germany
Return of products under warranty
Please contact our Service Team before returning a defective device. Ship the cleaned device to the address you have been given. If the device has been in contact with process fluids, it must be decontaminated/ disinfected before shipment. In that case, please attach a corresponding certificate, for the health and safety of our service personnel.
Disposal
Please observe the applicable local or national regulations concerning the disposal of “waste electrical and electronic equipment”.
Table of contents
Intended use ............................................................................5
Safety information .................................................................. 6
Overview of si794 P ............................................................... 11
Assembly ................................................................................12
Package contents ................................................................................ 12
Mounting plan ..................................................................................... 13
Pipe mounting, panel mounting ...................................................14
Installation and connection ..................................................16
Installation instructions .................................................................... 16
Terminal assignments ........................................................................ 16
pH wiring examples ........................................................................... 18
Protective wiring of relay outputs ................................................ 20
Interface and navigation ...................................................... 22
User interface........................................................................................ 22
Display ..................................................................................................... 23
Operation: Keypad ................................................................24
Safety functions ....................................................................25
Sensocheck, Sensoface sensor monitoring ...............................25
GainCheck device self-test ............................................................... 25
Automatic device self-test ............................................................... 25
Hold mode ...........................................................................................26
External activation of HOLD mode ...............................................27
Configuration ......................................................................... 28
Menu structure of configuration ................................................... 29
Overview of configuration steps ...................................................30
Output 1 .................................................................................................32
Output 2 .................................................................................................40
Temperature compensation ............................................................ 46
Calibration mode ................................................................................ 48
3
Alarm settings ...................................................................................... 50
Limit function .......................................................................................52
Switchover of parameter sets (manual) ...................................... 60
External switchover of parameter sets ........................................ 61
Default settings of parameter sets ...............................................63
Parameter set, individual settings ................................................. 64
Calibration ............................................................................. 66
pH calibration ....................................................................................... 67
Automatic calibration with Calimatic ......................................... 70
Manual calibration ..............................................................................72
Data entry of premeasured electrodes ....................................... 74
Product calibration ............................................................................ 76
Redox calibration ................................................................................78
Temp probe adjustment ................................................................... 80
Measurement .........................................................................80
Diagnostics functions ........................................................... 81
Controller functions ..............................................................84
PID controller ........................................................................................84
Pulse length / pulse frequency controller.................................. 86
Error messages (error codes) ................................................87
Calibration error messages ..............................................................89
Operating states .................................................................... 91
Sensoface ...............................................................................93
Appendix ................................................................................95
Product line and accessories........................................................... 95
Specifications ........................................................................................ 96
Buffer tables ........................................................................................102
Glossary ................................................................................110
Contact information ............................................................114
Limited warranty .................................................................116
Index .....................................................................................119
4
Intended use
The si794 P transmitter is used for pH/mV, ORP, and temperature measurement in industry, environment, food processing, and sewage treatment. The sturdy molded enclosure can be attached to a panel, wall, post or pipe railing. The optional hood provides protection against direct weather exposure and mechanical damage. The transmitter can easily be replaced and it accepts commercially available electrodes with a nominal zero point at pH 7 and ISFET sensors. It provides a second current output for temperature measurement, a PID controller (making use of the relay contacts), and a universal power supply for 24 ... 230 V AC/DC. For CIP applications, you can switch between two parameter sets.
5

Safety information

Be sure to read and observe the following!
The device has been manufactured using state of the art technology and it complies with applicable safety regulations. When operating the device, certain conditions may nevertheless lead to danger for the operator or damage to the equipment. Therefore, please read this entire manual before unpacking, setting up, or operating this equipment. Pay particular attention to all danger and caution statements.
Precautionary labels
Read all labels and tags attached to the instrument. Personal injury or damage to the instrument could occur if not observed. A symbol, if noted on the instrument, will be included with a danger or caution statement in the manual.
This symbol, if noted on the device, references the instruction manual for operation and/or safety information.
This symbol, when noted on a product enclosure or barrier, indicates that a risk of electric shock and/or electrocution exists.
This symbol, when noted on the product, identifies the location of a fuse or current limiting device.
This symbol, when noted on the product, identifies the location of the connection for Protective Earth (ground).
6
This symbol, when noted on the product, identifies a risk of chemical harm and indicates that only indi­viduals qualified and trained to work with chemicals should handle chemicals or perform maintenance on chemical delivery systems associated with the equipment.
This symbol, when noted on the product, identifies the presence of a noxious substance and a risk of chemical harm. Only individuals qualified and trained to work with chemicals should handle chemicals or perform maintenance on chemical delivery systems associated with the equipment.
This symbol, when noted on the product, indicates the presence of devices sensitive to electrostatic discharge (ESD) and indicates that care must be taken to prevent damage with the equipment.
Electrical equipment marked with this symbol may not be disposed of in European public disposal systems after 12 August of 2005. In conformity with European local and national regulations (EU Directive 2002/96/EC), European electrical equipment users must now return old or end-of life equipment to the Producer for disposal at no charge to the user.
Note:
You can obtain instructions on the correct disposal of all (marked and unmarked) electrical products that have been supplied or manufactured by Hach­Lange from your local Hach-Lange sales office.
7
Signal words for hazard information
This manual uses signal words to mark safety information. They are used alone or in combination with a safety symbol. If multiple hazards exist, this manual will use the signal word (Danger, Caution, Note) corresponding to the greatest hazard.
DANGER Indicates a potentially or imminently
hazardous situation which, if not avoided, could result in death or serious injury.
CAUTION Indicates a potentially hazardous situation
that may result in minor or moderate injury.
Important Note Information that requires special
emphasis.
Note Information that supplements points in
the main text.
8
General safety information
Do not use or install the si794 transmitter in any manner other than that which is specified in this manual.
Important Note
Commissioning must only be carried out by trained personnel. Whenever it is likely that protection has been impaired, the device shall be made inoperative and secured against unintended operation. The safety of the transmitter may be impaired if any of the following conditions have occurred:
visible damage• failure to operate properly• storage above 70 °C for prolonged periods• exposure to severe transport stresses•
If any of these conditions have occurred, return the device to the manufacturer for recertification.
Note
Before commissioning it must be proved that the transmitter may be connected with other equipment.
Important Note
Working with chemical samples, standards, reagents, and waste presents potential hazards. The device must only be operated by trained personnel authorized by the operating company. The manufacturer is not liable for any damages caused by process­related risks known to the operating company.
9
Information on how to prevent electrostatic discharges (ESD)
Important Note
The sensitive electronic components in the device can be damaged by static electricity. This can impair device performance and even lead to a complete failure of the device. Before connecting a sensor, for example, you should discharge any static electricity buildup from your body. To do so, you can touch an earth-grounded metal surface such as the chassis of a device or a metal conduit or pipe.
10
Overview of si794 P
Glass electrode
Reference electrode
Auxiliary electrode
RTD
RTD
Shield
ISFET +3V
ISFET
-3V
HOLD
HOLD/ CONTROL
CONTROL
1
pH / mV / temp input
2
3
E
Output 1
Output 2
R1
D
R2
9
10
11
12
13
14
+ Output 1
– Output 1/2
+ Output 2
Relay 1
Relay 1/2
Relay 2
C
± 3 V
4
for ISFET sensor
Alarm
15
16
Alarm
Alarm
5
Clean / PSet 2
Clean
HOLD
6
input
7
Control
8
input
Power
17
18
19
20
Clean / PSet 2
Power
Power
11

Assembly

11
10
9
8
76 5
4
1
2
3
Package contents
Check the shipment for transport damage and completeness. The package should contain:
• Front unit
• Rear unit
• Bag containing small parts
• User manual
• Specific test report
1 Jumper (2 x) 2 Washer (1 x), for conduit
mounting: Place washer between
enclosure and nut 3 Cable tie (3 x) 4 Hinge pin (1 x), insertable from
either side 5 Enclosure screw (4 x)
Fig.: Assembling the enclosure
12
6 Sealing insert (1 x) 7 Rubber reducer (1 x) 8 Strain relief (3 x) 9 Filler plug (3 x) 10 Hex nut (5 x) 11 Sealing plug (2 x),
for sealing in case of wall mounting
Mounting plan
144
144
15
42
84
80
32
21
43
105
27
72
6,2
12
3
4
Fig.: Mounting plan – All dimensions in mm!
1 Strain relief (3 x) 2 Strain relief or 1/2“ conduit
opening, ø 21.5 mm (2 x) Conduit hardware not included! 3 Knockout for pipe mounting (4 x ) 4 Knockout for wall mounting (2 x )
13
40 60
132
1
2
3 4
5
1
132165
173
1
Pipe mounting, panel mounting
1 Protective hood (LZY485) - if required 2 Hose clamp with worm gear drive to DIN 3017 (2 x) 3 Pipe-mount plate (1 x) 4 For vertical or horizontal posts or pipes 5 Self-tapping screw (4 x)
Fig.: Bracket kit (LZY483) – All dimensions in mm!
Fig.: LZY485 protective hood for wall and pipe mounting
– All dimensions in mm!
14
1
2
3
45
max. 25
78 27
1...22
1 Screw (4 x) 2 Gasket (1 x) 3 Control panel 4 Span piece (4 x) 5 Threaded sleeve (4 x)
Fig.: Panel mounting kit (LZY484) – All dimensions in mm!
15

