Elcometer 2300 Series, 2300 RV1-L, 2300 RV1-R, 2300 RV2-L, 2300 RV2-R Operating Instructions Manual

Elcometer 2300

Rotational Viscometer

and

ViscosityMaster Software

English

Operating Instructions

English

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The Elcometer Rotary Viscometer has been tested in accordance with EU regulations
governing Electro-magnetic compliance and it meets the required directives.
Note: Gauge readings may be affected if the unit is operated within a radio frequency
electromagnetic strength of greater than 3 V/m.

is a registered trademark of Elcometer Instruments Ltd.

All other trademarks acknowledged.

© Copyright Elcometer Instruments Ltd. 2006-2007.

All rights reserved. No part of this Document may be reproduced, transmitted, transcribed, stored
(in a retrieval system or otherwise) or translated into any language, in any form or by any means
(electronic, mechanical, magnetic, optical, manual or otherwise) without the prior written permission
of Elcometer Instruments Ltd.

A copy of this Instruction Manual is available for download on our Website via
www.elcometer.com/downloads.

Doc.No. TMA-0377 Issue 03

Text with Cover No: 19708

CONTENTS

CONTENTS

Section Page

SECTION A:VISCOMETER

1 About your Viscometer . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

2 Getting started . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4

2.1 The parts of the instrument . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4

2.2 Assembling the Viscometer . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5

2.3 Rear connections . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6

2.4 Control panel . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6

2.5 Configuring your Viscometer . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7

2.6 Fitting the spindle guard. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9

2.7 Spindle types . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10

2.8 Fitting the spindle. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11

2.9 Caution . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11

3 Using your Viscometer . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12

3.1 Before you start . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12

3.2 Setting spindle type and rotation speed. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12

3.3 Starting a measurement. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13

3.4 Viscosity measurement problems . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13

3.5 After use . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14

4 Printing test results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14

5 Using the optional accessories . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15

5.1 Adaptor for small sample volumes. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15

5.2 Adaptor for low viscosity samples . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16

5.3 Adaptor for helical movement . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17

6 Spindle selection tables . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19

6.1 L and TL Spindles (For use with RV1-L / RV2-L Viscometers).. . . . . . . . . . . . . . . . . . . 19

6.2 R and TR Spindles (For use with RV1-R / RV2-R Viscometers) . . . . . . . . . . . . . . . . . . 21

6.3 LCP Spindle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23

6.4 P series spindles . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 24

7 Calibration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 25

8 Maintenance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 25

9 Troubleshooting. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 26

10 Technical specification . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 27

11 Spare parts and accessories . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 28

12 Related equipment. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 29

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SECTION B:VISCOSITYMASTER SOFTWARE

13 About ViscosityMaster . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 30

13.1 System Requirements . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 30

14 Getting started . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 30

14.1 Installing ViscosityMaster. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 30

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CONTENTS

14.2 Uninstalling ViscosityMaster. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 31

14.3 Starting ViscosityMaster. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 31

14.4 Connecting your Viscometer . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 31

14.5 Preferences . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 31

14.6 Help . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 32

15 The user interface . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 33

16 Example data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 34

17 Operating modes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35

18 Instructions for RV1 Viscometers. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35

18.1 Setting up a batch . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35

18.2 Running a batch . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 37

19 Instructions for RV2 Viscometers. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 37

19.1 Setting up a batch . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 37

19.2 Setting up processes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 39

19.3 Running a batch . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 40

20 Working with Viscometer data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 41

20.1 Viewing Measurement Data and Standard Reports . . . . . . . . . . . . . . . . . . . . . . . . . . . . 41

20.2 Customising report window tabs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 43

20.3 Creating Custom Reports. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 43

20.4 Viewing a Custom Report. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 44

20.5 Exporting Measurement Data. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 45

20.6 Printing, Creating PDF Files and E-mailing from ViscosityMaster . . . . . . . . . . . . . . . . . 45

21 Using documents and images . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 46

22 The page designer . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 47

22.1 Designing a Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 48

22.2 The Property Editor . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 49

22.3 The Text Editor. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 50

22.4 Text Editor Data Field Buttons . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 51

23 Support . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 51

24 Index . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 52

ABOUT YOUR VISCOMETER

SECTION A: VISCOMETER

Thank you for purchasing this Elcometer Rotary Viscometer. Welcome to Elcometer.

Elcometer are world leaders in the design, manufacture and supply of inspection equipment for
coatings and concrete. Our products cover all aspects of coating inspection, from development
through application to post application inspection.

The Elcometer Rotary Viscometer is a world beating product. With the purchase of this product you
now have access to the worldwide service and support network of Elcometer. For more information
visit our website at www.elcometer.com

1 ABOUT YOUR VISCOMETER

The Elcometer Rotary Viscometer measures the viscosity of liquids in accordance with ISO 2555
and many ASTM standards.

A spindle fitted with a disc or a cylinder is rotated in the sample to be tested. A spring is connected
between the spindle and the motor shaft which rotates at a fixed speed. The angle of deviation
between the spindle and the motor shaft is measured electronically and converted to torque. The
torque measured by the Viscometer is a function of:

• spindle rotation speed

• spindle geometry (disc/cylinder size)

• viscosity of the test sample

Taking into account the spindle rotation speed and the spindle geometry, viscosity is calculated and
displayed directly in SI or CGS units.

A range of spindles is supplied with the Viscometer; the combination of the appropriate spindle and
spindle rotation speed allows readings to be taken over a very wide range of viscosity.

Optional accessories enable measurement of:

• Low viscosity samples - at temperatures up to 100°C (212°F)

• Low viscosity samples - at temperatures up to 200°C (392°F)

• Small volumes of sample

• Difficult-to-measure samples such as creams, gels, waxes and pastes, etc.

See “Spare parts and accessories” on page 28 for details of all accessories.

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1.1 These instructions

These instructions describe the operation of the following Elcometer Rotary Viscometers:

• Elcometer 2300 RV1-L (low to medium viscosity tests)

• Elcometer 2300 RV1-R (medium to high viscosity tests)

• Elcometer 2300 RV2-L (low to medium viscosity tests, PC controlled)

• Elcometer 2300 RV2-R (medium to high viscosity tests, PC controlled)

1

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ABOUT YOUR VISCOMETER

1.2 What the box contains

• Viscometer head

• Column with head mounting bracket

• Spindles L1 to L4 or R2 to R7 (R2 to R7 shown in illustration)

•Base

• Box spanner tool

• Hexagonal wrench

• Spindle guard

• Power supply cable

• Storage rack

• PT100 Temperature probe

• RS 232 connection cable

• ViscosityMaster software

• Calibration certificate

• Operating instructions

• Carrying case

2

ABOUT YOUR VISCOMETER

1.3 Standards

Your Viscometer can be used in accordance with the following National and International
Standards:

• BS 3900 A7-2

• ISO 2884-2

• ASTM D2196

1.4 Features of your Viscometer

• 19 speeds from 0.3 rpm to 200 rpm

• PT100 temperature probe

• RS 232 interface (bidirectional on RV2 models)

• Data download software

• Remote control via PC (RV2 models only)

• Audible warning if viscosity reading exceeds the optimum measuring range

• 4 line display showing:

• Viscosity (cP or mPa•s)

• Spindle rotation speed

• % scale (Brookfield)

• Sample temperature

• Auto range

• Shear rate (RV2 models only)

• Shear stress (RV2 models only)

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Your Elcometer Rotary Viscometer is packed in a cardboard and foam package. Please ensure that
this packaging is disposed of in an environmentally sensitive manner. Consult your local
Environmental Authority for further guidance.

To maximise the benefits of your new Elcometer Rotary Viscometer please take some time
to read these Operating Instructions. Do not hesitate to contact Elcometer or your Elcometer
supplier if you have any questions.

3

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GETTING STARTED

2 GETTING STARTED

This section of the instructions is intended for first-time users of the Elcometer Rotary Viscometer.
It contains information on the parts and controls of the instrument and advice on safe use of the
equipment. When you have finished reading this section you will be ready to start using your
Elcometer Rotary Viscometer.

