Delta OHM HD2305.0, HD2305 User Manual

Our instruments' quality level is the results of the product continuous development. This can bring about differences between the information written in this manual and the instrument that you have purchased. We cannot entirely exclude errors in the manual, for which we apologize. The data, figures and descriptions contained in this manual cannot be legally asserted. We reserve the right to make changes and corrections without prior notice.
HD2305.0
REV. 1.3
Nov.,10th2005
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pH meter - Thermometer
HD2305
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HD2305.0
1. Input for probes, 8-pole DIN45326 connector.
2. pH/mV input, female BNC
3. Battery symbol: displays the battery charge level.
4. Function indicators.
5. Secondary display line.
6. DATA/ENTER key: during normal operation displays the maximum (MAX), the minimum
(MIN) and the average (AVG) of current measurements. In the menu, confirms the current selection. In calibration mode, acquires the nominal buffer value.
7. pH-mV/ESC key: during normal operation switches the display between pH and mV; in the
menu, resets the value set with the arrows. In calibration mode, allows you to exit calibration.
8. key: in the menu, increases the current value. In calibration mode, increases the displayed
nominal buffer value.
9. °C/°F/MENU key: it allows selection of the unit of measurement; when pressed together with
the DATA key, it allows to open the menu.
10. CAL: starts the calibration procedure.
11. /REL-mV key: during normal operation enables the relative measurement (displays the
difference between the current value and the logged value when the key is pressed); press the key again to return to the normal measurement. It works only if you are displaying the mV. In the menu, decreases the current value. In calibration mode, decreases the displayed nominal buffer value.
12. ON-OFF/AUTO-OFF key: turns the instrument on and off; when pressed together with the
°C/°F/MENU key, disables the AutoPowerOff function.
13. MAX (maximum value), MIN (minimum value) and AVG (average value) symbols.
14. Main display line.
15. Line for symbols and comments.
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TABLE OF CONTENTS
1. GENERAL CHARACTERISTICS............................................................................................................................. 5
2. DESCRIPTION OF THE FUNCTIONS .................................................................................................................... 6
3. THE PROGRAMMING MENU ................................................................................................................................. 9
4. PROBES AND MEASUREMENTS.......................................................................................................................... 10
4.1 THE ELECTRODE FOR pH MEASUREMENT ................................................................................................................10
4.1.1 Automatic or manual pH compensation ......................................................................................................... 11
4.1.2 How to manually change the temperature ...................................................................................................... 11
4.2 pH ELECTRODE CALIBRATION .................................................................................................................................12
4.2.1 Calibration procedure..................................................................................................................................... 12
Temperature characteristics of Delta OHM buffer solutions .................................................................................. 14
4.3 Pt100 AND 2 WIRE Pt1000 TEMPERATURE PROBES ................................................................................................ 15
4.3.1 Temperature measurement............................................................................................................................. 15
4.3.2 Connecting the TP47 connector for the 4 wire Pt100 and 2 wire Pt1000 probes........................................... 15
4.3.3 Direct connection of 4 wire Pt100 sensors..................................................................................................... 17
5. WARNINGS................................................................................................................................................................ 18
6. INSTRUMENT SIGNALS AND FAULTS .............................................................................................................. 19
7. INSTRUMENT STORAGE....................................................................................................................................... 20
8. LOW BATTERY WARNING AND BATTERY REPLACEMENT ..................................................................... 21
8.1 WARNING ABOUT BATTERY USE.............................................................................................................................. 21
9. NOTES ABOUT WORKING AND OPERATIVE SAFETY ................................................................................. 22
10. TECHNICAL CHARACTERISTICS ....................................................................................................................23
10.1 TECHNICAL INFORMATION ON THE pH METER THERMOMETER.......................................................................... 23
10.2 ON LINE INSTRUMENT PROBES AND MODULES TECHNICAL DATA................................................... 24
10.2.1 Temperature probes Pt100 and SICRAM module........................................................................................ 24
10.2.2 4 wire Pt100 and 2 wire Pt1000 Probes........................................................................................................24
11. ORDER CODES....................................................................................................................................................... 25
11.1 PH ELECTRODES ................................................................................................................................................... 25
11.2 ORP ELECTRODES (REDOX) ...............................................................................................................................25
11.3 PH BUFFER SOLUTIONS ......................................................................................................................................... 25
11.4 ORP BUFFER SOLUTIONS (REDOX) ......................................................................................................................26
11.5 TEMPERATURE PROBES COMPLETE WITH SICRAM MODULE ................................................................................ 26
11.6 TEMPERATURE PROBES WITHOUT SICRAM MODULE .......................................................................................... 26
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1. GENERAL CHARACTERISTICS
The pH meter - Thermometer Model HD2305.0 is a portable instrument that allows measurement of pH and redox potential (ORP) in mV. It also measures the temperature using Pt100 or Pt1000 immersion, penetration or contact probes.
The electrode calibration can be carried out on one, two or three points at 4.01pH, 6.86pH and
9.18pH.
The probes are fitted with the SICRAM automatic detection module, with the factory calibration settings already being memorized inside.
