Hach NITRATAX plus sc, NITRATAX clear sc, NITRATAX eco sc User Manual

DOC023.52.03211
NITRATAX sc
USER MANUAL
11/2014, Edition 6A
© HACH Company, 2007–2012, 2014 All rights reserved. Printed in Germany. sd/sk
1
Section 1 Specifications.................................................................................................................... 3
Section 2 General Information......................................................................................................... 7
2.1 Safety information........................................................................................................................ 7
2.1.1 Use of hazard information................................................................................................... 7
2.1.2 Precautionary labels ........................................................................................................... 7
2.2 Product overview ......................................................................................................................... 8
2.3 Theory of operation...................................................................................................................... 9
Section 3 Installation........................................................................................................................ 11
3.1 Installation overview................................................................................................................... 11
3.2 Unpack the sensor..................................................................................................................... 12
3.3 Wiring safety information ........................................................................................................... 12
3.3.1 Sensor connection and wiring........................................................................................... 12
Section 4 System Start Up..............................................................................................................15
4.1 Power the instrument................................................................................................................. 15
Section 5 Operation.......................................................................................................................... 17
5.1 Use of an sc controller ............................................................................................................... 17
5.2 Sensor setup.............................................................................................................................. 17
5.3 Sensor data logging................................................................................................................... 17
5.4 Sensor diagnostics menu........................................................................................................... 18
5.5 Sensor setup menu.................................................................................................................... 18
5.6 Sensor calibration ...................................................................................................................... 20
5.6.1 Adjusting turbidity compensation ...................................................................................... 22
Section 6 Maintenance .................................................................................................................... 23
6.1 Maintenance schedule............................................................................................................... 23
6.2 Clean the measuring path.......................................................................................................... 24
6.3 Change the wiper profile............................................................................................................ 25
6.4 Check the calibration ................................................................................................................. 26
Section 7 Troubleshooting ............................................................................................................. 29
7.1 Error messages.......................................................................................................................... 29
7.2 Warnings.................................................................................................................................... 29
Section 8 Replacement Parts and Accessories......................................................................... 31
Section 9 Contact Information....................................................................................................... 33
Section 10 Warranty and liability .................................................................................................. 35
Index...................................................................................................................................................... 39
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Table of Contents
3
Section 1 Specifications
Specifications are subject to change without notice.
Component NITRATAX plus sc NITRATAX eco sc NITRATAX clear sc
NITRATAX sc tank sensor
Measuring technique UV absorption measurement, reagent-free
Measuring method Patented 2-beam method
Measuring path
1 mm (0.04 in.), 2 mm (0.08 in.), 5 mm (0.20 in.)
1 mm (0.04 in.) 5 mm (0.20 in.)
Measuring range with NO
3
-N standard solutions
0.1-100.0 mg/L NO
2+3
–N
(1 mm/0.04 in.)
0.1–50.0 mg/L NO
2+3
–N
(2 mm/0.08 in.)
0.1–25.0 mg/L NO
2+3
–N
(5 mm/0.20 in.)
1.0–20.0 mg/L NO
2+3
–N 0.5–20.0 mg/L NO
2+3
–N
Lower detection limit (mg/L) NO
3
-N
0.1 (5 mm/0.20 in.) 1 0.5
Upper detection limit (mg/L) NO
3
-N
100 (1 mm/0.04 in.) 20 20
Measuring error (mg/L) NO
3
-N
±3 % of the mean MW ±0.5 ±5 % of the mean MW ±1.0
±5 % of the mean MW ±0.5
Resolution (mg/L) 0.1 0.5 0.1
Sludge compensation yes yes
Measuring interval (>= min) 155
T100 response time (min) 1155
Integration >1 min, adjustable 15–30 min, adjustable >5 min, adjustable
Power consumption 2 W
Cable length 10 m (30 ft)
Sensor pressure limit maximum 0.5 bar (7 psi)
Ambient temperature 2 to 40 °C (36 to 100 °F)
Dimensions D x L (Figure 1 on page 5)
approximately 70 x 229–333 mm (3 x 13.1 in.)
approximately 75 x 323 mm (3 x 12.9 in.)
approximately 75 x 327 mm (3 x 12.7 in.)
Weight approximately 3.6 kg (7.9 lb) approximately 3.3 kg (7.3 lb) approximately 3.3 kg (7.3 lb)
NITRATAX sc sensors flow through units
Sample flow rate 0.5–10 L/h sample 0.5–10 L/h sample
Sample connection Tube ID 4 mm/AD 6 mm Tube ID 4 mm/AD 6 mm
Sample temperature 2 to 40 °C (36 to 100 °F) 2 to 40 °C (36 to 100 °F)
Dimensions
W x H x D approximately 500 x 210 x 160 mm (20 x 8.3 x 6.3 in.)
W x H x D approximately 500 x 210 x 160 mm (20 x 8.3 x 6.3 in.)