2.1 The parts of the instrument

Bubble level

Viscometer head with

display and control

panel

Temperature probe

4

Spindle

Base

Column

2.2 Assembling the Viscometer

To assemble your Viscometer:

1. Remove the nut from the bottom end of the column.

2. Fit the column onto the base with the slot facing
towards the front.

3. Fit the nut onto the bottom of the column and tighten
using the box spanner supplied with your Viscometer.

4. Place the base and column on a stable and flat surface.

5. Insert the rear rod of the Viscometer head through the
hole in the mounting bracket on the column.

6. Rotate the mounting bracket lever to lock the
Viscometer head in position.

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GETTING STARTED

7. Rotate the two adjustable legs of the base until the
Viscometer is level; use the bubble level on the top of
the instrument as a guide.

8. Remove the plastic protection cap from the bottom of
the Viscometer; pull the cap vertically down until it is
well clear of the drive coupling and then remove to one
side.

Do not throw the protection cap away. Always
replace the protection cap when the instrument is
not in use.

9. Connect the instrument to the mains.

5

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GETTING STARTED

2.3 Rear connections

PT 100

probe

socket

Power
supply
socket

RS 232

interface

Power

on/off

switch

2.4 Control panel

Your Viscometer is controlleda using the five buttons on the control panel on the front of the
Viscometer head.

Enter setup screen

ENTER

Start /

stop

motor

START

UP

DOWNSTOP

Increase /
decrease
speed and
modify setup
functions

a. Viscometer models RV2 can be connected to a PC and controlled remotely via the supplied ViscosityMaster

software - see the instructions supplied with the software.

6

GETTING STARTED

2.5 Configuring your Viscometer

Switch on the Viscometer by pressing the power on/off switch at the rear of the Viscometer head.
A welcome message will be displayed for a period of two seconds. The contents of the message
will depend upon the model, software version and language setting:

V2-R v4.3

English

While this message is displayed, press the [START] and then the [ENTER] buttons.

The language selection screen will appear:

Select Language

English

Using the [UP] or [DOWN] buttons, select the desired language (German, Catalan, Spanish,
French, English, Italian or Portuguese). Press [ENTER] to confirm your selection.

The viscosity units selection screen will appear:

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Viscosity Units

SI (mPas)

Using the [UP] or [DOWN] buttons, select the viscosity units, SI (mPa•s) or CGS (cP). Press
[ENTER] to confirm your selection.

Model RV2 only: The shear stress units selection screen will appear:

Shear Stress Units

SI (N/m2)

Using the [UP] or [DOWN] buttons, select the shear stress (S.S.) units, SI (N/m
(dyne/cm

2

). Press [ENTER] to confirm your selection.

2

) or CGS

7

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GETTING STARTED

The temperature units selection screen will appear:

Temperature Units

Celsius

Using the [UP] or [DOWN] buttons, select the temperature units, Celsius or Fahrenheit. Press
[ENTER] to confirm your selection.

The mode selection screen will appear:

Computer mode

Using the [UP] or [DOWN] buttons, select the required mode, Printer or Computer. Press [ENTER]
to confirm your selection.

The set clock screen will appear:

Set Clock

Tuesday (day)
15-11-05 (dd-mm-yy)
11:14:05 (hh:mm:ss)

The day of the week flashes.

Use the [UP] or [DOWN] buttons to change it, if necessary. Press [ENTER] to confirm your
selection.

The first digit of the date flashes.

Use the [UP] or [DOWN] buttons to change it, if necessary. Press [ENTER] to confirm your
selection.

And so on, until all date and time values are correct.

The presentation screen will appear for two seconds and immediately afterwards the data screen
will be displayed.

If the mode was changed (from Printer to Computer or vice versa), switch off the Viscometer and
then switch on again.

8

2.6 Fitting the spindle guard

The spindle guard supplied with your Viscometer has two
functions:

• It provides physical protection for spindle types L and R.

• It allows accurate measurements to be taken with the large
spindles (L1 and R1, R2, R3).

Use of the spindle guard with spindles other than the L1 and R1,
R2, R3 is optional.

To fit the spindle guard, attach the guard to the Viscometer head
using the knurled screw.

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GETTING STARTED

9

GETTING STARTED

2.7 Spindle types

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Spindle type Use with

L

R

TL

TR

LCP

(included with
Viscometer)

(included with
Viscometer)

(optional
accessory)

(optional
accessory)

(optional
accessory)

Elcometer 2300 RV1-L
Elcometer 2300 RV2-L

Elcometer 2300 RV1-R
Elcometer 2300 RV2-R

Elcometer 2300 RV1-L
Elcometer 2300 RV2-L

Elcometer 2300 RV1-R
Elcometer 2300 RV2-R

Elcometer 2300 RV1-L
Elcometer 2300 RV1-R
Elcometer 2300 RV2-L
Elcometer 2300 RV2-R

R1 R2 R3 R4 R5 R6 R7

Small sample volume

+

adaptor kit

Small sample volume

+

adaptor kit

Low viscosity

+

materials adaptor kit

Used for
measurement of

Low to medium
viscosity fluids

Medium to high
viscosity fluids

Small volumes of
fluid

Small volumes of
fluid

Low viscosity fluids

TR9 TR10 TR11TR8

L1 L2 L3 L4

See “Spindle selection tables” on page 19 for further details

10

TL5 TL6 TL7

2.8 Fitting the spindle

Note: This operation must be done very carefully to
ensure that the spindle is not bent and the motor drive
coupling or internal components are not damaged.

1. Consult “Spindle selection tables” on page 19 to identify
the correct spindle to use; the spindle type is stamped
into the spindle coupling.

2. Check that the threads and connecting surfaces of the
spindle and the motor drive coupling are clean.

3. If the spindle is of a disc type, it should be submerged
carefully in the sample to avoid bubbles forming under its
lower surface.

4. Grasp the motor drive coupling with one hand, raise it
slightly and then screw the spindle onto the coupling
gently. The screw has a left-hand thread.

5. Adjust the height of the Viscometer head until the spindle
is immersed in the sample up to the immersion point,
indicated by a groove on the spindle. Take care to avoid

knocking the sample container against the spindle during
this operation as this may damage the spindle and motor
drive coupling.

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GETTING STARTED

2.9 Caution

The Elcometer Rotary Viscometer has been manufactured with your safety in mind.
However, improper use can result in damage to the machine.

Please observe the precautions discussed in these operating instructions.

• To reduce the risk of electric shock, do not open the head of the Viscometer. There are no
user-serviceable parts inside.

• To reduce the risk of fire or electric shock, do not expose the Viscometer to rain or excess
moisture.

• The mains plug on your Viscometer may be fitted with a fuse. When replacing this fuse, ensure
a fuse of the correct rating is used.

11

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USING YOUR VISCOMETER

3 USING YOUR VISCOMETER

This section describes how to take measurements with your Viscometer. The instructions apply to
RV1 Viscometers and to RV2 Viscometers under manual operation. For additional instructions on
using RV2 Viscometers interfaced to a PC, refer to “ViscosityMaster Software” on page 30.

3.1 Before you start

1. Attach the spindle guard (if necessary) - See “Fitting the spindle guard” on page 9.

2. Attach the spindle - See “Fitting the spindle” on page 11.

3. Lower the spindle into the test sample.

4. Insert the temperature probe connector into the socket on the rear of the Viscometer head and
place the probe into the sample.

3.2 Setting spindle type and rotation speed

1. Switch on the Viscometer by pressing the power on/off switch at the rear of the Viscometer
head. A welcome message will be displayed for a period of two seconds. The contents of the
message will depend upon the model, software version and language setting:

V2-R v4.3

English

After two seconds, the data screen will be displayed, showing the latest spindle and speed
parameters used (these were stored in memory the last time the instrument was used).

rpm 60 R5
mPas
temp 20.5

o

C

range 10000 mPas

2. The spindle type flashes. Use the [UP] or [DOWN] buttons to modify the spindle type. Press
[ENTER] to confirm your selection.

The rotation speed (rpm) flashes. Use the [UP] or [DOWN] buttons to modify the rotation
speed. Press [ENTER] to confirm your selection.

The parameter ‘range’ indicates the maximum viscosity value which can be measured using
the selected combination of spindle and rotation speed.

The message ‘press start’ will flash on the fourth line of the display, indicating that the
Viscometer is now ready to be started.

rpm 60 R5
mPas
temp 20.5

o

C

Press start

12

USING YOUR VISCOMETER

3.3 Starting a measurement

1. Press [START] to start the measurement.

Stable flow conditions are reached quickly and the viscosity readings on the display of the
Viscometer can be considered correct within a few seconds (depending on the selected speed
and the viscosity of the sample).

If the viscosity reading exceeds the optimum measuring range (<10% and >90% of selected
full scale), the instrument will give a warning beep.

