Delta OHM HD3406.2 User Manual

Our instruments' quality level is the results of the product continuous development. This can bring about differences between the information written in this manual and the instru­ment that you have purchased. We cannot entirely exclude errors in the manual, for which we apologize. The data, figures and descriptions contained in this manual cannot be legally asserted. We reserve the right to make changes and corrections without prior notice.
REV. 1.0
31 Jan. 2006
HD3406.2
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Conductivity meter – Thermometer
HD3406.2
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HD3406.2
1. Connectors.
2. Battery symbol: indicates the battery level. The symbol does not appear when the external
power supply is connected.
3. CAL key: it starts the conductivity probe calibration.
4. REL key: enables the relative measurement (displays the difference between the current va-
lue and the logged value when the key is pressed); in the menu, decreases the current value.
5. LOG/DUMP LOG key: during normal operation, starts and ends the saving of the data in
the internal memory; in the menu, starts the data transfer from the instrument's memory to the PC.
6. χ--TDS Key: changes the main variable measurement between conductivity, resistivity,
total dissolved solids (TDS) and salinity.
7. SERIAL/ERASE LOG key: starts and ends the data transfer to the serial/USB communica-
tion port. In the menu, clears the data contained in the instrument's memory.
8. °C/°F key: when the probe is not connected, allows manual modification of the temperature.
When double pressed, changes the unit of temperature measurement from degrees Celsius to Fahrenheit.
9. Function indicators.
10. key: in the menu, confirms the current selection.
11. Line for symbols and comments.
12. Main display line.
13. ON-OFF/AUTO-OFF key: turns the instrument on and off. When pressed together with the
ENTER key, disables the automatic turn off.
14. MENU key: allows access to and exit from the menu.
15. ENTER key: in the menu, confirms the current selection; when pressed together with the
ON/OFF key, disables the automatic turn off.
16. ESC key: in the menu, cancels the operation in progress without making changes.
17. FUNC: key: during normal operation displays the maximum (MAX), the minimum (MIN)
and the average (AVG) of current measurements.
18. MAX, MIN and AVG symbols.
19.
Key : in the menu, decreases the current value.
20. Secondary display line.
21. External mains power supply connector input 12Vdc for 5.5mm - 2.1mm connector .
22. Not used
23. 8-pole DIN45326 connector, input for combined 4-ring or 2-ring conductivity/temperature
probes, for direct 4 wire Pt100 temperature probes and 2 wire Pt1000 probes complete with TP47 module.
24. 8-pole MiniDin connector for RS232C connection using cable HD2110CSNM, for USB 2.0
connection using cable HD2101/USB, and for S-print-BT printer connection using cable HD2110CSP.
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INTRODUCTION
The instrument series HD34… is made up of 4 bench top instruments for electrochemical measures: pH, conductivity, dissolved oxygen, and temperature.
The HD3406.2 measures conductivity, liquid resistivity, total dissolved solids (TDS), and salin- ity using combined 4-ring and 2-ring conductivity/temperature probes. Temperature is measured by Pt100 or Pt1000 immersion, penetration or contact probes. The probe can be calibrated either manually or automatically resorting to one or more of the 147μS, 1413μS, 12880μS or 111800μS/cm conductivity standard solutions
The displayed data can be stored (datalogger) and can be transferred to PC or serial printer thanks to the multi-standard serial ports RS232C and USB2.0 and software DeltaLog9 (Version 2.0 or later versions). The storing and printing parameters can be set from menu.
Display, printing and logging always show temperature in °C °F, and one of the parameters of con­ductivity measure (χ o Ω or TDS or NaCl).
Other common function of this instrument series include: Max, Min and Avg function, the Auto­HOLD function, the automatic turning off which can also be disabled.
The instruments have IP66 protection degree.
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KEYBOARD AND MENU DESCRIPTION
Foreword
The instrument keyboard is composed of single-function keys, like the MENU key, and double­function keys such as the LOG/DUMP LOG key. In the double-keys, the function in the upper part is the "main function", while the one in the bottom part is the "secondary function". When the instrument is in standard measurement mode, the main function is active. The secondary function of the is enabled in the menu. The pressing of a key is accompanied by a short confirmation beep: a longer beep sounds if the wrong key is pressed. Each key specific function is described in detail below.
ON-OFF key
The instrument is turned on and off using the ON/OFF key. Turning on enables all display seg­ments for a few seconds, starts an auto-test, and displays the current values of cell constant (CELL) and temperature coefficient α (ALPH). Finally, it sets the instrument ready for normal measure­ment.
MIN
cm
min
s
2 3
m
µmk
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During turning on, should no probes be connected, the last manually-set temperature ap­pears in the secondary line. The unit of measurement symbol (°C or °F) starts blinking, and a letter "m" meaning "manual" appears next to the battery symbol. The probe's data are captured upon turning the instrument on: if the ERR message ap­pears in the secondary line, it is necessary to turn the instrument off and then on again. Replace the probes when the instrument is off.
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Automatic turning off
The instrument has an AutoPowerOff function that automatically turns the instrument off after about 8 minutes if no key is pressed during the intervening time. The AutoPowerOff function can be dis­abled by holding the ENTER key: pressed down when turning the instrument on: the battery symbol will blink to remind the user that the instrument can only be turned off by pressing the <ON/OFF> key.
The automatic turning off function is disabled when external power is used. On the other hand, it cannot be disabled when the batteries are discharged.
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ENTER Key
In the menu, the ENTER key confirms the current parameter and then goes to the next one. Pressed together with the ON/OFF key, disables the automatic turn off.
MENU Key
The first menu item is accessed by initially pressing on the MENU key; press ENTER to go to the following items. To modify the item displayed, use the arrow keys ( and ). The current value is confirmed by pressing the ENTER key and the display moves on to the next parameter. If pressing ESC the setting is cancelled.
To exit the menu, press the MENU key at any time.
The menu items are listed in this order:
1) Management of memorized data: the message "LOG_DUMP_or_ERAS" (Transfer data
or erase) is scrolled in the comment line. The center figure reports the number of free mem­ory pages (FREE). All memory data are permanently erased by pressing SE­RIAL/EraseLOG. By pressing LOG/DumpLOG, the data transfer of the logged data on the serial port is started: the "BAUD-RATE" must have previously been set to the maximum value (please see the menu items described below and the paragraph "STORING AND TRANSFERRING DATA TO A PERSONAL COMPUTER" on page 30).
2) sets the interval in seconds between two loggings or data transfers to the serial port. The in-
terval can be set from 0s, 1s, 5s, 10s, 15s, 30s, 60s (1min), 120s (2min), 300s (5min), 600s (10min), 900s (15min), 1200s (20min), 1800s (30min) e 3600s (1 hour). If the value 0 is
set, SERIAL works on command: the sending of data to the serial port is performed each time the key is pressed. Recording (LOG) is performed with one second intervals
even if the interval is set to 0. With an interval from 1 to 3600s, continuous data transfer is started when the SERIAL key is pressed. To end the recording (LOG) and continuous data transfer operations (SERIAL with an interval greater than 0), press the same key again.
3) Sleep_Mode_LOG (Automatic turning off during recording:): this function controls the
instrument's automatic turning off during logging, occurring between the capture of a sample and the next one. When the interval is lower than 60 seconds, the instrument will always remain on. With intervals greater than or equal to 60 seconds, it is possible to turn off the in­strument between loggings: it will turn on at the moment of sampling and will turn off im­mediately afterwards, thus increasing the battery life. Using the arrows select YES and con­firm using ENTER in order to enable the automatic turning off, select NO and confirm to disable it and keep the instrument on continuously.
Note: even if Sleep_Mode_LOG=YES is selected, the instrument does not turn off for less than one minute intervals.
4) Identifier of the sample being measured it is an automatically increased progressive num-
ber associated with the single PRINT function (print interval set to 0) for the printing of labels. The index appears in the single sample printing together with date, time, conductivity (liquid resistivity, total dissolved solids or salinity) and temperature. This menu item allows
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the value of the first sample to be set: each time the PRINT key is pressed, the identification ID in the printing is increased by 1 allowing progressive measurement of all measured sam­ples. If the Auto-Hold function, described below in this chapter, is enabled, the print time in­terval is forced to zero. Pressing SERIAL only causes the print to occur when the measure­ment has stabilized (HOLD symbol still). Later, it is possible to repeat the print at will, but while the HOLD mode is on, the sample identifier number is not increased. This is useful when more labels must be printed with the same identification code without increasing the code each time. The message "SMPL ID UNT=RSET SER=PRNT" is scrolled in the comment line: using the arrows ( and ) the currently measured sample identifier value can be changed. By holding the °C/°F (Unit) key down the proposed number is rapidly set to zero. The instrument's heading information will be printed using the SERIAL key.