Weight (without sensor) approximately 3.6 kg (7.9 lb) approximately 3.6 kg (7.9 lb)
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Specifications
NITRATAX sc sensor material
Sensor
Sensor enclosure Stainless steel 1.4571 Stainless steel 1.4581
Wiper axle Stainless steel 1.4104 Stainless steel 1.4571
Cable gland Stainless steel 1.4305
Profile carrier 1 mm/2 mm Stainless steel 1.4310
Wiper arm 5 mm Stainless steel 1.4581
Wiper profile Silicone
Measuring windows SUPRASIL (quartz glass)
Enclosure seals Silicone
Seal, cable gland PVDF
Sensor cable
PUR
10 m (33 ft) standard
Optional extension cables available in 5, 10, 15, 20, 30, 50 m
Total maximum length: 60 m (196 ft)
Struts
Adaptor for filtration sensor
Stainless steel 1.4308
Struts Stainless steel 1.4301
Flow through cell (bypass)
Measuring cell PVC
Seals EPDM
Glands PVDF
Sample tube PVC
Component NITRATAX plus sc NITRATAX eco sc NITRATAX clear sc
5
Specifications
Figure 1 Sensor dimensions
1 NITRATAX plus sc 4 Wiper profile 1 and 2 mm (0.04 in. and 0.08 in.) 2 NITRATAX clear sc 5 Wiper profile 5 mm (0.20 in.) 3 NITRATAX eco sc
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Specifications
7
Section 2 General Information
2.1 Safety information
Please read this entire manual before unpacking, setting up or operating this equipment. Pay attention to all danger and caution statements. Failure to do so could result in serious injury to the operator or damage to the equipment.
Make sure that the protection provided by this equipment is not impaired, do not use or install this equipment in any manner other than that specified in this manual.
2.1.1 Use of hazard information
Note: Information that supplements points in the main text.
2.1.2 Precautionary labels
Read all labels and tags attached to the instrument. Personal injury or damage to the instrument could occur if not observed. A symbol, if noted on the instrument, will be included with a danger or caution statement in the manual.
DANGER
Indicates a potentially or imminently hazardous situation which, if not avoided, will result in death or serious injury.
WARNING
Indicates a potentially or imminently hazardous situation which, if not avoided, could result in death or serious injury.
CAUTION
Indicates a potentially hazardous situation that may result in minor or moderate injury.
NOTICE
Indicates a situation which, if not avoided, may cause damage to the instrument. Information that requires special emphasis.
This symbol, if noted on the instrument, references the instruction manual for operation and/or safety information.
Electrical equipment marked with this symbol may not be disposed of in European public disposal systems after 12 August of 2005. In conformity with European local and national regulations (EU Directive 2002/96/EC), European electrical equipment users must now return old or end-of life equipment to the Producer for disposal at no charge to the user.
Note: For return for recycling, please contact the equipment producer or supplier for instructions on how to return end-of-life equipment, producer-supplied electrical accessories, and all auxiliary items for proper disposal.
This symbol, when noted on a product enclosure or barrier, indicates that a risk of electrical shock and/or electrocution exists.
This symbol, if noted on the product, indicates the need for protective eye wear.
This symbol, when noted on the product, identifies the location of the connection for Protective Earth (ground).
This symbol, when noted on the product, identifies the location of a fuse or current limiting device.
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General Information
2.2 Product overview
The NITRATAX plus sc sensor (Figure 2, item 1) measures the nitrate concentration up to 100 mg/L N directly immersed in the medium. Use the sensor without the need for pumping and conditioning in activated sludge tanks in municipal sewage treatment plants, surface water, untreated water and treated drinking water. The system can also be used for checking the outlet on waste water treatment plants.
The NITRATAX eco sc (Figure 2, item 2) measures the nitrate concentration up to 20 mg/L N directly immersed in the medium. Use the sensor without the need for pumping and conditioning in activated sludge tanks in municipal sewage treatment plants.
The NITRATAX clear sc (Figure 2, item 3) measures the nitrate concentration up to 20 mg/L N directly immersed in the medium. Use the sensor without the need for pumping and conditioning in clear media such as surface water, treated drinking water and sewage treatment plant outlets.
Note: The flow-through units of the high precision NITRATAX plus sc and the NITRATAX clear sc sensors are used wherever direct measurement in the medium is not possible for structural reasons, or the medium load makes it necessary to measure a filtered sample (very high TS content, sewage treatment plant inlet, waste dump leachate, etc.).
Figure 2 NITRATAX sc sensor versions
1 NITRATAX sc plus 2 NITRATAX sc eco 3 NITRATAX sc clear
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General Information
2.3 Theory of operation
Nitrate dissolved in water absorbs UV light with wavelengths below 250 nm. This inherent absorption by nitrate makes it possible to photometrically determine the nitrate concentration without reagents by using a sensor positioned directly in the medium. As the measuring principle (Figure 3) is based on the evaluation of (invisible) UV light, the color of the medium has no effect.
The sensor contains a two-beam absorption photometer with turbidity compensation. The measuring window is mechanically cleaned using a wiper.
The measuring and cleaning intervals can be entered using the related controller. The measured value is displayed as NO
x
-nitrogen in mg/L NOx–N (NO2–N is included in the measured result as nitrite nitrogen) and provided on current outputs. Various operating modes for the outputs permit local regulation without further process data processing.
Figure 3 Measurement principle of the NITRATAX sc
1 Receiver, Reference Element 3 UV Lamp 5 Mirror 2 Two-sided Wiper 4 Measurement Slit 6 Receiver, Measuring Element
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General Information
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Section 3 Installation
3.1 Installation overview
Figure 4 shows an example of a NITRATAX sc sensor attached to an sc controller with a
bracket installation option.
CAUTION
Installation of this system may only be carried out by qualified experts in accordance with all local safety regulations.See the mounting instruction sheet for more information.
Figure 4 Installation example with optional accessories
1 sc controller with optional sun roof 4 Minimum distance of 100 mm (3.94 in.) to the ground 2 Sensor bracket 5 NITRATAX plus sc: 468–472 mm (18.4–19.6 in.)
NITRATAX eco sc: 466 mm (18.3 in.) NITRATAX clear sc: 462 mm (18.1 in.)
3 NITRATAX sc sensor
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