The message ‘ERROR’ appearing on the screen indicates that the maximum viscosity value
has been exceeded. In this case, the speed should be reduced or a higher range spindle
should be used.

2. When you are satisfied that the reading is stable, press [STOP] to stop the motor. The motor
will slow down smoothly until 0 rpm is reached; this protects the delicate parts of the
instrument.

The last viscosity reading will be retained on the display.

rpm 60 R5
mPas 5080 50.8%
temp 20.5
range 10000 mPas

On pressing [START] again, the Viscometer will restart at the preset speed.

If you are using an RV2 Viscometer

The information shown on the display of an RV2 Viscometer is identical to that shown on an RV1
Viscometer unless the optional accessories are being used.

If the Adaptor for Small Sample Volumes or the Adaptor for Low Viscosity Materials is being used,
the bottom two lines of the display will show the Shear Rate (S.R.) and the Shear Stress (S.S.).

o

C

R

rpm 60 LCP
mPas 4.05 40.9%
1/sec 73.38 20.5

o

C

N/m2 3.12

Changing spindle rotation speed and spindle type

To modify the spindle rotation speed and spindle type, while the motor is running, press [ENTER]
to return to the data screen.

3.4 Viscosity measurement problems

Unstable viscosity readings may be caused by changes in the temperature of the sample or by the
behaviour of the product itself.

If the readings obtained are not stable, the temperature of the sample should be controlled and
stabilised. If the readings remain unstable once the temperature has been controlled, the instability
is due to the interaction between the product sample and the movement of the spindle.

In this instance, the product is called ‘Non-Newtonian’ and the behaviour of the product can be
described as thixotropic, rheopexy, dilatant, pseudoplastic, etc. The same settings (spindle, speed

13

R

PRINTING TEST RESULTS

and temperature) should always be used to test this type of product and additional parameters
should be recorded such as the time elapsed before first measurement, sampling interval, etc.

3.5 After use

Clean the instrument and spindle.

Always remove the spindle from the instrument before cleaning. The spindle or motor
coupling will almost certainly be damaged if attempts are made to clean the spindle while it
is still attached to the instrument.

Do not use very aggressive solvents or wire brushes, metal scrapers, metal files or other
metallic tools. Do not use excessive force which might otherwise bend delicate spindles.

Clean the spindle and other parts using a suitable solvent only.

After cleaning and before storing the instrument ensure that all materials are removed and
that the instrument is dry.

4 PRINTING TEST RESULTS

Test results from your Viscometer can be printed using two methods:

• ViscosityMaster software

• Printing Mode

Use of ViscosityMaster software provides the greatest flexibility and allows for printing, storage
and graphical analysis of test results. Full instructions for ViscosityMaster can be found in
“ViscosityMaster Software” on page 30.

Printing Mode provides a quick and easy way to print
individual test results. Connect your Viscometer to a
suitable printer (see “Thermal printer” on page 29), press
the START button and the test results will be printed.

To use Printing Mode:

1. Switch on your Viscometer and set it to Printing
Mode - see “Configuring your Viscometer” on page 7.

2. Connect your Viscometer to the printer using a
null-modem

3. Whenever the START button is pressed the test
results will be sent to the printer.

Note: When Printing Mode is OFF, switch off your printer - otherwise a continuous stream of test
results will be printed.

b

cable.

b. Null-modem pin connections:

9 pin connector

(male)

Pin 7

Pin 2

Pin 3

(ground)

14

25 pin connector

(male)

Pin 5

Pin 3

Pin 2

USING THE OPTIONAL ACCESSORIES

5 USING THE OPTIONAL ACCESSORIES

A number of optional accessories are available which will extend the capabilities of your
Viscometer. For ordering information, See “Spare parts and accessories” on page 28

5.1 Adaptor for small sample volumes

The adaptor for small sample volumes allows precise
measurement of the viscosity of small sample volumes
(8 ml to 13 ml). The adaptor is suitable for use with all
models of the Elcometer Rotary Viscometer.

There are two types of this adaptor:

• without an integrated temperature sensor

• with an integrated temperature sensor

Although the following instructions describe the version
which does not have an integrated temperature sensor,
they may also be used for the version which does have a
temperature sensor as it is very similar in design.

The adaptor consists of a water jacket, sample chamber
and a mounting bracket. Special spindles types TL or TR
are used with this adaptor.

Water from an external heating bath is circulated through
the jacket surrounding the sample chamber; this allows the
sample to be maintained precisely at a set temperature of

-10°C to 100°C (14°F to (212°F).

See also “Small volume samples adaptor kit” on page 28.

Viscosity range

Version L: 3 mPa•s to 200 000 mPa•s

Version R: 40 mPa•s to 3 300 000 mPa•s

Using the adaptor

1. Attach the appropriate spindle to the Viscometer motor drive coupling using the screwed
coupling and mounting hook.

2. Attach one end of the mounting bracket to the water jacket, as shown; note the locating pin
which allows the bracket to be attached the correct way only.

3. Slide the water jacket slowly and carefully over the spindle and then attach the other end of the
bracket to the head of your Viscometer.

4. Fit the end cap to the bottom of the stainless steel sample chamber.

5. Fill the sample chamber with a suitable volume of the fluid to be tested; 8 ml to 13 ml (0.27 oz
to 0.44 oz) - depending upon spindle.

6. Slide the sample chamber up into the water jacket and rotate to lock into position.

7. Fit the cover around the spindle hook and lower it onto the top of the sample chamber.

8. Connect the external heating bath to the water jacket inlet and outlet and then leave it
operating for a sufficient amount of time for the temperature of the sample to stabilise.

The adaptor for small sample volumes is now ready to use.

R

15

R

USING THE OPTIONAL ACCESSORIES

5.2 Adaptor for low viscosity samples

The adaptor for low viscosity samples allows precise
measurement of the viscosity of low viscosity samples
(16 ml to 18 ml), both Newtonian and non Newtonian. The
adaptor is suitable for use with all models of the Elcometer
Rotary Viscometer.

There are two types of this adaptor:

• with water jacket - for indirect heating up to 100°C
(212°F)

• without water jacket - for sample temperatures up to
200°C (392°F)

Although the following instructions describe the version
which has a water jacket, they may also be used for the
unheated version which is very similar in design.

The adaptor consists of a water jacket, sample chamber, a
mounting bracket, a column extension piece and a special
cylindrical spindle (LCP).

Water from an external heating bath is circulated through
the jacket surrounding the sample chamber; this allows the
sample to be maintained precisely at a set temperature of

-10°C to 100°C (14°F to (212°F).

For ordering information see “Low viscosity adaptor kit ­with water jacket” on page 28 and “Low viscosity adaptor kit

- without water jacket” on page 28.

Viscosity range

Version L: 0.5 mPa•s to 2000 mPa•s

Version R: 4.8 mPa•s to 21 333 mPa•s

Using the adaptor

1. Fit the extension piece to the column. This raises the Viscometer head sufficiently to allow the
adaptor for low viscosity samples to be used correctly.

2. Attach the LCP spindle to the Viscometer motor drive coupling using the screwed coupling and
mounting hook.

3. Attach one end of the mounting bracket to the water jacket, as shown; note the locating pin
which allows the bracket to be attached the correct way only.

4. Slide the water jacket slowly and carefully over the spindle and then attach the other end of the
bracket to the head of your Viscometer.

5. Fit the end cap to the bottom of the stainless steel sample chamber.

6. Fill the sample chamber with a suitable volume of the fluid to be tested; 16 ml to 18 ml (0.54 oz
to 0.61 oz).

7. Slide the sample chamber up into the water jacket and rotate to lock into position.

8. Fit the cover around the spindle hook and lower it onto the top of the sample chamber.

9. Connect the external heating bath to the water jacket inlet and outlet and then leave it
operating for a sufficient amount of time for the temperature of the sample to stabilise.

The adaptor for low viscosity samples is now ready to use.

16

USING THE OPTIONAL ACCESSORIES

5.3 Adaptor for helical movement

The adaptor for helical movement allows precise
measurement of the viscosity of samples such as
cream, gel, wax, paste, putty, gelatine, etc. The
adaptor is suitable for use with all models of the
Elcometer Rotary Viscometer.

The adaptor moves the Viscometer head slowly up
and down. This movement causes the spindle to
trace a helical path through the sample, therefore
avoiding the creation of voids in the sample which
would otherwise make measurement impossible.