5) AUTO-HOLD function: the instrument normally operates in continuous view mode (de-
fault setting). In this mode the displayed measurement is updated every second. If the Auto­Hold function is enabled, the instrument performs the measurement and when it stabilizes it goes in HOLD mode. To update the display indication, press FUNC . In the following figure you can see an example of the measurement process with the Auto­Hold function enabled. In the following figure you can see an example of the measurement process with the Auto-Hold function enabled. A probe is immersed into a liquid at conduc-
tivity
χ
1
and, to perform the measurement, the FUNC key is pressed: The conductivity measurement raises progressively reaching the final value. The HOLD symbol blinks. In the stretch indicated by 1, the measurement remains stable for 10 seconds, within two digits: at the end of this interval (point 2), the instrument goes into HOLD mode, presenting the final stable value.
2 digit
10s
t
χ
χ
1
6) K CELL (Cell constant) sets the conductivity probe's cell constant nominal value. The val-
ues 0.1, 0.7, 1.0 and 10 cm-1 (with tolerances from –30% to +50% of nominal value) are admitted. The cell constant must be inserted before starting the probe calibration. An ERR signal is generated if the cell constant's actual value exceeds the limits –30% or +50% of nominal value. In this case it is necessary to check that the value set is correct, that the cali­bration solutions are in good state, and then proceed with a new calibration.
The cell constant change entails resetting the calibration date: a new calibration updates the calibration date.
7) LAST CAL m/d h/m (Last conductivity calibration): the display shows the month and
day (m/d) in the main line, and the hour and minutes (h/m) in the secondary line of the pre­vious calibration of the conductivity probe. This menu item cannot be modified. The calibra-
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tion year is not displayed. The cell constant change, using the K CELL parameter, resets the date.
8) ALPH_T (Temperature coefficient αT): the temperature coefficient αT is the percentage
measurement of the conductivity variation according to temperature and is expressed in %/°C (or %/°F). The admitted values vary from 0.00 to 4.00%/°C. Use the arrows ( and ) to set the desired coefficient αT, and confirm with ENTER.
9) REF_TEMP (reference temperature): it indicates the temperature to which the displayed
conductivity value is standardized and can be equal to 20°C or 25°C. Using the arrows ( and ), set the desired value and confirm with ENTER.
10) TDS (Conversion factor χ/TDS): it represents the ratio between the measured conductivity
value and the total quantity of dissolved solids in the solution, expressed in mg/l (ppm) or g/l (ppt). This conversion factor depends on the nature of the salts present in the solution: in the field of water quality treatment and control, where the main component is CaCO3 (Calcium Carbonate), a value of 0.5 is usually used. For agriculture water, for fertilizers preparation, and in hydroponics, a factor of about 0.7 is used. Using the arrows ( and ), set the de­sired value, selecting it in the 0.4…0.8 range, and confirm with ENTER.
11) RCD MODE (Record mode): the instrument captures a conductivity and a temperature
value every second. If the RCD MODE parameter is set to "conductivity" (factory default), the maximum (MAX) and minimum (MIN) values displayed using FUNC refer to conduc­tivity: the indicated temperature is that measured at the maximum and minimum conductiv­ity and is not the maximum and minimum temperature. If the RCD MODE parameter is set to "tp" (=temperature), the maximum and minimum values displayed using FUNC refer to temperature: the indicated conductivity is that meas­ured at the maximum and minimum temperature and is not the maximum and minimum conductivity. Finally, if the RCD MODE parameter is set to "Indep" (=independent), the maximum and minimum values displayed using FUNC are independent: the indicated conductivity and temperature are the maximum and minimum measured values but are not necessarily re­ferred to the same measurement moment.
12) Probe type (the message "PRBE_TYPE" is scrolled in the comment line. The main line in
the center of the display shows the type of temperature probe connected to the instrument. Conductivity/temperature combined probes with Pt100 or Pt1000 sensor, or temperature only probes can be connected to the input:
4 wire PT100 using the TP47 module
2 wire PT1000 using the TP47 module
Upon being turned on, the instrument automatically detects the temperature probes: the
Probe Type menu item is configured by the instrument and cannot be modified by the user. If no temperature probe or combined probe with temperature sensor is connected, the in­strument displays a dotted line (- - - -).
13) YEAR: to set the current year. Use the arrows to modify this parameter and confirm using
ENTER.
14) MNTH (month): to set the current month. Use the arrows to modify this parameter and con-
firm using ENTER.
15) DAY: to set the current day. Use the arrows to modify this parameter and confirm using
ENTER.
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16) HOUR: to set the current hour. Use the arrows to modify this parameter and confirm using
ENTER.
17) MIN: to set the current minutes. In order to correctly synchronize the minute, it is possible
to reset the seconds by pressing the °C/°F key. Use the arrows to set the current minute plus one, and as soon as that minute is reached press °C/°F: this synchronizes the time to the second. Press ENTER to go onto the next item.
18) BAUD_RATE: indicates the frequency used for the serial communication with the PC.
Values from 1200 to 38400 baud. Use the arrows to modify this parameter and confirm us­ing ENTER. The communication between instrument and PC (or serial port printer) only works if the instrument and PC baud rates are the same. If the USB connection is used this parameter value is automatically set (please see the details on page 30).
FUNC key
It enables the display and logging of the maximum (MAX), minimum (MIN) and average (AVG) value of the conductivity, liquid resistivity, total dissolved solids, salinity and temperature meas­urements, updating them with the acquisition of new samples. The acquisition frequency is once a
second. Use the χ--TDS key to switch from conductivity to liquid resistivity, to total dissolved solids or to salinity.
MAX, MIN and AVG measurements remain in the memory until the instrument is on, even after exiting the calculation function. To reset the previous values and restart with a new measure­ment session, press FUNC until the message "FUNC CLR" appears, then use the arrows to se­lect YES and confirm using ENTER.
The conductivity (or resistivity or total dissolved solids or salinity) and temperature values are displayed at the same time. According to settings in the "RCD Mode" menu item, the maximum, minimum and average indications have different meanings: please see the descrip­tion of this MENU key.
Attention: the data captured using the Record function cannot be transferred to the PC.
ESC key
In the menu, the key clears or cancels the active function (ESC).
CAL key
It starts the conductivity probe (please see the paragraph dedicated to calibration page 15).
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REL Key
In measurement mode, it displays the difference between the current value and that measured on pressing the key. The REL message appears on the display; press the key again to return to the cur­rent measurement.
LOG/DumpLOG key
In measurement mode, this function starts and stops the logging of a data block to be saved in the instrument's internal memory. The data logging frequency is set in the "Print and log interval" menu parameter. The data logged between a start and subsequent stop represent a single session .
When the logging function is on, the LOG indication is displayed, the battery symbol blinks and a beep is issued each time a logging occurs; the battery symbol does not appear when using an external power supply. To end the logging, press LOG.
If the Auto-HOLD function is enabled (please see the menu), the data logging is disabled.
The HD3406.2 can turn off during logging between one capture and the next: the function is controlled by the Sleep_Mode_LOG parameter. When the logging interval is less than one minute, the logging instrument remains on; with an interval of at least one minute, it turns off between one capture and the next if the parameter Sleep_Mode_LOG=YES.
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Dump LOG
When the LOG key is pressed after the MENU key, the transfer of the logged data on the serial port is started. Please see the paragraph dedicated to data transfer on page 30.
χ--TDS (conductivity - resistivity - total dissolved solids - salinity) key
Changes the main variable measurement between conductivity, resistivity, total dissolved solids (TDS) and salinity. The selected parameter is used for display, printing and logging.
The instrument has an Auto-Hold function, which can be set in the MENU, that "freezes" the meas­urement automatically when it has been stable (within 1 digit) for over 10 seconds: the message HOLD is displayed. To perform a new measurement, it is necessary to press the FUNC key. The HOLD message starts blinking, while the display follows the actual measurement trend, until it stabilizes again and the HOLD message remains still.
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SERIAL/EraseLOG key
In measurement mode, this function starts and stops the data transfer to the RS232C serial output
According to the settings entered in the Print and log interval menu item, a single sample can be printed if Print and log interval = 0 or a continuous indefinite printing of the measured data can be set up if Print and log interval = 1…3600. The printing operation is accompanied by the display of the RS232 symbol and the blinking of the battery symbol; when using an external power supply the battery symbol does not appear. Press SERIAL to end the continuous printing.
Before starting the printing with SERIAL, set the baud rate. To do so, select the Baud Rate menu item and select the maximum value equal to 38400 baud by using the arrows. Confirm by pressing ENTER. The DeltaLog9 software for PC will automatically set the baud rate value during connection. If you
are using a different program than DeltaLog9, be sure the baud rate is the same for both the instrument and the PC: the communication will only work in this way.
