CHEMetrics V-2000 Operator's Manual

OPERATORS MANUAL
V-2000 Photometer
CHEMetrics, Inc.
4295 Catlett Road Calverton, Virginia 20138 Toll Free 1-800-356-3072
Phone: 540-788-9026
Fax: 540-788-4856
Sept. 09, Rev. 13
Table of Contents
Chapter 1 - Introduction
1-1 Battery Installation .................................. 1
1-2 Sample Cell Adapters ................................ 1
1-3 LCD Display ....................................... 2
1-4 Keypad ........................................... 3
1-5 Program Number Designation ......................... 4
Chapter 2 - Setup Menu Functions
2-1 Blank............................................. 5
2-2 Verify ............................................ 5
2-3 Digits............................................. 5
2-4 Clock............................................. 6
2-5 Set Baud.......................................... 6
2-6 Print ............................................. 6
2-7 Auto Print ......................................... 7
2-8 Auto Log .......................................... 7
2-9 Self-Test .......................................... 7
2-10 Upload ........................................... 7
Chapter 3 - Setup and Measurement Procedures
3-1 General Operating Instructions ......................... 8
3-2 Procedure A - Zeroing, Program Selection and Measuring . . . 8
3-3 Procedure B - Zeroing, Program Selection, Setting Reagent Blank
and Measuring ................................... 9
Chapter 4 - Data Logging
4-1 Logging Data Manually ............................... 10
4-2 Logging Data Automatically ........................... 10
4-3 Displaying the Log .................................. 10
4-4 Clearing the Log .................................... 10
Chapter 5 - Use with Printers and Computers
5-1 Printing Logged Data Directly to a Printer ................. 11
5-2 Downloading Logged Data to a Computer ................ 11
5-3 Uploading Method Revisions .......................... 12
Chapter 6 - Error Messages .................................. 14
Chapter 7 - Custom User Programs
7-1 Creating a Custom User Program ...................... 15
7-2 Calibrating a Custom User Program ..................... 15
7-3 Replacing or Reviewing a Custom User Program .......... 16
Chapter 8 - Specifications & Features ......................... 17
Chapter 9 - Product Information
9-1 Instrument & Accessories ............................. 18
9-2 Warranty Information ................................ 18
9-3 European Union’s WEEE Directive 2002/96/EC ............ 18
9-4 List of Supported Parameters .......................... 19
Chapter 1
Introduction
1-1 Battery Installation
The V-2000 requires 4 AA alkaline or lithium batteries. With alkaline batteries, the expected life is 2,500 hours of operation. With lithium batteries, the expected life is 10,000 hours of operation. The V-2000 has a battery saving auto-shutoff feature that turns the instrument off after 20 minutes of non-use. Remove batteries when photometer is not in use.
To install batteries, carefully loosen the 2 captive screws on the battery cover (back of instrument). Remove the cover, and insert the batteries with the correct orientation as illustrated in the battery compartment. Replace the battery cover and replace the captive screws.
1-2 Sample Cell Adapters
The V-2000 comes with 2 sample cell adapters: 13 mm adapter for Vacu-vials; 16 mm adapter for COD Vials. The adapters ensure correct alignment of the ampoule or vial being used. If the ampoule or vial is not aligned correctly (i.e. wrong adapter or no adapter is used), measurement errors will occur.
To insert an adapter, the male tabs on the adapter (left and right sides) should be matched up with the alignment slots to the left and right of the sample cell compartment. Insert the adapter with the correct alignment and push down firmly until it snaps into place.
Important Note: Above the sample cell compartment, the instrument says
cuvette adapter = lock-unlock <”. Disregard this message!
There is no lock, unlock feature to the current cell adapters. They go straight in and out. DO NOT attempt to turn the adapter from left to right when inserting it or removing it.