Installation and connection

Installation instructions
Caution!
Any work on the electrical installation may only be undertaken by experienced and qualified personnel in accordance with the applicable local safety regulations.
• Always disconnect power to the device when making any electrical
connections!
• Be sure to follow the instructions in the user manual!
• Only connect the power supply when all internal wirings have been
completed and the system is correctly grounded! When using an external voltage supply, always connect a ground-fault circuit interrupter (tripping current max. 30 mA) between mains and controller system! A ground-fault circuit interrupter is not required when safety extra-low voltages (24 V DC supply via rechargeable batteries or 24 V DC/AC supply through an isolation transformer)! When operating the system outdoors, connect a surge voltage protection between mains and controller system! The terminals are suitable for single wires and flexible leads up to
2.5 mm² (AWG 14). Attach end ferrules to the leads.
Terminal assignments
Danger of electric shock!
Fig.: si794 P terminal assignments
16
4
3
1 ESD shield covering the signal inputs (Screw off for assembly)
Note:
The cable shield must end under the ESD shield. (Cut lines if required)
2 Terminals for temperature probe and outer shield 3 Terminals for electrode 4 Power supply connection
1
2
Fig.: Information on installation, rear side of device
17
pH wiring examples
Example 1:
pH measurement with monitoring of glass electrode
Jumper across 2 and 3
Cable shield –
Do not ground!
Color
Top 68
Assign-
ment
Jumper
cable
Coax core
Coax (shield)
Terminal
1 Glass
elec­trode
2 Ref.
elec­trode
(
3
2-3)
C Shield Green/
D RTD Red Green Red E RTD White White White
SMEK cable
Trans­parent (coax core)
Black (coax shield)
yellow
8350.0
Trans­parent (coax core)
Black (coax shield)
18
Example 2:
pH measurement with monitoring of glass and reference electrode
Terminal
Assign-
1 Glass
electrode
2 Reference
electrode 3 SG Blue C Shield D RTD Red E RTD White
Cable shield –
Do not ground!
ment
Color
8350.3
8350.4
8350.5
Transparent (coax core)
Black (coax shield)
19
1
2
3
1
2
3

Protective wiring of relay outputs

Protective wiring of relay contacts
Relay contacts are subject to electrical erosion. Especially with inductive and capacitive loads, the service life of the contacts will be reduced. For suppression of sparks and arcing, components such as RC combinations, nonlinear resistors, series resistors, and diodes should be used.
Typical AC applications with inductive load
1 Load 2 RC combination, e.g. RIFA PMR 209 Typical RC combinations for 230 V AC: Capacitor 0.1µF / 630V, Resistor 100 ohms / 1 W 3 Contact
20
Typical protective wiring measures
A: DC application with inductive load B: AC/DC applications with capacitive load C: Connection of incandescent lamps
A1 Inductive load A2 Free-wheeling diode, e.g. 1N4007 (Observe polarity) A3 Contact B1 Capacitive load B2 Resistor, e.g. 8 Ω / 1 W at 24 V / 0.3 A B3 Contact C1 Incandescent lamp, max 60 W / 230 V, 30 W / 115 V C3 Contact
Warning! Make sure that the maximum ratings of the relay contacts are not exceeded even during switching!
21

Interface and navigation

The si794 transmitter user interface contains a display, indicators, and keys for navigation and menu selection.
User interface
Use the arrow and enter keys to scroll through the menu and change settings. Use the indicators to identify which mode the transmitter is in.
6
5
4
3
2
1
Fig.: si794 user interface
1 Calibration key 7 Wash mode indicator 2 Congure key 8 Conguration mode indicator 3 Measure mode indicator 9 Up arrow key 4 Calibration mode indicator 10 Right arrow key 5 Alarm indication 6 Display
11 Enter key
7
8
9
10
11
22
Display
Interface and navigation
4.3 Display
Figure 11 identifies all of the possible icons and symbols that may be
seen in the si792 transmitter display.
The gure below identies all of the possible icons and symbols that may be seen in the si794 transmitter display.
Fig.: si794 display
1 Passcode 13 Secondary display 2 Temperature 14 Alarm mode 3 4–20 mA/HART output 15 Manual temperature on 4 Limit values 16 Calibration mode 5 Alarm 17 Hold mode active 6 Sensocheck: Sensor error 18 Hourglass (waiting indication) 7 Calibration active 19 Measure mode active 8 Calibration interval 20 Calibration complete
8 Parameter display 21 Calibration: zero or rst point 10 Enter prompt 22 Calibration: second point 11 Conguration mode 12 Main display
23 Sensofaces
23
Operation: Keypad
Start, end calibration
Start, end configuration
Select digit position (selected position blinks)
Edit digit
• Calibration:
Continue in program sequence
• Configuration: Confirm entries,
next configuration step
• Measuring mode: Display output current
Cal Info: Display of offset (zero point) and slope
Error Info: Display of last error message
24
+
Start GainCheck device self-test

Safety functions

Sensocheck, Sensoface sensor monitoring
Sensocheck continuously monitors the sensor and its wiring. Sensocheck can be switched o (Conguration).
Sensoface provides information on the electrode condi­tion. The oset (zero point), slope, and response time during calibration are evaluated. The three Sensoface indicators provide the user with information about wear and required maintenance of the electrode.
GainCheck device self-test
A display test is carried out, the software version is displayed, and the memory and signal transfer are checked.
Start GainCheck device self-test:
Automatic device self-test
The automatic device self-test checks the memory and signal transfer. It runs automatically in the background at xed intervals.
+
25
Safety functions
Hold mode
Display:
The Hold mode is a safety state during conguration and calibra­tion. Output current is frozen (Last) or set to a xed value (Fix). Alarm and limit contacts are disabled. If the calibration or conguration mode is exited, the transmitter remains in the Hold mode for safety reasons. This prevents un­desirable reactions of the connected peripherals due to incorrect conguration or calibration. The measured value and “HOLD” are displayed alternately. The transmitter only returns to measuring mode after enter is pressed and 20 seconds have passed.
Conguration mode is also exited automatically 20 minutes (timeout) after the last keystroke. The transmitter returns to measuring mode.
Timeout is not active during calibration.
Response of output signal: Last: The output current is frozen at its last value.
Recommended for short conguration procedures. The process should not change decisively during con­guration. Changes are not noticed with this setting!
Fix: The output current is set to a value that is noticeably
dierent from the process value in order to signal the control system that the transmitter is being worked at.
26
External activation of HOLD mode
The Hold mode can be activated from outside by sending a signal to the Hold input (e.g. from the process control system).
Power supply
Hold
12...24 V AC/DC
6
input
si794
7
Process control system
Hold active Hold inactive 10 ... 30 V AC/DC 0 ... 2 V AC/DC
Alarm
The alarm delay is congurable. During an error message the alarm LED blinks or lights.
Error messages can also be signaled by a 22 mA output current. The alarm contact is activated by alarm or power failure, see also Pg 50.
The alarm LED on the front panel can be congured as follows HOLD o: Alarm: LED blinks HOLD on: Alarm: LED on. HOLD: LED blinks
27

