ENMET SPECTRUM User Manual

ENMET
PO Box 979
Ann Arbor, MI 48106-0979
Corporation
Spectrum ON-LINE
80003-033
September 1997
MCN-186; 03/06/98 MCN-204; 10/20/99 MCN-221; 11/10/99 MCN-228; 11/30/99 MCN-244; 09/25/00 MCN-252; 04/05/01 MCN-268; 11/05/01 MCN-276; 05/10/02 MCN-293; 05/27/03 MCN-308; 10/16/03 MCN-315; 02/12/04
Table of Contents
INTRODUCTION............................................................................................................................................................. 1
1.1 Unpack............................................................................................................................................................................... 1
1.1.1 Check Order................................................................................................................................................................1
1.1.2 Serial Numbers ...........................................................................................................................................................1
1.2 Turn the instrument ON.....................................................................................................................................................2
1.2.1 Verify...........................................................................................................................................................................2
1.2.2 Acknowledge alarm.....................................................................................................................................................2
1.2.3 Remove gas .................................................................................................................................................................2
1.2.4 Contact ENMET.........................................................................................................................................................2
2.0 F
EATURES AND INSTALLATION................................................................................................................................2
2.1 Features..............................................................................................................................................................................2
2.2 Installation .........................................................................................................................................................................3
2.2.1 Mount Enclosure.........................................................................................................................................................3
2.2.2 Relay Contacts............................................................................................................................................................3
2.2.3 Turn On.......................................................................................................................................................................3
3.0 O
PERATION ........................................................................................................................................................... 4
3.1 Operational Menu ..............................................................................................................................................................4
3.2 Gas Concentration Display and Alarms.............................................................................................................................5
3.4 Alarm Acknowledge..........................................................................................................................................................5
3.5 Data....................................................................................................................................................................................5
3.6 Interference Gases..............................................................................................................................................................5
4.0 M
AINTENANCE....................................................................................................................................................... 6
4.1 Maintenance Menu ............................................................................................................................................................6
4.1.1 Key ..............................................................................................................................................................................7
4.1.2 Zero.............................................................................................................................................................................7
4.1.3 Calibration..................................................................................................................................................................8
4.1.4 Changing the Alarm Level ..........................................................................................................................................9
4.1.5 Setting a New Key .......................................................................................................................................................9
4.2 Changing Components.......................................................................................................................................................9
4.2.1 Sensor Removal and Replacement..............................................................................................................................9
5.0 R
EPLACEMENT PART NUMBERS ........................................................................................................................... 10
6.0 WARRANTY...................................................................................................................................................... 11
A
PPENDIX A: CALIBRATION DATA TABLES ................................................................................................................. 12
A
PPENDIX B: INTERFERENCE GASES.......................................................................................................................... 14
List of Illustrations
Figure 1: SPECTRUM ON-LINE Features.......................................................................................................................................3
Figure 2: Operation Menu Diagram.............................................................................................................................................4
Figure 3: Maintenance Menu Diagram........................................................................................................................................6
Figure 4:Intial Calibration of Replacement Sensor......................................................................................................................8
Table 1: Gas Ranges, Alarm Points and Sensor Life................................................................................................................. 12
Table 2: Spectrum Calibration Voltage and Countdown Times ................................................................................................13
Figure 5: Identification of Calibration Adapters & Sample Draw System ................................................................................13
Reference information:
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OTE: [important information about use of instrument – if not followed may have to redo some steps.]
C
AUTION: [affects equipment – if not followed may cause damage to instrument, sensor etc…]
WARNING: [affects personnel safety – if not followed may cause bodily injury or death.]
Spectrum ON-LINE ENMET Corporation
Introduction
The SPECTRUM ON LINE is a small powered by an AC adapter operated single channel gas detection instrument. Depending on the sensor supplied with the instrument, it can detect one of a number of potential target gases. An electrochemical cell detects the gas, and the gas concentration is displayed on an LCD. Audio and visual alarms occur when the target gas concentration exceeds a preset alarm point. At relatively low concentrations of the gas, an alarm can be acknowledged, which results in the temporary cessation of the audio alarm. Operation and maintenance procedures are managed with two pushbutton switches. For ruggedness and EMF protection, the instrument enclosure is an aluminum die casting. The instrument is shown in Figure 1.
A number of sensors have been qualified for target gases, the list is found in Table 1.
NOTE: All specifications stated in this manual may change without notice.
1.1 Unpack
Unpack the SPECTRUM ON LINE and examine it for shipping damage. If such damage is observed, notify both ENMET customer service personnel and the commercial carrier involved immediately.
Regarding Damaged Shipments
NOTE: It is your responsibility to follow these instructions. If they are not followed, the carrier will
not honor any claims for damage.
This shipment was carefully inspected, verified and properly packaged at our company and delivered to the
carrier in good condition.
When it was picked up by the carrier at ENMET, it legally became your company’s property.
If your shipment arrives damaged:
Keep the items, packing material, and carton “As Is.” Within 5 days of receipt, notify the carrier’s local
office and request immediate inspection of the carton and the contents.
After the inspection and after you have received written acknowledgment of the damage from the carrier,
contact ENMET Customer Service for return authorization and further instructions. Have your Purchase Order and Sales Order numbers available.
ENMET either repairs or replaces damaged equipment and invoices the carrier to the extent of the liability
coverage, usually $100.00. Repair or replacement charges above that value are your company’s responsibility.
The shipping company may offer optional insurance coverage. ENMET only insures shipments with the
shipping company when asked to do so in writing by our customer. If you need your shipments insured, please forward a written request to ENMET Customer Service.
Regarding Shortages
If there are any shortages or questions regarding this shipment, please notify ENMET Customer Service within 5 days of receipt at the following address:
ENMET Corporation
680 Fairfield Court
Ann Arbor, MI 48108
734-761-1270 734-761-3220 Fax
1.1.1 Check Order
Check, the contents of the shipment against the purchase order. Verify that the SPECTRUM ON LINE is received as ordered. Each S they are present. Check the contents of calibration kits. Notify ENMET customer service personnel of any discrepancy immediately.