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Erase memory
When pressed after the MENU key, the SERIAL key permanently erases all the data contained in the instrument's memory.
°C/°F key
When the temperature probe is connected, the measured value is used to compensate the conductiv­ity measurement; the key changes the unit of measurement from degrees Celsius to Fahrenheit. If the probe is not present, the compensation temperature must be entered manually: to manually change the value shown in the display lower line, press °C/°F once. The temperature indicated starts blinking. While the display is blinking, it is possible to change the compensation temperature using the arrows ( and ). Confirm using ENTER. The display stops blinking, and that temperature is used for compensation. If the temperature probe is not present, to change the unit of measurement between °C and °F, it is necessary to press twice the °C/°F key.
Up Arrow
When used in the menu, it increases the current variable value. During measurement, if the tempera­ture probe is not present, it increases the temperature value for conductivity compensation.
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Down Arrow
When used in the menu, it decreases the current variable value. During measurement, if the tem­perature probe is not present, it decreases the temperature value for conductivity compensation.
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CONDUCTIVITY MEASUREMENT
The instruments work with conductivity/temperature combined probes, 4-ring and 2-ring only con­ductivity probes, or temperature probes. The 4 wire Pt100, 2 wire Pt1000 probes may be used for measuring temperature, which is used for the automatic compensation of the conductivity
The instrument obtains the following from the measurement of conductivity:
the liquid resistivity measurement (Ω, kΩ, MΩ),
the concentration of total dissolved solids (TDS) according to the χ/TDS conversion factor,
which can be modified using the menu,
the salinity (NaCl quantity in the solution, expressed in g/l).
The conductivity, resistivity, TDS or salinity indication is displayed in the main line, while the sec­ondary line shows the temperature.
The conductivity probes must be periodically calibrated. To facilitate this operation, four automatic calibration solutions are provided:
0.001 Molar KCl solution (147μS/cm @25°C),
0.01 Molar KCl solution (1413μS/cm @25°C),
0.1 Molar KCl solution (12880μS/cm @25°C),
1 Molar KCl solution (111800μS/cm @25°C).
User calibration of the temperature sensors is not required.
The probes are detected during turn on, and this cannot be performed when the instrument is already on, therefore if a probe is connected and the instrument is on, it must be turned off and back on again.
Standard probe
The standard 4-electrode combined conductivity/temperature probe code is SP06T. The cell measurement zone is delimited by a bell in Pocan. A positioning key, present in the probe's end part, orients the bell correctly when the probe is introduced. For cleaning, simply pull the bell along the probe's axis without rotating it.
It is not possible to perform measurements without this bell.
This probe's temperature measuring range is -50°C a +90°C.
4- ring or 2- ring probes
The conductivity HD3406.2 uses 4-electrode or 2-electrode probes for conductivity measurement. The 4- ring probes are preferred to measure high conductivity solutions, either over an extended range or in presence of pollutants. The 2- ring probes operate in a shorter measurement range but with an accuracy comparable with the 4- ring probes. The probes can be in glass or plastic: the first can work in presence of aggressive pollutants, the lat­ter are more resistant to collisions, and so more suitable for industrial use.
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Cells with temperature sensor
All probes are fitted with a built-in Pt100 or Pt1000 temperature sensor: the simultaneous measure­ment of conductivity and temperature allows automatic correction of the effect of the latter on the solution conductivity.
Choosing the cell constant
The constant is a piece of information which characterizes the cell. It depends on its geometry and is expressed in cm–1. There is no cell capable of measuring the entire conductivity scale accurately enough. Consequently, cells with different constants are used allowing exact measurements on dif­ferent scales. The cell with constant K = 1cm
–1
allows measurements from low conductivity up to relatively high conductivity. The theoretical measurement cell is made of two 1cm2 metallic plates separated one from the other by 1cm. This type of cell has a cell constant Kcell of 1cm–1. In essence, the number, form, material and dimensions of the plates are very different from model to model, from manufacturer to manu­facturer. The low constant K probes are preferably used for low conductivity values, the high constant ones for high values. The indicative measurement range is reported in the following diagram:
Automatic or manual conductivity compensation
The conductivity measurement refers to a standard temperature, called reference temperature T_REF: that is, the instrument proposes the conductivity you would get if the temperature were T_REF. This temperature could be 20°C or 25°C according to the setting in the T_REF menu item. The conductivity increase per each grade of temperature variation is a characteristic of the solution and is indicated by the term "temperature coefficient α
T
": admissible values from 0.00 to 4.00%/°C, default value 2.00%/°C. When a combined probe with temperature sensor is present, the instrument automatically applies the temperature compensation function, and proposes the measurement using the reference tempera­ture T_REF according to the coefficient αT on the display. In absence of the temperature probe, the lower display shows the manually set compensation tem­perature (default=25°C). To point this condition out, the °C or °F symbol blinks intermittently near the temperature value. On the main display an "m" (manual) is turned on near the battery symbol (if on). The MT indica­tion is printed on the print-outs. On the other hand, if the temperature probe is present, the AT sym­bol appears.
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To manually change the compensation temperature press the °C/°F key once: the indicated tempera­ture value starts blinking. Select the desired temperature value by using the arrows and confirm with ENTER. The display stops blinking, and the temperature displayed is used for compensation. To change the unit of measurement between °C and °F, press the °C/°F key twice.
Calibration of conductivity
The probe calibration can be carried out on one, two or three points using the standard solutions automatically detected by the instrument (automatic calibration) or other solutions with known value (manual calibration). The CAL symbol will blink when the cell constant is modified using the menu (please see the de­scription of the K_CELL menu item on page 6).
Automatic calibration of conductivity using memorized standard solutions
The instrument can recognize four standard calibration solutions:
0.001 Molar KCl solution (147μS/cm @25°C),
0.01 Molar KCl solution (1413μS/cm @25°C),
0.1 Molar KCl solution (12880μS/cm @25°C),
1 Molar KCl solution (111800μS/cm @25°C),
Using one of these solutions, the calibration is automatic; the procedure can be repeated with one or more of the remaining standard solutions. The manual calibration is possible with a different conductivity solution from that used in the auto­matic calibration.
The solution temperature for the automatic calibration must be between 15°C and 35°C: if the solution temperature is under 15°C or over 35°C, the calibration is rejected: CAL ERR indication appears.
1. Turn the instrument on with the ON/OFF key.
2. Set the probe's cell constant by selecting it from the admitted values: 0.01, 0.1, 0.7, 1.0 o 10.0.
3. Dip the conductivity meter cell in the calibration solution until the electrodes are covered with
liquid.
4. Stir the probe lightly to remove any possible air inside the measurement cell.
5. Press the CAL key. The unit of measurement (μS/cm or mS/cm) appears on the comment line.
The central line shows the solution conductivity value at the measured temperature, or if the
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probe is not present, at the manually-set temperature. In the lower line, the closest temperature compensated standard buffer value.
6. Press the CAL key. The unit of measurement (μS/cm or mS/cm) appears on the comment line.
The central line shows the solution conductivity value at the measured temperature, or if the probe is not present, at the manually-set temperature. In the lower line, the closest temperature compensated standard buffer value.
If the measurement is in TDS, resistivity or salinity, by pressing CAL, the instrument goes automatically into conductivity calibration mode.
7. Press ENTER to confirm the displayed value. The cell constant nominal value (KCELL) and the
set temperature coefficient αT are displayed. Pressed repeatedly the ENTER key allows the cali­bration on the point to be repeated, for example, in order to obtain a more stable value.
8. To end the probe calibration, press ESC.
9. Rinse the probe with water. If you are then going to perform low conductivity measurements, we
recommend rinsing the probe using distilled or bidistilled water.
The instrument is calibrated and ready for use.
Manual calibration of conductivity using non memorized standard solutions
Manual calibration is possible at any calibration solution and temperature if it is within the instru­ment measurement limits and provided that you know the solution's conductivity at the temperature at which the calibration is performed. Proceed as follows:
1. Turn the instrument on with the ON/OFF key.
2. Set the probe's cell constant by selecting it from the admitted values: 0.01, 0.1, 0.7, 1.0 or 10.0
3. Dip the conductivity meter cell into a known conductivity solution until the electrodes are cov-
ered with liquid.
4. Stir the probe lightly to remove any possible air inside the measurement cell.
5. Press MENU, and then FUNC/ENTER until the item ALPH appears. The temperature coeffi-
cient αT is displayed. Note down the value displayed as it must be set again at the end of the procedure. Set the value to 0.00. This excludes the temperature compensation during the con­ductivity measurement.
6. Measure the temperature by pressing °C/°F. According to the temperature detected, determine
the calibration solution conductivity using the table specifying the conductivity according to temperature.
