Extech Instruments ExStik FL700 User Manual

User Guide
ExStik® FL700
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Introduction
The model FL700 is a system specifically designed for the quick and accurate measurement of fluoride ions in drinking water and other aqueous samples. Unlike other electrode based systems the FL700 consists of the sensing electrode, measuring electronics, and the display in one convenient package. This meter is shipped fully tested; with proper use, this instrument will provide years of reliable service.
Features
Automatic temperature compensation (±10
o
C of calibration temperature)
Automatic calibration
Stability sensing to optimize accuracy
Internal Datalogger for storing up to 25 readings
Direct reading of ppm, mV, or mg/l units
Automatic power off after 12 minutes to preserve battery life
Internal error detection
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Description
Meter Description
1. Battery compartment cover
2. LCD Display
3. MODE/HOLD button
4. CAL/RECALL button
5. ON/OFF button
6. Electrode Retaining Collar (ring)
7. Electrode Sensor
(Note: The Electrode storage cap is not shown this diagram)
Electrode Sensor Description
The sensing electrode is a europium doped lanthanum fluoride single crystal that has been incorporated into a removable sensing module that houses a reference electrode and temperature measurement system. The high resistance electrode signals are impedance converted to a low resistance output in the sensing module to ensure stable and noise free performance.
Reagent Tablets
The FL700 allows the users to follow the ASTM and EPA standard methodology using any of the TISAB reagents and standards already in use. Also, Extech has developed tablet-form TISAB which contains all of the essential and approved chemicals that are found in the usual TISAB reagents. A total ionic strength adjustment buffer (TISAB) is a buffer solution which increases the ionic strength of a solution to a relatively high level.
The “dry” TISAB reagent does not contribute to sample dilution. The benefits of this method are:
1. No volumetric errors
2. Independent of sample size (± 20% of nominal sample volume)
3. Easy to use in the field or laboratory
4. Can be shipped more easily than liquid reagents
5. Lower cost per test
LCD Display
1. Bargraph display
2. Measurement units
3. Main display
4. Low (L) and High (H) Calibration icons
5. Data HOLD indicator
6. Low Battery indicator
7. Temperature display
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Operation
Preparation for use
1. Remove the FL700, electrode module and sample cup from its box. Remove caps from module
2. If not already done, fit the electrode module onto the end of the meter body, making sure that the slots line up correctly, and turn the module retaining ring to secure the assembly.
Powering the FL700
Press the ON/OFF button to turn the meter on or off. If the batteries are weak, the ‘BAT’ indicator appears on the LCD.
Power-On Diagnostics
1. When the meter is switched ON the LCD displays “SELF” and “CAL” while the meter runs a diagnostic routine
2. During this time the meter is recalling the user calibration data, performing self diagnostics & initializing the circuitry
3. When completed, the meter proceeds to the normal measurement mode
Calibration
The FL700 can be calibrated between 1.0 ppm and 10 ppm or between 0.5 and 5.0 ppm Fluoride ion. Set the Mode to ppm. The following calibration procedure assumes the normal 1.0 to 10 ppm range has been chosen.
1. Prepare a 1 ppm fluoride standard solution by placing one TISAB tablet into a sample cup and add 20 mls of the 1ppm Fluoride standard into the sample cup.
Note: if your 1ppm Fluoride standard already contains TISAB do not use a TISAB tablet.
2. Create a rinse solution that can be used between sample measurements buy dissolving 1 TISAB tablet in 20ml of Distilled water. The rinse solution promotes faster response times.
3. Rinse the end of the FL700 module in this Rinse solution or in Distilled water and then wipe thoroughly with a paper tissue.
4. Place the FL700 into the prepared 1 ppm standard and switch the instrument ON using the ON/OFF button. The instrument will now go through its self-calibration.
5. The instrument will enter HOLD mode in about 35 seconds when stabilized in the 1.0 ppm standard solution.
6. Press and HOLD the CAL key, CAL will appear in the display followed by 0.5ppm and
5.0ppm. Continue holding the CAL button until 1.0 ppm and CAL appear in the display. Release the CAL key.