1.1.2 Serial Numbers
Each SPECTRUM ON LINE is serialized. These numbers are on tags on the equipment and are on record in an ENMET database.
PECTRUM ON LINE is labeled with its target gas. If there are accessories on the order, ascertain that
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1.2 Turn the instrument ON
Turn the instrument ON, by plugging the power supply into a standard 110 VAC wall outlet. In uncontaminated air, for most instruments the display should read 0000 within ten seconds of turn-on. For an oxygen S the display reads near 20.9%.
N
OTE: Instruments using biased sensors, this time is extended to 4 minutes, stabilization may take as long as 1 hour.
See Table 1.
1.2.1 Verify
The SPECTRUM ON LINE is calibrated prior to shipment. However, if the target gas is available, expose the sensor to it to verify that no damage occurred during shipment.
1.2.2 Acknowledge alarm
If the concentration of the target gas is greater than the alarm set point, the instrument indicates an alarm condition. Acknowledge the alarm by pressing and releasing the right hand pushbutton, SELECT; this silences the audio alarm for four minutes unless the concentration of the target gas is greater than the upper alarm limit. See Table 1 for a list of alarm set points and upper alarm limits for various target gases.
1.2.3 Remove gas
Remove the source of the target gas. After the display reads zero or close to it, unplug the instrument.
1.2.4 Contact ENMET
If the instrument does not operate as described, contact ENMET customer service personnel immediately.
PECTRUM ON LINE,
2.0 Features and Installation
2.1 Features
The features of the SPECTRUM ON LINE are shown in Figure 1. These are:
DISPLAY An LCD upon which either the gas concentration, or prompts for the operational and maintenance
menus, are given.
PUSHBUTTON
SWITCHES
OPTION The left hand switch.
SELECT The right hand switch.
These switches are used to access and utilize the operational and maintenance menus.
SENSOR HOUSING A small cylindrical turret on the display surface; the membrane of the electrochemical sensor is
VISUAL ALARM A red LED which is ON whenever the target gas concentration is above the alarm point.
AUDIO ALARM A small horn, which is ON whenever, the gas concentration is above the alarm point, until the
COVER Retained with four screws and removed to change the sensor and access the terminal strip.
RELAY CONTACTS On a terminal strip inside the enclosure.
There are two of these, as follows:
exposed to the atmosphere through the hole in the turret.
alarm is acknowledged.
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p
Pushbutton Switches
Cove
Top View
Sensor Housing
Visual Alarm
Display
Audio Alarm
Exterior View
Side View
Interior View
Terminal Stri
Figure 1: SPECTRUM ON-LINE Features
2.2 Installation
2.2.1 Mount Enclosure
Mount enclosure at an appropriate location using the four mounting holes accessible inside the enclosure. See Figure 1
Dimensions are in inches.
2.2.2 Relay Contacts
One set of alarm relay contacts are accessible on a spring-clamp terminal strip inside the enclosure after removing the cover. See below for Terminal strip locations and suggested relay wiring.
Terminal position Connection
10 C 11 NC 12 NO
Contact position refers to the unpowered condition that is also the
C NC NO
Terminal Strip
alarm condition. Relay contacts are rated at 2amps. Instrument ground is accessible at terminal strip locations 2 and 3, and +12
DC is available at locations 5, and 6. When powering an
V auxiliary device with +12 V
DC, do not overload the power supply
(exceed 200mA). If desired, the relay wires exit through the hole
110VAC
or
24 – 24VDC
VAC High or +24 – 24VDC
Strobe or Horn
on the right side of the enclosure. Remove the hole plug and use an appropriate strain relief. The strain relief is available from
VAC Neutral or –24 – 24VDC
ENMET; see Section 5.0, Replacement Parts List.
Suggested Relay wiring
2.2.3 Turn On
Plug the power supply into a 110 VAC outlet. The display should read “0000” within ten seconds when the monitor is supplied with uncontaminated air.
OTE: Instruments using biased sensors, this time is extended to 4 minutes and stabilization may take as long as 1
N
hour. See Table 1.
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N
N
N
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3.0 Operation
3.1 Operational Menu
The operational menu diagram is shown in Figure 2. This menu is accessed with the OPTION pushbutton switch, the left hand switch as viewed from the front of the instrument. Successive displays are achieved by repeatedly pushing the switch; as indicated by “O” in the menu diagram. The alarm acknowledgement function, the displays and function in the “see DATA” area, are accessed with SELECT pushbutton, indicated by “S” in the menu diagram.
Operational
Display
XXXX
O
Batt=OK*
O
Alm=XXXX
O
O
go Setup
O
Maintenance
Menu Key
See Figure 3
*may also be “low” or “LOW”
S
S
S
S
S
Acknowledge Alarm
o
Function
o
Function
Max=XXXXSee DATA
Min=XXXX
Clr DATA
O
O
O
XX YY °C
S
S
S
S
o
Function
o
Function
Reset Data
o
Function
O
O = Option Switch S = Select Switch
Figure 2: Operation Menu Diagram
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3.2 Gas Concentration Display and Alarms
The LCD furnishes a numerical display of the target gas concentration from 0000 to the upper limit of the range, shown in Table 1. The display of the target gas concentration is termed the "operational display". If the target gas concentration exceeds the upper limit of the range, the display is the numerical upper limit and a plus sign, for example,"0200+", for hydrogen sulfide. When the concentration of the target gas exceeds the alarm set point, the audio and visual alarms are activated. The gas concentration continues to be displayed during alarm. The alarm point is adjustable between a lower and upper alarm limit by accessing the maintenance menu; these and the factory setting of the alarm point are also given in Table 1. A user should have a justifiable application-based reason for setting the alarm point higher than the factory setting. When the target gas concentration drops below the alarm point, the audio and visual alarms cease operation. The alarm point setting can be observed on the display by pushing the OPTION pushbutton twice.
