Cole-Parmer 03013-01, 03013-06 Instruction Manual

Analog Melting Point
Apparatus

User Guide

Version 1.2

Instructions for use

1. Insert the thermometer.

2. Insert a 1.9mm sealed end capillary tube with sample into block.

3. Set the heating controller to 20°C/min.

4. Reduce to 10°C/min once the thermometer reaches 60% of the expected melting point.

5. Continue to reduce so heating rate is on 1°C/min when within 15°C of expected melt.

6. Observe the melt through the eyepiece, while recording the temperature on the thermometer.

7. Turn off to begin cooling. A brass plug can be used if more rapid cooling is required.

Heating control dial

IEC power inlet socket (at rear)

Magnifying lens

Capillary tube

Thermometer

Thermometer
support

Figure 1

Figure 2

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Analog Melting Point Apparatus

Introduction

Thank you for purchasing this Cole-Parmer product. To get the best performance from the
equipment, and for your own safety, please read these instructions carefully before use.
Before discarding the packaging check that all parts are present and correct.

This equipment is designed to operate under the following conditions:

❖ For indoor use only

❖ Use in a well ventilated area

❖ Ambient temperature range 5°C to 40°C (41°F to 104°F)

❖ Altitude to 2000 m (6500 ft)

❖ Relative humidity not exceeding 80%

❖ Power supply fluctuation not exceeding 10% of nominal

❖ Overvoltage category II IEC60364-4-443

❖ Pollution degree 2 IEC664

❖ Use with a minimum distance all round of 200 mm (8 in.) from walls or other items

If the equipment is not used in the manner described in this manual and with accessories other than
those recommended by the manufacturer, the protection provided may be impaired.

Electrical Installation

THIS EQUIPMENT MUST BE GROUNDED

Before connection please ensure that the line supply corresponds to that shown on the
rating plate.

Power requirements

120 V Models 230 V Models

03013-01 50 W 03013-06 50 W

The 120 V Models are provided with a NEMA 5-15 plug. The 230 V Models are provided with a UK
3-pin and a “Schuko” 2-pin plug. Should the cable not be suitable for connecting to the power
supply, replace the plug with a suitable alternative.

THIS OPERATION SHOULD ONLY BE UNDERTAKEN BY A QUALIFIED ELECTRICIAN.

NOTE: Refer to the equipment rating plate to ensure that the plug and fusing are suitable for the

voltage and wattage stated.

The wires in the power cable (120 V) are colored as follows:
BLACK - HOT/LIVE
WHITE - NEUTRAL
GREEN - EARTH

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The wires in the power cable (230 V) are colored as follows:
BROWN - HOT/LIVE
BLUE - NEUTRAL
GREEN/YELLOW - EARTH

IF IN DOUBT CONSULT A QUALIFIED ELECTRICIAN

Should the power cable need replacing, a cable of 1mm
an IEC320 plug should be used.

The appropriate power cable should be connected BEFORE connection to the power supply.

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of harmonized code H05W-F connected to

General Description

The Cole-Parmer Analog Melting Point Apparatus has been designed to be quick and easy to
operate – making it ideal for educational use. Supplied with a nonhazardous, spirit-filled mercury-free
thermometer. Using the manually adjustable heating rate, the block will rapidly heat samples up to
20°C per minute to the melt temperature and up to the maximum temperature of 250°C. An accurate
reading to within 1°C of the melt temperature can be achieved by using a slower heating rate of
between 1 and 10°C per minute. The sample is observed through the magnifying lens until the melt
occurs and the melt temperature read from the thermometer. Up to three samples can be viewed and
tested at any one time. Samples are illuminated by a bright white LED and viewed via a magnifying
lens. The magnifying lens can be detached for cleaning using the simple instructions printed on the
instrument.

Available separately are packs of capillary tubes that have been pre-sealed, a brass plug to speed
cooling time and spare thermometers. Please visit the Cole-Parmer website www.coleparmer.com for
further information.

Safety Advice

Users should be aware of the following safety advice:

❖ HIGH TEMPERATURES ARE DANGEROUS as they can cause serious burns to operators and

ignite combustible material.

❖ USE CARE AND WEAR PROTECTIVE GLOVES TO PROTECT HANDS.

❖ DO NOT use combustible substances near hot objects.

❖ NEVER lift or carry the instrument until it has been switched off and allowed to cool for at least 30

minutes. The thermometer markings will give guidance.

❖ The unit should be carried using both hands with the fingers under the side edges.

❖ NEVER move or carry the unit while still connected to the power supply.

❖ DO NOT position the unit such that it is difficult to disconnect it from the power by removing the

power cable from the socket at the back.

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