The adaptor consists of:

• drive mechanism with head mounting bracket
and mains lead

• spindle clamp/coupling and weight

• spacer tube

• ring clamp, x 2

• set of P series spindles

water jacket, sample chamber, a mounting
bracket, a column extension piece and a special
cylindrical spindle (LCP).

The adaptor is used with special T-type spindles ­PA, PB, PC, PD, PE, PF

See also “Helical movement adaptor kit” on
page 29.

Viscosity range

Version L: 156 mPa•s to 3 120 000 mPa•s

Version R: 1660 mPa•s to 33 300 000 mPa•s

Using the adaptor

1. Remove the standard head mounting bracket from the column.

2. Slide the spacer tube (A) onto the column until it rests on the base.

3. Slide one of the ring clamps (B) onto the column.

4. Press and hold lever (C) of the drive mechanism upwards and slide the drive mechanism (D)
onto the column. Release lever (C) to engage the drive mechanism with the column.

R

17

R

USING THE OPTIONAL ACCESSORIES

5. Slide the second ring clamp onto the
column.

6. Insert the rod of the Viscometer head
through the hole in the mounting
bracket on the drive mechanism and
rotate the mounting bracket lever to lock
the Viscometer head in position.

7. Screw the weight onto the spindle
clamp/coupling.

8. Select the appropriate spindle (See “P
series spindles” on page 24) and insert
it into the spindle clamp/coupling. Twist
the body of the clamp to lock the spindle
in position.

9. Attach the spindle clamp/coupling to the
Viscometer motor drive coupling - See
“Fitting the spindle” on page 11.

10. Adjust the position of the two ring
clamps to give the desired amount of
vertical movement and clamp into
position.

The adaptor for helical movement is now
ready to use. Connect to the mains supply
and press the power on/off switch to switch it
on.

D

C

B

A

18

SPINDLE SELECTION TABLES

6 SPINDLE SELECTION TABLES

6.1 L and TL Spindles (For use with RV1-L / RV2-L Viscometers).

R

Table 1: Spindle type L

Spindle
speed (rpm)

Maximum

L1

a

b

measurable viscosity (mPa•s)

c

L2 L3 L4

0.3 20 000 100 000 400 000 2 000 000

0.5 12 000 60 000 240 000 1 200 000

0.6 10 000 50 000 200 000 1 000 000
1 6000 30 000 120 000 600 000

1.5 4000 20 000 80 000 400 000
2 3000 15 000 60 000 300 000

2.5 2400 12 000 48 000 240 000
3 2000 10 000 40 000 200 000
4 1500 7500 30 000 150 000
5 1200 6000 24 000 120 000

6 1000 5000 20 000 100 000
10 600 3000 12 000 60 000
12 500 2500 10 000 50 000
20 300 1500 6000 30 000
30 200 1000 4000 20 000
50 120 600 2400 12 000
60 100 500 2000 10 000

100 60 300 1200 6000
200 30 150 600 3000

Resolution 1 mPa•s 1 mPa•s 10 mPa•s 10 mPa•s

a. Type L spindles are the standard spindles supplied with RV1-L/RV2-L Viscometers.

b. The minimum recommended reading is 15% of the full scale value.
c. The L1 spindle is used for low viscosity measurement. The spindle guard must be used with this spindle in

order to obtain correct viscosity readings. For higher accuracy when measuring low viscosity samples, use
the Adaptor for Low Viscosity Materials and the special cylindrical spindle (LCP); See “Spare parts and
accessories” on page 28.

19

R

SPINDLE SELECTION TABLES

Table 2: Spindle type TL

a

Spindle
speed (rpm)

Maximum

b

measurable viscosity (mPa•s)

TL5

c

TL6

d

TL7

e

0.3 10 000 100 000 200 000

0.5 6000 60 000 120 000

0.6 5000 50 000 100 000
1 3000 30 000 60 000

1.5 2000 20 000 40 000
2 1500 15 000 30 000

2.5 1200 12 000 24 000
3 1000 10 000 20 000
4 750 7500 15 000
5 600 6000 12 000

6 500 5000 10 000
10 300 3000 6000
12 250 2500 5000
20 150 1500 3000
30 100 1000 2000
50 60 600 1200
60 50 500 1000

100 30 300 600
200 15 150 300

Resolution 0.1 mPa•s 1 mPa•s 10 mPa•s

a. Type TL spindles are the optional spindles for use with the Adaptor for Small Sample Volumes; See “Spare

parts and accessories” on page 28.

b. The minimum recommended reading is 15% of the full scale value.
c. TL5 shear rate: 1.32 x rpm with sample volume of 8.0 cm³
d. TL6 shear rate: 0.34 x rpm with sample volume of 10.0 cm³
e. TL7 shear rate: 0.28 x rpm with sample volume of 9.5 cm³

20

SPINDLE SELECTION TABLES

6.2 R and TR Spindles (For use with RV1-R / RV2-R Viscometers)

R

Table 3: Spindle type R

Spindle
speed
(rpm)

R1

a

Maximum

c

R2 R3 R4 R5 R6 R7

b

measurable viscosity (mPa•s)

0.3 33 300 133 300 333 300 666 600 1 300 000 3 330 000 13 300 000

0.5 20 000 80 000 200 000 400 000 800 000 2 000 000 8 000 000

0.6 16 600 66 600 166 600 333 300 666 600 1 600 000 6 600 000
1 10 000 40 000 100 000 200 000 400 000 1 000 000 4 000 000

1.5 6600 26 600 66 600 133 300 266 600 666 600 2 600 000
2 5000 20 000 50 000 100 000 200 000 500 000 2 000 000

2.5 4000 16 000 40 000 80 000 160 000 400 000 1 600 000
3 3300 13 300 33 300 66 600 133 300 333 300 1 300 000
4 2500 10 000 25 000 50 000 100 000 250 000 1 000 000
5 2000 8000 20 000 40 000 80 000 200 000 800 000

6 1600 6600 16 600 33 300 66 600 166 600 666 000
10 1000 4000 10 000 20 000 40 000 100 000 400 000
12 833 3300 8300 16 600 33 300 83 300 333 300
20 500 2000 5000 10 000 20 000 50 000 200 000
30 333 1300 3300 6600 13 300 33 300 133 300
50 200 800 2000 4000 8000 20 000 80 000
60 166 660 1600 3300 6600 16 600 66 600

100 100 400 1000 2000 4000 10 000 40 000
200 50 200 500 1000 2000 5000 20 000

Resolution 1 mPa•s 1 mPa•s 10 mPa•s 10 mPa•s 10 mPa•s 100 mPa•s 100 mPa•s

a. Type R spindles are standard spindles supplied with RV1-R/RV2-R Viscometers.

b. The minimum recommended reading is 15% of the full scale value.
c. Spindle R1 is used for measurement of samples having low viscosity. The spindle guard must be used with

this spindle in order to obtain correct viscosity readings. Because models RV1-R and RV2-R are normally
used for medium viscosity ranges, the spindle R1 is not very frequently used, therefore is not supplied as
standard equipment with your Viscometer. However, it is available on request; See “Spare parts and acces­sories” on page 28.

21

R

SPINDLE SELECTION TABLES

Table 4: Spindle type TR

a

Spindle
speed (rpm)

TR8

Maximum

c

b

measurable viscosity (mPa•s)

TR9

d

TR10

e

TR11

f

0.3 166 600 833 300 1 600 000 3 300 000

0.5 100 000 500 000 1 000 000 2 000 000

0.6 83 300 416 600 833 300 1 600 000
1 50 000 250 000 500 000 100 000

1.5 33 300 166 600 333 300 666 600
2 25 000 125 000 250 000 500 000

2.5 20 000 100 000 200 000 400 000
3 16 600 83 300 166 600 333 300
4 12 500 62 500 125 000 250 000
5 10 000 50 000 100 000 200 000

6 8300 41 600 83 300 166 600
10 5000 25 000 50 000 100 000
12 4160 20 830 41 600 83 300
20 2500 12 500 25 000 50 000
30 1600 8300 16 600 33 300
50 1000 5000 10 000 20 000
60 830 4160 8300 16 600

100 500 2500 5000 10 000
200 250 1250 2500 5000

Resolution 10 mPa•s 100 mPa•s 100 mPa•s 100 mPa•s

a. Type TR spindles are the optional spindles for use with the Adaptor for Small Sample Volumes; See “Spare

parts and accessories” on page 28.

b. The minimum recommended reading is 15% of the full scale value.
c. TR8 shear rate: 0.93 x rpm with sample volume of 8.0 cm³
d. TR9 shear rate: 0.34 x rpm with sample volume of 10.5 cm³
e. TR10 shear rate: 0.28 x rpm with sample volume of 11.5 cm³
f. TR11 shear rate: 0.25 x rpm with sample volume of 13.0 cm³

The Shear Rate (S.R.) has been calculated assuming the characteristics of newtonian products.