The units of measurement for the measurable quantities are:
pH
mV
°C
°F
Using the Max, Min and Avg function of this instrument respectively obtains the maximum, minimum or average values.
Other available functions are:
the relative measurement REL;
the automatic turning off which can also be disabled.
For further details see chapter 2.
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2. DESCRIPTION OF THE FUNCTIONS
The keyboard of the pH meter Model HD2305.0 is composed of double-function keys. The function on the key is the "main function", while the one above the key is the "secondary function". When the instrument is in standard measurement mode, the main function is active. Once the Settings Menu has been opened, by pressing simultaneously the DATA+°C/°F keys, the secondary function is enabled. The pressing of a key is accompanied by a short confirmation "beep": a longer "beep" sounds if the wrong key is pressed. Each key specific function is described in detail below.
This key has two functions:
ON/OFF: to turn the instrument on press ON, to turn it off press OFF. The turning on enables all display segments for a few seconds, starts an Auto-test including the detection of the probe connected to the input, and sets the instrument ready for normal measurement. The following is displayed:
MIN
cm
min
s
2 3
m
µmk
>>>
AUTO/OFF: the AutoPowerOff function can be disabled by simultaneously pressing this key
and the "°C/°F-MENU" key when turning the instrument on.
During turning on, should no probes be connected, the "NO_PRBE_SER_NUM" message is displayed in the line for symbols for a few seconds, while the "ERR" message is shown in the central part of the display, and the last manually-set temperature appears in the secondary line. The unit of measurement symbol (°C or °F) starts blinking, and a letter "m" meaning "manual" appears next to the battery symbol. When the probe fitted with SICRAM module is inserted into a functioning instrument, the "NEW_PROB_DET" (New probe detected) message appears, while the "ERR" message is shown in the central part of the display, and a sequence of "beeps" is simultaneously issued. As the data are captured upon turning the instrument on, it is necessary to turn it off and on again.
Caution! Replace the probes when the instrument is off.
ON-OFF and AUTO-OFF key
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The "pH-mV" key has three functions:
pH-mV: pressing this key once switches the display between pH and mV;
ESC: once the MENU has been opened with the DATA+°C/°F keys, the "pH-mV" key will
allow to cancel the parameters set using the and arrows.
In calibration mode, it allows to exit calibration.
The "DATA" key is used for the following functions:
DATA: during normal measurement, by pressing this key once the maximum (MAX) value of
the measurements captured by the probe connected to the instrument is displayed, updating it with the acquisition of new samples;
- by pressing this key again the minimum (MIN) value is displayed;
- by pressing this key a third time the average (AVG) value is displayed.
The acquisition frequency is once a second.
The MAX, MIN and AVG values remain in the memory until the instrument is on, even after exiting the DATA display function. When the instrument is off, the previously memorized data are cleared. Upon turning on, the instrument automatically starts memorizing the MAX, MIN and AVG values. To reset the previous values and start with a new measurement session:
press DATA until the FUNC_CLRD message appears;
use the and arrows to select YES;
confirm by pressing ENTER.
ENTER: once the MENU has been opened with the DATA+°C/°F keys, the DATA key will
perform the ENTER function and the MENU can be browsed and the displayed parameter confirmed. In calibration mode, acquires the nominal buffer value.
Once the MENU has been opened with the DATA and °C/°F keys, the key will allow to increase the value of the selected parameter. In calibration mode, it allows to increase the nominal buffer value.
The " C/°F" key is used for the following functions:
°C/°F: when the temperature probe is connected, the key changes the unit of measurement from
degrees Celsius to Fahrenheit. If the probe is not present, the compensation temperature must be entered manually: to manually change the value shown in the display lower line, press °C/°F once. The temperature indicated starts blinking. While the display is blinking, it is possible to change the compensation temperature using the arrows ( and ). Confirm using
DATA/ENTER key
pH-mV/ESC key
key
°C/°F/MENU key
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DATA/ENTER. The display stops blinking, and the temperature displayed is used for compensation. If the temperature probe is not present, to change the unit of measurement between °C and °F, it is necessary to press twice the °C/°F key.
MENU: to access to the menu press simultaneously DATA+°C/°F: the Probe Type will be
displayed.
use the  and arrows (respectively located above the HOLD and REL keys) to modify
the displayed value;
press DATA/ENTER to confirm the modification and go onto the next item;
press CLR/ESC to cancel the modification;
to exit the menu, press the °C/°F key again.
For further information see chapter 3.
Press this key to start the calibration procedure (see par. 4.2 pH electrode calibration).
The "/ REL-mV" key is used for the following functions:
REL-mV: it displays the difference between the current value and that measured on pressing
the key. The "REL" message is displayed on the left. To return to the normal measurement, press the key again. It only works with mV, so to enable the REL function select the "mV" unit of measurement using the "pH-mV" key.
: Once the MENU has been opened with the °C/°F/MENU key, the key will allow to
decrease the value of the selected parameter. During electrode calibration, it allows to decrease the nominal buffer value.