Configuration

In the Configuration mode you set the device parameters. The device can store two different parameter sets and switch between them. Sensor data and “Clean/Pset2” output are edited in parameter set 1 only. They are valid for both parameter sets.
Configuring
Parameter set 1
Configure:
Press conf.
Enter mode code “1200”: Edit parameter set 1 with and , con­firm/proceed with enter.
Parameter set 2
Configure: “88” appears in the display.
Enter mode code “1288”: Edit parameter set 2 with firm/proceed with enter.
and , con-
The output current is frozen
Hold
During configuration the device remains in the Hold mode.
Input errors
HOLD icon
(at its last value or at a preset fixed value, depending on the configurati­on), limit and alarm contacts are inac­tive. The controller is in the configured state, Sensoface is off, mode indicator “Configuration” is on.
The configuration parameters are checked during the input. In the case of an incorrect input “Err” is dis­played for approx. 3 s. The incorrect parameters cannot be stored. Input must be repeated.
End End with conf. The measured value
and Hold are displayed alternately, “enter” flashes. End Hold mode with enter . The display shows the measu­red value. The output current remains frozen for another 20 s (HOLD icon on, “hourglass” flashes).
28
Menu structure of conguration
The conguration steps are assigned to dierent menu groups. Use the arrow keys to jump between the individual menu groups. Each menu group contains menu items for setting the parameters. Press enter to access a menu item. Use the arrow keys to edit values. Press enter to conrm/save the settings. To return to measurement, press conf and then enter.
Select menu group
Menu group Code Display
Output 1 o1.
Menu item 1
Menu item 2
Menu item ...
Output 2 o2.
Temperature compensation
Calibration mode CA.
Alarm settings AL.
Relay rL.
Cleaning contact PSet 2 selection
tc.
Cn.
...
Select menu item
Previous menu group:
29
Overview of conguration steps
Code
Menu
Output 1
out1
o1.
Select process variable Select electrode type
Select current range Enter current start
Enter current end
Time averaging filter
22 mA signal in the case of error
Signal response during HOLD
Enter fixed value
Output 2
out2
o2.
Select temperature unit
Select temperature probe
Select current range
Enter current start Enter current end
Time averaging filter
22 mA signal for temp error
Signal
response
Enter fixed value
Temperature compensation
tc.
tc.
Temp detection during meas Temp detection during cal Enter TC process medium
Calibration mode
CAL
CA.
Select calibration mode
Enter cal timer interval
during HOLD
Choices Default
PH/ORP PH (GLAS EL/FEt EL ) GLAS EL 0-20 mA/4-20 mA 4-20 mA xxxx 00.00 pH xxxx 14.00 pH xxxx SEC 0 SEC ON / OFF OFF Last / Fix Last xxx.x mA 021.0 mA
°C / °F °C 100 Pt/1000 Pt/30NTC/
8.55NTC/3000B 1000 Pt 0-20 mA/4-20 mA 4-20 mA xxx.x 000.0 °C xxx.x 0100.0 °C 0000 ... 0120 SEC) 0 SEC ON / OFF OFF Last / Fix Last xxx.x mA 021.0 mA
Auto/man (man: xxx.x °C) Auto/man (man: xxx.x °C) xx.xx %/K 00.00%/K
BUF/MAN/DAT 06 BUF xxxx h 0000 h
30
Code
Menu
Alarm settings
ALrt
AL.
Select Sensocheck
Enter alarm delay
LED in HOLD mode
Relay 1/2: Limit values, controller
rL AY
rL.
Select limit function / controller
Select contact function
L1.
Select contact response Enter setpoint Enter hysteresis Enter delay Select contact function
L2.
Select contact response
Enter setpoint
Enter hysteresis Enter delay
Enter controller setpoint
Ct.
Enter neutral zone
(P) Controller gain K
(I) Reset time T
(D) Rate time T
Pulse length/frequency controller
PLC: Pulse length PFC: Pulse frequency
Select HOLD response
Cleaning contact
Cln.
Cn.
Select cleaning contact or signaling of parameter set 2
Cleaning interval
rinse
Cleaning duration Select contact response
Choices Default
ON / OFF OFF xxxx sec 0010 sec ON / OFF OFF
LiMIT / CtROL LiMIT Lo / Hi Lo N/O / N/C N/O xxxx 00.00 pH xxxx 00.50 pH xxxx SEC 0010 SEC
Lo / Hi Hi
N/O / N/C N/O xxxx xxxx 00.50 pH xxxx SEC 0010 sec xxxx 07.00 pH xxxx 01.00 pH xxxx % 0100 %
P
R
D
xxxx SEC 0000 SEC xxxx SEC 0000 SEC
PLC / PFC PLC xxxx SEC 0010 SEC xxxx /min 0060 /min Y Last / Y Off Y Last
rinse / Pset2 rinse
xxx.x h 000.0 h xxxx SEC 0060 SEC N/O / N/C N/O
14.00 pH
31
Conguration
Output 1 Select type of electrode / Measurement procedure
Menu group
Output 1
Code
o1.
Display
Select menu item
Select process variable
Select electrode type
Select 0-20 / 4-20 mA
Enter current start
Enter current end
Set output filter
22 mA for error
HOLD mode
Exit: Press conf, then enter.
32
Code Display
o1.
After correct input a welcome text (CONF) is displayed for approx. 3 sec
Action
Select configuration (Press conf.)
Enter passcode “1200” (Use to select the position, use to edit the number. When the display reads “1200”, press enter to confirm.)
The transmitter goes to HOLD mode. (HOLD icon is active, red LED blinks when “HOLD ON” has been configured.)
Choices
Select parameter pH/ORP Select using key Press enter to proceed
Only with pH selected: Select electrode type:
• Glass electrode
• ISFET electrode
Select using key Press enter to proceed
Note: Characters represented in gray are blinking and can be edited.
pH/ORP
Glass
(FEt EL)
33
Conguration
Output 1 Output current range / Current start / Current end
Menu group
Output 1
Code
o1.
Display
Select menu item
Select process variable
Select electrode type
Select 0-20 / 4-20 mA
Enter current start
Enter current end
Set output filter
22 mA for error
HOLD mode
34
Exit: Press conf, then enter.
Code
o1.
Display
Action
Set output current range Select using key Press enter to proceed
Choices
4 - 20 mA
(0 - 20 mA)
Current start Enter lower end of scale, depending on the process variable selected (pH or ORP) Select using , edit number using . Press enter to proceed.
Current end Enter upper end of scale, depending on the process variable selected (pH or ORP) Select using , edit number using . Press enter to proceed.
Assignment of measured values: Current start and current end
Example 1: Range pH 0 ... 14 Example 2: Range pH 5 ... 7 .
[pH]
14
0
Output current
20 4
Advantage: Higher resolution in
[mA]
range of interest
[pH]
7
5
Output current
pH -2 ... 16
(-1500 mV ... +1500mV)
pH -2 ... 16
(-1500 mV ... +1500mV)
20 4
[mA]
35
Conguration
Output 1 Time averaging lter
Menu group
Output 1
Code
o1.
Display
Select menu item
Select process variable
Select electrode type
Select 0-20 / 4-20 mA
Enter current start
Enter current end
Set output filter
22 mA for error
HOLD mode
Exit: Press conf, then enter.
36
Display Action
Code
o1.
Time interval of output filter Default setting: 0 sec (inactive). To specify a time interval: Select position using , edit number using . Press enter to proceed.
Choices
0 sec
0...120 sec
Time averaging filter
To smoothen the current output, a low-pass filter with adjustable filter time can be switched on. When there is a jump at the input (100 %), the output level is at 63 % after the time interval has been reached. The time interval can be set from 0 to 120 sec. If the time interval is set to 0 sec, the current output follows the input.
Note:
The filter only acts on the current output, not on the display, the limit values, or the controller!
Time interval 0 to 120 sec
37
Conguration
Output 1 Output current during Error and HOLD
Menu group
Output 1
Code
o1.
Display
Select menu item
Select process variable
Select electrode type
Select 0-20 / 4-20 mA
Enter current start
Enter current end
Set output filter
22 mA for error
HOLD mode
Exit: Press conf, then enter.
38
Code
o1.
Display
Action
22 mA signal for error message Select using key Press enter to proceed
Choices
OFF
(ON)
Output signal during HOLD LAST: During HOLD the last measured value is maintained at the output FIX: During HOLD a value (to be entered) is maintained at the output Select using key Press enter to proceed
Only with FIX selected: Enter current which is to flow at the output during HOLD Select position usingkey and edit number using key. Press enter to proceed
Output signal during HOLD:
Output current [mA]
21
4
Output signal for HOLD FIX setting = 21.0 mA
HOLD active
LAST
(FIX)
21.0 mA
(00.0 ...
21.0 mA)
Output signal for HOLD LAST setting
HOLD active
39
Conguration
Output 2 Temperature unit and probe / Output current
Menu group
Output 2
Code
o2.
Display
Select menu item
Select °C/°F
Select temperature probe
Select 0-20 / 4-20 mA
Enter current start
Enter current end
Set output filter
22 mA for temp error
HOLD mode
Exit: Press conf, then enter.
40
Code
o2.
Display
Action
Specify temperature unit Select using key Press enter to proceed
Select temperature probe Select using key Press enter to proceed
Set output current range Select using key Press enter to proceed
Choices
°C
(°F)
1000 PT
(100 PT, 30NTC,
8.55NTC, 3000B)
4 - 20 mA
(0 - 20 mA)
Current start: Enter lower end of scale. Select using , edit number using. Press enter to proceed.
Current end: Enter upper end of scale. Select using , edit number using. Press enter to proceed.
Process temperature: Current start and current end
Example 1: Range 0 ... 100 °C Example 2: Range 50 ... 70 °C
[°C]
Process temperature
100
0
Output current
20 4
Advantage: Higher resolution in
[mA]
range of interest
Process temperature
[°C] 70
50
000.0 °C
100.0 °C
Output current
20 4
[mA]
41
Conguration
Output 2 Time averaging lter
Menu group
Output 2
Code
o2.
Display
Select menu item
Select °C/°F
Select temperature probe
Select 0-20 / 4-20 mA
Enter current start
Enter current end
Set output filter
22 mA for temp error
HOLD mode
Exit: Press conf, then enter.
42
Code
o2.
Display
Action
Time averaging filter Default setting: 0 sec (inactive). To specify a time constant: Select using , edit number using. Press enter to proceed.
Choices
0 sec
(0...120 sec)
Time averaging filter
To smoothen the current output 2, a low-pass filter with adjustable filter time can be switched on. When there is a jump at the input (100 %), the output level is at 63 % after the time interval has been reached. The time interval can be set from 0 to 120 sec. If the time interval is set to 0 sec, the current output follows the input.
Note:
The filter only acts on the current output, not on the display, the limit values, or the controller!
Time interval 0 to 120 sec
43
Conguration
Output 2 Temperature error / Output current during HOLD
Menu group
Output 2
Code
o2.
Display
Select menu item
Select °C/°F
Select temperature probe
Select 0-20 / 4-20 mA
Enter current start
Enter current end
Set output filter
22 mA for temp error
HOLD mode
Exit: Press conf, then enter.
44
Code
o2.
Display
Action
22 mA signal for error message Select using key Press enter to proceed
Choices
OFF
(ON)
Output signal during HOLD LAST: During HOLD the last measured value is maintained at the output FIX: During HOLD a value (to be entered) is maintained at the output Select using key Press enter to proceed
Only with FIX selected: Enter current which is to flow at the output during HOLD Select position usingkey and edit number using key. Press enter to proceed
Output signal during HOLD:
Output current [mA]
21
4
Output signal for HOLD FIX setting = 21.0 mA
HOLD active
LAST
(FIX)
21.0 mA
(00.0 ...
21.0 mA)
Output signal for HOLD LAST setting
HOLD active
45
Conguration
Temperature compensation Temp detection for meas/cal / TC process medium
Menu group
Temperature compensation
Code
tc.
Display
Select menu item
Temp during meas.
Temp during calibration
TC of process medium
46
Exit: Press conf, then enter.
Code
tc.
Display
Action
Select temp detection during measurement (Auto/MAN) AUTO: Temp detection with temperature probe MAN: Manual temperature input Select using key, press enter to proceed
Choices
AUT
(MAN)
Only with manual temp detection selected (MAN) Enter temperature. Select position using key, edit number using key. Press enter to proceed
Select temp detection during calibration (Auto/MAN) Select using key, press enter to proceed
Only with manual temp detection selected (MAN) Enter temperature. Select position using key, edit number using key. Press enter to proceed
For pH measurement only: Enter temperature compensation of process medium Select position using key, edit number using key. Press enter to proceed
25.0 °C
(xxx.x °C)
AUT
(MAN)
25.0 °C
(xxx.x °C)
00.00 %/K
(-19.99 ...
19.99 %/K)
47
Conguration
Calibration mode
Menu group
Calibration mode
Code
CA.
Display
Select menu item
Calibration mode
Cal timer interval
Exit: Press conf, then enter.
48
Code
CA.
Display
Action
For pH measurement only: Select calibration mode BUF: Calibration with Calimatic automatic buffer selection. To do so, you must select your buffer set:
-01- BUF: Mettler-Toledo
-02-BUF: Merck Titrisols, Riedel Fixanals
-03- BUF: Ciba (94)
-04-BUF: NIST technical buffers
-05-BUF: NIST standard buffers
-06-BUF: HACH buffers
-07-BUF: WTW technical buffers
-08- BUF: Hamilton Duracal
MAN: Calibration with Manual Buffer Entry
DAT: Entry of offset and slope of premeasured electrodes Select using key, proceed.
press enter to
Choices
-01-BUF (-02-BUF/
-03-BUF/
-04-BUF/
-05-BUF/
-06-BUF/
-07-BUF/
-08-BUF/ MAN/ DAT )
Enter calibration interval: Entry of time interval within which the transmitter is to be calibrated. With a time interval of 0000 hrs the calibration timer is not active. Select using , edit number using.
Press enter to proceed.
0000 h
(0000 ... 9999 h)
49
Conguration
Alarm settings
Menu group
Alarm settings
Alarm
Code
AL.
Display
Select menu item
Select Sensocheck
Delay
LED in HOLD mode
Exit: Press conf, then enter.
Alarm contact
15
The alarm contact is closed during normal operation (N/C). It opens in the case of alarm or power outage. As a result,
16
a failure message is provided even in the case of line breakage (fail-safe behavior). For contact ratings, see Specifications.
Error messages can also be signaled by a 22 mA output current.
The operating behavior of the alarm contact is shown on Pg 91.
The alarm delay acts on the LED, the 22 mA signal, and the alarm contact.
50
Code
Display
Action
Choices
AL.
Select Sensocheck (continuous monitoring of glass and reference electrode) Select using
press enter to proceed.
Alarm delay
Select using, edit number using
LED in Hold mode
Select using  key,
press enter to proceed.
LED state:
Setting
ON
OFF
key,
. Press
enter to proceed.
Alarm HOLD
on blinks
blinks off
ON/OFF
0010 sec
(xxxx sec)
ON/OFF
51
Conguration
Limit function Relay 1
Menu group
Relay / Controller
Code
rL.
Display
Select menu item
Contact function
L1.
Contact response
Enter setpoint
Enter hysteresis
Delay
L2.
Relay 2 menu group Controller menu group
Ct.
Exit: Press conf, then enter.
52
Code
rL.
Display
Action
Use of relays:
Limit function (LiMIT )
• Controller (CtROL)
Select using
Press enter to proceed.
Note: Selecting CtROL leads to Ct. controller menu group.
.
Choices
LiMIT
(CtROL)
L1.
For limit 1 function principle, see page 55. Select using
Press enter to proceed.
Limit 1 contact response N/C: normally closed contact N/O: normally open contact
Select using .
Press enter to proceed
Limit 1 setpoint
Select using , edit number
. Press enter to proceed.
using
Limit 1 hysteresis
Select using , edit number
. Press enter to proceed.
using
Limit 1 delay
The contact is activated with delay (deactivated without delay) Select using using
, edit number
. Press enter to proceed.
.
Lo
(Hi)
N/C (N/O)
00.00 pH
(
xx.xx pH)
00.50 pH
(
xx.xx pH)
0010 sec
(
0 ... 9999
sec)
53
Configuration
Limit function Relay 2
Menu group
Relay / Controller
Code
rL.
Display
Select menu item
Relay 1 menu group
L1.
Contact function
L2.
Contact response
Enter setpoint
Enter hysteresis
Delay
Controller menu group
Ct.
Exit: Press conf, then enter.
54
Code
Display Action
Choices
L2.
Limit Lo
Hysteresis +
Setpoint
Contact
For limit 2 function principle, see Fig. below. Select using
.
Hi
(Lo)
Press enter to proceed.
Limit 2 contact response N/C: normally closed contact
N/C (N/O)
N/O: normally open contact
Select using .
Press enter to proceed.
Limit 2 setpoint
Select using using
, edit number
. Press enter to proceed.
Limit 2 hysteresis
Select using
. Press enter to proceed.
using
, edit number
Limit 2 delay
The contact is activated with delay (deactivated without delay)
Select using using
Signal
1
0
, edit number
. Press enter to proceed.
Limit Hi
Setpoint
Hysteresis -
1
Contact
0
14.00 pH
(
xx.xx pH)
00.50 pH
(
xx.xx %)
0010 sec
(
0 ...
9999 sec)
Signal
55
Conguration
Controller (For description see Pg 84 and the following) Setpoint / Neutral zone
Menu group
Relay / Controller
Code
rL.
Display
Select menu item
Relay 1 menu group
L1.
Relay 2 menu group
L2.
Ct.
Controller setpoint
Enter neutral zone
(P) Controller gain
(I) Reset time TR
(D) Rate time TD
Pulse length / Pulse frequency controller
PLC: Pulse length
PFC: Pulse frequency
HOLD response
Exit: Press conf, then enter.
56
Code
Ct.
Display
Action
Setpoint
Select using , edit number
. Press enter to proceed.
using
Neutral zone (dead band)
Select using , edit number
. Press enter to proceed.
using
Controller: P action
Select using , edit number
. Press enter to proceed.
using
Choices
07.00 pH
(xx.xx pH)
01.00 pH
(xx.xx pH)
0100 %
(xxxx %)
Controller: I action (reset time)
Select using , edit number
. Press enter to proceed.
using
Controller: D action (rate time)
Select using , edit number
. Press enter to proceed.
using
Pulse length / Pulse frequency Select using
Press enter to proceed.
PLC: Pulse length
Select using , edit number using
PFC: Pulse frequency
Select using , edit number using
Behavior during HOLD
Select using .
Press enter to proceed.
.
. Press enter to proceed.
. Press enter to proceed.
0000 sec
(xxxx sec)
0000 sec
(xxxx sec)
PLC
(PFC)
0010 sec
(xxxx sec)
0060/min
(xxxx /min)
Y Last
(Y Off)
57
Configuration
Controlling a rinsing probe or Signaling parameter set 1/2
Menu group
Contact: CLEAN / PSet2
Code
Display
Cn.
rinse
58
Code
Cn.
Display
Select menu item
Select CLEAN / PSet2
Rinsing interval
Rinse time
Contact response
Action (rinsing probe)
Function selection*:
• Control of rinsing probe (rinse)
Signaling active parameter set 2
Select using , proceed.
Rinsing interval * Select using , edit number
, press enter to proceed.
using
Rinse duration * Select using , edit number
, press enter to proceed.
using
Select contact response* N/O: normally open contact N/C: normally closed contact Select using , proceed
*) These parameters are only edited in parameter set 1.
They are valid for both parameter sets.
press enter to
press enter to
Choices
rinse
(rinse / PSet2)
For
PSet2 see next page
000.0 h
(xxx.x h)
0060 sec (xxxx sec)
N/O
(
N/O
N/C)
:
Controlling a rinsing probe
The “Clean” contact can be used to connect a simple rinsing probe. Rinse duration and rinsing interval are defined during configuration. Contact response can be set as N/O or N/C.
e.g. spray cleaning
Clean
17
18
Signaling parameter set 1/2
Depending on the selected parameter set, the relay is active or inactive. The signal can be used for super­ordinated process control systems. Parameter set 2 is indicated by “88” in the upper left corner of the display.
Clean PSet2
17
18
si794
Parameter set 1 selected
Parameter set 2 selected
Power supply
Power supply
Process control system
Power supply: AC< 250 V / < 3 A / < 750 VA DC< 30 V / < 3 A / < 90 W
59