22

6.3 LCP Spindle

R

SPINDLE SELECTION TABLES

Table 5: Spindle type LCP

Spindle
speed (rpm)

Maximum

a

b

measurable

viscosity (mPa•s)

RV1-L / RV2-L RV1-R / RV2-R

0.3 2000 21 333

0.5 1200 12 800

0.6 1000 10 666
1 600 6400

1.5 400 4266
2 300 3200

2.5 240 2560
3 200 2133
4 150 1600
5 120 1280

6 100 1066
10 60 640
12 50 533
20 30 320
30 20 213
50 12 128
60 10 106

100 6 64
200 3 32

Resolution 0.01 mPa•s 0.16 mPa•s

a. Type LCP spindle is supplied as part of the Adaptor for Low Viscosity Materials kit of parts; See “Spare parts

and accessories” on page 28.

b. The minimum recommended reading is 15% of the full scale value.

Volume of sample container = 18 ml (0.61 oz)

Shear Rate (S.R.) = 1.224 x rpm

23

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SPINDLE SELECTION TABLES

6.4 P series spindles

Table 6: P series spindles for RV1-L and RV2-L Viscometers

a

Spindle
speed
(rpm)

Maximum

PA PB PC PD PE PF

b

measurable viscosity (mPa•s)

0.3 62 400 124 800 312 000 624 000 1 560 000 3 120 000

0.5 37 440 74 880 187 200 374 400 936 000 1 872 000

0.6 31 200 62 400 156 000 312 000 780 000 1 000 000
1 18 720 37 440 93 600 187 200 468 000 936 000

1.5 12 480 24 960 62 400 124 800 312 000 624 000
2 9360 18 720 46 800 93 600 234 000 468 000

2.5 7488 14 976 37 440 74 880 187 200 374 400
3 6240 12 480 31 200 62 400 156 000 312 000
4 4680 9360 23 400 46 800 117 000 234 000
5 3744 7488 18 720 37 440 93 600 187 200

6 3120 6240 15 600 31 200 78 000 156 000
10 1872 3744 9360 18 720 46 800 93 600
12 1560 3120 7800 15 600 39 000 78 000

Resolution 1 mPa•s 1 mPa•s 2 mPa•s 4 mPa•s 8 mPa•s 16 mPa•s

a. Type P series spindles are the optional spindles for use with the Adaptor for Helical Movement - See “Spare

parts and accessories” on page 28.

b. The minimum recommended reading is 15% of the full scale value.

Table 7: P series spindles for RV1-R and RV2-R Viscometers

Spindle
speed
(rpm)

Maximum

PA PB PC PD PE PF

b

measurable viscosity (mPa•s)

a

0.3 666 600 1 300 000 3 300 000 6 600 000 16 600 000 33 300 000

0.5 400 000 800 000 2 000 000 4 000 000 10 000 000 20 000 000

0.6 333 300 666 600 1 600 000 3 300 000 8 300 000 16 600 000

1 200 000 400 000 1 000 000 2 000 000 5 000 000 10 000 000

1.5 133 300 266 600 666 600 1 300 000 3 300 000 6 600 000

2 100 000 200 000 500 000 1 000 000 2 500 000 5 000 000

2.5 80 000 160 000 400 000 800 000 2 000 000 4 000 000

3 66 600 133 300 333 300 666 600 1 600 000 3 300 000

4 50 000 100 000 250 000 500 000 1 250 000 2 500 000

5 40 000 80 000 200 000 400 000 1 000 000 2 000 000

6 33 300 66 600 166 600 333 300 833 300 1 600 000
10 20 000 40 000 100 000 200 000 500 000 1 000 000
12 16 600 33 300 83 300 166 600 416 600 833 200

Resolution 5 mPa•s 10 mPa•s 25 mPa•s 50 mPa•s 125 mPa•s 250 mPa•s

a. Type P series spindles are the optional spindles for use with the Adaptor for Helical Movement - See “Spare

parts and accessories” on page 28.

b. The minimum recommended reading is 15% of the full scale value.

24

CALIBRATION

7 CALIBRATION

Your Viscometer was calibrated at the factory before shipment and a calibration certificate was
included in the box. Additional calibration checks at regular intervals over the life of the Viscometer
are a requirement of quality management procedures, e.g. ISO 9000, and other similar standards.

Calibration checks may be carried out by the user of the Viscometer (see instructions below),
however if the calibration of the Viscometer is found to need adjustment, please contact Elcometer
or your local Elcometer supplier.

Checking Viscometer calibration

The following calibration checking procedure requires the use of the Adaptor for low viscosity
samples - See “Spare parts and accessories” on page 28.

Use of this adaptor helps to eliminate fluctuations in the temperature of the sample and variations
due to differences in the sample container.

It is recommended that calibrated viscosity oil is used for checking calibration. Oils between
100 mPa•s to 125 mPa•s for version R and 5 mPa•s for version L should be adequate for the
calibration procedure.

1. Fit the adaptor for low viscosity samples and fill with the recommended volume of calibration
oil - See “Adaptor for low viscosity samples” on page 16.

2. Switch on and start the Viscometer; begin with viscosity readings at the highest speed
permitted by the combination of speed/spindle (taking into account the nominal viscosity and
temperature values of the calibration oil).

3. Once the desired sample temperature has been reached, check the viscosity reading on the
display. If the reading is identical to the nominal viscosity of the calibration oil, your Viscometer
is calibrated correctly.

R

8 MAINTENANCE

The Elcometer Rotary Viscometer is designed to give many years reliable service under normal
operating and storage conditions.

The Elcometer Rotary Viscometer does not contain any internal user-serviceable components. In
the unlikely event of a fault, the instrument should be returned to your local Elcometer supplier or
directly to Elcometer.

Details of Elcometer offices around the world are given on the outside cover of these Operating
Instructions. Alternatively visit the Elcometer website, www.elcometer.com

25

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TROUBLESHOOTING

9 TROUBLESHOOTING

The instrument does not operate

Check:

• the connection to the mains electricity supply

• the power on/off switch position at the rear of the Viscometer head

The spindle does not rotate concentrically

Check:

• that the spindle is correctly adjusted to the shaft

• that the union between spindle and shaft is clean

The instrument does not read zero in vacuum

Check:

• that the instrument is levelled correctly

Viscosity reading is not stable or not very accurate

Check:

• that the instrument is levelled correctly

• that the rotation speed/spindle type selection is correct

• that the temperature of the sample is stable

Viscometer head slips down the column

• tighten the two nylon grub screws on the head mounting bracket using the hexagonal wrench
supplied

26

TECHNICAL SPECIFICATION

10 TECHNICAL SPECIFICATION

Room temperature: 10°C to 40°C (50°F to 104°F)

Relative humidity: < 80%

R

Speeds: 0.3, 0.5, 0.6, 1, 1.5, 2, 2.5, 3, 4, 5, 6, 10,

12, 20, 30, 50, 60, 100, 200 rpm

Accuracy (speed): > 0.5% of the absolute value

Viscosity range, Version L: 3 mPa•s to 2 000 000 mPa•s in 76 ranges

19 speeds with 4 spindles.
(For low to medium viscosity test fluids)

Version R: 20 mPa•s to 13 000 000 mPa•s in 114 ranges

19 speeds with 6 spindles.
(For medium to high viscosity test fluids)

Accuracy (measurement): ± 1% of full scale

Repeatability: ± 0.2%

Maximum altitude: 2 000 m (6500 ft) above sea level

Surge class: Class II (domestic/light industry)

Contamination: Level 2

Thermometer, Range: -15°C to +180°C (5°F to 356°F)

Resolution: 0.1°C (0.1°F)

Accuracy: ± 0.1°C (0.18°F)

Operating voltage: UK, 240 V AC 50 Hz

EUR, 220 V AC 50 Hz
US, 110 V AC 60 Hz

Power consumption: 23 W

Dimensions (of carry case): 495 mm x 420 mm x 200 mm

(19.5" x 16.5" x 8")