Some types of gases are difficult to detect in an ambient/static atmosphere. For these types of gases ENMET recommends using a sampling system similar to ENMET Sample Draw Module 03700-029. See Appendix A Table 2.
For the oxygen S (adjustable) and 23.5% (fixed).
If an alarm concentration is encountered when the display is at a location in the operational menu other than the operational display, the audio and visual alarms are activated and the alarm cannot be acknowledged.
If the display is left idle at a location other than the operational display for 45 seconds it automatically transfers to the operational display.
PECTRUM ON LINE, the zero gas display is 20.9% oxygen, and the two alarm points are at 19.5%
3.4 Alarm Acknowledge
When the instrument is in alarm, and the target gas concentration is below the upper alarm limit, the alarm can be acknowledged by pressing and releasing the SELECT pushbutton, but only when the instrument is at the operational display. The acknowledgement causes the temporary cessation of the audio alarm; the red LED continues to be ON. The audio alarm is OFF for a period of four minutes, after which it is reactivated, if the gas concentration is still above the alarm point. The alarm can again be acknowledged. However, acknowledgement of the alarm at gas concentrations above the upper alarm limit does not result in audio alarm cessation, and if the gas concentration rises above the upper alarm limit during an alarm condition which has been acknowledged, the audio alarm resumes operation.
3.5 Data
The SPECTRUM ON LINE retains the maximum and minimum gas concentration values encountered since turn-on, or since the data was cleared and reset. To access this press the OPTION pushbutton three times; "see DATA" is displayed. Press the SELECT pushbutton; the maximum concentration since turn-on or last reset is displayed. Press the OPTION pushbutton again; the minimum concentration since turn-on or last reset is displayed. Press the OPTION pushbutton again; "clr DATA" is displayed. Pushing the SELECT pushbutton clears the data and resets it to the current concentration. See comments on the use of this feature in Section 4.1.3, Calibration.
Pushing the OPTION pushbutton once more results in a display the internal temperature of the instrument in degrees centigrade and Fahrenheit. Another push of the OPTION pushbutton results in a display of the version of the code stored in the instrument. Push the OPTION pushbutton three more times to return to the operational display.
3.6 Interference Gases
For each target gas, some gases other than the target gas cause a sensor response, and thus are termed "interference gases". A compilation of known interference gases for the various target gases is given in Appendix B, along with gases that are known to not cause a sensor response.
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N
t
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4.0 Maintenance
4.1 Maintenance Menu
From the operational display, press the OPTION pushbutton four times; "go SETUP" is displayed. This is the entrance to the maintenance menu. The maintenance menu flow diagram is shown in Figure 3.
To Operational
Display
INVALID
go SETUP
S
Key=0000
VALID
run ZERO
run CAL
From Operational Display
O
S
S
O
S
O
Changes digit indicated by underscore cursor
Locks underscored digit and moves cursor
AIR SET?
S
z30:0.0v
AIR SET?
S
z30:0.0v
GAS=XXXX
S
GAS SET?
S
XXX:Y.Yv
O
VALID
INVALID
O
O or S
O
O
VALID
INVALID
To Exit
To Operational Display
C-FAULT
To Exi
o Function
o Function
To Exit
To Operational Display
C-FAULT
INVALID
set ALM
O
set KEY
O
O
Exi
S
S
S
ALM=0000
new=XXXX
KEY=0000
new=XXXX
To Operational Display
O
Changes digit indicated by underscore cursor
Locks underscored digit and moves cursor
S
O or S
O
Changes digit indicated by underscore cursor Locks underscored digit and moves cursor
S
O or S
To ExitTo Exit
To Exit
O = Option Switch S = Select Switch
Figure 3: Maintenance Menu Diagram
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4.1.1 Key
Entrance to the maintenance menu is guarded with a four digit numerical key. The factory default setting of the key is 1270(The process by which a different key is set is given in paragraph 4.1.5, below). When the valid numerical key is inserted, the user is allowed to enter the maintenance menu.
When in the "go SETUP" location, press the SELECT pushbutton; "Key=0000" is displayed. The underscore cursor is under the left hand digit. To insert the key, press the OPTION pushbutton to change the left hand digit, and choose the correct digit; then press the SELECT pushbutton, which locks in the chosen left hand digit and moves the underscore cursor one space to the right. Continue this process until the four digit key is complete. When the valid key is inserted in this manner, the display is transferred to the "run ZERO" portion of the maintenance menu. When an invalid key is inserted, "INVALID" is briefly displayed, and the instrument returns to the operational display.
4.1.2 Zero
A valid key entry sets the instrument at the "run ZERO" location, of the maintenance menu, which enables the setting of the zero gas concentration point. This is desirable if the zero reference of the gas sensor has drifted over a period of time, indicated by a persistent gas concentration reading in a clean environment. Note that the calibration sequence given below also includes setting the zero point. If a full calibration is required, instead of setting just the zero point, push the OPTION button once; "run CAL" is displayed. See paragraph 4.1.3, below.
To set the zero point without performing full calibration, from the "run ZERO" location press the SELECT pushbutton; "AIR SET?" is displayed. Be certain that the instrument is in clean air, uncontaminated by the target gas. If uncertain of the environment, use pure compressed air from a pressurized cylinder, and flow it over the sensor at a low rate.
With the instrument in “AIR SET?”, press the SELECT pushbutton again. "z30:0.0v" is displayed; this is a counter that counts down in seconds from 30 to 0. The validity of the new zero setting is then examined; if it is with in preset parameters, the display is transferred to the operational display in the operation menu.
If the new zero setting is not between preset parameters, "C-FAULT" is displayed. Unplugging and then plugging in the power supply turns the instrument OFF, then ON again. This re-boots the system with the most recent valid zero setting.