/ REL-mV key
CAL key
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3. THE PROGRAMMING MENU
To access to the menu press simultaneously the following keys:
The item to be set is:
Probe type: the "PRBE_TYPE_RTD_" message is displayed in the comment line. The main line in the center of the display shows the type of probe connected to the instrument. The following probes can be connected to the input:
temperature probes Pt100 complete with SICRAM module
4 wire Pt100 probes
2 wire Pt1000 probes
The probes fitted with SICRAM module, and Delta Ohm Pt1000 probes, are automatically detected by the instrument upon turning on: the Probe Type menu item is configured by the instrument and cannot be modified by the user. The temperature probes direct 4 wire Pt100, and the Pt1000 probes that are not manufactured by Delta OHM, when turned on display the message "NO_PRBE_SER_NUM". In this case the probe type must be entered manually.
Access to the menu by selecting Probe type using the DATA and °C/°F keys at the same time:
- use the and arrows to modify the displayed value;
- press DATA/ENTER to confirm the modification and go onto the next item;
- press pH-mV/ESC to cancel the modification;
- to exit the menu, press the °C/°F key again.
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4. PROBES AND MEASUREMENTS
The instrument works with the following probes:
electrodes for pH measurement;
electrodes for redox potential ORP measurement (REDOX);
specific ion electrodes.
Caution! The pH measurement is influenced by the temperature measurement.
The temperature is used for the automatic compensation of the Nernst coefficient with the pH electrode.
The measurement can be performed using probes with the following sensor:
4 wire Pt100;
2 wire Pt1000;
Some probes are fitted with SICRAM module that acts as an interface between the sensor on the probe and the instrument. There is a microprocessor circuit with a permanent memory inside the module that enables the instrument to recognize the type of probe connected and to read its calibration information.
The Delta Ohm Pt1000 probes are automatically detected while the direct 4 wire Pt100 temperature probe is not automatically detected by the instrument and must be set up in the Probe type menu item (please see the menu description on chapter 3).
The pH or mV indication is displayed in the main line; the secondary line shows the temperature.
The probes are detected during turn on, and this cannot be performed when the instrument is already on, therefore if a probe is connected and the instrument is on, it is necessary to turn it off and on.
The probes fitted with SICRAM module are calibrated in the factory; no calibration is required by the user.
4.1 THE ELECTRODE FOR pH MEASUREMENT
The electrode for pH measurement, generally in glass, generates an electrical signal proportional to the pH according to Nernst law. Of this signal the following aspects are considered:
Zero point: The pH where the electrode generates a potential of 0 mV. In most electrodes, this
value is found at about 7 pH.
Offset or Asymmetry Potential: represents the potential (in mV) generated by an electrode when immersed in a buffer solution at 7 pH. Generally oscillates between ± 20 mV.
Slope: response of the electrode expressed in mV per pH units. The theoretical electrode slope at
25°C is 59.16 mV/pH. When the electrode is new the slope is close to the theoretical value.
Sensitivity: it is the electrode's slope expression in relative terms. It is obtained by dividing the
actual value of the slope by the theoretical value, and is expressed as a %. The asymmetry potential and the slope vary in time with the use of the electrode, which necessitates regular calibration.
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The pH electrodes must be calibrated using the buffer solutions (see paragraph 4.2 pH electrode calibration).
The ORP and specific ion electrodes do not need calibration as their absolute voltage is measured. The ORP (REDOX) buffer solutions are only used to check the quality of an ORP (REDOX) electrode.
User calibration of the temperature sensor is not required: the sensor is calibrated in the factory and the Callendar Van Dusen parameters are recorded in the SICRAM module using the DO9847 multifunction device.
4.1.1 Automatic or manual pH compensation
In a correct measurement of pH, the results need to be expressed together with the temperature value at which the reading is performed. The electrode slope varies according to the temperature in a known mode according to Nernst law: e.g., a 1pH variation, that at 25°C means 59.16mV, at 100°C means 74.04mV.
6pH 7pH
pH
8pH
74.04mV
-74.04mV
59.16mV
-59.16mV
54.20mV
-54.20mV
0mV
mV
T=100°C, 74.04mV/pH
T=25°C, 59.16mV/pH
T=0°C, 54.20mV/pH
When a temperature probe is present, the instrument automatically applies the ATC function: automatic temperature compensation. To disable it, the temperature probe must be disconnected. If the temperature probe is not present, and the correct value is not entered manually, the extent of the error committed in pH measurement is proportional to temperature and pH value itself.
In absence of the temperature probe, the lower part of the display shows the manually set compensation temperature. By default it is equal to 25°C (see par. 4.1.2 how to manually change the temperature). To point this condition out, the °C or °F symbol blinks intermittently near the temperature value. Moreover, in the main line an "m" (that is, manual) is turned on near the battery symbol.
4.1.2 How to manually change the temperature
In absence of the temperature probe, it is possible to manually set the temperature. Proceed as follows:
press the °C/°F key once: the indicated temperature value starts blinking;
select the solution temperature value by using the arrows;
confirm by pressing DATA: the display stops blinking, and the temperature displayed is used
for compensation.