7. Wait until the display stops blinking; the instrument will enter the normal measurement mode.
8. The instrument is now calibrated and ready for use.
9. The circled L and H icons on the display indicate that the low range (L) and high range (H) calibrations have been completed.
Calibration frequency
Calibrate the FL700 prior to each new measurement batch or if more than 12 hours has elapsed since the last calibration.
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Other standards
The FL700 can also be calibrated between 0.5 and 5.0 ppm F. Follow the calibration instructions above but substitute 0.5 ppm for 1.0 ppm and 5.0 ppm for 10 ppm.
Slope Adjustment
1. Slope adjustment although not a frequent requirement can be carried out by following the
instructions in Calibration steps above except for the fact that a 10 ppm standard is used after calibrating with the 1 ppm standard
2. Press the Cal button until 10 ppm appears. Slope adjustment is then complete.
Measurement Mode
1. Prepare 20ml of test solution by adding one TISAB reagent to the unknown sample. Thoroughly wipe the end of the FL700. Wait for the tablet to dissolve and then mix thoroughly before proceeding.
2. Rinse the end of the FL700 in your rinse solution or in distilled water, wipe dry.
3. Place the FL700 into the prepared unknown sample. If the instrument is in the HOLD mode, press MODE/HOLD to unlock HOLD
4. After ~35 seconds, the instrument will display the value of the unknown concentration and will then enter the HOLD mode
Note: The readings can be stored in the memory by pressing the MODE/HOLD key for ~ 3 seconds.
Electrode Storage
1. It is recommended that the electrode be stored WET in the last test solution used by the instrument (fluoride ion plus TISAB reagent).
2. The module and can be stored dry. If stored dry it will be necessary to allow approximately 15 minutes of soaking in a fluoride solution before the specified performance can be achieved. The instrument will give an error code when the electrode can no longer be calibrated
Temperature Units (ºF / ºC)
1. With the unit OFF, press and hold the CAL/RECALL button
2. With the CAL/RECALL button depressed, momentarily press the ON/OFF button to turn the unit ON
3. The CAL/RECALL button can be released when ‘Self Cal’ is shown in the display
4. To switch back to the previous unit of measure, repeat steps 1 through 3.
Units of Measure
The FL700 has 3 different units of measure. (ppm, mV, and mg/l).
To change the units of measure follow these steps:
1. Turn on the meter.
2. Press and Hold the MODE/HOLD button and it will cycle through the 3 different units of measure (ppm, mV, mg/L).
3. Release the Mode/Hold button when the preferred unit is selected.
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Auto-Power OFF Feature
The auto power off feature automatically shuts the meter off 12 minutes after the most recent button press.
Disabling the Auto-Power OFF Feature
With the unit ON, momentarily press the CAL/RECALL button, then quickly press and hold both the MODE/HOLD and ON/OFF buttons until ‘oFF’ is displayed. To restore the Auto Power Off Feature (auto power OFF enable) simply turn the meter off and on again using the ON/OFF button.
Low Battery Indication
When the battery voltage falls below the operating threshold, ‘BAT’ will appear on the display. Refer to the Maintenance section for battery replacement information.
Storing Readings
Up to 25 readings can be stored in memory for later recall.
1. With the meter in the HOLD mode, press and hold the MODE/HOLD button for three (3) seconds to store a reading. Release the button when the memory location number appears on the lower display.
2. After approx. 30 seconds (measurement duration) the meter will return to the HOLD mode and another reading can then be stored.
3. If more than 25 readings are stored, previously stored readings (starting with reading number
1) are overwritten.
Recalling Stored Readings
1. Momentarily press the CAL/RECALL button and then within 4 seconds momentarily press the MODE/HOLD. The last stored data point location will be displayed (1 to 25). Each time the MODE/HOLD button is momentarily pressed the next most recently stored data point will be
displayed.