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4.1.3 Calibration
NOTE: Calibration must be performed at normal room temperature (20-25°C) for optimal performance. If the
instrument is exposed to temperature extremes just prior to calibration, allow it to stabilize to room temperature. The internal temperature of the instrument is verified by cycling through the "see DATA" menu.
In order to calibrate the instrument, it is first zeroed in a procedure similar to the one described above. Then the sensor is presented with a known concentration of the target gas, in air or an inert gas such as nitrogen, called the "span gas". After an appropriate interval, which is timed, the new span setting is examined for validity.
In some cases, the concentration of target gas in the span gas is greater than the concentration expected in the workplace. If action is not taken, the calibration gas concentration may become the permanent maximum concentration retained and displayed as data (see Section 3.5). It is good practice to record any data desired before calibration, and then to reset after calibration to clear the calibration gas concentration form memory.
A valid key entry sets the instrument at the "run ZERO" location of the maintenance menu. Press the OPTION pushbutton once to access the "run CAL" display, then press the SELECT pushbutton; "AIR SET?" is displayed. Zero the instrument as described in paragraph 4.1.2 above. When the zero timer is complete, the display indicates "GAS=XXXX", where the numbers indicate the correct span gas concentration the instrument is equipped to detect; for a CO SPECTRUM the span gas is 100 ppm CO, for Cl2 SPECTRUM the span gas is 5 ppm chlorine, and so forth. The correct span gas is given in Table 2 of Appendix A, for various target gases.
At the “GAS=XXXX” display:
1. Assure that the correct span gas is available.
2. Connect the calibration adapter to the cylinder along with the correct calibration cover; see Appendix A Table 2.
3. Open the calibration valve so that the span gas flows.
4. Press the SELECT pushbutton; "GAS SET?" is displayed.
5. Connect the span gas to the instrument so the calibration gas flows over the sensor.
6. Press the SELECT pushbutton; "XXX:Y.Yv" is displayed.
7. Remove span gas
The XXX is a counter which counts down in seconds to zero from the correct starting time to provide the proper time interval for calibration; this time interval may vary depending on your target gas. The Y.Y v indicates a sensor signal which is used during the sensor replacement procedure. When the timer reaches zero, the new calibration and zero gas settings are examined for validity. If the value is with in preset parameters, the display is transferred to the gas operational display in the operations menu.
During calibration the audio alarm is disabled, and after calibration is complete the audio alarm remains disabled for up to 2.5 minutes.
If the new settings are not within preset parameters, "C-FAULT" is displayed. Unplugging and then plugging in the power supply turns the instrument OFF, then ON again. This re-boots the system with the most recent valid zero and calibration settings. Recalibrate. If after recalibration the instrument still displays “C-FAULT” the sensor may be expired. Replace the sensor in accordance with Section 4.2.1.
Opaque, Calibration Cup
*Centered over Sensor
Senso
Spectrum PCB
Sensor, Bottom View
*CAUTION: Having the calibration cup too tight will cause the sensor to become deadheaded resulting in an inaccurate
calibration.
Figure 4:Intial Calibration of Replacement Sensor
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4.1.4 Changing the Alarm Level
A valid key entry sets the instrument at the "run ZERO" location of the maintenance menu. Press the OPTION pushbutton twice to access the "set ALM" display, then press the SELECT pushbutton; ALM=0000" is displayed. This is called the alarm update window, and the value displayed is the present alarm setpoint. The underscore cursor is under the far left digit. Press the OPTION pushbutton to change the underscored digit; select the desired digit, and press the SELECT pushbutton to lock in the desired digit and move the underscore cursor one position to the right. When the desired new alarm point is set “new=XXXX” is displayed. Press either the OPTION or SELECT pushbutton to exit the alarm update window. If the new alarm setting is valid, "exit" is displayed. Press the OPTION pushbutton to return to the operational display, or the SELECT pushbutton to return to “run ZERO”.
For the safety of the user, there are upper and lower limits past which the alarm setting is invalid, and the instrument does not accept them. If an invalid alarm setting is attempted, after the numerical value is inserted in the "ALM=0000" window, pressing the OPTION or SELECT pushbutton results in a momentary display of "INVALID" after which the display returns to the alarm update window. Exiting the alarm update window at this point results in an alarm point setting unchanged from the value present when the procedure was begun.
Factory default alarm setpoints and alarm limits are shown in Table 1.
4.1.5 Setting a New Key
A valid key entry sets the instrument at the "run ZERO" location of the maintenance menu. Press the OPTION pushbutton four times to access the "set KEY" display. Press the SELECT pushbutton once; "KEY=0000 is displayed. A new key can be set by changing the underscored number with the OPTION pushbutton and moving the underscore cursor with the SELECT pushbutton. After the new key is entered “new-XXXX” is displayed, press the
OPTION or SELECT pushbutton to display to “exit”, then press the OPTION pushbutton to return to “run ZERO”.
OTE: Four digit key numbers should be selected carefully and recorded. Without the correct key, the maintenance
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menu cannot be accessed. If a four digit key number is lost, call ENMET customer service personnel.
4.2 Changing Components
Changing the sensor, or the display requires that the cover of the instrument to be removed; remove the four phillips head, cover retaining, screws and then the cover.
4.2.1 Sensor Removal and Replacement
A sensor must be replaced when it no longer responds adequately to the target gas. This is indicated by a low gas concentration reading when exposed to a known concentration of the target gas, and the inability to calibrate the instrument, without a "C-FAULT" display after calibration. Expected sensor lifetimes in normal environments are given in Table 1.
After removing the cover of the enclosure, unplug the sensor from the circuit board.
AUTION: New sensors may come with a shorting clip that must be removed for proper operation.
C
Remove the shorting clip (if present) from the new sensor and plug the new sensor in place. Allow the sensor to stabilize in the instrument with the power on for one hour before the initial calibration of a new sensor.
