DataApex GC-2014C User Manual

Clarity Controls
Shimadzu GC-2014C
GC ENG
Date: 13.5.2008
Phone: +420 251 013 400 DataApex Ltd. 2008 Fax: +420 251 013 401 Podohradska 1 clarity@dataapex.com 155 00 Prague 5 www.dataapex.com The Czech Republic
Clarity®, DataApex® and ® are trademarks of DataApex Ltd. Microsoft® and WindowsTM are trademarks of Microsoft Corporation.
DataApex reserves the right to make changes to manuals without prior notice. Updated manuals can be downloaded from www.dataapex.com.
Author: DM
Shimadzu GC-2014C
Contents
Contents
1 Shimadzu GC-2014C Control module .....................................1
2 Requirements ........................................................................2
3 Installation Procedure............................................................3
3.1 Hardware - Wiring ................................................................. 3
3.2 Shimadzu GC-2014C setup - communication ........................3
3.3 Clarity Configuration .............................................................4
4 Using the control module .......................................................6
4.1 Hardware Configuration......................................................... 6
4.2 Method Setup - GC ................................................................ 7
4.2.1 Oven/Zones .................................................................... 7
4.2.2 INJ 1(2) ........................................................................... 8
4.2.3 DET 1 (..4)....................................................................... 9
4.2.4 Time Events .................................................................. 11
4.2.5 Pre Run......................................................................... 13
4.2.6 Other ............................................................................ 14
4.2.7 Gradients ...................................................................... 16
4.3 Method Setup - Acquisition.................................................. 17
4.4 Device Monitor..................................................................... 18
4.5 Shimadzu GC-2014C Setup ................................................. 19
5 Report Setup........................................................................ 24
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Contents
Shimadzu GC-2014C
To facilitate the orientation in the Shimadzu GC-2014C manual and Clarity station, different fonts are used throughout the manual. Meanings of these fonts are:
Instrument (blue text) marks the name of the window, to which the text refers.
Open File (dark brown bold) describes the commands and names of fields in Clarity.
chromatography
WORK1 (capitals) indicates the name of the file and/or directory.
ACTIVE (orange capital italics) marks the state of the station or its part.
Administrator (green italics) refers to a value or text inserted into a field.
The bold text is sometimes also used for important parts of the text and the name of the Clarity station. Moreover, there are text sections written in format other than normal text. These sections are closed in boxes with the appropriate pictogram:
- Note - notifies the reader of possibly interesting information.
- Caution - warns the user of possibly dangerous or very important information.
- Question - marks the problem statement or trouble question.
- Answer - marks the response to the question.
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Shimadzu GC-2014C
1 Shimadzu GC-2014C Control module
1 Shimadzu GC-2014C Control module
This manual describes the setting of the Shimadzu GC­2014C chromatograph. The control module enables direct
control of the instrument over serial line.
Fig. 1 Shimadzu GC-2014C (with AOC-20i autosampler)
Shimadzu GC-2014C control module provides the means for the direct control of the Shimadzu GC-2014C chromatograph. It allows a limited control of the GC-2014 and GC-2010 - only the digital data acquisition and temperature zone control is supported at the moment, the APC (automatic pressure control) and AFC (automatic flow control) parameters must be set from the GC keyboard.
1
2 Requirements
2 Requirements
Clarity Installation CD ROM with GC Control module (p/n
A23).
Free serial COM port in the PC.
Modern computers usually have only 1 (if any) serial (COM) port installed. To use more devices requiring the port, the MultiCOM adapter (p/n MC01) is available.
Serial cross DB9F-DB9F cable (p/n SK01).
Cables are not part of Clarity Control Module. It is strongly recommended to order required cables together with the Control Module.
Clarity Controls
2
Shimadzu GC-2014C
3 Installation Procedure
3.1 Hardware - Wiring
Start and Ready signals are communicated with Clarity through the Serial cross DB9F-DB9F cable, so it is not necessary to connect additional starting cables. The signal cable has to be connected according to the following scheme. In a set with the Autosampler synchronization cables might be necessary.
Typical connections of a set with Autosampler can be found in the Getting Started manual (chapter Device Setup and Wiring).
Typical serial cable wiring is described in the picture.
3 Installation Procedure
Fig. 2 Serial cross cable DB9F – DB9F
3.2 Shimadzu GC-2014C setup - communication
The GC must be fully configured prior to connecting to
Clarity. No special settings have to be made on the Shimadzu GC-2014C chromatograph, only the
communication protocol of the instrument (set on the FUNC key screen by using 6. GC CONFIGURATION - 3. TRANSMISSION PARAMETER) has to be set to LEVEL3. Baud rate set in the instrument must correspond to the
Baud Rate set in the
locally connected instruments with short interconnecting cable the Baud Rate set as default (115200) is recommended. With the rising length of the cable or when connected via the network the Baud Rate should be set lower.
Shimadzu GC-2014C Setup dialog. For
3
3 Installation Procedure
3.3 Clarity Configuration
Menu Path: Clarity -> System -> Configuration
In the System Configuration dialog press the Add button to
invoke the Available Control Modules dialog.
Clarity Controls
Fig. 3 Available Control Modules
Select the Shimadzu GC-2014C in the GC section and press
the Add button.
The
Shimadzu GC-2014C Setup dialog will appear.
Fig. 4 Shimadzu GC-2014C Setup
4
Shimadzu GC-2014C
Fill in the Port, Baud Rate and Name according to the
settings and the connection of the GC (for more details see chapter Shimadzu GC-2014C Setup on pg. 19).
Press the Autodetect button to read all settings from the
instrument and apply them in the dialog.
It is strongly recommended not to change the settings gained through the Autodetect function. When opening the
Instrument window, those settings are checked against the
settings of the GC and in case they are not the same the warning message is issued and no control is possible.
Switch to the Signals tab (for more details see the Shimadzu
GC-2014C Setup
dialog section later in the manual), select the
correct number of signals you want to acquire, name them and possibly check the Enable to start device(s) from
Clarity checkbox. Press the OK button.
The Shimadzu GC-2014C item
Control Modules list of the
Drag the GC icon from the Setup Control Modules list on
the left side to the desired Instrument tab side
, or use the button to do so.
3 Installation Procedure
Shimadzu GC-2014C Setup
will appear in the Setup
System Configuration dialog.
on the right
Fig. 5 System Configuration
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