Weight (including carry case): 9 kg (20 lb)

27

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SPARE PARTS AND ACCESSORIES

11 SPARE PARTS AND ACCESSORIES

The following spare parts and accessories for your Elcometer Rotary Viscometer are available from
your local supplier or direct from Elcometer:

11.1 Standard spindles

Spindle set, standard, type L (L1 to L4) KT00230019698

Spindle set, standard, type R (R2 to R7) KT00230019699

Spindle, R1 KT00230019700

11.2 Low viscosity adaptor kit - with water jacket

Adaptor kit for low viscosity samples, with water jacket KT00230019710

Adaptor kit for low viscosity samples, with water jacket,
plus integrated temperature sensor KT00230020174
(indirect heating by water up to 100°C)

(This adaptor kit is
supplied complete
with LCP cylindrical
spindle for low
viscosity samples)

11.3 Low viscosity adaptor kit - without water jacket

Adaptor kit for low viscosity samples, without water jacket KT00230019711
(for testing of samples up to 200°C)

(This adaptor kit is
supplied complete
with LCP cylindrical
spindle for low
viscosity samples)

(Comes complete with LCP cylindrical spindle for low viscosity samples)

11.4 Small volume samples adaptor kit

Adaptor kit for small volume samples KT00230019702

Adaptor kit for small volume samples + integrated temperature sensor KT00230019784

(This adaptor kit requires a
spindle set for small volume
samples - see below)

Spindle set, small volume samples, (TL5, TL6 and TL7) KT00230019703

Spindle set, small volume samples, (TR8, TR9, TR10 and TR11) KT00230019704

28

RELATED EQUIPMENT

11.5 Helical movement adaptor kit

Helical movement adaptor, 240 V (UK) KT00230019705

220 V (EU) KT00230019706
110 V (USA) KT00230019707

(This adaptor kit is supplied
complete with six special T-type
spindles - PA, PB, PC, PD, PE,
PF)

11.6 Thermal printer

Thermal printer, null modem cable + adaptor 240 V (UK) KT00230020179

220 V (EU) KT00230020178
110 V (USA) KT00230020180

R

12 RELATED EQUIPMENT

In addition to the Elcometer Rotary Viscometer, Elcometer produces a wide range of other
equipment for determining the physical characteristics of surface coatings.

Users of the Elcometer 2300 may also benefit from the following Elcometer products:

• Elcometer 2000 Muller Laboratory Grinder

• Elcometer Fineness of Grind Gauges

• Elcometer Viscosity Cups

• Elcometer Film Applicators

For further information contact Elcometer, your local supplier or visit www.elcometer.com

29

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ABOUT VISCOSITYMASTER

SECTION B: VISCOSITYMASTER SOFTWARE

13 ABOUT VISCOSITYMASTER

ViscosityMaster is powerful but easy-to-use software which simplifies and enhances the use of your
Viscometer:

• Design test processes on your PC and upload
Viscometer.

• Download readings data from your Viscometer to the ViscosityMaster data management
system.

• Keep your test notes, reports, photographs and all your other test information in one place ­ViscosityMaster.

• Create accurate and professional reports configured to allow your data to be understood easily
at all levels.

• Create PDF versions of your reports and e-mail direct from ViscosityMaster.

13.1 System Requirements

To use the software on this CD you will need an Elcometer 2300 Rotational Viscometer, a computer
and a data transfer cable.

The software will run on PC compatible computers under Windows
XP. The software will not run on Mac OS.

A data transfer cable to connect your Viscometer to the PC is required. This cable is supplied as
standard equipment with Elcometer 2300 RV2 Rotational Viscometer. Spare cables are available
as an accessory; contact Elcometer or your local supplier for ordering details.

a

them to your Elcometer 2300 RV2 Rotational

®

98, 98SE, 2000, ME, NT and

14 GETTING STARTED

This section of the instructions is intended for first-time users of ViscosityMaster. It describes the
steps you must take before you can start using the software, how to customise your working
environment and where to get help.

14.1 Installing ViscosityMaster

To install ViscosityMaster software on your PC:

1. Place the CD in the CD drive of your PC. The software installation wizard should run
automatically. If it does not run automatically:

• Choose Start > Run

• Type D:ViscosityMasterSetup (where ‘D’ is the letter of your CD drive)

• Click OK. The software installation wizard will run.

2. Follow the on-screen installation instructions.

a. Uploading of test processes to Elcometer 2300 RV1 models is not possible.

30

GETTING STARTED

14.2 Uninstalling ViscosityMaster

To uninstall the software follow the usual Windows procedure for removing programs. For Windows
XP:

• Choose Start > Control Panel > Add or Remove Programs > ViscosityMaster 1.xx > Remove

14.3 Starting ViscosityMaster

Start ViscosityMaster just as you would any software application:

• Choose Start > Programs > ViscosityMaster > ViscosityMaster

14.4 Connecting your Viscometer

You must connect the Viscometer to your computer if you want to transfer information to and from
your Viscometer

To connect your Viscometer:

1. Plug the 9-pin female D-type connector on one end of the data transfer cable into the COM

port

2. Plug the 9-pin connector on the other end of the data transfer cable into the RS232 connector
at the rear of the Viscometer.

3. Switch on the Viscometer.

b

c

on the PC.

.

14.5 Preferences

Use this menu to customise your ViscosityMaster working environment. Choose between metric
and imperial units of measurement, quality of report page thumbnails and whether e-mail report

R

b. If your Viscometer is not connected to your computer, you can still use ViscosityMaster to create batch

templates, view data downloaded previously and produce reports.

c. An RS232 to USB transfer cable is available which allows you to connect your Viscometer to a USB port on

your computer; part number T99916716. Contact Elcometer or your local supplier for ordering details.

31

R

GETTING STARTED

format is PDF or JPEG image. Also set default values for Viscometer model, spindle type, company
and operator and which COM port your Elcometer 2300 Rotational Viscometer is connected to.

14.6 Help

Help for your ViscosityMaster software is provided by this help file. A PDF version of this help file is
included on the ViscosityMaster installation CD. If you need to print any sections of this help file,
print from the PDF version as this will give a better quality document.

If you need help with your Elcometer 2300 Rotational Viscometer, refer to the operating instructions
which were included with your Viscometer.

If you cannot find the answer to your question, please do not hesitate to contact Elcometer
or your Elcometer supplier.

32

THE USER INTERFACE

15 THE USER INTERFACE

The ViscosityMaster user interface is very similar to a standard Windows Explorer interface:

1. Toolbar: New, cut, copy, delete, auto, manual, stop, export, etc.

2. Explorer Window: Lists the files and folders on your PC and on your Viscometer. All data is
stored in \My Documents\My ViscoMeter Data.

3. List Window: Lists the files in a folder or the files on your Viscometer.

4. Report Window: Displays the contents of a file (click on to maximise/minimise the
window).

Many menu commands and actions can be accessed by clicking using the right mouse button in
one of the user interface windows; experiment as you use ViscosityMaster to find which method of
working (buttons or right click) you find most comfortable.

R

33

R

EXAMPLE DATA

16 EXAMPLE DATA

When you install Elcometer ViscosityMaster software, a set of example data is loaded into your local
folder; click on ‘Viscometer Data’ in the Explorer Window and then look for ‘Example Batch’ in the
List Window.

Double click on Example Batch to load the data into the Report Window and spend some time
looking at the readings and charts - you will soon learn the basics of ViscosityMaster and what it
can do.

Deleting the example data (when you have finished learning about ViscosityMaster, for example)
will not affect the operation of your ViscosityMaster software.

34

OPERATING MODES

17 OPERATING MODES

Your ViscosityMaster software has two operating modes; manual and automatic.

•In manual mode your ViscosityMaster software records measurements as they are taken by
the instrument but it does not control the operation of the Viscometer.

•In automatic mode your ViscosityMaster software records measurements and it controls the
operation of the Viscometer.

Note: RV1 models can only be used in manual mode. RV2 models can be used in Manual mode
and in Automatic mode.

18 INSTRUCTIONS FOR RV1 VISCOMETERS

Note: RV1 Viscometers can only be used in manual mode - they cannot be used in automatic mode.

18.1 Setting up a batch

1. Click on ‘New’ and select ‘New Batch’.

2. Type a name for the batch and then press the Return key.

R

35

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INSTRUCTIONS FOR RV1 VISCOMETERS

3. The Model, Spindle type, Company and Operator will already be set from ‘Preferences’ when
ViscosityMaster was run for the first time. If necessary, amend these details as required.