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During manual compensation, to change the unit of measurement between °C and °F, it is
necessary to press twice the °C/°F key.
4.2 pH ELECTRODE CALIBRATION
The electrode calibration is used to compensate the zero potential and slope departures to which the electrode is subject with time. The calibration frequency depends on the accuracy desired by the user and by the effects that the measured sample have on the electrode. Generally, we recommend daily calibration, but it is the user's responsibility from personal experience, to establish the most appropriate frequency.
The calibration may be carried out using 1, 2 or 3 points.
when using 1 point, the electrode offset is corrected;
with 2 points the offset and the gain is corrected;
finally, in case a three points calibration is carried out two offsets and two slopes are calculated,
the second point is the one in which the zero is performed.
The instrument has a memory of 3 buffers with relevant temperature compensation tables (ATC), one for the acid, one for the neutral, and one for the alkaline band:
@25°C
BUFR_1 (NEUTRAL)
6.860
BUFR_2 (ACID)
4.010
BUFR_3 (ALKALINE)
9.180
If electrode calibration was not carried out on the instrument, or the batteries have been changed or the last calibration failed, the display blinks the CAL message.
4.2.1 Calibration procedure
1) Insert the temperature probe and the electrode in the solution of a calibration buffer. If no
temperature probe is available, use another thermometer and enter the value manually as indicated in the paragraph 4.1.1.
2) The electrode calibration is started by pressing CAL.
3) Among the three prepared buffers, the instrument automatically detects the closest to the pH
value being read and flags it up on the lower part of the display. If the buffer is not detected the first buffer BUFR_1 is proposed.
4) At this point the CAL symbol is not blinking on the display and the following is shown from the upper side downward: a) the chosen buffer nominal value at 25°C (scrolling indication) b) the pH measurement value with the current calibration c) the temperature compensated buffer value
The detected and temperature compensated buffer value, shown in the lower line, can be modified using the arrows.
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5) Press DATA/ENTER to proceed with the calibration. The electrode offset mV value (OFFS) is shown on the display for few seconds. After a few seconds the instrument shows the measurement again, corrected according to the new calibration, but remains in calibration mode. Pressed repeatedly the DATA/ENTER key allows the calibration on the point to be repeated, for example, in order to obtain a more stable value.
6) To end the electrode calibration press pH/mV (ESC), or continue the calibration for the second point.
7) Extract the electrode from the buffer, clean it carefully, and insert it in the following buffer.
8) Press one time the °C/°F key (MENU).
9) The instrument displays the value detected on the new buffer: continue by repeating the steps
from point 3.
NOTES:
After calibration, the instrument displays an electrode quality indication:
- no signal: electrode functioning.
- a small square blinking on the lower right: electrode almost exhausted.
- two small squares blinking on the lower right: electrode exhausted to be replaced.
The 3 point calibration must always be carried out according to the fixed sequence: NEUTRAL>>ACID>>BASIC. The basic buffer must be the last in the sequence.
Without having pressed DATA/ENTER at all, the calibration is interrupted by pressing pH/mV (ESC); the previous values will continue to be used.
The buffers are always presented in the sequence set in the menu with the parameters:
- BUFR_1,
- BUFR_2,
- BUFR_3.
The 2 point calibration is possible using the sequence BUFR_1 - BUFR_2 or BUFR_2 - BUFR_3 or even BUFR_1 - BUFR_3.
The 3 point calibration is only possible using the exact sequence BUFR_1 - BUFR_2 - BUFR_3.
Allowed calibration sequences
1 BUFR_1 BUFR_2 BUFR_3
2 BUFR_1 - BUFR_2 BUFR_2 - BUFR_3 BUFR_1 - BUFR_3
Number of
calibration
points
3 BUFR_1 - BUFR_2 - BUFR_3
In any case where no operation is performed, the “calibration” mode automatically stops after 60 seconds.
If the calibration is rejected by the instrument because it is considered to be excessively corrupted, the CAL ERR message will appear, followed by a long beep. The instrument remains in calibration mode and maintains the previous calibration values: at this point, if the calibration is interrupted using pH-mV/ESC, the instrument signals the anomaly through the CAL message blinking.
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Temperature characteristics of Delta OHM buffer solutions
The 3 standard buffers are memorized in the instruments with relevant variations according to temperature: the characteristics of the three Delta Ohm standard buffers at 6.86pH, 4.01pH and
9.18pH (@25°C) are reported below.