Selecting parameter set 1/2

Manually or via a signal at the Control input
Display
After correct input a welcome text (CONF) is displayed for approx. 3 sec
Action Choices
To select a parameter set, press conf, enter code: 7654 Select position using , edit number using ,
Wrong settings change the measurement properties! If an invalid code is entered, the transmitter returns to measuring mode.
press enter to proceed.
Select:
• Parameter set 1 (MAN)
• Parameter set 2 (MAN)
• Automatic switchover via
control input (Ctr-EXT)
Select using ,
With -1- or -2- selected: Since the complete device configura­tion is changed in one step, there is a security prompt (No/Yes).
Note: When pressing enter directly, the selection is not stored. Activation of parameter set 2 is indicated by “88” in the upper left corner of the display.
press enter to proceed.
-1-
(-1- MAN
-2-MAN Ctr-EXT)
For Ctr-EXT, see next page
60
Display
Action Choices
With Control input You can switch between the parameter sets by applying an external signal to the Control input (see below).
Ctr-EXT selected:
External switchover of parameter sets
The parameter set can be selected from outside by sending a signal to the Control input (e.g. from the process control system). To do so, Ctr-EXT is set during configuration.
Control
Power supply
7
input
si794
Note:
Parameter set 2 is indicated by “88” in the upper left corner of the display.
8
Process control system
0 ... 2 V AC/DC Parameter set 1 selected
10 ... 30 V AC/DC Parameter set 2 selected
61
62