2. After the last data point is displayed, pressing the MODE/HOLD button again returns the display to the beginning of the list.
3. Pressing the CAL/RECALL button at anytime stops the data retrieval process and returns the meter to the normal measurement mode.
Clearing Stored Readings
1. With the unit ON press and hold the ON/OFF button for 4 seconds
2. When “CLR” is shown in the main display the memory is cleared.
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Maintenance
Battery Replacement
1. Twist off the battery compartment cover
2. Holding the battery housing in place with a finger, pull out the battery carrier using the two small tabs
3. Replace the four (4) CR2032 batteries observing proper polarity
4. Replace the battery carrier, reattach the battery compartment cap and tighten securely
Electrode Replacement
1. To remove the electrode, first turn the instrument OFF and then unscrew and remove the electrode retaining collar. (turn the collar counter-clockwise to remove)
2. Gently rock the electrode from side to side, pulling it away from the meter until it disconnects
3. To attach an electrode, align the positioning “keys” on the electrode and the main body housing and then carefully push the electrode into the meter socket until it is fully seated
4. Tighten the electrode retaining collar firmly enough to seal the electrode with the meter
Electrode Storage
3. It is recommended that the electrode be stored wet in the last test solution used by the instrument (fluoride ion plus TISAB reagent).
4. The module and can be stored dry. If stored dry it will be necessary to allow approximately 15 minutes of soaking in a fluoride solution before the specified performance can be achieved. The instrument will give an error code when the electrode can no longer be calibrated
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Specifications
Range 0.10 to 9.99ppm (mg/l)
Accuracy ± 3% of reading or ± 0.1ppm (whichever is greater)
Resolution 0.1ppm
Display 2000 count, Dual function 3 ½ digit LCD with Bargraph,
Display size: 24 mm x 20 mm
Electrode Europium doped lanthanum fluoride single crystal
Electrode life 6 months minimum
Measurement method In compliance with EPA Method 340.2 (Potentiometric Ion
Selective Electrode)
Response Time 90% of change in less than 30 seconds (typical)
Operating Temp. Range 32 to 140°F (0 to 60°C)
ATC Range 32 to 140°F (0 to 60°C)
Measurement Storage 25 tagged (numbered) data sets with recall
Battery Power Four (4) CR2032 button batteries
Low Battery Indication ‘BAT’ appears on the LCD
Auto Power Off After 12 minutes of inactivity
Dimensions/Weight 1.4 x 6.8 x 1.6” (36 x 173 x 41mm); 7.4 oz (210g)
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Warranty
FLIR Systems, Inc. warrants this Extech Instruments brand device to be free of defects in parts and
workmanship for one year from date of shipment (a six month limited warranty applies to sensors and cables). If it should become necessary to return the instrument for service during or beyond the warranty period, contact the Customer Service Department for authorization. Visit the website www.extech.com for contact information. A Return Authorization (RA) number must be issued before any product is returned. The sender is responsible for shipping charges, freight, insurance and proper packaging to prevent damage in transit. This warranty does not apply to defects resulting from action of the user such as misuse, improper wiring, operation outside of specification, improper maintenance or repair, or unauthorized modification. FLIR Systems, Inc. specifically disclaims any implied warranties or merchantability or fitness for a specific purpose and will not be liable for any direct, indirect, incidental or consequential damages. FLIR’s total liability is limited to repair or replacement of the product. The warranty set forth above is inclusive and no other warranty, whether written or oral, is expressed or implied.
Calibration, Repair, and Customer Care Services
FLIR Systems, Inc. offers repair and calibration services for the Extech Instruments products we sell. NIST certification for most products is also provided. Call the Customer Service Department for information on calibration services available for this product. Annual calibrations should be performed to verify meter performance and accuracy. Technical support and general customer service is also provided, refer to the contact information provided below.