6.86 pH @ 25°C 4.01 pH @ 25°C
°C pH °C pH °C pH °C pH
0 6.98 50 6.83 0 4.01 50 4.06
5 6.95 55 6.83 5 4.00 55 4.07 10 6.92 60 6.84 10 4.00 60 4.09 15 6.90 65 6.85 15 4.00 65 4.10 20 6.88 70 6.85 20 4.00 70 4.13 25 6.86 75 6.86 25 4.01 75 4.14 30 6.85 80 6.86 30 4.01 80 4.16 35 6.84 85 6.87 35 4.02 85 4.18 40 6.84 90 6.88 40 4.03 90 4.20 45 6.83 95 6.89 45 4.05 95 4.23
9.18 pH @ 25°C
°C pH °C pH
0 9.46 50 9.01
5 9.39 55 8.99 10 9.33 60 8.97 15 9.28 65 8.94 20 9.22 70 8.92 25 9.18 75 8.90 30 9.14 80 8.88 35 9.10 85 8.86 40 9.07 90 8.85 45 9.04 95 8.83
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4.3 Pt100 AND 2 WIRE Pt1000 TEMPERATURE PROBES
The instrument accepts the input of Platinum temperature probes with resistances of 100 (Pt100) and 1000Ω (Pt1000). The Pt100 are connected to 4 wires, the Pt1000 to 2 wires; the excitation current was chosen in order to minimize the sensor self-heating effects.
All probes with SICRAM module are calibrated in the factory; the 2 or 4 wire probes with direct input are checked for conformity with class A tolerance according to norm IEC751 - BS1904 ­DIN43760. For the temperature probes without SICRAM module (Pt100 4 wires, and Pt1000) the model configuration is required (please see the description of the Probe Type menu, chapter 3).
4.3.1 Temperature measurement
The response time for the measurement of the temperature in air is greatly reduced if the air is moving. If the air is still, stir the probe. Please remember that the response times in any case are longer than those for liquid measurements.
The temperature measurement by immersion is carried out by inserting the probe in the liquid for at least 60 mm; the sensor is housed in the end part of the probe.
In the temperature measurement by penetration the probe tip must be inserted to a depth of at least 60 mm, the sensor is housed in the end part of the probe.
NOTE: when measuring the temperature on frozen blocks it is convenient to use a mechanical tool to bore a cavity in which to insert the tip probe.
In order to perform a correct contact measurement, the measurement surface must be even and smooth, and the probe must be perpendicular to the measurement plane.
So as to obtain the correct measurement, the insertion of a drop of oil or heat-conductive paste between the surface and the probe is useful (do not use water or solvents). This method also improves the response time.
4.3.2 Connecting the TP47 connector for the 4 wire Pt100 and 2 wire Pt1000 probes
All probes produced by Delta Ohm are provided with a connector. The HD2305.0 instrument also work with direct 4 wire Pt100, and 2 wire Pt1000 probes manufactured by other producers: for the instrument connection is prescribed the TP47 connector to which the probe's wires should be welded.
The instructions to connect the Platinum probe to the TP47 module are provided below. The TP47 module is supplied complete with fairlead and gasket for 5 mm maximum diameter cables. Do the following to open the module and connect a probe:
1. unscrew the fairlead;
2. extract the gasket;
3. remove the label using a cutter;
4. unscrew the ring on the opposite side as illustrated in the figure:
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5. open the two module shells: the printed circuit to which the probe must be connected is
housed inside. On the left there are the 1…4 points on which the sensor wires must be welded. The JP1…JP4 jumpers are in the center of the board. These must be closed with a tin bead for some type of sensors:
1
2
3
4
Pt100 3 wires
Pt1000
Ni1000
Not Used
Caution! Before welding, pass the probe cable through the fairlead and gasket.
6. Weld the wires as shown in the table:
Sensor Board connection Jumper to close
Pt100 4 wires
4
JP4
3
JP3
1
JP1
2JP2
Pt100 4 wires
None
Pt1000 2 wires
JP4
4
JP3
3
JP1
1
JP22
Pt1000 2 wires
JP2
Ensure the welds are clean and perfect.
7. Once the welding operation is complete, close the two shells;
8. insert the gasket in the module;
9. screw the fairlead and the ring. Make sure the cable is not twisted while you are screwing
the fairlead. Now the probe is ready.
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4.3.3 Direct connection of 4 wire Pt100 sensors
4 wire Pt100 sensors can be soldered directly
to the pins of the flying female connector without making use of the TP47 board. The 4 wires of the Pt100 sensors have to be soldered as indicated in the figure on the left. In order to use this type of probe it is necessary to set up the menu item “Probe Type” as described at page 9. The P100 probe is recognized upon turning on the instrument: connect the probe when the instrument is switched off and then turn it on.
Sensor Direct soldering to the connector
Pt100 4
wires
View of the soldering side
of the flying female connector
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5. WARNINGS
1. Do not expose the probes to gases or liquids that could corrode the material of the sensor or the
probe itself. Clean the probe carefully after each measurement.
2. Do not bend the probe connectors or force them upward or downward.
3. Do not bend or force the contacts when inserting the probe connector into the instrument.
4. Do not bend, deform or drop the probes, as this could cause irreparable damage.
5. Always select the most suitable probe for your application.
6. Do not use the temperature probes in presence of corrosive gases or liquids. The sensor
container is made of AISI 316 stainless steel, while the contact probe container is made from AISI 316 stainless steel plus silver. Avoid contact between the probe surface and any sticky surface or product that could corrode or damage it.
7. Above 400°C and below –40°C, avoid violent blows or thermal shocks to Platinum temperature
probes as this could cause irreparable damage.