7. Select the conductivity measurement by pressing χ--TDS.
8. Press the CAL key. The CAL symbol is turned on. The unit of measurement (μS/cm or
mS/cm) appears on the comment line. If the calibration solution conductivity is sufficiently close (-30% to +50%) to one of the standard solutions, the secondary line displays the value. Otherwise it displays the calculated value according to current settings. In the central line the solution conductivity value is indicated according to the cell constant current settings.
9. Use the arrows to select the conductivity value determined at point 4 and confirm using EN-
TER. If the ERR indication appears, see the note below.
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10. The cell constant nominal value (KCELL) and the temperature coefficient αT set to 0 are dis-
played. Pressed repeatedly the ENTER key allows the calibration on the point to be repeated, for example, in order to obtain a more stable value.
11. To end the probe calibration, press ESC.
12. Go back to the MENU and select ALPH: re-enter the temperature coefficient as it was before
the calibration.
13. Rinse the probe with water. If you are then going to perform low conductivity measurements,
we recommend rinsing the probe using distilled or bidistilled water.
The instrument is now calibrated and ready for use.
NOTES:
Without having pressed ENTER at all, the calibration is interrupted by pressing ESC; the
previous values will continue to be used.
Upon confirming the calibration by using ENTER, the instrument checks that the correction to
the conductivity does not exceed the 70% or 150% limits of the theoretical value. If the calibra­tion is rejected because it is considered to be excessively corrupted, the CAL ERR message will appear, followed by a long beep. The instrument remains in calibration mode and maintains the previous calibration values.
The most frequent causes of error are due to the probe malfunctioning (deposits, dirt,…) or to the
standard solutions deterioration (bad preservation conditions, alteration due to pollution with dif­ferent conductivity solutions,…).
If the measurement is in TDS, resistivity or salinity, on the pressing of CAL, the instrument goes
automatically in conductivity calibration.
Table of standard solutions at 147μS/cm, 1413μS/cm, 12.88mS/cm and 111.8mS/cm
The table reports the standard solutions automatically detected by the instrument according to tem­perature.
°C µS/ cm µS/ cm mS/ cm mS/c m
°C µS/cm µS/c m mS/ cm mS/ cm
15.0
121 1147
10.48 92.5
26.0
150 1440 13.13 113.8
16.0
124 1173 10.72 94.4
27.0
153 1467 13.37 115.7
17.0
126 1199 10.95 96.3
28.0
157 1494 13.62 117.7
18.0
128 1225 11.19 98.2
29.0
161 1521 13.87 119.8
19.0
130 1251 11.43 100.1
30.0
164 1548 14.12 121.9
20.0 133 1278 11.67 102.1
31.0
168 1581 14.37 124.0
21.0
136 1305 11.91 104.0
32.0
172 1609 14.62 126.1
22.0
138 1332 12.15 105.9
33.0
177 1638 14.88 128.3
23.0
141 1359 12.39 107.9
34.0
181 1667 15.13 130.5
24.0
144 1386 12.64 109.8
35.0
186 1696 15.39 132.8
25.0 147 1413 12.88 111.8
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18
DIRECT INPUT INTO Pt100 AND Pt1000 TEMPERATURE PROBE WITH TP47 MODULE
The instrument accepts the input of Platinum temperature probes with resistances of 100 and 1000. The Pt100 are connected to 4 wires, the Pt1000 to 2 wires, with the excitation current chosen mini­mizing the sensor self-heating effects.
The 4 wire and 2 wire probes with direct input are checked for conformity with class A toler­ance according to norm IEC751 - BS1904 - DIN43760.
The temperature probes are automatically detected by the instrument (please see the description of the Probe Type menu on page 8).
The °C or °F unit of measurement can be chosen for display, printing, and logging using the °C/°F key.
How to measure
The temperature measurement by immersion is carried out by inserting the probe in the liquid for at least 60mm; the sensor is housed in the end part of the probe.
In the temperature measurement by penetration the probe tip must be inserted to a depth of at least 60mm, the sensor is housed in the end part of the probe. When measuring the temperature on frozen blocks it is convenient to use a mechanical tool to bore a cavity in which to insert the tip probe.
In order to perform a correct contact measurement, the measurement surface must be even and smooth, and the probe must be perpendicular to the measurement plane.
So as to obtain the correct measurement, the insertion of a drop of oil or heat-conductive paste is useful (do not use water or solvents). This method also improves the response time.
Instructions to connect the TP47 module for conductivity/temperature combined probes, 4 wire Pt100 probes and 2 wire Pt1000 probes
All Delta Ohm probes are provided with a module TP47. The HD3406.2 also work with conductiv­ity/temperature combined probes, direct 4 wire Pt100 probes, 2 wire Pt1000 probes manufactured by other producers: for the instrument connection is prescribed the TP47 connector to which the probe's wires should be welded.
Instructions to connect the probe to the module are provided below. The module is supplied complete with fairlead and gasket for 5mm maximum diameter cables.
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19
Do the following to open the module and connect a probe: unscrew the fairlead and extract the gasket, remove the label using a cutter, unscrew the ring on the opposite side as illustrated in the figure:
Open the two module shells: the printed circuit to which the temperature probe must be connected is housed inside. The wires coming from the conductivity cell are welded directly onto the 1 - 2 - 4 - 5 connector's pins. On the left there are the 1…4 points on which the Pt100 or Pt1000 sensor wires must be welded. The JP1…JP4 jumpers are in the center of the card. These must be left open:
1
2
3
4
Pt100 3 fil i
Pt1000
Ni1000
Not Used
Before welding, pass the probe cable through the fairlead and gasket. Weld the temperature sensor wires as shown in the table:
Sensor TP47 card connection Jumper
Pt100 4 wires
None
Pt1000 2 wires
None
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20
The wires coming from the conductivity probe are welded directly on the DIN45326 connector as reported in the following table:
Sensor Direct connection to the connector Jumper
2-electrode
conductivity
probe
Internal view of the connector
Jumper between
pins 1 and 4
Jumper between
pins 2 and 5
4-electrode
conductivity
probe
Internal view of the connector
None
As an alternative, the Pt100 and Pt1000 sensors can be welded directly on the connector's pins DIN45326, as reported in the following table:
Sensor Direct connection to the connector Jumper
Pt100 4 wires
Pt100
Internal view of the connector
None
Pt1000 2 wires
Pt1000
Internal view of the connector
Jumper between
pins 6 and 7
Jumper between
pins 3 and 8
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21
The wires coming from the conductivity/Pt100 temperature combined probe are welded directly on the connector as reported in the following table:
Sensor Direct connection to the connector Jumper
2-electrode
conductivity
probe
Pt100 tempera-
ture sensor
Pt100
Internal view of the connector
Jumper between
pins 1 and 4
Jumper between
pins 2 and 5
4-electrode
conductivity
probe
Pt100 tempera-
ture sensor
Pt100
Internal view of the connector
None
Ensure the welds are clean and perfect. Once the welding operation is complete, close the two shells, insert the gasket in the module, screw the fairlead. At the other end of the module, enter the ring with the O-Ring as indicated in the picture.
Make sure the cable is not twisted while you are screwing the fairlead. Now the probe is ready.
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22
WARNINGS AND OPERATING INSTRUCTIONS
1. Do not expose the probes to gases or liquids that could corrode the material of the sensor or the
probe itself. Clean the probe carefully after each measurement.
2. Do not bend the probe connectors or force them upward or downward.
3. Do not bend or force the contacts when inserting the probe connector into the instrument.
4. Do not bend, deform or drop the probes, as this could cause irreparable damage.
5. Always select the most suitable probe for your application.
6. Do not use probes in presence of corrosive gases or liquids. The sensor container is made of
AISI 316 stainless steel, while the contact probe container is made from AISI 316 stainless steel plus silver. Avoid contact between the probe surface and any sticky surface or substance that could corrode or damage it.
7. Above 400°C and below –40°C, avoid violent blows or thermal shocks to Platinum temperature
probes as this could cause irreparable damage.
8. To obtain reliable measurements, temperature variations that are too rapid must be avoided.
9. Temperature probes for surface measurements (contact probes) must be held perpendicular
against the surface. Apply oil or heat-conductive paste between the surface and the probe in or­der to improve contact and reduce reading time. Whatever you do, do not use water or solvent for this purpose. A contact measurement is always very hard to perform. It has high levels of uncertainty and depends on the ability of the operator.
10. Temperature measurements on non-metal surfaces usually require a great deal of time due to the
low heat conductivity of non-metal materials.
11. Probes are not insulated from their external casing; be very careful not to come into contact with
live parts (above 48V). This could be extremely dangerous for the instrument as well as for the operator, who could be electrocuted.