The initial calibration of a new sensor must be performed with the cover removed from the instrument enclosure. Follow the procedure for calibrating the instrument as outlined in Section 4.1.3 of this manual with the following modification:
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OTE: During this procedure put the OPAQUE calibration cup, 02552-008, directly over the sensor and make sure it stays
centered.
During the application of the span gas, the counter counts down from an upper value given in Table 2. When the counter gets down to 60, adjust the potentiometer located to the left of the display on the instrument circuit board, so that the display to the right of the counter reads a little above the calibration voltage given for the target gas in Table 2. As the counter continues, turn the pot so that the calibration voltage is reached when the counter reaches 30. This is a one-time adjustment to align the sensor output with the instrument electronics. It should only be performed upon sensor replacement. All future calibrations should follow the procedure in Section 4.1.3.
Replace the cover of the instrument. Recalibrate the instrument according to the procedure in Section 4.1.3. to assure sensor output alignment.
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OTE: that the sensor must be replaced with a sensor for the same target gas; the instrument cannot be changed to detect
a different target gas without modifications in addition to changing the sensor type.
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5.0 Replacement Part Numbers
ENMET part numbers for replacement parts and accessories:
Calibration Equipment
Cylinder Adapter, 34 liters 02506-002 Cylinder Adapter, 17 liters 02506-004 *Calibration cup, (Initial Calibration) 02552-008 (Opaque) Calibration cup 03620-011 (White) Sampling Adapter 03620-018 Female Quick Release 73073-020
*Used on all Sensor Replacements.
Calibration Gas
Calibration gas, chlorine 03231-005 Calibration gas, hydrogen sulfide 03214-020 Calibration gas, hydrogen cyanide 03203-010 Calibration gas, sulfur dioxide 03215-015 Calibration gas, ammonia 03218-025 Ozone generator 04055-0800
Other calibration gases are available, contact ENMET for details.
Replacement Sensors and parts
Replacement chlorine sensor 67020-0100 Replacement hydrogen sulfide sensor 67020-0200 Replacement hydrogen cyanide sensor 67020-0300 Replacement hydrogen chloride sensor 67020-0400 Replacement sulfur dioxide sensor 67024-0500 Replacement phosgene sensor 67020-0600 Replacement hydrogen fluoride sensor 67020-0700 Replacement ozone sensor 67020-0803 Replacement oxygen sensor 67016-1114 Replacement carbon monoxide sensor 67020-1200 Replacement fluorine sensor 67020-1400 Replacement hydrogen sensor 67020-1500 Replacement nitrogen dioxide sensor 67020-1700 Replacement nitrous oxide sensor 67020-1750 Replacement ammonia sensor 67020-2400 Replacement arsine sensor 67020-4000 Replacement silane sensor 67020-4003
Display Assembly 62022-007 Strain relief 73046-002
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6.0 WARRANTY
ENMET warrants new instruments to be free from defects in workmanship and material under normal use for a period of one year from date of shipment from ENMET. The warranty covers both parts and labor excluding instrument calibration and expendable parts such as calibration gas, filters, batteries, etc... Equipment believed to be defective should be returned to ENMET within the warranty period (transportation prepaid) for inspection. If the evaluation by ENMET confirms that the product is defective, it will be repaired or replaced at no charge, within the stated limitations, and returned prepaid to any location in the United States by the most economical means, e.g. Surface UPS/FedEx Ground. If an expedient means of transportation is requested during the warranty period, the customer is responsible for the difference between the most economical means and the expedient mode. ENMET shall not be liable for any loss or damage caused by the improper use of the product. The purchaser indemnifies and saves harmless the company with respect to any loss or damages that may arise through the use by the purchaser or others of this equipment.
This warranty is expressly given in lieu of all other warranties, either expressed or implied, including that of merchantability, and all other obligations or liabilities of ENMET which may arise in connection with this equipment. ENMET neither assumes nor authorizes any representative or other person to assume for it any obligation or liability other than that which is set forth herein.
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OTE: When returning an instrument to the factory for service:
Be sure to include paperwork.A purchase order, return address and telephone number will assist in the expedient repair and return of your unit.Include any specific instructions.For warranty service, include date of purchaseIf you require an estimate, please contact ENMET Corporation.
There is Return for Repair Instructions and Form on the last pages of this manual. This form can be copied or used as needed.
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Appendix A: Calibration Data Tables
Table 1: Gas Ranges, Alarm Points and Sensor Life
Gas Range
Ammonia
Arsine
Carbon Monoxide
Chlorine
Fluorine
Hydrogen
Hydrogen Chloride {
Hydrogen Cyanide
Hydrogen Fluoride
Hydrogen Sulfide
Nitric Oxide {
Nitrogen Dioxide
Oxygen
Ozone
Phosgene
Alarm
lower limit
0-100ppm 15ppm 50ppm 25ppm 1 year
0-0.99ppm 0.03ppm 0.10ppm 0.05ppm 1-1.5 years
0-1000ppm 5ppm 200ppm 35ppm 2-3 years
0-10ppm 0.5ppm 5.0ppm 1.0ppm 1-2 years
0-10ppm 1ppm 5ppm 1ppm 2-3 years
0-1000ppm 200ppm 750ppm 200ppm 1-2 years
0-20ppm 3.0ppm 10.0ppm 5.0ppm 1-2 years
0-20ppm 3.0ppm 10ppm 4.7ppm 2-3 years
0-10ppm 2.0ppm 6.0ppm 3.0ppm 1 year
0-200ppm 5.0ppm 25ppm 10ppm 2-3 years
0-100ppm 15ppm 50ppm 25ppm 1-2 years
0-10ppm 1.0ppm 5.0ppm 3.0ppm 1-2 years
0-25% 16% 23.5% 19.5% & 23.5% 1.5-2 years
0-0.99ppm 0.05ppm 0.2ppm 0.1ppm 1-1.5 years
0-0.99ppm 0.05ppm 0.20ppm 0.1ppm 1 years
Alarm
upper limit
Factory Alarm
Set Point
Expected Sensor
Lifetime
Phosphine
Silane
Sulfur Dioxide
0-0.99ppm 0.15ppm 0.30ppm 0.50ppm 1-1.5 years
0-30ppm 3ppm 5ppm 5ppm 1-1.5 years
0-20ppm 2.0ppm 10ppm 5ppm 1-2 years
NOTE: All specifications stated in this manual may change without notice.