Default settings of parameter sets

Two complete parameter sets are stored in the EEPROM. As delivered, the two sets are identical but can be edited. Note: Fill in your configuration data on the following pages.
Code. Parameter Default setting
o1. pH/ORP unit pH o1. Electrode type GLASS o1. 0/4-20 mA 4-20 mA o1. Current start 00.00 pH o1. Current end 14.00 pH o1. Filter time 0 s o1. 22mA signal OFF o1. HOLD response Last o1. Fix current 021.0 mA o2. Unit °C / °F °C o2. Temp probe 1000 PT o2. 0/4 ...20mA 4-20 mA o2. Current start 000.0 °C o2. Current end 100.0 °C o2. Filter time 0 s o2. 22mA signal OFF o2. HOLD response Last o2. Fix current 021.0 mA tc. TC measurement Auto tc. Measuring temp 025.0 °C tc. TC calibration Auto tc. Calibration temp 025.0 °C tc. TC medium 00.00 %/K CA. Cal solution -06-BUF CA. Cal interval 0000 h AL. Sensocheck OFF AL. Alarm delay 0010 sec AL. LED Hold OFF
Code. Parameter Default setting
rL. Relay function Limit L1. Contact function Lo L1. Contact response N/C L1. Setpoint 00.00 pH L1. Hysteresis 00.50 pH L1. Delay 0010 sec L2. Contact function H i L2. Contact response N/C L2. Setpoint 14.00 pH L2. Hysteresis 00.50 pH L2. Delay 0010 sec Ct. Setpoint 07.00 pH Ct. Neutral zone 01.00 pH Ct. P action 0100 % Ct. I action 0000 sec Ct. D action 0000 sec Ct. PLC/PFC controller PLC Ct. Pulse length 0010 sec Ct. Pulse frequency 0060 /min Ct. Hold response Last Cn. Rinse/Par.set 2 Rinse Cn. Rinsing interval 000.0 h Cn. Rinse duration 0060 sec Cn. Contact type N/C
63
Parameter set, individual settings
Code. Parameter Setting
o1. pH/ORP unit ____________ ____________ o1. Electrode type ____________ ____________ o1. 0/4-20 mA ____________ ____________ o1. Current start ____________ ____________ o1. Current end ____________ ____________ o1. Filter time ____________ ____________ o1. 22mA signal ____________ ____________ o1. HOLD response ____________ ____________ o1. Fix current ____________ ____________
o2. Unit °C / °F ____________ ____________ o2. Temp probe ____________ ____________ o2. 0/4 ...20mA ____________ ____________ o2. Current start ____________ ____________ o2. Current end ____________ ____________ o2. Filter time ____________ ____________ o2. 22mA signal ____________ ____________ o2. HOLD response ____________ ____________ o2. Fix current ____________ ____________
tc. TC measurement ____________ ____________ tc. Measuring temp ____________ ____________ tc. TC calibration ____________ ____________ tc. TC medium ____________ ____________
CA. Cal solution ____________ ____________ CA. Cal interval ____________ ____________
AL. Sensocheck ____________ ____________ AL. Alarm delay ____________ ____________ AL. LED Hold ____________ ____________
64
Code Parameter Setting
rL. Relay function ____________ ____________
L1. Contact function ____________ ____________ L1. Contact response ____________ ____________ L1. Setpoint ____________ ____________ L1. Hysteresis ____________ ____________ L1. Delay ____________ ____________
L2. Contact function ____________ ____________ L2. Contact response ____________ ____________ L2. Setpoint ____________ ____________ L2. Hysteresis ____________ ____________ L2. Delay ____________ ____________
Ct. Setpoint ____________ ____________ Ct. Neutral zone ____________ ____________ Ct. P action ____________ ____________ Ct. I action ____________ ____________ Ct. D action ____________ ____________ Ct. PLC/PFC controller ____________ ____________ Ct. Pulse length ____________ ____________ Ct. Pulse frequency ____________ ____________ Ct. Hold response ____________ ____________
Cn. Rinse /Par.set2 ____________ ____________ Cn. Rinsing interval ____________ ____________ Cn. Rinse duration ____________ ____________ Cn. Contact type ____________ ____________
65

Calibration

Calibration adjusts the transmitter to the electrode.
Activation Activate with cal
Enter passcode. Use and to edit a parameter. Press enter to conrm/continue. (To exit, press cal, then enter.)
HOLD
During cali­bration the transmitter remains in the Hold mode.
HOLD icon
Input errors
Exit
During calibration the transmit­ter remains in the Hold mode for reasons of safety. Output current is frozen (last value or preset xed value, depending on conguration), limit and alarm contacts are inactive. The controller is in the congured state, Sensoface is o, “Calibra­tion” mode indicator is on. The red LED blinks when “HOLD ON” has been set.
The calibration parameters are checked during the input. In the case of an incorrect input “Err” is displayed for approx. 3 sec. The incorrect parameters cannot be saved. Input must be repeated.
Press cal to exit. The measured value is shown in the main display alternately with “Hold”, “enter” blinks, Sensoface is active. Press enter key to end the Hold mode. The measured value is displayed. The output current remains frozen for another 20 sec (HOLD icon on, “hourglass” blinks).
66
pH calibration
Calibration is used to adapt the transmitter to the individual electrode characteristics, namely oset and slope. Calibration can be performed with Calimatic automatic buer recognition, with manual buer input, by entering premeasured electrode data, or by sampling the product. When using ISFET sensors, you must adjust the zero point rst. Then you can conduct either a one or a two-point calibration. Caution
All calibration procedures must be performed by trained
personnel. Incorrectly set parameters may go unnoticed, but change the measuring properties.
The response time of the electrode and temperature probe is
considerably reduced when the electrode is rst moved about in the buer solution and then held still.
The transmitter can only operate properly when the buer
solutions used correspond to the congured set. Other buf­fer solutions, even those with the same nominal values, may demonstrate a dierent temperature response. This leads to measurement errors.
When using ISFET sensors or electrodes with a zero point other than pH 7, the nominal zero point must be adjusted each
time a new electrode is connected. This is important if you want to obtain reliable Sensoface messages. The Sensoface messages issued during all further calibrations are based on this basic calibration.
67

Zero adjustment (ISFET)