12. Avoid taking measurements in presence of high frequency sources, microwave ovens or large
magnetic fields; results may not be very reliable.
13. Clean the probe carefully after use.
14. The instrument is water resistant and IP66, but is not watertight and therefore should not be
immersed in water without closing the free connectors using caps. The probe connectors must be fitted with sealing gaskets. Should the instrument fall into the water, check for any water in­filtration. Gently handle the instrument in such a way as to prevent any water infiltration from the connectors' side.
Notes on conductivity measurement
The service life of a cell can be unlimited, provided that the necessary maintenance is performed and that it does not break. Some of the most frequent problems and their possible solutions are re­ported below.
Measurement of conductivity different from the expected value. Check that the cell used is suit­able for the measurement range. Check that the cell is not dirty, that there are no air bubbles inside it. Calibrate again using the appropriate standard.
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23
Slow response or instability. Check that the cell is not dirty, that there are no traces of oil or air bubbles inside it. If you work with a black Platinum cell, new platinum-coating of the electrode could be necessary.
Cell constant value not accepted. Check that the standard solutions are in good condition, that the probe's constant cell value coincides with that selected in the instrument and that the solution tem­perature is within the range 15…35°C.
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24
INSTRUMENT SIGNALS AND FAULTS
The following table lists all error indications and information displayed by the instrument and sup­plied to the user in different operating situations:
Display indications Explanation
ERR
This appears if the conductivity/temperature probe is measuring a value exceeding the set measuring range.
CAL
ERR
This appears when, during calibration, the read value exceeds the limits of -30% or +50% of the buffer's value compensated for temperature or the solution temperature is lesser than 15°C or higher than 35°C.
LOG
MEM
FULL
Memory full; the instrument cannot store further data, the memory space is full.
CAL
blinking
No calibration has yet been effected, or the cell constant value has been modified in the menu (please see the description of the K_CELL menu item on page 7).
m
No probe with temperature sensor connected. The letter "m" indicates that the displayed temperature was entered manually.
SYS
ERR
#
Instrument management program error. Contact the instrument's supplier and communicate the numeric code # reported by the display.
CAL
LOST
Program error: it appears after turning on for a few seconds. Contact the instrument's supplier.
BATT TOO LOW
CHNG NOW
Indication of insufficient battery charge appearing on turning on. The in­strument issues a long beep and turns off. Replace the batteries.
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25
The following table reports the indications provided by the instrument as they appear on the display, together with their description.
Display indication Explanation
ALPH
temperature coefficient α
T
AUTO HOLD
automatic function holding the displayed measurement
BATT TOO LOW - CHNG NOW
battery discharged - replace it immediately
BAUDRATE
baud rate value
COMM STOP
printing complete
COMM STRT
printing started
DAY_
day
DUMP_END
data transfer complete
DUMP_IN_PROG
data transfer in progress
FUNC CLR
max, min and average values clearing
FUNC CLRD
max, min and average values cleared
HOUR
hour
KCEL
Cell constant K
KOHM
measurement of resistivity in kΩ
LAST CAL m/d h/m
last calibration date month/day hour/minutes
LOG IN PROG
logging in progress
LOG MEM FULL
memory full
LOG_CLRD
memory data cleared
LOG_DUMP_OR_ERAS
transfer or erase data
LOG_STOP
logging complete
LOG_STRT
logging started
MIN >>> USE_UNIT_TO_ZERO SEC
minutes >>> use the UNIT key to reset the seconds
MNTH
month
MOHM
measurement of resistivity in MΩ
NaCl
measurement of salinity in g/l
OHM
measurement of resistivity in Ω
PLS_EXIT >>> FUNC RES_FOR_FACT ONLY
please exit using ESC >>> function reserved to factory calibra­tion
PRBE_TYPE
type of probe connected
PRNT AND LOG INTV
printing and logging intervals
PRNT INTV
printing interval
PROB COMM LOST
lost communication with probe
RCD MODE
record function operating mode (max, min, avg)
REF_TEMP
reference temperature
SLP_MODE_LOG
turning off during recording mode
SMPL ID REL=RSET SER=PRINT
identifier of the sample - REL=reset - SERIAL=print heading
SYS ERR #
program error number #
TDS
total dissolved solids
UNDR
minimum limit exceeded
YEAR
year
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26
LOW BATTERY WARNING AND BATTERY REPLACEMENT
The battery symbol on the display constantly shows the battery charge status. To the extent that batteries have dis­charged, the symbol "empties". When the charge decreases still further it starts blinking…
If you wish to continue using the instrument, remove the flat batteries and supply it using the exter­nal power supply. Data stored on memory are maintained even without power supply.
If the battery charge level is insufficient, the following message appears when you turn the in­strument on:
BATT TOO LOW
CHNG NOW
The instrument issues a long beep and turns off. In this case, replace the batteries or use the external power supply, in order to turn the instrument back on.
In order to avoid data loss, the logging session is ended, if the HD3406.2 is logging and battery voltage falls below the minimum operating level.
The battery symbol turns off when the external power supply is connected.
To replace the batteries, switch the instrument off and unscrew the battery cover counter clockwise. After replacing the batteries screw the cover on clockwise.
After replacing the batteries, the menu parameters must be set again. To go to the next item press ENTER; to return to measurement mode, press MENU. In order to avoid losing the menu settings, before removing the batteries, connect the external power supply.
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27
MALFUNCTIONING UPON TURNING ON AFTER BATTERY REPLACEMENT
After replacing the batteries, the instrument may not restart correctly; in this case, repeat the opera­tion. After disconnecting the batteries, wait a few minutes in order to allow circuit condensers to discharge completely; then reinsert the batteries.
WARNING ABOUT BATTERY USE
Batteries should be removed when the instrument is not used for an extended time.
Flat batteries must be replaced immediately.
Avoid batteries leaking.
Always use good quality leakproof alkaline batteries. Sometimes on the market, it is possi-
ble to find new batteries with an insufficient charge capacity.
INSTRUMENT STORAGE
Instrument storage conditions:
Temperature: -25…+65°C.
Humidity: less than 90%RH without condensation.
Do not store the instrument in places where:
Humidity is high. The instrument may be exposed to direct sunlight. The instrument may be exposed to a source of high temperature. The instrument may be exposed to strong vibrations. The instrument may be exposed to steam, salt or any corrosive gas.
MAINTENANCE
The instrument case is made of ABS plastic and the protections are rubber: do not use any incom­patible solvent for cleaning.
In the conductivity/temperature combined probe the bell and the body of the probe are made of Po­can, the conductivity and temperature sensors are made of Platinum. During the use control the compatibility of these materials with the liquid that you want to measure. The probe must be preserved in a dry space. At regular intervals check that no deposits or corrosion are present on the sensitive part of the probe. Any possible deposits should be removed using detergent on a wet rag. Particularly resistant depos­its can be removed leaving the probe immersed in soap water for some hours and then rinsing it. Do not allow hands to touch the electrodes after cleaning.
Do not use any abrasive product for cleaning.
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28
SERIAL INTERFACE AND USB
The HD3406.2 is fitted with an electrically isolated RS-232C and USB2.0 serial interface. The USB connection requires the previous installation of a driver in the instrument software. Install the driver before connecting the USB cable to the PC (please see the details on page. 32).
The instrument standard serial transmission parameters are:
Baud rate 38400 baud
Parity None
N. bit 8
Stop bit 1
Protocol Xon/Xoff
It is possible to change the RS232C serial port baud rate by setting the "Baudrate" parameter in the menu (please see page 9). The possible values are: 38400, 19200, 9600, 4800, 2400, 1200. The other transmission parameters are fixed. The USB 2.0 connection does not require the setting of parameters.
The instruments are provided with a complete set of commands and data queries to be sent via the PC.
All the commands transferred to the instrument must have the following structure:
XYcr where: XY is the command code and cr is the Carriage Return (ASCII 0D)
Command Response Description
P0 & Ping (locks the instrument keyboard for 70 seconds) P1 & Unlocks the instrument keyboard
S0 AT 21.3 1000
Captured measurements (24 characters) AT = automatic temperature compensation, temperature
G0 Model HD3406 -2 Instrument model G1 M=conductivity meter Model description G2 SN=12345678 Instrument serial number G3 Firm.Ver.=01-01 Firmware version G4 Firm.Date=2004/06/15 Firmware date G5 cal 0000/00/00 00:00:00 Calibration date and time G6 Probe=Cond + Pt100 Type of probe connected to input GB User ID=0000000000000000 User code (set with T2xxxxxxxxxxxxxxxx) GC Immediate printing of data
K1
PRINTOUT IMMEDIATE MODE
Stop printing data
K0 Start logging data K4 & Stop logging data K5 & Immediate printing of data K7 & Enable REL function K6 & Disable REL function KP & Auto-power-off function=ENABLE KQ & Auto-power-off function=DISABLE LN &1999 Number of free pages in the flash memory LD PRINTOUT OF LOG Print data logged in flash LE & Erase data in flash memory
LUAn
&
Sets the unit of measurement for the temperature n=0 > °C
n=1 > °F
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29
Command Response Description
LUBn
&
Sets the unit of measurement for the conductivity n=0 > μS/cm n=1 > Ω n=2 > TDS n=3 > NaCl
RA & # Reading of LOG/PRINT interval set RP & 600 Battery level (Resolut. 0.01V) RUA U= °C Temperature measurement unit RUB U= uS Conductivity measurement unit
WA# &
Setting LOG/PRINT interval. # is a hexadecimal number 0…D that represents the position of the in­terval in the list 0, 1, 5, 10, …, 3600 seconds.