8. To obtain reliable measurements, temperature variations that are too rapid must be avoided.
9. Temperature probes for surface measurements (contact probes) must be held perpendicular
against the surface. Apply oil or heat-conductive paste between the surface and the probe in order to improve contact and reduce reading time. Whatever you do, do not use water or solvent for this purpose. A contact measurement is always very hard to perform. It has high levels of uncertainty and depends on the ability of the operator.
10. Temperature measurements on non-metal surfaces usually require a great deal of time due to the
low heat conductivity of non-metal materials.
11. Probes are not insulated from their external casing; be very careful not to come into contact with
live parts (above 48V). This could be extremely dangerous for the instrument as well as for the operator, who could be electrocuted.
12. Avoid taking measurements in presence of high frequency sources, microwave ovens or large
magnetic fields; results may not be very reliable.
13. Clean the probe carefully after use.
14. The instrument is water resistant and IP67, but should not be immersed in water. The probe
connectors must be fitted with sealing gaskets. Should the instrument fall into the water, check for any water infiltration. Gently handle the instrument in such a way as to prevent any water infiltration from the connectors' side.
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6. INSTRUMENT SIGNALS AND FAULTS
The following table lists all error indications and information displayed by the instrument and supplied to the user in different operating situations:
Display indications Explanation
>>>_PRBE_TYPE
type of probe connected
BATT TOO LOW - CHNG NOW
battery discharged - replace it immediately
BAUDRATE >>>
baud rate value
BUFR_1
first buffer value
BUFR_2
second buffer value
BUFR_3
third buffer value
CAL
LOST
Program error: it appears after turning on for a few seconds. Contact the instrument's supplier.
CAL
blinking
Calibration not completed correctly.
CAL ERR
calibration error
ERR
This message appears if the pH measurement exceeds the
-2.000pH…19.999pH limits, if the mV measurement exceeds the ±2.4V limits, if the temperature probe, already detected by the instrument, is disconnected. At the same time an intermittent beep is issued.
FUNC CLRD
max, min and average values cleared
NEW_PROB_DET
new probe detected
OFFS
offset
OVER
Measurement overflow: this appears when the probe measures a value exceeding the measurement range or the mV measurement is included in the +2.0…+2.4V range.
PLS_EXIT >>> FUNC
RES_FOR_FACT ONLY
please exit using ESC >>> function reserved to factory calibration
PRBE_SER #### ####
serial number #### #### of the connected probe
PROB
ERR
A probe with SICRAM module has been inserted when not admissible for that specific instrument.
PROB COMM LOST
This appears if the probe, has already been detected by the instrument, but is disconnected. At the same time an intermittent beep is issued.
SLPE%
gain %
SYS
ERR
#
Instrument management program error. Contact the instrument's supplier and communicate the numeric code # reported by the display.
UNDR
Measurement overflow: this appears when the mV measurement is included in the -2.4…-2.0V range.
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7. INSTRUMENT STORAGE
Instrument storage conditions:
Temperature: -25…+65°C.
Humidity: less than 90%RH without condensation.
Do not store the instrument in places where:
humidity is high;
the instrument may be exposed to direct sunlight;
the instrument may be exposed to a source of high temperature;
the instrument may be exposed to strong vibrations;
the instrument may be exposed to steam, salt or any corrosive gas.
The instrument case is made of ABS plastic: do not use any incompatible solvent for cleaning.
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8. LOW BATTERY WARNING AND BATTERY REPLACEMENT
The battery symbol on the display constantly shows the battery charge status. To the extent that batteries have discharged, the symbol "empties". When the charge decreases still further it starts blinking.
In this case, batteries should be replaced as soon as possible. If you continue to use it, the instrument can no longer ensure correct measurement. The memory data are maintained.
If the battery charge level is insufficient, the following message appears when you turn the instrument on:
BATT TOO LOW
CHNG NOW
The instrument issues a long beep and turns off. In this case, replace the batteries in order to turn the instrument back on.
To replace the batteries, proceed as follows:
1. switch the instrument off;
2. unscrew the battery cover counter clockwise;
3. replace the batteries (3 1.5V alkaline batteries - type AA);
4. screw the cover on clockwise.
Malfunctioning upon turning on after battery replacement
After replacing the batteries, the instrument may not restart correctly; in this case, repeat the operation. After disconnecting the batteries, wait a few minutes in order to allow circuit condensers to discharge completely; then reinsert the batteries.
8.1 WARNING ABOUT BATTERY USE
Batteries should be removed when the instrument is not used for an extended time.
Flat batteries must be replaced immediately.
Avoid batteries leaking.
Always use good quality leakproof alkaline batteries. Sometimes on the market, it is
possible to find new batteries with an insufficient charge capacity.
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9. NOTES ABOUT WORKING AND OPERATIVE SAFETY
Authorized use
The technical specifications as given in chapter TECHNICAL CHARACTERISTICS must be observed. Only the operation and running of the measuring instrument according to the instructions given in this operating manual is authorized. Any other use is considered unauthorized.