Allows use of electrodes with diering nominal zero (pH only)
Display
Action
Press cal, enter code: 1001 Select position using , edit number using , press enter to proceed.
Ready for calibration “CAL” and “enter” are blinking.
Immerse electrode in a pH 7.00 buffer. Enter the perature-corrected pH value in the range 6.50 to 7.50 using the arrow keys (see buffer table). Press enter to confirm.
Stability check. The measured value [mV] is displayed. The “hourglass” icon is blinking.
tem-
Remark
The transmitter is in the Hold mode. If an invalid code is entered, the transmitter returns to measuring mode.
Display (3 sec)
If the zero offset of the electrode is too large (> ± 200 mV ), the CAL ERR error message is generat­ed. In that case the electrode cannot be calibrated.
Note: Stability check can be stopped (by pressing cal). However, this reduces calibration accuracy.
68
Display
Action
At the end of the adjustment procedure the zero offset [mV] of the electrode is displayed (based on 25 °C). Press enter to proceed.
Remark
This is not the final calibration value of the electrode! Zero point and slope must be determined using a complete 2-point calibration (cal 1100) (see following pages).
Confirmation prompt. Display of pH value (alternately with Hold) and temperature, “enter” blinks, Sensoface is active.
Place electrode in process.
Press enter to end zero calibration.
After end of calibra­tion, the outputs remain in Hold mode for approx. 20 sec.
Note for zero adjustment
After having adjusted the nominal zero point, be sure to calibrate the electrode following one of the procedures as described on the next pages:
• Automatic calibration with Calimatic
• Manual calibration
• Data entry of premeasured electrodes
69
Automatic calibration with Calimatic (BUF -xx-) Automatic or manual temperature detection
The transmitter can only operate properly when the buffer solutions used correspond to the configured set. Other buffer solutions, even those with the same nominal values, may demonstrate a different temperature response. This leads to measurement errors.
Display
70
Action
Press cal, enter code: 1100 Select position using , edit number using press enter to proceed.
Remove the electrode and temperature probe, clean them, and immerse them in the first buffer solution (in any order). When “Manual temp detection” has been configured, enter the value in the secondary display using the arrow keys. Press enter to start.
Buffer recognition While the “hourglass” icon is blinking, the electrode and temperature probe remain in the first buffer solution.
Buffer recognition terminated, the nominal buffer value is displayed.
,
Remark
If an invalid code is entered, the trans­mitter returns to measuring mode.
Transmitter in Hold mode, measured value frozen. Sensoface inactive.
The response time of the electrode and temperature probe is consider­ably reduced when the electrode is first moved about in the buffer solu­tion and then held still.
Display Action
Stability check: The measured mV value is displayed.
Calibration with the first buffer is terminated. Remove the electrode and temp probe from the first buffer solution and rinse them thoroughly.
Remark
To abort stability check: Press cal.
(accuracy reduced)
• One-point calibration:
Press cal to end the calibration. Slope [%] and offset [mV ] of the electrode are displayed. Press enter to proceed.
• Two-point calibration:
Immerse sensor and tempera­ture probe in the second buffer solution.
enter to start.
Press Retract electrode and temp
probe out of second buffer, rinse off, re-install. Repeat calibration: cal End calibration:
pH value and “Hold” are displayed alternately. Sensoface is active, “enter” blinks. Press
enter
Hold is deactivated after 20 sec.
enter
to proceed.
For one-point calibration only:
The calibration pro­cess runs again as for the first buffer.
Slope and offset of electrode (related to 25 °C) are displayed.
Confirmation prompt.
71
Manual Calibration Automatic or manual temperature detection
For calibration with manual buer specication, you must enter the pH value of the buer solution used in the transmitter for the proper tempera­ture. This presetting enables calibration with any desired buer solution. The MAN calibration mode and the type of temperature detection are selected in the conguration mode.
Display
72
Action
Press cal, enter code: 1100 Select position using , edit number using , press enter to proceed.
Remove the electrode and temperature probe, clean them and immerse them in the first buffer solution (in any order). When “Manual temp detection” has been configured, enter the value in the secondary display using the arrow keys. Press enter to start.
Enter the pH value of your buffer solution for the proper temperature. While the “hour­glass” icon is blinking, the elec­trode and temperature probe remain in the buffer solution.
Remark
If an invalid code is entered, the trans­mitter returns to measuring mode.
Transmitter in Hold mode, measured value frozen. Sensoface inactive.
The response time of the electrode and temperature probe is consider­ably reduced when the electrode is first moved about in the buffer solu­tion and then held still.
Display Action
Stability check: The measured mV value is displayed.
Calibration with the first buffer is terminated. Remove the electrode and temp probe from the first buffer solution and rinse them thoroughly.
Remark
To abort stability check: Press cal.
(accuracy reduced)
• One-point calibration:
Press cal to end the calibration. Slope [%] and offset [mV ] of the electrode are displayed. Press enter to proceed.
• Two-point calibration:
Immerse electrode and temperature probe in the second buffer solution. Enter pH value of second buffer solution. Press
Retract electrode and temp probe out of second buffer, rinse off, re-install. Repeat calibration: cal End calibration:
pH value and “Hold” are displayed alternately. Sensoface is active, “enter” blinks. Exit using Hold is deactivated after 20 sec.
enter to start.
enter
enter
key.
For one-point calibration only:
The calibration process runs again as for the first buf­fer.
Slope and offset of electrode (related to 25 °C) are displayed.
Confirmation prompt.
73

Data entry of premeasured electrodes

You can directly enter the values for slope and oset of an electrode. The values must be known, e.g. determined beforehand in the laboratory. The DAT calibration mode must have been preset during conguration.
Display
Action
Press cal, enter code: 1100 Select position using , edit number using , press enter to proceed.
Ready for calibration Start with
Enter offset [mV]. Select position using , enter number using , press
Enter slope [%]. Select using , edit number using , press
The transmitter displays the new slope and offset (at 25 °C). Press
pH value and “Hold” are displayed alternately. Sensoface is active, “enter” blinks. Press Hold is deactivated after 20 sec.
enter
enter
enter
enter
enter
.
to proceed.
to proceed.
to proceed.
to proceed.
Remark
If an invalid code is entered, the trans­mitter returns to measuring mode.
Transmitter in Hold mode, measured value frozen. Sensoface inactive.
Confirmation prompt.
74
Converting slope [%] to slope [mV/pH] at 25 °C:
% mV/pH
78 46.2 80 47.4 82 48.5 84 49.7 86 50.9 88 52.1 90 53.3 92 54.5 94 55.6 96 56.8 98 58.0
100 59.2
102 60.4
Converting offset to electrode zero point:
ZERO = 7 -
V
[mV]
OFF
S [mV / pH]
ZERO V
OFF
S
Electrode zero point Offset Slope
75

Product calibration

Calibration by sampling
During product calibration the electrode remains in the process. The measurement process is only interrupted briefly.
Procedure: During sampling the currently measured value is saved in the transmitter. The transmitter immediately returns to measuring mode. The calibration mode indicator blinks and reminds you that calibra­tion has not been terminated. The sample is measured in the lab or directly on the site using a portable meter. To ensure an exact calibration, the sample tempera­ture should correspond to the measured process temperature. The measured sample value is then entered in the transmitter. From the difference between the saved measured value and entered sample value, the transmitter calculates the new offset (one-point calibration). If the sample is invalid, you can take over the value saved during sampling. In that case the old calibration values are saved. Afterwards, you can start a new product calibration.
Display
76
Action
Product calibration step 1: Press cal, enter code: 1105 (Presskey to select position, enter number usingkey, press enter to confirm)
Take sample and save value. Press enter to proceed.
Remark
If an invalid code is entered, the transmitter returns to measuring mode.
Now the sample can be measured in the lab.
Display
Action
Remark
Measuring mode:
From the blinking CAL mode indicator you see that sample calibration has not been terminated.
Product calibration step 2: When the sample value has been determined, open the product calibration once more (cal, code 1105).
Enter lab value. The new offset is calculated.
Display of slope and new offset (related to 25°C). Press enter to end calibration.
The measured value is shown in the main display alternately with “Hold”. Sensoface is active, “enter” blinks. Press enter to exit calibration.
Until the sample value is deter­mined and can be entered, the transmitter is in measuring mode.
Display (approx. 3 sec)
New calibration: Press cal.
After end of calibration, the outputs remain in Hold mode for approx. 20 sec.
77

ORP calibration

ORP calibration mode is automatically preset when ORP measurement is configured. The potential of a redox electrode is calibrated using a redox (ORP) buffer solution. In the course of that, the difference between the measured potential and the potential of the calibration solution is deter­mined according to the following equation. During measurement this difference is added to the measured potential.
mV
mV
ORP = mVmeas
The electrode potential can also be related to another reference system – e.g. the standard hydrogen electrode. In that case the temperature­corrected potential (see table) of the reference electrode used must be entered during calibration. During measurement, this value is then added to the ORP measured. Please make sure that measurement and calibration temperature are the same, since the temperature response of the reference electrode is not automatically taken into account.
+ ∆mV
mV ∆mV =
displayed ORP
=
ORP
=
direct electrode potential
meas
delta value, determined during calibration
Temperature dependence of commonly used reference systems
Temperature [°C]
0 10 20 25 30 40 50 60 70 80
Ag/AgCl/KCl 1 mol/L [∆mV]
249 244 240 236 233 227 221 214 207 200
Ag/AgCl/KCl 3 mol/L [∆mV]
224 217 211 207 203 196 188 180 172 163
Thalamid [∆mV]
-559
-564
-569
-571
-574
-580
-585
-592
-598
-605
Mercury sulfate [∆mV]
672 664 655 651 647 639 631 623 613 603
78
Display
Action
Select calibration (Press cal). Enter passcode: 1100 Select position using , enter number using , press enter to proceed.
Remove the electrode and temperature probe, clean them and immerse them in the redox buffer.
Enter setpoint value for redox buffer (secondary display: electrode potential displayed for approx. 6 sec) Select position using , enter number using , press enter to proceed.
Display of electrode data (delta value) Press enter to proceed. Rinse electrode and tempera­ture probe and reinstall them.
Remark
If an invalid code is entered, the transmitter returns to measuring mode.
Display (approx. 3 sec) The transmitter is in the Hold mode.
After approx. 6 sec the secondary display shows the measured temperature.
“Zero” and “enter” icons are blinking, Sensoface is active.
The measured ORP value [mV] is shown in the main display alternately with “Hold”, “enter” blinks, Sensoface is active. Press enter to exit calibration.
After end of cali­bration, the out­puts remain in Hold mode for approx. 20 sec.
79

Temp probe adjustment

Display
Action
Select calibration (Press cal, enter passcode: 1015) Select position usingkey, edit number using Press
Measure the temperature of the process medium using an external thermometer
Measurement
Display
Remark
In the measuring mode the main display shows the configured process variable (pH or ORP [mV]) and the lower display the temperature. During calibration you can return to measuring mode by pressing the cal key, during configuration by pressing conf. (Waiting time for signal stabilization approx. 20 sec).
key.
key.
enter to proceed.
Enter measured temperature value. Select position usingkey, edit number using Press
enter to proceed. Press enter to exit adjustment. HOLD will be deactivated after 20 sec.
Remark
Wrong settings change the mea­surement proper­ties! If an invalid code is entered, the transmitter returns to measuring mode.
The transmitter is in the Hold mode.
Default: Value of secondary display.
80