4. Enter details in the Identifier and Notes fields. This information is used later, typically within
test reports.

36

INSTRUCTIONS FOR RV2 VISCOMETERS

18.2 Running a batch

1. Lower the Viscometer spindle into the test sample.

2. Click on ‘Manual’ and then press ‘Start’ on the Viscometer.

3. The measurements and charts will be shown in real time.

R

4. If necessary, adjust the content of the chart X and Y axes to show the information you require.

5. Click on ‘Stop’ when you have obtained enough measurements.

6. Review the measurements/charts. If you are not happy with the results, click on ‘Clear’ to clear
the measurements and start the test again.

After you have stopped the test you can:

• review readings

• review charts

• create reports

• export readings to Excel or csv files

• print, create pdf or email charts and reports.

See “Working with Viscometer data” on page 41 for further details.

19 INSTRUCTIONS FOR RV2 VISCOMETERS

Note: The instructions in this section apply to RV2 models only - RV1 models can only be used in

manual mode.

19.1 Setting up a batch

The first section of the procedure is identical to the instructions given for operation in manual mode:

1. Click on ‘New’ and select ‘New Batch’.

37

R

INSTRUCTIONS FOR RV2 VISCOMETERS

2. Type a name for the batch and then press the Return key.

3. The Model, Spindle type, Company and Operator will already be set from ‘Preferences’ when
ViscosityMaster was run for the first time. If necessary, amend these details as required.

4. Enter details in the Identifier and Notes fields. This information is used later, typically within
test reports.

The procedure for automatic mode now differs from the procedure for manual mode because of
‘Processes’ - see Setting up processes .

38

INSTRUCTIONS FOR RV2 VISCOMETERS

19.2 Setting up processes

In automatic mode the Viscometer is controlled using processes. Processes are groups of data
which specify settings such as spindle speed, rotation duration, measurement frequency, etc.

A single batch can incorporate any number of processes.

1. Click on the ‘Processes’ tab.

2. Click on ‘New Process’.

A Process Wizard will start. Follow the instructions given in the wizard to create a single
process. You will be asked to define the following process variables:

Identifier A name or number for the process

Start RPM Spindle speed at the start of the process

End RPM Spindle speed at the end of the process

Time Duration of the process (seconds)

Start delay Time delay before measurements start (seconds)

Start temperature

Measurements

Delay start until when above this temperature, or
Delay start until when below this temperature

Number of measurements to take during the
process

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3. Click on ‘Finish’ at the end of the process.

The process will appear as a line item under the ‘Processes’ tab.

4. Go on defining as many processes as you need to define the test procedure.

39

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INSTRUCTIONS FOR RV2 VISCOMETERS

19.3 Running a batch

1. Lower the Viscometer spindle into the test sample.

2. Click on ‘Automatic’.

The Viscometer will start under control of ViscosityMaster and the measurements and charts
will be shown in real time.

3. If necessary, adjust the content of the chart X and Y axes to show the information you require.

4. The Viscometer will stop automatically at the end of the test procedure. Alternatively, click on
‘Stop’ to stop the procedure at any time.

5. Review the measurements/charts. If you are not happy with the results, click on ‘Clear’ to clear
the measurements and start the test again.

After you have stopped the test you can:

• review readings

• review charts

• create reports

• export readings to Excel or csv files

• print, create pdf or email charts and reports.

See “Working with Viscometer data” on page 41 for further details.

40

WORKING WITH VISCOMETER DATA

20 WORKING WITH VISCOMETER DATA

This section describes what you can do with your Viscometer batch data once it has been
downloaded into ViscosityMaster:

• Viewing Measurement Data and Standard Reports

• Customising report window tabs

• Creating Custom Reports

• Viewing a Custom Report

• Exporting Measurement Data

• Printing, Creating PDF Files and E-mailing from ViscosityMaster

20.1 Viewing Measurement Data and Standard Reports

Viewing measurement data and producing standard reports is quick and easy using
ViscosityMaster software.

To view measurement data for a batch:

1. In the Explorer Window, navigate to the folder where your data is stored.

2. In the List Window, click on the batch or batches you want to view. To select more than one
batch, hold down the ‘Ctrl’ key and click on the batches required.

3. In the Report Window, click on the Measurements tab.

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41

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WORKING WITH VISCOMETER DATA

4. Adjust the contents of the chart using the X axis and Y axis drop down lists.

5. To zoom in to an area on the chart, use your mouse to left click and drag. To reset the zoom
click on the Reset Zoom button.
To scroll the chart, use your mouse to right click and drag

To view standard reports for a batch:

1. In the Explorer Window, navigate to the folder where your data is stored.

2. In the List Window, click on the batch or batches you want to view. To select more than one
batch, hold down the ‘Ctrl’ key and click on the batches required.

3. In the Report Window, click on the tab required: Paged Run Chart, Overview Run Chart.

4. Click on a thumbnail of a report on the left side of the Report Window to view an individual
page of the report. Use the Zoom pull-down list to adjust the size of the report on the screen.

42

WORKING WITH VISCOMETER DATA

20.2 Customising report window tabs

The Header, Measurements and My Reports tabs are always visible in the Report Window. All other
tabs (and user defined tabs) can be added or deleted:

1. In the Explorer Window, click on Reports.

2. In the List Window, all reports in the ‘Tab Reports’ column will appear as tabs in the Report
Window. Use the arrows between the two columns to add or remove reports from this column.

• All reports with a blue icon are standard reports which cannot be deleted.

• All reports with a brown icon are user defined reports which may be deleted if needed.

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20.3 Creating Custom Reports

ViscosityMaster software includes a built-in report designer which can be used to create reports
customised to your requirements.

To create a custom report:

1. In the Explorer Window, click on ‘Reports’.

2. In the Toolbar, click ‘New Report’.

3. Choose a name for your report and press ‘Return’.

43

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WORKING WITH VISCOMETER DATA

4. In the Report Window, click ‘New Page’ and then choose between ‘Opening’, ‘Inner’ and
‘Closing’ page types.

• Opening pages: Typically used for report title page; can contain text, shapes and graphics;

cannot be used to display reading data; prints first when printing a report.

• Inner pages: Typically used for showing reading data (run charts, measurements); prints in

the middle when printing a report.

• Closing pages: Typically used for report notes/summary page; can contain text, shapes

and graphics; cannot be used to display reading data; prints last when printing a report.

The new page will then appear in the Report Window.

5. Click on the page in the Report Window and then click on the Edit button. The Page Designer
will start.

6. Follow the instructions in “The page designer” on page 47 to define your report.

7. Click ‘Save’ to save your report layout when you are finished.

20.4 Viewing a Custom Report

To view a custom report:

1. In the Explorer Window, navigate to the folder where your data is stored.

2. In the List Window, click on the batch or batches you want to view. To select more than one
batch, hold down the ‘Ctrl’ key and click on the batches required.

44

WORKING WITH VISCOMETER DATA

3. In the Report Window, click on My Reports tab and then select the report from the Reports
drop-down list.

4. Click on a thumbnail of a report on the left side of the Report Window to view an individual
page of the report. Use the Zoom drop-down list to adjust the size of the report on the screen.

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20.5 Exporting Measurement Data

Measurement data can be exported in Microsoft Excel format and in CSV (comma separated
values) format.

Highlight the batch required and then click on ‘Export’. Choose between Excel and CSV.

20.6 Printing, Creating PDF Files and E-mailing from ViscosityMaster

Any report currently displayed in the Report Window can be:

•Printed

• Saved as an Adobe PDF (Portable Document Format) file

45

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USING DOCUMENTS AND IMAGES

• Sent via e-mail as an attachment

Click the appropriate button in the Report Window and follow the standard Windows instructions
which follow.

d

21 USING DOCUMENTS AND IMAGES

Use ViscosityMaster to store your test notes, reports, spreadsheets and all your other test
information. Group these files by product, customer, project, production shift, etc.

To store a document, image or any other type of file, use the standard Windows techniques of ‘drag
and drop’ or ‘copy and paste’ to place your file in the List Window.

d. Select the format of your e-mail attachment (PDF file or JPEG image) in Preferences .