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1-3 LCD Display
1 calibrate Displays when the instrument is in the calibration mode 2 setup Displays when the instrument is in the setup mode 3 measure Displays when the instrument is taking a measurement 4 zero Displays when the instrument is zeroing 5 blank Displays when a blank is active for a selected method 6 units Displays the chosen unit of measure 7 ? Displays when the instrument is prompting the user for a response 8 timer Displays when the timer is active
9 log Displays if data is stored in the log 10 battery Displays if battery is low 11 print Displays when the instrument is printing (or downloading) 12 verification Displays when the instrument is in the verification mode 13 XXX program Displays the active program number
14 ЗЗЗЗЗЗЗЗ Alphanumeric display
15 -8.8:8.8 Numeric display 16 range Displays to indicate over range condition
2
1-4 Keypad
KEY FUNCTION
power Turns the instrument on or off print / 0 Initiates print mode or inputs a 0 yes / . Confirms a selection, functions as Enter key, or inputs a decimal point units / 1 Allows selection of unit of measure or inputs a 1 log / 2 Initiates data log mode or inputs a 2
? / 3 Scroll down or inputs a 3
setup / 4 Allows access to user selectable functions (Blank, Verify, Digits, Clock, Set
Baud, Print, AutoPrint, Auto Log, Self-Test, Upload, User Prgm, Cal User) or inputs a 4
timer / 5 Initiates timer, allows access to time/date and stopwatch or inputs a 5
> / 6 Scroll up or inputs a 6
prgm / 7 Initiates program number input or inputs a 7 zero / 8 Initiates a zero measurement or inputs an 8 meas / 9 Initiates a measurement or inputs a 9
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1-5 Program Number Designation
The V-2000 offers the user access to approximately 50 pre-programmed water analysis methods for use in conjunction with Vacu-vials ampoules and COD Vials (program numbers 5 -189 reserved for this function). For these pre-programmed methods, the instrument gives direct readout test results.
The V-2000 also offers the user the option of taking readings in absorbance or % Transmittance at each of the 4 available wavelengths (program numbers 1 - 4). Absorbance readings can then be used to generate a user specific calibration equation. A scientific calculator or software package with a linear regression function can be used to convert absorbance units to concentration values.
Finally, the V-2000 offers the user the ability to store up 10 user specific custom methods.
Program Number Designation
0 manual zeroing; equivalent to using the zero key
1 420 nm absorbance or % Transmittance 2 520 nm absorbance or % Transmittance 3 580 nm absorbance or % Transmittance 4 610 nm absorbance or % Transmittance 5-189 pre-programmed water analysis methods 190-199 user generated custom methods
4
Chapter 2
Setup Menu Functions
To view the Setup menu functions, press the setup key and use the or – keys to scroll through
the list of functions.
2-1 Blank
The blank function is employed for specific methods that require the generation and use of a reagent blank ampoule or vial. The following methods require the use of this function: Aluminum, Chloride, COD, Fluoride, Hydrazine, Ozone 2 (K-7413). The procedure for using the blank function is found in Chapter 3, Section 3-3 Procedure B - Zeroing, Program Selection, Setting Reagent Blank and Measuring.
If the blank is accidentally set (blank icon appears on the LCD display for a method other than one of the 5 listed above), it is important to clear the blank before running the method.
To Clear Blank:
1. Press the setup key and use the or – keys until “BLANK” is displayed, then press the yes
key.
2. “SET BLNK?” will be displayed.
3. Use the or – keys to toggle from “SET BLNK?” to “CLR BLNK”. When “CLR BLNK” is
displayed, press the yes key.
4. “CLEARED” will be displayed.
5. Press the meas key to exit the setup menu.
2-2 Verify
Disregard this function. It offers no added value to the instrument user.
2-3 Digits
The digits function allows the user to select the resolution of the reading (the number of significant digits in the displayed test result): 0.000, 0.00, 0.0, and 0. The default setting for this function is
0.000, however the test range on the parameter specific test kit instructions and in the List of Supported Parameters in Chapter 9 of this manual is displayed with the suggested number of significant digits for each particular method.
NOTE: The digits resolution setting on the V-2000 is not method specific, and therefore must be
reset as needed when moving from one preprogrammed method to another.