Diagnostics functions

Display
Remark
Display of output currents
Press enter while in measuring mode. The current at output 1 is shown in the main display, the current at output 2 in the secondary display. After 5 sec the transmitter returns to measuring mode.
Display of calibration data (Cal Info)
Press cal while in measuring mode and enter code:
0000. The slope is shown in the main display, the offset in the secondary display. After 20 sec the transmitter returns to measuring mode (immediate return at pressing enter).
Display uncorrected electrode potential
(Sensor monitor) Press conf while in measuring mode and enter code:
2222. The (uncompensated) electrode potential is shown in the main display, the measuring tempera­ture in the secondary display. Press enter to return to measurement.
Display of last error message
(Error info) Press conf while in measuring mode and enter code:
0000. The last error message is displayed for approx. 20 sec. After that the message will be deleted (immediate return to measurement at pressing enter).
81
Diagnostics functions
These functions are used for testing the connected peripherals.
Display
82
Select a relay
Test 0/1 Return to
measure­ment
Action / Remarks
Specify current at output 1
• Press conf, enter code: 5555 The current indicated in the main display for output 1 can be edited. Select position using , edit number using , press
enter to confirm. Then the entered value will be shown in the secondary display. The transmitter is in Hold mode. Press conf, then enter to return to measurement (Hold remains active for another 20 sec).
Specify current at output 2
• Press conf, enter code: 5556 The current indicated in the main display for output 2 can be edited. Select position using , edit number using ,
enter to confirm. Then the entered value will
press be shown in the secondary display. The transmitter is in Hold mode. Press conf, then enter to return to measurement (Hold remains active for another 20 sec).
Relay test (manual test of contacts)
• Press conf, enter code: 5557 The relays are frozen. This state is indicated in the display. The 4 digits in the display correspond to the 4 relays (as located on the terminal plate): 1st digit: R1 2nd digit: R2 3rd digit: AL 4th digit: CLN Function test using arrow keys – see left column. When exiting the function (enter), the relays are set corresponding to the measured value.
Display
Controller characteristic
The arrows indicate which relay (valve) is active:
+100 %
Controller output
Setpoint
-100 %
Relay 2 active (Meas. value > setpoint)
Relay 1 active (Meas. value < setpoint)
Action / Remarks
Controller test (manual specification of controller output)
• Press conf, enter code: 5559 After function activation “Ctrl” is displayed for approx. 3 sec. With the controller turned off, “OFF” is displayed in addition, then return to measuring mode. The function is used to start up control loops or check the actuators. For bumpless changeover to automatic operation (exiting this function), configure an I-action component (reset time).
Specify value: Select usingkey, edit number usingkey. Press
enter to proceed.
The transmitter is in Hold mode. Press enter to return to measurement (Hold remains active for another 20 sec).
Controller output -100 to 0 %: Relay 2 active
Controller output 0 to +100 %: Relay 1 active
Momentary controller output (adjusted value has not been saved yet)
83

Controller functions

PID controller
P Controller
Application in integrating systems (e.g. closed tank, batch processes).
PI controller
Application in non-integrating systems (e.g. drains).
PID controller
The additional derivative action compensates for measurement peaks.
Controller characteristic
Proportional action Y
P
[%]
Neutral zone Yp=0
Relay 1
+100 %
Setpoint
84
-100 %
pH
Relay 2
Controller equations
Controller output Y = YP + YPdt + T
P action
1
T
R
I action
dY
D
dt
D action
P
Proportional action Y
Setpoint - Meas. value
YP =
Constant
P
*
KC
with: Y T
T
K
Constant 5 (for pH) 500 mV (for ORP)
P R
D
C
Proportional action Reset time [s]
Rate time [s]
Controller gain [%]
Neutral zone (Y=0)
Tolerated deviation from desired value. With the setting “1 pH”, for example, a deviation of ± 0.5 pH from the desired value does not activate the controller.
Proportional action (Gradient KC [%])
100 %
Controller
50 %
output Y
X
w
KC = 500 %
1 / (100) 2 / (200)
Deviation
KC = 200 %
KC = 100 %
KC = 50 %
3 / (300)
4 / (400)
(Process variables: pH/ (mV))
5 / (500)
85
Controller functions
Pulse length / pulse frequency controller
Pulse length controller (PLC)
The pulse length controller is used to operate a valve as an actuator. It switches the contact on for a time that depends on the controller output. The period is constant. A minimum ON time of 0.5 sec is maintained even if the controller output takes corresponding values.
Output signal (relay contact) of pulse length controller
ON time (Y = 20 %)
0
0
ON time (Y = 80 %)
Pulse length
Pulse frequency controller (PFC)
The pulse frequency controller is used to operate a frequency­controlled actuator. It varies the frequency with which the contacts are switched on. The maximum pulse frequency [pulses/min] can be defined. It depends on the actuator. The contact ON time is constant. It is automatically calculated from the user-defined maximum pulse frequency:
Output signal (relay contact) of pulse frequency controller
1 0
1 0
ON time
Pulse frequency ( Y = 20%)
Pulse frequency ( Y = 80%)
86

Error messages (error codes)

Error
ERR 01
ERR 02
ERR 98
ERR 99
Display
Measured value blinks
Measured value blinks
“Conf” blinks
“FAIL” blinks
Problem Possible causes
pH electrode
• Electrode defective
• Too little electrolyte in electrode
• Electrode not connected
• Break in electrode cable
• Incorrect electrode connected
• Measured pH value < -2 or > 16
• Measured ORP value
< -1999 mV or > 1999 mV
Redox electrode
• Electrode defective
• Electrode not connected
• Break in electrode cable
• Incorrect electrode connected
• Electrode potential < -1500 mV
• Electrode potential > 1500 mV
System error
Configuration or calibration data defective; completely reconfigure and recalibrate the transmitter. Memory error in device program
Factory settings
EEPROM or RAM defective This error message only occurs in the case of a total defect. The transmitter must be repaired and recalibrated at the factory.
Red LED
Out 1 (22 mA)
Alarm contact
xx
xx
xx
xx
Out 2 (22 mA)
x
x
x
x
x
x
87
Error
ERR 03
ERR 11
ERR 12
ERR 13
ERR 21
ERR 22
ERR 23
ERR 41 ERR 42
ERR 33 ERR 34
Icon (blinks)
Problem Possible causes
Temperature probe
Open or short circuit Temperature range exceeded
Current output 1
Current below 0 (3.8) mA
Current output 1
Current above 20.5 mA
Current output 1
Current span too small / too large
Current output 2
Current below 0 (3.8) mA
Current output 2
Current above 20.5 mA
Current output 2
Current span too small / too large
Rinsing probe: Communication Calibration error
Sensocheck: Glass electrode Reference electrode
• Zero error, Sensoface active, see Pg 93
• Slope error, Sensoface active, see Pg 93
Red LED
Out 1 (22 mA)
Alarm contact
xx
xx
xx
xx
xx
xx
xx
xx
xx
Out 2 (22 mA)
x
x
x
x
x
x
x
x
x
x
x
88
• Response time exceeded, Sensoface active, see Pg 93
• Calibration interval expired, Sensoface active, see Pg 93

Calibration error messages

Icon blinks:
Problem Possible causes
Offset out of range (±60 mV)
• Electrode worn out
• Buffer solutions unusable or contaminated
Buffer does not belong to configured buffer set
Temperature probe not immersed in buffer
solution (for automatic temperature compensation)
• Wrong buffer temperature set
(for manual temperature specification)
• Nominal electrode zero point ≠ pH 7
Electrode slope out of range (80...103 %)
• Electrode worn out
• Buffer solutions unusable or contaminated
Buffer does not belong to configured buffer set
Temperature probe not immersed in buffer
solution (for automatic temperature compensation)
Wrong buffer temperature set (for manual
temperature specification)
• Electrode used has different nominal slope
Problems during recognition of the buffer solution
Same or similar buffer solution was used for both calibration steps
Buffer solution used does not belong to buffer set currently configured in the transmitter
89
Icon blinks:
Problem Possible causes
Problems during recognition of the buffer solution (continued)
During manual calibration the buffer solutions
were not used in the specified order
• Buffer solutions unusable or contaminated
• Wrong buffer temperature set
(for manual temperature specification)
• Electrode defective
• Electrode not connected
• Electrode cable defective
Calibration was canceled after approx. 2 minutes because the electrode drift was too large.
• Electrode defective
• Electrode dirty
• No electrolyte in the electrode
Electrode cable insufficiently shielded or
defective
Strong electric fields influence the measure-
ment
Major temperature fluctuation of the buffer
solution
• No buffer solution or extremely diluted
90

Operating states

Operating state
Measuring
Alarm contact
LED
Rel.1/2
Controller
Limit value
Out 2
Out 1
Rel.1/2
Timeout
Cal Info (cal) 0000
Error Info (conf) 0000
Calibration (cal) 1100
Temp adjustment (cal) 1015
Explanation:
active as configured (Last/Fix or Last/Off )
LED blinks during HOLD (configurable)
20 s
20 s
91
Operating state
Product calibration Step 1: (cal) 1105 Step 2: (cal) 1105
Configuration (conf) 1200
Parameter set 1/2 (conf) 7654
Sensor monitor (conf) 2222
Current source 1 (conf) 5555
Current source 2 (conf) 5556
Relay test (conf) 5557
Manual controller (conf) 5559
Rinse function
HOLD input
Alarm contact
LED
20 min
20 min
20 min
20 min
20 min
20 min
20 min
Timeout
Rel.1/2
Out 2
Out 1
Rel.1/2
Controller
Limit value
92