{ Biased Sensors: Instruments using biased sensor, stabilization time is extended to 4 minutes. Complete stabilization
may take as long as 1 hour. When instrument is turned on it may display XXXX has been off for an extended amount of time it may be necessary to “cycle” (turn on and off) the instrument several times.
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+ . If instrument
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Table 2: Spectrum Calibration Voltage and Countdown Times
NOTE: The following are values used for production calibration. Not all gases are available for field calibration;
contact ENMET customer service personnel.
Gas Calibration Gas
Ammonia Arsine (2) Carbon Monoxide Chlorine (2) Fluorine (2) Hydrazine Hydrogen Hydrogen Chloride (2) Hydrogen Cyanide Hydrogen Fluoride (1) Hydrogen Sulfide Nitric Oxide Nitrogen Dioxide Oxygen Ozone (1) Phosgene (1) Phosphine (2) Silane Sulfur Dioxide
0.5ppm PH
3ppm Cl2= 7.5ppm
= 0.38ppm
3
100ppm * 03620-011 1.70 120 sec
800ppm * 03620-011 2.20 180 sec
20.9%(air) * 03620-011 2.80 120 sec
0.66ppm
* Calibration Cup
25ppm * 03620-011 0.67 180 sec
03620-018
5ppm
0.3ppm
10ppm
10ppm * 03620-011 2.10 120 sec
5ppm 20ppm * 03620-011 0.46 120 sec 25ppm
5ppm * 03620-011 1.30 120 sec
0.3ppm
0.5ppm * 03620-011 0.13 120 sec 5ppm
10ppm
03620-011
03620-011
TBD
03620-018
TBD
TBD
03620-018
03620-018
TBD TBD
Calibration Voltage Countdown Time
0.10 120 sec
1.40 180 sec
1.80 240 sec
0.91 240 sec
2.10 180 sec
1.40 240 sec
0.67 90 sec
0.75 240 sec
0.18 240 sec
0.54 120 sec
2.10 90 sec
NOTE: All specifications stated in this manual may change without notice.
TBD – To Be Determined
(1) Require use of Sample Draw System. See Figure 5. (2) Recommended use of Sample Draw System, for enhanced sensitivity and speed of response. See Figure 5.
* Initial Calibration Cup 02552-008
For ALL Sensor Replacement
Calibration Cup 03620-011
To Sensor
To Sensor
Initial Calibration Cup 02552-023
For Sensor Replacement
To Sensor
Sample Adapter 03620-018
73073-020
quick release
To Sensor
Figure 5: Identification of Calibration Adapters & Sample Draw System
Gas Cylinder
& Regulator
Example of Sample Draw System
Sample Draw System 04565-314 Shown with Spectrum OnLine attached
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ENMET Corporation Spectrum ON-LINE
Appendix B: Interference Gases
Interference Table for Selected Spectrum Sensors
SPECTRUM Series for AMMONIA (3E-100 sensor)
The following gases cause a reading:
Interferant Gas/Vapor
ethanol 1000 1 isopropanol 450 1 hydrogen sulfide 14 10 methanol 1200 3 hydrogen 1000 80 carbon monoxide 300 100 sulfur dioxide 25 -21 nitrogen dioxide 50 25 hydrogen cyanide 10 -18
The following gases or vapors have been tested and do not cause a reading:
Interferant Gas/Vapor Concentration in ppm
chlorine 5 unsaturated hc (ethylene) 1.0 % saturated hydrocarbons abundant
Interferant Concentration in ppm
Instrument Reading in ppm
SPECTRUM Series for CARBON MONOXIDE (3E sensor)
The following gases cause a reading:
Interferant Gas/Vapor
hydrogen 1000 450 nitric oxide 100 25
The following gases or vapors have been tested and do not cause a reading:
Interferant Gas/Vapor Concentration in ppm
ammonia 100 chlorine 5 hydrogen cyanide 10 ethylene 2.0 % * carbon dioxide 5,000 methane 10,000 sulfur dioxide 10 * hydrogen sulfide 10 * nitrogen dioxide 10 * isopropanol 1,025 * gasoline vapor saturated *
*with onboard filter; continuous high level exposure may reduce the filter efficiency
Interferant Concentration in ppm
Instrument Reading in ppm
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SPECTRUM Series for CHLORINE (3E sensor)
The following gases cause a reading:
Interferant Gas/Vapor
Interferant Concentration in ppm
Instrument Reading in ppm
hydrogen sulfide 10 -0.3 sulfur dioxide 5 -1.2 nitrogen dioxide 5 0.1 bromine 1 1.0 chlorine dioxide 0.32 0.3 ammonia 1,000 -1.1
The following gases or vapors have been tested and do not cause a reading:
Interferant Gas/Vapor Concentration in ppm
carbon monoxide 300 carbon dioxide 100,000 nitrogen 100. % hydrogen chloride 20 hydrocarbons, general % range hydrogen 1,000 ethanol 6.6 % ammonia 65
SPECTRUM Series for HYDROGEN SULFIDE (3E sensor)
The following gases cause a reading:
Interferant Gas/Vapor
Interferant Concentration in ppm
carbon monoxide 100 3 chlorine 20 -1 ethylene 500 2 hydrogen 100 5 hydrogen 20,000 100 hydrogen cyanide 10 1 sulfur dioxide 10 3
The following gases or vapors have been tested and do not cause a reading:
Interferant Gas/Vapor Concentration in ppm
ammonia 100 carbon dioxide 5,000 methane 10,000 sulfur dioxide 3 nitrogen dioxide 10
Instrument Reading in ppm
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ENMET Corporation Spectrum ON-LINE
SPECTRUM Series for Hydrogen Chloride (3E 30 sensor)
The following gases cause a reading:
Interferant Gas/Vapor
Interferant Concentration in ppm
Instrument Readilng in ppm
hydrogen bromide 5 5 hydrogen sulfide 14 30 sulfur dioxide 5 3.5 chlorine 5 1 hydrogen cyanide 14 1 arsine 330 ppb .4 ethanol 6.6% 6
The following gases or vapors have been tested and do not cause a reading:
Interferant Gas/Vapor Concentration in ppm