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1. Press the setup key and use the or – keys until “DIGITS” is displayed, then press the yes
key.
2. Use the or – keys until the desired resolution is displayed, then press the yes key.
3. Press the meas key to exit the setup menu.
2-4 Clock
The clock function allows the user to set the time and date.
1. Press the setup key and use the or – keys until “CLOCK” is displayed, then press the yes
key.
2. “20__” will be displayed. Enter the year.
3. “__Month” will be displayed. Enter the month.
4. “__Day” will be displayed. Enter the day.
5. “__:__ (24) hour” will be displayed. Enter the time.
6. Press the meas key to exit the setup menu.
2-5 Set Baud
The set baud function allows the user to select the baud rate:1200, 2400, 4800, and 9600. The default setting for this function is 1200.
1. Press the setup key and use the or – keys until “SET BAUD” is displayed, then press the yes key.
2. Use the or – keys until the desired baud rate is displayed, then press the yes key.
3. Press the meas key to exit the setup menu.
2-6 Print
The print function allows the user to select the printout format. The user can select between a standard printout (used if printing directly to a printer) and a comma delimited format (used for importing data into a spreadsheet).
1. Press the setup key and use the or – keys until “PRINT” is displayed, then press the yes
key.
2. Use the or – keys to toggle between “STND PRN” and “CMA DELM”. When the desired
printout format is displayed, press the yes key.
3. Press the meas key to exit the setup menu.
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2-7 Auto Print
The auto print function allows the user to automatically send readings to a printer.
1. Press the setup key and use the or – keys until “AUTO PRT” is displayed, then press the yes key.
2. Use the or – keys to toggle between “AUTO OFF” and “AUTO ON”. When the desired
printing function is displayed, press the yes key.
3. Press the meas key to exit the setup menu.
2-8 Auto Log
The auto log function allows the user to automatically save up to 100 test results in the
photometer’s memory. The procedure for using the auto log function is found in Chapter 4, Section 4-2 Logging Data Automatically.
2-9 Self-Test
The self-test function puts the photometer into self-diagnostic mode. It is not recommended as a routine test, but rather as a troubleshooting tool to be used if the unit gives an error message, produces a suspect test result or in any way malfunctions. If an instrument fails any portion of the self-test, contact CHEMetrics Technical Services Department.
1. Before initiating the self-test, the sample cell adapter must be removed and the light shield must be in place.
2. Press the setup key and use the or – keys until “SELFTEST” is displayed, then press the yes key.
3. The instrument will display “KBD TEST”. Then it will prompt the user to press each of the
keys beginning with the 7 key.
4. When the test is complete, the instrument should display “UNIT OK”.
5. Press any key to view the complete LCD display capabilities. Compare the instrument display to the display graphic in Chapter 1, Section 1-3 LCD Display.
6. Press any key to exit the self-test.
7. Press the meas key to exit the setup menu.
2-10 Upload
The upload function allows the user to update the V-2000 to the most current method program revision. The V-2000 is updated by logging on to the CHEMetrics website, www.chemetrics.com and clicking on the V-2000 Upload New Methods link. To ensure that the most current method calibrations are being used, it is recommended that every V-2000 user check the CHEMetrics website frequently. For more information, see Chapter 5, Section 5-3 Uploading Method Revisions.
7
Chapter 3
Setup and Measurement Procedures
3-1 General Operating Instructions
The following guidelines can be considered general operating instructions for the V-2000 photometer. More parameter specific information is provided in the kit instructions supplied with each Vacu-vial or COD test kit.
# The V-2000 must be zeroed prior to each series of measurements. Additionally, if the
ampoule/vial adapter has been removed or comes loose during operation, the V-2000 should be re-zeroed.
# For best results, always cover the ampoule or vial with the light shield prior to zeroing
the instrument, setting a reagent blank value or measuring a sample.