Sensoface

(Sensocheck must have been activated during configuration.)
The smiley in the display (Sensoface) alerts to electrode problems (defective sensor, defective cable, maintenance required). The permitted calibration ranges and the conditions for a friendly, neutral, or sad Sensoface are summarized in the following table. Additional icons refer to the error cause.
Sensocheck
Continuously monitors the electrodes and wires for short circuits or open circuits. Critical values make the Sensoface “sad” and the corresponding icon blinks:
The Sensocheck message is also output as error message Err 33. The alarm contact is active, the red LED is lit, output current 1 is set to 22 mA (when configured correspondingly). Sensocheck can be switched off during configuration (then Sensoface is also disabled). Exception: After a calibration a smiley is always displayed for confirmation.
Note
The worsening of a Sensoface criterion leads to the devaluation of the Sensoface indicator (Smiley becomes “sad”). An improvement of the Sensoface indicator can only take place after calibration or removal of the electrode defect.
93
Display
Problem
Offset and slope
Status
Offset (zero point) and slope of the electrode are still okay, however, the electrode should be replaced soon.
Offset and slope of the electrode have reached values which no longer ensure proper calibration. Replace the electrode.
94
Calibration timer
Electrode defect
Over 80 % of the calibration interval has already past.
The calibration interval has been exceeded.
Check the electrode and its connections (see also error messages Err 33 and Err 34).

Appendix

Product line and accessories
Devices Order No.
si794 P LXV505.99.00002
Mounting accessories
Bracket kit LZY483 Panel mounting kit LZY484 Protective hood LZY485 Pillar incl. protective hood and bracket kit LZY576
Spare parts
Installation kit, si792 / si794 LZY486 Rear housing, si792 / si794 LZY487
95
Specications
pH/mV input Input for pH or ORP electrodes or ISFET sensors
Measuring range -1500 ... +1500 mV Display range pH value -2.00 ... 16.00 ORP -1999 ... +1999 mV Glass electrode input Input resistance > 0.5 x 1012 ohms Input current < 2 x 10 Reference electrode input Input resistance > 1 x 1010 ohms Input current < 1 x 10 Meas. error pH value < 0.02 TC: 0.002 pH/K (display) mV value < 1 mV TC: 0.1 mV/K
pH sensor standardization * pH calibration Operating modes BUF Calibration with Calimatic automatic buffer
MAN Manual calibration with input of individual
DAT Data entry of pre-measured electrodes
Zero adjustment ±200 mV Max. calibration range Offset: ±60 mV Slope: 80 ... 103 % (47.5 ... 61 mV/pH)
ORP sensor standardization * ORP calibration Max. calibration range -700 ... +700 ∆mV
Cal timer 0000 ... 9999 h
Sensocheck Automatic monitoring of glass and reference
Sensoface Provides information on the sensor condition,
1,2,3
1
-12
-10
A
A
1
recognition
buffer values
electrode (can be disabled)
evaluation of zero/slope, response time, calibration interval, Sensocheck
96
Temperature input * Pt100/Pt1000/NTC 30 kΩ/NTC 8.55 kΩ/Balco 3kΩ
2-wire connection, adjustable Measuring range Pt 100/Pt 1000 -20.0 ... +200.0 °C (-4 ... +392 °F) NTC 30 kohms -20.0 ... +150.0 °C (-4 ... +302 °F) NTC 8.55 kohms -10.0 ... +130.0 °C (-4 ... +266 °F) Balco 3 kohms 0.0 ... +100.0 °C (+32 ...+212 °F) Adjustment range 10 K Resolution 0.1 °C / 1 °F Measurement error
Temp compensation Linear –19.99 ... +19.99 %/K of process medium (reference temp 25 °C) HOLD input Galvanically separated (OPTO coupler)
Function Switches transmitter to HOLD mode Switching voltage 0 ... 2 V (AC/DC) Inactive 10 ... 30 V (AC/DC) Active
CONTROL input Galvanically separated (OPTO coupler) Function Control input for automatic cleaning/calibration
Switching voltage 0 ... 2 V (AC/DC) Inactive 10 ... 30 V (AC/DC) Active Output 1 0/4 to 20 mA, max. 10 V, floating (galvanically connected to output 2) Measured variable * pH or mV value Overrange Output averaging filter * Low-pass, filter time interval 0 ... 120 s Measurement error Start/end of scale Configurable within the measuring range for
Span allowed pH 2.00 ... 18.00 / 200 ... 3000 mV
*
1,2,3
1
<0.5 K (<1 K for Pt100; <1 K for NTC >100°C)
system
22 mA in the case of error messages
< 0.3% current value + 0.05 mA
pH or mV
97
Specications
Output 2 0/4 ... 20 mA, max. 10 V, floating
(galv. connected to output 1) Process variable Temperature Overrange Output averaging filter * Low-pass, filter time interval 0 ... 120 s Measurement error Start/end of scale * 20 ... 200 °C / -4 ... 392 °F Span allowed 20 ... 220 K (36 ... 396 °F)
Power output For operating an ISFET adapter +3 V (V –3 V (V0 = -4.8 ... –3,7 V / Ri = 360 Ω
Alarm contact Relay contact, floating Contact ratings AC< 250 V / < 3 A / < 750 VA DC< 30 V / < 3 A / < 90 W Contact response N/C (fail-safe type) Alarm delay 0000 ... 0600 sec
Limit values Output via relay contacts R1, R2 Contacts R1, R2 floating but inter-connected Contact ratings AC< 250 V / < 3 A / < 750 VA DC< 30 V / < 3 A / < 90 W Contact response Delay Setpoints Hysteresis * 00.00 ... 05.00 pH / 0000 ... 0500 mV
PID process controller Output via relay contacts R1, R2 (see limit values) (Relay R1: base valve, relay R2: acid valve) Setpoint specification * pH -02.00 ... 16.00 / -1500 ... +1500 mV Neutral zone * pH 00.00 ... 05.00 pH / 0000 ... 0500 mV P-action component I-action component (0000 s = no integral action) D-action component * Rate time Td: 0000 ... 9999 s (0000 s = no derivative action) Controller type Pulse period * 0001 ... 0600 s, min. ON time 0.5 (pulse length controller)
*
*
*
*
*
22 mA in the case of temp error messages
1
*
*
< 0.3% current value + 0.05 mA
= 2.9 ... 3.1 V / Ri = 360 Ω
0
N/C or N/O 0000 ... 9999 s As desired within range
Controller gain KP: 0010 ... 9999 % Reset time Tr: 0000 ... 9999 s
Pulse length or pulse frequency controller
98
Max. pulse frequency * 0001 ... 0180 min (pulse frequency controller)
Display LC display, 7-segment with icons Main display Character height 17 mm, unit symbols 10 mm Secondary display Character height 10 mm, unit symbols 7 mm Sensoface 3 status indicators (friendly, neutral, sad face)
Mode indication 5 mode indicators “meas”, “cal”, “alarm”, “cleaning”, “config” 18 further icons for configuration and messages Alarm indication Red LED in case of alarm or HOLD, user defined
-1
Keypad 5 keys: [cal] [conf ] [ Service functions
Current source Current specifiable for output 1 and 2 (00.00 to 22.00 mA) Manual controller Controller output entered directly (start of control process) Device self-test Automatic memory test (RAM, FLASH, EEPROM) Display test Display of all segments Last error Display of last error occurred Sensor monitor Display of direct, uncorrected sensor signal (electrode) Relay test Manual control of the four relay contacts
Parameter sets* Two selectable parameter sets for different applications
Data retention Parameters and calibration data > 10 years (EEPROM)
Protection against electric shock
Safe electrical isolation of all extra-low-voltage circuits
against mains by double insulation acc. to EN 61010-1
Power supply 24 (-15%) ... 230 V AC/DC (+10%); approx. 5 VA, 2.5 W AC: 45 ... 65 Hz Overvoltage category II, protection class II
] [] [enter]
99
Specications
Nominal operating conditions
Ambient temperature -20 ... +55 °C Transport/Storage temp -20 ... +70 °C Relative humidity 10 ... 95% not condensing Power supply 24 (-15%) ... 230 V AC/DC (+10%) Frequency for AC 45 ... 65 Hz
EMC EN 61326 Emitted interference Class B (residential area) Class A for mains > 60 V DC Immunity to interference Industry
Enclosure Molded enclosure made of PBT (polybutyleneterephtalate) Color Bluish gray RAL 7031
Assembly • Wall mounting
• Pipe mounting: Ø 40 ... 60 mm
• Panel mounting, cutout to DIN 43 700
sealed against panel Dimensions H 144 mm, W 144 mm, D 105 mm Ingress protection IP 65 / NEMA 4X Cable glands 3 knockouts for M20x1.5 cable glands 2 knockouts for NPT 1/2” or rigid metallic conduit Weight Approx. 1 kg
* User-defined
1) To IEC 746 Part 1, at nominal operating conditions
2) ± 1 count
3) Plus sensor error
30 ... 45 mm
100
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