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Garantie
FLIR Systems, Inc. garantit que cet appareil Extech Instruments est exempt de défauts matériaux et de
fabrication pendant un an à partir de la date d’envoi (une garantie limitée de six mois s’applique aux capteurs et aux câbles). Si le renvoi de l’appareil pour réparation devient nécessaire durant ou après la période de garantie, contactez le service client pour autorisation. Pour obtenir les coordonnées, visitez le site Web suivant : www.extech.com. Un numéro d’autorisation de retour (AR) doit être délivré avant tout retour de produit. L’expéditeur prend à sa charge les frais d’expédition, le fret, l’assurance et l’emballage correct de l’appareil afin de prévenir toute détérioration durant le transport. Cette garantie ne s’applique pas aux dommages imputables à l’utilisateur, tels que l’usage impropre ou abusif, un mauvais câblage, une utilisation non conforme aux spécifications, un entretien ou une réparation incorrecte, ou toute modification non autorisée. FLIR Systems, Inc. déclinera spécifiquement toute garantie ou qualité marchande ou aptitude à l’emploi prévu, et ne sera en aucun cas tenu responsable pour tout dommage conséquent, direct, indirect ou accidentel. La responsabilité totale de FLIR est limitée à la réparation ou au remplacement du produit. La garantie définie ci-dessus est inclusive et aucune autre garantie, écrite ou orale, n’est exprimée ou implicite.
Calibrage, réparation et services après-vente
FLIR Systems, Inc. offre des services de calibrage et de réparation pour les produits Extech Instruments que nous commercialisons. Nous fournissons également une certification NIST pour la plupart des produits. Contactez notre service client pour toute information sur les services de calibrage disponibles pour ce produit. Un calibrage doit être effectué chaque année pour vérifier les performances et la précision du mètre. Nous offrons également une assistance technique et un service à la clientèle. Veuillez vous reporter aux coordonnées fournies ci-dessous.
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Tous droits réservés, y compris la reproduction partielle ou totale sous quelque forme que ce soit.
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Garantía
FLIR Systems, Inc.
, garantiza este dispositivo marca Extech Instruments para estar libre de defectos en partes o mano de obra durante un año a partir de la fecha de embarque (se aplica una garantía limitada de seis meses para cables y sensores). Si fuera necesario regresar el instrumento para servicio durante o después del periodo de garantía, llame al Departamento de Servicio a Clientes para obtener autorización. Visite www.extech.com para Información de contacto. Se debe expedir un número de Autorización de Devolución (AD) antes de regresar cualquier producto. El remitente es responsable de los gastos de embarque, flete, seguro y empaque apropiado para prevenir daños en tránsito. Esta garantía no se aplica a defectos resultantes de las acciones del usuario como el mal uso, alambrado equivocado, operación fuera de las especificaciones, mantenimiento o reparación inadecuada o modificación no autorizada. FLIR Systems, Inc., rechaza específicamente cualesquier garantías implícitas o factibilidad de comercialización o idoneidad para cualquier propósito determinado y no será responsable por cualesquier daños directos, indirectos, incidentales o consecuentes. La responsabilidad total de FLIR está limitada a la reparación o reemplazo del producto. La garantía precedente es inclusiva y no hay otra garantía ya sea escrita u oral, expresa o implícita.
Servicios de calibración, reparación y atención a clientes
FLIR Systems, Inc., ofrece servicios de reparación y calibración para los productos que vendemos de Extech Instruments. Además ofrecemos certificación NIST para la mayoría de los productos. Llame al Departamento de Servicio al Cliente para solicitar información de calibración para este producto. Para verificar el funcionamiento y precisión se debe realizar la calibración anual. Además se provee Soporte Técnico y servicios generales al cliente, consulte la información de contacto en seguida.
Líneas de soporte: EE.UU. (877) 439-8324; Internacional: +1 (603)
324-7800
Soporte Técnico Opción 3; correo electrónico: support@extech.com
Reparación / Devoluciones: Opción 4; correo electrónico: repair@extech.com
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