# For COD testing, LED based photometers do not produce accuracy, precision and
sensitivity equivalent to that attainable from spectrophotometers. For NPDES reporting purposes for COD, a spectrophotometer is the preferred method of measurement. A full comparison of the range and accuracy claims for COD on the two different instrument platforms is available from the CHEMetrics Technical Services Department.
# A 13 mm sealed ampoule containing distilled water is supplied in each Vacu-vials Test
Kit for use as a ZERO ampoule for Vacu-vial test procedures.
# A 16 mm screw cap vial containing distilled water is supplied with the V-2000
Photometer for use as a zeroing vial for the COD test procedure.
# Methods that do not specifically call for the generation of a reagent blank should follow
Procedure A - Zeroing, Program Selection and Measuring below.
# Methods that do specifically call for the generation of a reagent blank (Aluminum,
Chloride, COD, Fluoride, Hydrazine, Ozone 2 (K-7413) should follow Procedure B -
Zeroing, Program Selection, Setting Reagent Blank and Measuring below.
3-2 Procedure A - Zeroing, Program Selection and Measuring
1. Install the appropriate sample cell adapter into the photometer.
2. Turn the photometer on by pressing the power key.
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3. Insert the ZERO ampoule into the V-2000, cover the ZERO ampoule with the light shield, and
press the zero key. “Wait” is displayed, then the result is displayed as “0.000".
4. Press the prgm key, enter the appropriate program number, then press the yes key. The
instrument will display the appropriate method name and program number.
NOTE: If the program number is a 3 digit number, the yes key does not have to be pressed.
5. Follow the parameter specific Test Procedure supplied with the Test Kit on the sample to be tested and insert the resulting test ampoule into the V-2000. Cover the test ampoule with the light shield.
6. Press meas key. If a color development wait time is specified in the parameter specific Test
Procedure, the V-2000 timer will begin to countdown. The V-2000 will automatically proceed to the measure mode when wait time is complete. The instrument will read the test ampoule and display the test result. The test result can either be recorded manually, logged manually or logged automatically. The instrument displays under and over-range results only very briefly. Under and over-range results cannot be logged.
NOTE: To bypass the timer feature, simply press the timer key. The instrument will immediately
initiate measurement mode.
3-3 Procedure B - Zeroing, Program Selection, Setting Reagent Blank and Measuring
1. Install the appropriate sample cell adapter into the photometer.
2. Turn the photometer on by pressing the power key.
3. Insert the zeroing vial into the V-2000, cover the zeroing vial with the light shield, and press
the zero key. “Wait” is displayed, then the result is displayed as “0.000".
4. Press the prgm key, enter the appropriate program number, then press the yes key. The
instrument will display the appropriate method name and program number.
NOTE: If the program number is a 3 digit number, the yes key does not have to be pressed.
5. Press the setup key and use the or – keys until “BLANK” is displayed, then press the yes
key.
6. “SET BLNK?” will be displayed, press the yes key.
7. “SAMPLE?” will be displayed.
8. Follow the parameter specific instructions supplied with the test kit for Generating a Reagent Blank. Insert the Reagent Blank into the V-2000. Cover the Reagent Blank with the light
shield, then press the yes key. The instrument will read the blank, display an absorbance
value momentarily, and then move to the next setup function.
9. Press the meas key to exit the setup menu. The instrument display will return to the
appropriate method name and program number.
10. Follow the parameter specific Test Procedure supplied with the test kit on the sample to be tested, and insert the resulting test ampoule or vial into the V-2000. Cover the test ampoule with the light shield.
11. Press the meas key. If a color development wait time is specified in the parameter specific
Test Procedure, the V-2000 timer will begin to countdown. The V-2000 will automatically proceed to the measure mode when wait time is complete. The instrument will read the test ampoule or vial and display the test result. The test result can either be recorded manually, logged manually or logged automatically. The instrument displays under and over-range results only very briefly. Under and over-range results cannot be logged.
NOTE: To bypass the timer feature, simply press the timer key. The instrument will immediately
initiate measurement mode.