General safety instructions
This measuring system is constructed and tested in compliance with the EN 61010-1 safety regulations for electronic measuring instruments. It left the factory in a safe and secure technical condition. The smooth functioning and operational safety of the measuring system can only be guaranteed if the generally applicable safety measures and the specific safety instructions in this operating manual are followed during operation. The smooth functioning and operational safety of the instrument can only be guaranteed under the environmental and electrical operating conditions that are in specified in chapter TECHNICAL CHARACTERISTICS.
Do not use or store the product in places such as listed below:
Rapid changes in ambient temperature which may cause condensation.
Corrosive or inflammable gases.
Direct vibration or shock to the instrument.
Excessive induction noise, static electricity, magnetic fields or noise.
If the measuring system was transported from a cold environment to a warm environment, the formation of condensate can impair the functioning of the measuring system. In this event, wait until the temperature of the measuring system reaches room temperature before putting the measuring system back into operation.
Obligations of the purchaser
The purchaser of this measuring system must ensure that the following laws and guidelines are observed when using dangerous substances:
EEC directives for protective labour legislation National protective labour legislation Safety regulations
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10. TECHNICAL CHARACTERISTICS
10.1 TECHNICAL INFORMATION ON THE pH METER THERMOMETER
Instrument
Dimensions (Length x Width x Height) 140x88x38mm
Weight 160g (complete with batteries)
Material ABS
Display 2x4½ digits plus symbols
Visible area: 52x42mm
Operating conditions
Operating temperature -5…50°C
Warehouse temperature -25…65°C
Working relative humidity 0…90%RH without condensation
Protection degree IP67
Power
Batteries 3 x 1.5V type AA batteries
Autonomy 200 hours with 1800mAh alkaline
batteries
Power absorbed with instrument off < 20μA
Connections
Input module for the temperature probes 8-pole male DIN45326 connector
pH/mV input Female BNC
Unit of Measurement pH - mV
°C - °F;
Measurement of pH by Instrument
Measurement range -2.00…+19.999pH
Resolution 0.01
Accuracy ±0.01pH ±1digit
Input impedance >10
12
Ω
Calibration error @25°C |Offset| > 20mV
Slope < 50mV/pH or Slope > 63mV/pH
Sensitivity < 85% or Sensitivity > 106.5%
Measurement of mV by Instrument
Measurement range -1999.9…+1999.9mV
Resolution 0.1mV
Accuracy ±0.1mV ±1digit
Drift after 1 year 0.5mV/year
Measurement of temperature by Instrument
Pt100 measurement range -200…+650°C
Pt1000 measurement range -200…+650°C
Resolution 0.1°C
Accuracy ±0.1°C ±1digit
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Drift after 1 year 0.1°C/year
EMC standard regulations
Security EN61000-4-2, EN61010-1 level 3
Electrostatic discharge EN61000-4-2 level 3
Electric fast transients EN61000-4-4 level 3,
EN61000-4-5 level 3
Voltage variations EN61000-4-11
Electromagnetic interference susceptibility IEC1000-4-3
Electromagnetic interference emission EN55020 class B
10.2 ON LINE INSTRUMENT PROBES AND MODULES TECHNICAL DATA
10.2.1 Temperature probes Pt100 and SICRAM module
Model Type Application range Accuracy
TP87 Immersion
-50°C…+200°C ±0.25°C (-50°C…+200°C)
TP472I.0 Immersion
-50°C…+400°C
±0.25°C (-50°C…+350°C)
±0.4°C (+350°C…+400°C)
TP473P.0 Penetration
-50°C…+400°C
±0.25°C (-50°C…+350°C)
±0.4°C (+350°C…+400°C)
TP474C.0 Contact
-50°C…+400°C
±0.3°C (-50°C…+350°C)
±0.4°C (+350°C…+400°C)
TP475A.0 Air
-50°C…+250°C ±0.3°C (-50°C…+250°C)
TP472I.5 Immersion
-50°C…+400°C
±0.3°C (-50°C…+350°C)
±0.4°C (+350°C…+400°C)
TP472I.10 Immersion
-50°C…+400°C
±0.3°C (-50°C…+350°C)
±0.4°C (+350°C…+400°C)
Common characteristics
Resolution 0.1°C Temperature drift @20°C 0.003%/°C
10.2.2 4 wire Pt100 and 2 wire Pt1000 Probes
Model Type Application range Accuracy
TP87.100 4 wire Pt100 -50…+200°C Class A
TP87.1000 2 wire Pt1000 -50…+200°C Class A
Common characteristics
Resolution 0.1°C Temperature drift @20°C 0.005%/°C
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11. ORDER CODES
HD2305.0KE The kit is composed of: instrument HD2305.0, KP30 electrode, TP87
temperature probe, 4.01pH and 6.86pH buffer solutions, 3 1.5V alkaline
batteries, operating manual and case.
HD2305.0K The kit is composed of: instrument HD2305.0, TP87 temperature probe, 3 1.5V
alkaline batteries, operating manual and case. The electrodes and the solutions
must be ordered separately.