carbon monoxide 300 carbon dioxide 5000 nitrogen 100% hydrocarbons % range hydrogen 1000 phosgene .5 chlorinated hydrocarbons % range ammonia 300
SPECTRUM Series for Hydrogen Fluoride (3E 10 sensor)
The following gases cause a reading:
Interferant Gas/Vapor
Interferant Concentration in ppm
chlorine or bromine 5 .51 sulfur dioxide 2 2 hydrogen chloride 5 .75
The following gases or vapors have been tested and do not cause a reading:
Interferant Gas/Vapor Concentration in ppm
alcohols (i.e. IPA) 1000 ammonia 100 hydrogen 1000 carbon monoxide 50 carbon dioxide 10% unsaturated HC(ethylene) 1% hydrogen sulfide 20
Instrument Reading in ppm
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SPECTRUM Series for Fluorine (3E 10 sensor)
The following gases cause a reading:
Interferant Gas/Vapor
Interferant Concentration in ppm
Instrument Reading in ppm
chlorine 1 2 hydrogen sulfide 10 -1 sulfur dioxide 5 -3.2 nitrogen dioxide 5 .5 bromine 1 3 ammonia 1000 -3.1
The following gases or vapors have been tested and do not cause a reading:
Interferant Gas/Vapor Concentration in ppm
carbon monoxide 300 carbon dioxide 100000 nitrogen 100% hydrogen chloride 10 hydrocarbons % range hydrogen 1000 hydrogen cyanide 10 ethanol 4%
SPECTRUM Series for Hydrogen (2E 2000 sensor)
The following gases cause a reading:
Interferant Gas/Vapor
Interferant Concentration in ppm
Instrument Reading in ppm
carbon monoxide 50 .06 ethylene 500 .28 sulfur dioxide 2 .06 isopropanol 1090 180
The following gases or vapors have been tested and do not cause a reading:
Interferant Gas/Vapor Concentration in ppm
ammonia 100 carbon dioxide 1000 chlorine 5 hydrogen cyanide 10 hydrogen sulfide 10* methane 10000 nitrogen dioxide 10 sulfur dioxide 2
*with onboard filter; continuous high level exposure may reduce the filter efficiency
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ENMET Corporation Spectrum ON-LINE
SPECTRUM Series for Nitric Oxide (3E 100 sensor)
The following gases or vapors have been tested and do not cause a reading:
Interferant Gas/Vapor Concentration in ppm
chlorine 5 nitrogen dioxide 100 hydrogen 1000 carbon monoxide 1000 carbon dioxide 10000 saturated HC, alcohols abundant sulfur dioxide 50
SPECTRUM Series for Nitrogen Dioxide (3E sensor)
The following gases cause a reading:
Interferant Gas/Vapor
Interferant Concentration in ppm
Instrument Reading in ppm
chlorine 1 3 ozone 1 0.7
The following gases or vapors have been tested and do not cause a reading:
Interferant Gas/Vapor Concentration in ppm
hydrogen chloride 5 nitrogen oxide 100 hydrogen 1000 carbon monoxide 1000 carbon dioxide 10000 saturated HC, alcohols abundant sulfur dioxide 50 ammonia 30
SPECTRUM Series for Hydrazine (2E sensor)
The following gases cause a reading:
Interferant Gas/Vapor
Interferant Concentration in ppm
ammonia 200 0.4 methyl hydrazine 1 0.72
1.1 dimethyl hydrazine 1 0.45 chlorine 3 –0.02 hydrogen sulfice 20 0.1
The following gases or vapors have been tested and do not cause a reading:
Interferant Gas/Vapor Concentration in ppm
ethanol 1000 Isopropanol 450 hydrogen peroxide 10 hydrogen chloride 7 methanol 1200 hydrogen 2000 carbon monoxide 1000 carbon dioxide 5000 unsaturated HC (ethylene) 1%
Instrument Reading in ppm
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Spectrum ON-LINE ENMET Corporation
SPECTRUM Series for Ozone (3E 1 sensor)
The following gases cause a reading:
Interferant Gas/Vapor
Interferant Concentration in ppm
Instrument Reading in ppm
chlorine 1 0.80 fluorine 100ppb 0.07 germane 1 1 nitrogen dioxide 1 0.09
The following gases or vapors have been tested and do not cause a reading:
Interferant Gas/Vapor Concentration in ppm
hydrogen sulfide 1 sulfur dioxide 2 phosphine 100 ppb carbon monoxide 300 carbon dioxide 5000 nitrogen 100% nitrogen monoxide 10 hydrocarbons % range hydrogen 1000 hydrogen cyanide 10 ammonia 10 hydrogen fluoride 3.8 hydrochloric acid 10
SPECTRUM Series for Hydrogen Cyanide (2E 30 sensor)
The following gases cause a reading:
Interferant Gas/Vapor
Interferant Concentration in ppm
Instrument Reading in ppm
hydrogen sulfide 15 40 chlorine 5 -1 nitrogen dioxide 100 -40
The following gases or vapors have been tested and do not cause a reading:
Interferant Gas/Vapor Concentration in ppm
hydrogen chloride 10* methane 2000 carbon monoxide 300 carbon dioxide 10 % freon 12 5000 petrol 300 sulfur dioxide 50* nitrogen 100 % nitrogen monoxide 100
cholrinated hydrocarbons <200 Long term exposure may destroy the sensor. *with onboard filter; continuous high level exposure may reduce the filter efficiency
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ENMET Corporation Spectrum ON-LINE
SPECTRUM Series for Sulphur Dioxide(4S sensor)
The following gases cause a reading:
Interferant
Gas/Vapor
Interferant Concentration in ppm
Instrument Reading in ppm
carbon monoxide 300 <3
hydrogen sulphide 15 0
nitric oxide 35 0
nitrogen dioxide 5 ≈-5
The following gases or vapors have been tested and do not cause a reading:
Interferant Gas/Vapor Concentration in ppm
chlorine 1
hydrogen 200
hydrogen cyanide 10
hydrogen chloride 5
ethylene 100
SPECTRUM Series for Arsine (2E sensor)
The following gases cause a reading:
Interferant Gas/Vapor
Interferant Concentration in ppm