WC0 & Setting SELF off WC1 & Setting SELF on
Command characters are exclusively upper case characters. Once a correct command is entered, the instrument responds with "&"; when any wrong combination of characters is entered, the instrument responds with "?". The instrument response strings end with the sending of the CR command (Car­riage Return). The instrument does not send the LF command (Line Feed). Before sending commands to the instrument via the serial port, locking the keyboard to avoid func­tioning conflicts is recommended: use the P0 command. When complete, restore the keyboard with the P1 command.
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30
STORING AND TRANSFERRING DATA TO A PERSONAL COMPUTER
The HD3406.2 instrument can be connected to a personal computer via an RS232C serial port, and exchange data and information through the DeltaLog9 software (Version 2.0 or later versions) running in a Windows operating environment. The measured values can be sent directly to the PC, through the SERIAL function in real time or store them in the internal memory using Logging function (LOG key) in their internal memory. If necessary, the data stored in the memory can be transferred to a PC later.
THE LOGGING FUNCTION
The Logging function allows the recording up to 36.000 data pair measurements [T-χ] registered by the probes connected to the inputs. Logging always includes two parameters. Each data pair is com­posed of: temperature in °C or °F, conductivity or resistivity or TDS or NaCl.
The logged parameters are selected using the “°C/°F” and “χ--TDS” keys”. The time interval between two consecutive measurements can be set from 1 second to 1 hour. The logging starts by pressing the LOG key and ends by pressing the same key again: the data memo­rized in this way form a continuous block of samples.
See the description of the menu items on page 6.
If the automatic turning off option between two recordings (MENU >> Sleep_Mode_LOG) is en­abled, upon pressing the LOG key the instrument logs the first data and turns off. 15 seconds before the next logging instant, it turns on again to capture the new sample, and then turns off.
The data stored in the memory can be transferred to a PC using the DUMP LOG command: MENU >> LOG. During data transfer the display shows the message DUMP; to stop the data transfer press ESC on the instrument or on the PC.
CLEARING THE MEMORY
To clear the memory use the Erase Log function (MENU >> SERIAL). The instrument starts clearing the internal memory; at the end of the operation, it goes back to nor­mal display.
NOTES:
Data transfer does not cause the memory to be erased; the operation can be repeated as many
times as required.
The stored data remain in the memory independently of battery charge conditions.
In order to print the data to a parallel interface printer, you must use a parallel-serial adaptor (not
supplied).
The direct connection between instrument and printer via a USB connector does not work.
Some keys are disabled during logging. The following keys work: ON/OFF, FUNC (Max-Min-
Avg) and SERIAL.
The recording started with the display in Max-Min-Avg mode proceeds normally with the actual
measured values. Only the display shows respectively the Max, Min or Avg values.
The logging is disabled, if the Auto-HOLD function is enabled.
If the logging is started when the display is in REL mode, the relative values are logged.
It is possible to activate both the logging (LOG) and direct transfer (PRINT) functions at the
same time.
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31
THE PRINT FUNCTION
The PRINT function sends the measurements taken in real time by the instrument inputs directly to a PC. Print data units of measurements are the same as those used on the display. Printing always includes two parameters. Each data pair is composed of: temperature in °C or °F, conductivity or
resistivity or TDS or NaCl. The printed parameters are selected using the “°C/°F”, and “χ--TDS” keys.
The function is started by pressing SERIAL. The time interval between two consecutive prints can be set from 1 second to 1 hour (please see the Print and log interval menu item on page. 6). If the print interval is equal to 0s, by pressing SERIAL the single data is sent to the connected device. If the print interval is higher than 0, the data transfer continues until the operator stops it by pressing SERIAL again.
See the description of the menu items on page 6.
Connect the S-print-BT printer using cable HD2110CSP.
NOTES:
The print out is formatted across 24 columns.
Some keys are disabled during serial transmission. The following keys work: ON/OFF, FUNC
(Max-Min-Avg) and LOG.
The FUNC key has no effect on the print-outs, only on the display.
If the Auto-Hold function is enabled, the print time interval is forced to zero: pressing SE-
RIAL only causes the print to occur when the measurement has stabilized (HOLD symbol still). Later, it is possible to repeat the print at will, but while the HOLD mode is on, the sample iden­tifier number is not increased. This is useful when more labels must be printed with the same identification code without increasing the code each time.
If the serial transfer is started when the display is in REL mode, the relative values are trans-
ferred.
It is possible to activate both the logging (LOG) and direct transfer (PRINT) functions at the
same time.
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32
CONNECTION TO A PC
The connection to the RS232C serial port of the PC uses the cable with code HD2110CSNM: sub D 9-pole female connector on one end - 8-pole MiniDin on the other end. The connection to the USB port uses the cable with code HD2101/USB: USB type A connector on one end – 8-pole MiniDin on the other end.
The instrument is supplied with the DeltaLog9 software (version from 2.0) that manages the con­nection, data transfer, graphic presentation, and printing operations of the captured or logged meas­urements.
The DeltaLog9 software is complete with "On-line Help" (also in PDF format) describing its characteristics and functions.
The HD3406.2 instrument is compatible with the HyperTerminal communication program supplied with the Windows operating systems (from Windows 98 to Windows XP
CONNECTION TO THE RS232C SERIAL PORT
1. The measurement instrument must be switched off.
2. Using the Delta Ohm HD2110CSNM cable, connect the measurement instrument to the first free
serial port (COM) of the PC.
3. Turn on the instrument and set the baud rate to 38400 (MENU >> ENTER until the Baud Rate
parameter >> select 38400 using the arrows >> confirm with ENTER). The parameter remains in the memory until replacement of the batteries.
4. Launch the DeltaLog9 application and press CONNECT. Wait for the connection to occur and
follow the indications on the screen. For a description of the DeltaLog9 application, please refer to its on-line Help.
CONNECTION TO THE USB 2.0 PORT
The USB connection requires the installation of the drivers. They are contained in the Delta-
Log9 CD-Rom (Version 2.0 or later versions).
Proceed as follows:
1. Do not connect the instrument to the USB port until you are expressly requested to do it.
2. Insert the DeltaLog9 CD-Rom, and select the “Install/Remove USB driver" item”.
3. The application checks the presence of the drivers on the PC: the installation starts if they are
not present; if they are already installed, the drivers are removed by pressing the key.
4. The installation wizard prompts the software user license: to proceed, the software usage
terms must be accepted - click on YES.
5. On the next page the folder where the drivers will be installed is indicated: confirm without
modifying.
6. Complete the installation by clicking on Finish. Wait few seconds until the DeltaLog9 page
appears.
7. Close DeltaLog9.
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33
8. Connect the instrument to the PC USB port. When Windows detects the new device, the "New
software installation wizard" is started”.
9. If you are asked for the authorization to search an updated driver, answer NO and continue .
10. In the installation window, select “Install from a list or specific location”.
11. In the next window select “Search for the best driver in these locations” and “Include this lo-
cation in the search”.
12. Using Browse, indicate the installation folder provided at point 5:
C:\Program Files\Texas Instruments\USB-Serial Adapter
Confirm with OK..
13. If you get the message that the software did not pass the Windows Logo testing, select “Con-
tinue”.
14. The USB driver are installed: at the end, click on “Finish .
15. The installation wizard requests the files location once more: repeat the just described
steps and provide the location of the same folder (see point 12).
16. Wait: the operation could take a few minutes..
17. The installation procedure is now complete: the device will be detected on each new connec-
tion automatically.
In order to check if the entire operation was successful, in CONTROL PANEL double click on SYSTEM. Select "Device Manager" and connect the instrument to the USB port . The following items should appear:
“UMP Devices >> UMP3410 Unitary driver" and "Ports (COM and LPT) >> UMP3410 Se-
rial Port (COM#)" for Windows 98 e Windows Me,
“Multiport serial boards >> TUSB3410 Device” and "Ports (COM and LPT) >> USB-
Serial Port (COM#)” for Windows 2000, NT e Xp.