11.1 PH ELECTRODES
KP20 Combined pH electrode, gel-filled, with screw connector S7, body in Epoxy,
Ag/AgCl sat. KCl.
KP30 Combined pH electrode, cable 1m, gel-filled, body in Epoxy, Ag/AgCl sat. KCl.
KP60 Combined pH electrode, 1 diaphragm, gel-filled, with screw connector S7, body
in glass, Ag/AgCl sat. KCl.
KP61 Combined pH electrode, 3 diaphragms for milk, cream, etc. gel-filled, with screw
connector S7, body in glass, Ag/AgCl sat. KCl.
KP62 Combined pH electrode, 1 diaphragm for pure water, paints, etc. gel-filled, with
screw connector S7, body in glass, Ag/AgCl sat. KCl.
KP70 Combined pH electrode, micro diam. 6 x L=70 mm, gel-filled, with screw
connector S7, body in glass, Ag/AgCl sat. KCl.
KP80 Combined pointed pH electrode, gel-filled, with screw connector S7, body in
glass, Ag/AgCl sat. KCl.
CP Extension cable 1.5m with BNC connectors on one side and S7 on the other side
for electrode without cable.
CE Screw connector S7 for pH electrode.
BNC Female BNC for electrode extension.
11.2 ORP ELECTRODES (REDOX)
KP90 ORP PLATINUM electrode (REDOX), with screw connector S7, gel-filled, body
in glass.
11.3 PH BUFFER SOLUTIONS
HD8642 Buffer solution 4.01pH - 200cc.
HD8672 Buffer solution 6.86pH - 200cc.
HD8692 Buffer solution 9.18pH - 200cc.
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11.4 ORP BUFFER SOLUTIONS (REDOX)
HDR220 ORP buffer solution (REDOX) 220mV 0.5 l.
HDR468 ORP buffer solution (REDOX) 468mV 0.5 l.
11.5 TEMPERATURE PROBES COMPLETE WITH SICRAM MODULE
TP87 Pt100 sensor immersion probe. Probe's stem Ø 3 mm, length 70 mm. Cable length
1 metre.
TP472I.0 Pt100 sensor immersion probe. Stem Ø 3 mm, length 230 mm. Cable length 2
metres.
TP473P.0 Pt100 sensor penetration probe. Stem Ø 4 mm, length 150 mm. Cable length 2
metres.
TP474C.0 Pt100 sensor contact probe. Stem Ø 4 mm, length 230 mm, contact surface Ø 5
mm. Cable length 2 metres.
TP475A.0 Pt100 sensor air probe. Stem Ø 4 mm, length 230 mm. Cable length 2 metres.
TP472I.5 Pt100 sensor immersion probe. Stem Ø 6 mm, length 500 mm. Cable length 2
metres.
TP472I.10 Pt100 sensor immersion probe. Stem Ø 6 mm, length 1000 mm. Cable length 2
metres.
11.6 TEMPERATURE PROBES WITHOUT SICRAM MODULE
TP87.100 Pt100 sensor immersion probe. Probe's stem Ø 3 mm, length 70 mm. Connection
cable 4 wires with connector, length 1 metre.
TP87.1000 Pt1000 sensor immersion probe. Probe's stem Ø 3 mm, length 70 mm. Connection
cable 2 wires with connector, length 1 metre.
TP47 Only connector for probe connection: direct 4 wire Pt100, 2 wire Pt1000.
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GARANZIA GUARANTEE
GARANTIE
GARANTIA
Questo certificato deve accompagnare l'apparecchio spedito al centro assistenza. IMPORTANTE: La garanzia è operante solo se il presente tagliando sarà compilato in tutte le sue parti.
This guarantee must be sent together with the instrument to our service centre. N.B.: Guarantee is valid only if coupon has been correctly filled in all details.
Le certificat doit porter le cachet du revendeur et la date d'achat. A défaut, la garantie sera comptée à partir de la date de la sortie d'usine.
ATTENTION: Pour bénéficier de la garantie, le présent certificat doit obligatoirement accompagner l'appareil présumé défectueux.
Dieser Garantieschein muss der Spedition beigelegt werden, wenn das Gerät an das Kundendienstzentrum gesandt wird.
WICHTIG: Die Garantie ist nur gültig, wenn dieser Abschnitt bis ins Einzelne ausgefüllt ist.
Este certificado debe acompañar al aparato enviado al centro de asistencia. IMPORTANTE: La garantía es válida solo si el presente cupón ha sido completado en su totalidad.
Instrument type
HD2305.0
Serial number
RENEWALS
Date Date
Inspector Inspector
Date Date
Inspector Inspector
Date Date
Inspector Inspector
CE CONFORMITY
Safety
EN61000-4-2, EN61010-1 LEVEL 3
Electrostatic discharge EN61000-4-2 LEVEL 3
Electric fast transients EN61000-4-4 LEVEL 3
Voltage variations EN61000-4-11
Electromagnetic interference susceptibility IEC1000-4-3
Electromagnetic interference emission EN55020 class B
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