Instrument Reading in ppm
phosphine 100 ppb 110 chlorine 5 -400 hydrogen cyanide 10 100 ammonia 100 10 diborane 100 35 silane 1 100 germane 1.1 100 hydrogene selenide 50 ppb 5
The following gases or vapors have been tested and do not cause a reading:
Interferant Gas/Vapor Concentration in ppm
hydrogen sulfide 1* sulfur dioxide 2 hydrochloric acid 5 carbon monoxide 300 carbon dioxide 5000 nitrogen 100 % hydrocarbons % range hydrogen 1000
*with onboard filter; continuous high level exposure may reduce the filter efficiency
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SPECTRUM Series for Phosgene (3E sensor)
The following gases cause a reading:
Interferant Gas/Vapor
Interferant Concentration in ppm
Instrument Reading in ppm
ammonia 50 5, drops to 0 in short time abundant change in humidity yes
The following gases or vapors have been tested and do not cause a reading:
Interferant Gas/Vapor Concentration in ppm
hydrogen sulfide 1* sulfur dioxide 2 hydrochloric acid 5* carobn monoxide 300 carbon dioxide 5000 nitrogen 100% chlorine 1 hydrocarobons % range hydrogen 1000 sulfuric acid 5
*with onboard filter; continuous high level exposure may reduce the filter efficiency
SPECTRUM Series for Silane (3E 50 sensor)
The following gases cause a reading:
Interferant Gas/Vapor
Interferant Concentration in ppm
Instrument Reading in ppm
chlorine 0.5 -4 hydrogen cyanide 10 1 ammonia 100 <1 diborane 100 0.4 arsine 1 0.7 germane 1 1 disilane 5 yes phosphine 300ppb 0.2
The following gases or vapors have been tested and do not cause a reading:
Interferant Gas/Vapor Concentration in ppm
hydrogen sulfide 1* sulfur dioxide 2 hydrochloric acid 5 carobn monoxide 300 carbon dioxide 5000 nitrogen 100% chlorine 1.5 hydrocarobons % range hydrogen 1000 hydogen fluoride 3.8
hydrogen selenide 50ppb *with onboard filter; continuous high level exposure may reduce the filter efficiency short term gas exposure (min.)
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ENMET Corporation Spectrum ON-LINE
Notes:
22
PO Box 979 680 Fairfield Court Ann Arbor, Michigan 48106-0979
734.761.1270 Fax 734.761.3220
Returning an Instrument for Repair
ENMET instruments may be returned to the factory or any one of our Field Service Centers for regular repair service or calibration. The ENMET Repair Department and Field Service Centers also perform warranty service work.
When returning an instrument to the factory or service center for service, paperwork must be included which contains the following information:
¾ A purchase order number or reference number.
¾ A contact name with return address, telephone and fax numbers
¾ Specific instructions regarding desired service or description
of the problems being encountered.
¾ Date of original purchase and copy of packing slip or invoice
for warranty consideration.
¾ If a price estimate is required, please note it accordingly and be
sure to include a fax number.
Providing the above information assists in the expedient repair and return of your unit.
Failure to provide this information can result in processing delays.
ENMET charges a one hour minimum billing for all approved repairs with additional time billed to the closest tenth of an hour. All instruments sent to ENMET are subject to a minimum $30 evaluation fee, even if returned unrepaired. Unclaimed instruments that ENMET has received without appropriate paperwork or attempts to advise repair costs that have been unanswered, after a period of 60 days, may be disposed of or returned unrepaired COD with the evaluation fee.
Service centers may have different rates or terms. Be sure to contact them for this information.
Repaired instruments are returned by UPS/FedEx Ground and are not insured unless otherwise specified. If expedited shipping methods or insurance is required, it must be stated in your paperwork.
Note: Warranty of customer installed components.
If a component is purchased and installed in the field, and fails within the warranty term, it can be returned to ENMET and will be replaced, free of charge, per ENMETs returned goods procedure.
If the entire instrument is returned to ENMET Corporation with the defective item installed, the item will be replaced at no cost, but the instrument will be subject to labor charges at half of the standard rate.
Repair Return Form
Mailing Address:
ENMET Corporation PO Box 979 Ann Arbor, Michigan 48106
Phone Number: 734.761.1270 FAX Number: 734.761.3220
Your Mailing Address:
Contact Name: __________________________ Your Phone: _______________________
Your PO/Reference Number: _______________ Your FAX: _______________________
Shipping Address:
ENMET Corporation Attn: Repair Department 680 Fairfield Court Ann Arbor, Michigan 48108
Your Shipping Address:
Payment Terms: T COD
(Check one) T VISA / MasterCard______________________ ________
Card number Expiration
Return Shipping Method:
T UPS: T Ground T 3 Day Select T Next Day Air T ND Air Saver T 2-Day Air
T Federal Express: T Ground T Express Saver T P-1 T Standard T 2-Day Air
T FedEx Account number: ________________________
Would you like ENMET to insure the return shipment?
T No T Yes Insurance Amount: $_________________
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