When the USB cable is disconnected, these two items disappear and come back when it is con­nected again.
Notes.
1. If the instrument is connected to the USB port before installing the drivers, Windows signals the
presence of an unknown device: in this case, cancel the operation and repeat the procedure illus­trated at the beginning of this section.
2. In the documentation supplied with the DeltaLog9 CD-Rom, is included a detailed version of
this chapter with pictures. Moreover, the necessary steps to remove the USB drivers are reported.
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34
FUNCTIONING NOTES AND OPERATING SECURITY
Authorized use
Comply with the technical specifications outlined in the chapter “TECHNICAL CHARACTERIS­TICS” Its use is authorized only in conformity with the instructions written in this manual. Any dif­ferent use is considered improper.
General instructions on security
This instrument has been manufactured and tested according to safety regulation EN 61010-1 con­cerning electronic measurement instruments and was delivered ex factory in perfect security condi­tions. Its regular functioning and operating security can be ensured only if all the normal safety measures as well as the specifications described in this manual are complied with. Its regular functioning and operating security can be ensured only within the climatic conditions specified in the chapter “TECHNICAL CHARACTERISTICS”.
Do not use or store the instrument in ways and/or places in which there are:
Quick environment temperature changes that could cause condensation.
Corrosive or inflammable gases.
Direct vibrations or shocks against the instrument.
High intensity electromagnetic fields, static electricity.
If the instrument is moved from a cold to a hot environment, the condensation can disturb its func­tioning. In this case, you need to wait for the instrument to reach the environment temperature be­fore using it.
User obligations
The user of the instrument must ensure that the following regulations and directives concerning the handling of hazardous materials are complied with:
CEE directives on job safety National laws on job safety Accident prevention regulations
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35
INSTRUMENT TECHNICAL CHARACTERISTICS
Measured quantities
χ
, Ω, TDS, NaCl, °C, °F
Instrument
Dimensions (Length x Width x Height) 220x120x55mm
Weight 460g (complete with batteries)
Materials ABS, rubber
Display 2x4½ digits plus symbols
Visible area: 52x42mm
Operating conditions
Operating temperature -5…50°C
Warehouse temperature -25…65°C
Working relative humidity 0…90%RH without condensation
Protection degree IP66
Power
Batteries 3 type AA batteries
Autonomy (only batteries) 100 hours with 1800mAh alkaline batteries
Power absorbed with instrument off 20μA
Mains (cod. SWD10) Output mains adapter 100-240Vac/12Vdc-1A
Security of memorized data Unlimited
Time
Date and time Schedule in real time
Accuracy 1min/month max departure
Measured values storing
Type 2000 pages containing 18 samples each
Quantity 36000 pairs of measurements [χ or o
TDS or NaCl] e [°C or °F]
Selectable storage interval 1s, 5s, 10s, 15s, 30s, 1min, 2min, 5min,
10min, 15min, 20min, 30min and 1hour
Interface RS232C
Type RS232C electrically isolated
Baud rate Can be set from 1200 to 38400 baud
Data bit 8
Parity None
Stop bit 1
Flow Control Xon/Xoff
Serial cable length Max 15m
Selectable print interval immediate or 1s, 5s, 10s, 15s, 30s, 1min,
2min, 5min, 10min, 15min, 20min, 30min and 1hour
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36
USB interface
Type 1.1 - 2.0 electrically isolated
Connections
Input for temperature probes complete with TP47 module pole male DIN45326 connector
Conductivity input 8-pole male DIN45326 connector
Serial interface and USB 8-pole MiniDin connector
Mains adapter 2-pole connector (positive at centre)
12Vdc/1A
Measurement of conductivity by instrument
Measurement range (Kcell=0.01) / Resolution 0.000…1.999μS/cm / 0.001μS/cm
Measurement range (Kcell=0.1) / Resolution 0.00…19.99μS/cm / 0.01μS/cm
Measurement range (Kcell=1) / Resolution 0.0…199.9μS/cm / 0.1μS/cm
200…1999μS/cm / 1μS/cm
2.00…19.99mS/cm / 0.01mS/cm
20.0…199.9mS/cm / 0.1mS/cm
Measurement range (Kcell=10) / Resolution 200…1999mS/cm / 1mS/cm
Accuracy (conductivity) ±0.5% ±1digit
Measurement of resistivity by Instrument
Measurement range (Kcell=0.01) / Resolution Up to 1GΩ⋅cm / (*)
Measurement range (Kcell=0.1) / Resolution Up to 100MΩ⋅cm / (*)
Measurement range (Kcell=1) / Resolution 5.0…199.9Ω⋅cm / 0.1Ω⋅cm
200…999Ω⋅cm / 1Ω⋅cm
1.00k…19.99kΩ⋅cm / 0.01kΩ⋅cm
20.0k…99.9kΩ⋅cm / 0.1kΩ⋅cm
100k…999kΩ⋅cm / 1kΩ⋅cm
1…10MΩ⋅cm / 1MΩ⋅cm
Measurement range (Kcell=10) / Resolution 0.5…5.0Ω⋅cm / 0.1Ω⋅cm
Accuracy (resistivity) ±0.5% ±1digit
Measurement of total dissolved solids (with coefficient χ/TDS=0.5)
Measurement range (Kcell=0.01) / Resolution 0.00…1.999mg/l / 0.005mg/l
(*) The resistivity measurement is obtained from the reciprocal of conductivity measurement. Close to the bottom of the scale, the indication of resistivity appears like reported in the table below.
K cell = 0.01 cm
-1
K cell = 0.1 cm-1
Conductivity
(μS/cm)
Resistivity
(MΩ⋅cm)
Conductivity
(μS/cm)
Resistivity
(MΩ⋅cm)
0.001 μS/cm 1000 MΩ⋅cm 0.01 μS/cm 100 MΩ⋅cm
0.002 μS/cm 500 MΩ⋅cm
0.02 μS/cm 50 MΩ⋅cm
0.003 μS/cm 333 MΩ⋅cm
0.03 μS/cm 33 MΩ⋅cm
0.004 μS/cm 250 MΩ⋅cm
0.04 μS/cm 25 MΩ⋅cm
… … … …
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Measurement range (Kcell=0.1) / Resolution 0.00…19.99mg/l / 0.05mg/l
Measurement range (Kcell=1) / Resolution 0.0…199.9 mg/l / 0.5 mg/l
200…1999 mg/l / 1 mg/l
2.00…19.99 g/l / 0.01 g/l
20.0…99.9 g/l / 0.1 g/l
Measurement range (Kcell=10) / Resolution 100…999 g/l / 1 g/l
Accuracy (total dissolved solids) ±0.5% ±1digit
Measurement of salinity
Measurement range / Resolution 0.000…1.999g/l / 1mg/l
2.00…19.99g/l / 10mg/l
20.0…199.9g/l / 0.1g/l
Accuracy (salinity) ±0.5% ±1digit
Measurement of temperature by Instrument
Pt100 measurement range -50…+200°C
Pt1000 measurement range -50…+200°C
Resolution 0.1°C
Accuracy ±0.25°C
Drift after 1 year 0.1°C/ year
Automatic/manual temperature compensation 0…100°C con αT = 0.00…4.00%/°C
Reference temperature 20°C o 25°C that can be selected
χ/
TDS conversion factor 0.4…0.8
Cell constant K (cm-1) 0.01 - 0.1 - 0.7 - 1.0 - 10.0
Standard solutions automatically detected (@25°C)
147μS/cm
1413μS/cm
12880μS/cm
111800μS/cm
EMC standard regulations
Security EN61000-4-2, EN61010-1 level 3
Electrostatic discharge EN61000-4-2 level 3
Electric fast transients EN61000-4-4 level 3,
EN61000-4-5 level 3
Voltage variations EN61000-4-11
Electromagnetic interference susceptibility IEC1000-4-3
Electromagnetic interference emission EN55020 class B
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TECHNICAL DATA OF PROBES
2 AND 4 ELECTRODE CONDUCTIVITY PROBES WITH TP47 MODULE
ORDER CODE
MEASURING RANGE
AND USE
DIMENSIONS
SP06T
K=0.7
5μS/cm …200mS/cm
0…90°C
4-electrode cell
in Platinum
Probe material Pocan
General use
Not heavy duty
Ø 17
156
20
Ø 12
16 50
D=5
SPT401.001
K=0.01
0.04μS/cm …20μS/cm
0…120°C
2-electrode cell in AISI 316
Ultra pure water
Measurement in closed-cell
SPT01G
K=0.1
0.1μS/cm …500μS/cm
0…80°C
2-electrode cell
in Platinum-wire
Probe material glass
Pure water
SPT1G
K=1
10μS/cm …10mS/cm
0…80°C
2-electrode cell in Platinum
wire
Probe material glass
General use heavy duty ,
average conductivity
SPT10G
K=10
500μS/cm …200mS/cm
0…80°C
2-electrode cell in Platinum
wire
Probe material glass
General use heavy duty,
high conductivity
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Pt100 4 WIRE PROBES AND Pt1000 2-WIRE PROBES COMPLETE WITH TP47 MODULE
Model Type Application range Accuracy
TP47.100 Pt100 4 wires -50…+200°C Class A
TP47.1000 Pt1000 2 wires -50…+200°C Class A
TP87.100 Pt100 4 wires -50…+200°C Class A
TP87.1000 Pt1000 2 wires -50…+200°C Class A
Temperature drift @20°C 0.005%/°C
TP47 Module for the connection of Pt100 4-wire and Pt1000 2-wire probes to instrument series
HD34…, without amplifying electronics and linearization.