46

THE PAGE DESIGNER

22 THE PAGE DESIGNER

This section describes how to use the Page Designer - a utility built in to ViscosityMaster which
allows you to create your reports:

• Designing a Page

• The Property Editor

• The Text Editor

R

1. Object Picker Window

2. Toolbar

3. Object Selector Window

4. Property Editor

5. Page Layout Window

47

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THE PAGE DESIGNER

22.1 Designing a Page

The contents of a page are ‘Objects’ such as shapes, memos, readings, etc. To add an object to
the page, choose the object in the Object Picker Window (1), move the cursor to the Page Layout
Window (5) and then click and drag the object to the required size. Once the object has been
created it can be moved by dragging, and resized by dragging on the handles around the edge of
the object.

Precise control over the layout, attributes and content of an object is obtained by modifying the
properties of the object in the The Property Editor (4).

When an object is added to the page, the name of the object appears in the Object Selector Window
(3).

The buttons on the Toolbar (2) Zoom, Save, Delete, Cut, Copy and Paste using standard Windows
techniques.

48

THE PAGE DESIGNER

22.2 The Property Editor

Precise control over the layout, attributes and content of an object is obtained by modifying the
properties of the object using the Property Editor.

Object properties which are adjustable using the Property Editor are listed below. The list of
properties available depends upon the type of object selected (shape, memo, graphic, overview
chart, etc.):

Property Description

3D:

Alignment:

Anchor:

AspectRatio: Defines how a graphic fits within its bounding box.

Bold: Make text in a memo block bold.

ColumnWidthDate: In measurements object - Width of date column (mm)

ColumnWidthPercentFS:

ColumnWidthRPM: In measurements object - Width of RPM column

ColumnWidthSheerRate: In measurements object - Width of Sheer rate column

ColumnWidthSheerStress:

ColumnWidthTemperature:

ColumnWidthTime: In measurements object - Width of Time column

ColumnWidthViscosity: In measurements object - Width of Viscosity column

FillColor: Fill colour of shapes.

FillStyle:

FontColour: Colour of text in a memo block.

FontName: Defines font type (Arial, Times, etc.)

FontSize: Size (in points) of text in a memo block.

Graphic: Selects graphic file.

Grid: Displays grid lines on histogram and run charts.

Height (mm): Height of an object in mm.

Italic:

Left (mm):

LineColor: Defines colour of bounding line of shapes.

LineStyle:

LineWidth: Defines thickness of bounding line of shapes.

Select between 3 dimensional or 2 dimensional run
charts.

Alignment of text in a memo block (top, middle, left,
right, etc.)

Defines how a block is anchored to the page. Anchor
position remains constant if page size is changed.

In measurements object - Width of percentage of full
scale column (mm)

In measurements object - Width of Sheer stress
column

In measurements object - Width of Temperature
column

Fill style of shapes (solid, diagonals, cross hatched,
etc.)

Defines whether text in a memo block is italic or
upright.

Defines gap between left edge of page and left edge
of block (see also Top).

Defines style of bounding line of shapes (solid, dash,
dot, etc.)

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49

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THE PAGE DESIGNER

Property Description

Name:

PageWidth (mm): Defines width of the page in mm.

PageHeight (mm): Defines height of the page in mm.

PageType: Defines page type; Opening, Inner or Closing.

PageOrientation: Portrait (default) or Landscape.

PaperSize: Paper dimensions; A3, A4, Letter, etc.

ReadingsPerPage:

RowsPerPage:

Shape:

ShowColumnHeader:

ShowLegend: Defines whether colour key bar and legend is visible.

Strikeout:

Text: Opens The Text Editor .

Top (mm):

Underline:

Width (mm): Width of an object in mm.

WordWrap:

Defines name of object. Object names are displayed
in Object Selector Window.

Number of readings of a batch displayed on one
page of a report.

Number of rows of a batch displayed on one page of
a report.

Shape object type; Rectangle, Horizontal Line or
Vertical Line.

Defines whether titles at the top of readings columns
are visible.

Defines text style in a memo block as strikeout
(strikeout

).

Defines gap between top edge of page and top edge
of block (see also Left).

Defines text style in a memo block as underline
(underline

).

Defines whether text in a memo block will wrap onto
the line below.

22.3 The Text Editor

Use the Text Editor to enter text and data fields onto the Page Layout Window of The page designer .

• To enter text, click in the text editor window and type your text. Use the carriage return key to
enter a new line.

50

SUPPORT

• To enter data fields, click in the text editor window and then click on a data field button.
Explanations of the data field buttons are given in “Text Editor Data Field Buttons” on page 51.

When you have finished, click on the OK button to enter your text onto the Page Layout Window.

22.4 Text Editor Data Field Buttons

Descriptions of the data field buttons are given below:

Data Field Button Description

Batch ID: The batch name

File Path: The location of the data file on your computer

Todays Date: Today’s date

Page No. Page number in the report

Model: Viscometer type (RV1/RV2 etc.)

Spindle: Spindle type (R1, L1, etc.)

Company: Information added in header when creating a New Batch

Operator: Information added in header when creating a New Batch

Identifier: Information added in header when creating a New Batch

Note: Information added in header when creating a New Batch

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23 SUPPORT

For support with this software, information on the Elcometer product range and details of your local
supplier, contact any of the Elcometer offices worldwide. Contact details can be found under ‘Help’
in ViscosityMaster, on the outside cover of these instructions and at www.elcometer.com

51

INDEX

24 INDEX

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A

Accessories 28

Overview 1
Adaptor for helical movement 17
Adaptor for low viscosity samples 16
Adaptor for small sample volume 15
Assembly (of Viscometer) 5

B

Batch

Creating

RV1 35
RV2 37

Running

RV1 37

RV2 40
Box spanner 5
Buttons 6

C

Calibration 25
Caring for your Viscometer 25
Cleaning 14
Clock, setting 8
Closing page (ViscosityMaster) 44
Computer mode 8
Configuring (Viscometer) 7
Connections at rear 6
Contents of the box 2
Control panel 6
CSV files, exporting to 45

D

Data 41

Exporting 45
Date, setting 8
Demo data, ViscosityMaster 34
Documents, in ViscosityMaster 46

E

E-mailing 45
ERROR message 13
Excel spreadsheets 45
Exporting 45

F

Features of Viscometer 3

G

Guard (for spindles) 9

H

Helical movement adaptor 17

Spares 29

Help

ViscosityMaster 32, 51

I

Images, in ViscosityMaster 46
Inner pages (ViscosityMaster) 44
Interfaces 6

K

Keypad 6

L

Language, selecting 7
List of parts 2
Low viscosity adaptor kit

Spares 28

M

Maintenance 25
Maximising the window 33
Measurement data 41

Exporting 45
Viewing 41

Mode, operating (Viscometer) 8

N

Null-modem cable connections 14

O

Opening pages (ViscosityMaster) 44
Operation

Features 3
Overview 1
Taking a measurement 13

P

Packaging materials 3
Page designer (ViscosityMaster) 47
PDF files, creating 45
Plastic cap 5
Printer mode 8

52

Printer, thermal 29
Printing 45
Printing Mode 14
Printing test results 14
Problems with measurements (Viscometer)
13
Processes, setting up (RV2) 39
Property editor (designing reports) 49

R

Report page designing (ViscosityMaster) 48
Rotation speed

Changing 13

S

SAFETY 11
Setup options 7
Shear Rate 13
Shear Stress 13
Shear stress units, selecting 7
Small sample volume 15
Small volume samples adaptor

Spares 28
Spanner 5
Spare parts 28
Specifications 27
Spindle guard 9
Spindle speed

Adjusting 13
Spindles

Fitting 11

Identification of 11

Selection of type 12

Selection table

L 19
LCP 23
P 24
R 21
TL 20

TR 22
Setting speed 12
Spare parts 28
Type

LCP 16

P series 17

TL 15

TR 15
Types of 10

Spreadsheets 45

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INDEX

Standards 3
Stopping the motor 13

T

Technical specifications 27
Temperature (high) 16
Temperature units, selecting 8
Thermal printer

Spares 29
Time and Date 8
Troubleshooting 13, 26

V

Viscometer data 41
Viscosity

Low viscosity samples 16
Viscosity units, selecting 7
ViscosityMaster

Automatic mode 35

Connecting to your Viscometer 31

Example data 34

Features 30

Help 32

Installing 30

Manual mode 35

Preferences 31

Report window tabs 43

Reports

Creating 43
Viewing custom 44

Viewing standard 41
Starting 31
System requirements 30
Uninstalling 31
User interface 33
Using with RV1 Viscometers 35
Using with RV2 Viscometers 37

Volume, small samples 15

53