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ORDER CODES
HD3406.2K The kit is composed of: instrument HD3406.2 datalogger, for the measurement of
conductivity - resistivity - TDS - salinity - temperature, 3 1.5V alkaline batteries, operating manual, software DeltaLog9 version 2.0.
The conductivity probes, temperature probes, standard reference solutions, cables for data download to PC or printer have to be ordered separately
HD2110CSNM 8-pole connection cable Mini Din - Sub D 9-pole female for RS232C, for connec-
tion to PC without USB input.
HD2101/USB Connection cable USB 2.0 connector type A - 8-pole Mini Din for connection to
PC with USB input.
SWD10 Stabilized power supply at 100-240Vac/12Vdc-1A mains voltage.
S’print-BT Portable, serial input, 24 column thermal printer, 58mm paper width.
HD2110CSP Connection cable for instruments series HD34…to printer S’print-BT.
HD22.2 Laboratory electrode holder composed of basis plate with incorporated magnetic
stirrer, staff and replaceable electrode holder. Height max. 380mm. For ∅12mm electrodes.
HD22.3 Laboratory electrode holder with metal basis plate. Flexible electrode holder for
free positioning. For Ø 12mm probes.
TP47 Module for the connection of Pt100 4-wire and Pt1000 2-wire probes to instru-
ment series HD34…, without amplifying electronics and linearization.
CONDUCTIVITY PROBES AND COMBINED CONDUCTIVITY AND TEMPERATURE PROBES
SP06T Combined conductivity and temperature 4-electrode cell in Platinum, body in Po-
can. Cell constant K = 0.7. Measurement range 5μS/cm …200mS/cm, 0…90°C.
SPT401.001 Combined conductivity and temperature 2- electrode cell in stainless steel AISI
316. Cell constant K = 0.01. Measurement range 0.04μS/cm …20μS/cm, 0…120°C. Measurement in closed-cell.
SPT01G Combined conductivity and temperature 2-electrode Platinum-wire cell, glass
body. Cell constant K = 0.1. Measurement range 0.1μS/cm …500μS/cm, 0…80°C.
SPT1G Combined conductivity and temperature 2-electrode Platinum-wire cell, glass
body. Cell constant K = 1. Measurement range 10μS/cm …10mS/cm, 0…80°C.
SPT10G Combined conductivity and temperature 2-electrode Platinum-wire cell, glass
body. Cell constant K = 10. Measurement range 500μS/cm …200mS/cm, 0…80°C.
STANDARD CONDUCTIVITY CALIBRATION SOLUTIONS
HD8747 Standard calibration solution 0.001mol/l equal to 147μS/cm @25°C - 200cc.
HD8714 Standard calibration solution 0.01mol/l equal to 1413μS/cm @25°C - 200cc.
HD8712 Standard calibration solution 0.1mol/l equal to 12880μS/cm @25°C - 200cc.
HD87111 Standard calibration solution 1mol/l equal to 111800μS/cm @25°C - 200cc.
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TEMPERATURE PROBES COMPLETE WITH TP47
TP47.100 Direct 4 wire Pt100 sensor immersion probe with connector. Probe's stem Ø 3mm,
length 230mm. 4 wire connection cable with connector, length 2 metres.
TP47.1000 Pt1000 sensor immersion probe. Probe's stem Ø 3mm, length 230mm. 2 wire con-
nection cable with connector, length 2 metres.
TP87.100 Pt100 sensor immersion probe. Probe's stem Ø 3mm, length 70mm. Connection
cable 4 wires with connector, length 1 metre.
TP87.1000 Pt1000 sensor immersion probe. Probe's stem Ø 3mm, length 70mm. Connection
cable 2 wires with connector, length 1 metre.
TP47 Module for the connection of Pt100 4-wire and Pt1000 2-wire probes to instru-
ment series HD34…, without amplifying electronics and linearization. (the connection instructions are outlined on page 18).
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CONTENTS
INTRODUCTION ............................................................................................................................................................ 4
KEYBOARD AND MENU DESCRIPTION.................................................................................................................. 5
Conductivity measurement............................................................................................................................................ 13
Automatic or manual conductivity compensation................................................................................................... 14
Calibration of conductivity...................................................................................................................................... 15
Automatic calibration of conductivity using memorized standard solutions .......................................................... 15
Manual calibration of conductivity using non memorized standard solutions ........................................................16
Table of standard solutions at 147μS/cm, 1413μS/cm, 12.88mS/cm and 111.8mS/cm.......................................... 17
Direct input into Pt100 AND Pt1000 temperature probe with TP47 module........................................................... 18
How to measure ......................................................................................................................................................18
Instructions to connect the TP47 module for conductivity/temperature combined probes, 4 wire Pt100 probes and
2 wire Pt1000 probes............................................................................................................................................... 18
WARNINGS AND OPERATING INSTRUCTIONS.................................................................................................. 22
Notes on conductivity measurement ....................................................................................................................... 22
INSTRUMENT SIGNALS AND FAULTS .................................................................................................................. 24
LOW BATTERY WARNING AND BATTERY REPLACEMENT ......................................................................... 26
INSTRUMENT STORAGE........................................................................................................................................... 27
Maintenance................................................................................................................................................................. 27
SERIAL INTERFACE AND USB................................................................................................................................. 28
STORING AND TRANSFERRING DATA TO A PERSONAL COMPUTER........................................................ 30
The Logging function ..................................................................................................................................................30
Clearing the memory....................................................................................................................................................30
The PRINT function ................................................................................................................................................... 31
CONNECTION TO A PC............................................................................................................................................. 32
Connection to the RS232C serial port.......................................................................................................................... 32
Connection to the USB 2.0 port ................................................................................................................................... 32
Functioning Notes and Operating Security .................................................................................................................. 34
INSTRUMENT TECHNICAL CHARACTERISTICS .............................................................................................. 35
TECHNICAL DATA OF PROBES............................................................................................................................. 38
2 and 4 electrode conductivity probes with TP47 module ........................................................................................... 38
Pt100 4 –wire probes and Pt1000 2-wire probes complete with TP47 module.......................................................... 39
ORDER CODES............................................................................................................................................................. 40
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GARANZIA GUARANTEE
GARANTIE
GARANTIA
Questo certificato deve accompagnare l'apparecchio spedito al centro assistenza. IMPORTANTE: La garanzia è operante solo se il presente tagliando sarà compilato in tutte le sue parti.
This guarantee must be sent together with the instrument to our service centre. N.B.: Guarantee is valid only if coupon has been correctly filled in all details.
Le certificat doit porter le cachet du revendeur et la date d'achat. A défaut, la garantie sera comptée à partir de la date de la sortie d'usine.
ATTENTION: Pour bénéficier de la garantie, le présent certificat doit obligatoirement accompagner l'appa­reil présumé défectueux.
Dieser Garantieschein muss der Spedition beigelegt werden, wenn das Gerät an das Kundendienstzent­rum gesandt wird.
WICHTIG: Die Garantie ist nur gültig, wenn dieser Abschnitt bis ins Einzelne ausgefüllt ist.
Este certificado debe acompañar al aparato enviado al centro de asistencia. IMPORTANTE: La garantía es válida solo si el presente cupón ha sido completado en su totalidad.
Instrument type
HD3406.2
Serial number
RENEWALS
Date Date
Inspector Inspector
Date Date
Inspector Inspector
Date Date
Inspector Inspector
CE CONFORMITY
Safety
EN61000-4-2, EN61010-1 LEVEL 3
Electrostatic discharge EN61000-4-2 LEVEL 3
Electric fast transients EN61000-4-4 LEVEL 3
Voltage variations EN61000-4-11
Electromagnetic interference susceptibility IEC1000-4-3
Electromagnetic interference emission EN55020 class B
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