9
Chapter 4
Data Logging
The V-2000 allows the user to store up to 100 test results in the photometer’s memory.
4-1 Logging Data Manually
When a test result is being displayed by the instrument, press the log key. The log icon will
appear in the display. The V-2000 will display “1 LOGGED”. As new test results are logged, the number preceding LOGGED will append to reflect the number of saved test results.
4-2 Logging Data Automatically
Auto log automatically saves test results to the photometer’s memory.
1. Press the setup key and use the or – keys until “AUTO LOG” is displayed, then press the yes key.
2. Use the or – keys to toggle between “AUTO OFF” and “AUTO ON”. When the desired
function is displayed, press the yes key.
3. Press the meas key to exit the setup menu.
4. With auto log turned on, the log icon will appear in the display. After the first data point is logged, the V-2000 will display “1 LOGGED”. As new test results are logged, the number preceding LOGGED will append to reflect the number of saved test results.
NOTE: Under and over-range results are not logged.
4-3 Displaying the Log
1. Press and hold the log key for approximately 4 seconds.
2. “DISPLAY” will be displayed and the last test result saved into the log will be displayed.
3. Use or the – keys to scroll through the log test results.
4. Press the meas key to escape log display.
4-4 Clearing the Log
1. Press and hold the log key for approximately 4 seconds.
2. Press the zero key; “CLR LOG?” will be displayed.
NOTE: It is recommended to print or download the log prior to clearing.
3. Press the yes key to clear the log. “DELETED” will be displayed and the V-2000 will return
to the measurement mode.
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Chapter 5
Use with Printers and Computers
The V-2000 photometer allows communication directly to a printer or bidirectional communication with a computer.
Connecting to a printer or a computer requires the use of the supplied RS-232 serial cable. This cable has a special 3-pin connector on one end for the V-2000. The RS-232 port is on the underside of the instrument. When connecting the RS-232 cable to a computer, a serial connector may be required (a 25 pin to 9 pin adapter is included with the V-2000). If your computer or printer does not have a serial port, you will need to purchase a separate adapter that will allow you to connect the V-2000 RS-232 serial cable to the USB port on your printer or computer. The following USB to serial adapters are compatible with multiple computer operating systems:
Manufacturer Manufacturer Part No. Supplier Supplier Part No.
Aten Technologies
aten-usa.com
CP Technologies
cptechusa.com
5-1 Printing Logged Data Directly to a Printer
1. With the V-2000 power off, connect the V-2000 to a printer using the supplied RS-232 serial cable.
2. Press the power key.
3. Press the setup key and use the or – keys until “PRINT” is displayed, then press the yes
key.
4. Use the or – keys to toggle between “STND PRN” and “CMA DELM”. When “STND PRN”
is displayed, press the yes key.
5. Press the meas key to exit the setup menu.
6. Press and hold the log key for approximately 4 seconds.
7. Press and hold the print key for approximately 4 seconds to download all saved data.
5-2 Downloading Logged Data to a Computer
UC232A CDW Company
www.cdw.com
CP-US-03 CDW Company
www.cdw.com
325871
767105
Logged data can be sent to a terminal emulator program (example: Hyper Terminal) and then exported to a spreadsheet or database software application.
1. Create a text file (*.txt) to receive the V-2000 logged data.
2. With the V-2000 power off, connect the V-2000 to a computer using the supplied RS-232 serial cable.
3. Press the power key.
4. Press the setup key and use the or – keys until “PRINT” is displayed, then press the yes
11
key.
5. Use the or – keys to toggle between “STND PRN” and “CMA DELM”. When “CMA DELM”
is displayed, press the yes key.
6. Press the meas key to exit the setup menu.
7. Open HyperTerminal by going to the Start button, then clicking on Programs/ Accessories/Communications/HyperTerminal.
8. A “New Connection” window will open. Enter a name to call the terminal program, for example, “V2000". Select an icon to represent the terminal program.
9. A “Connect To” window will open. Select the Com (serial) port to which V-2000 is connected.
10. Enter the port transmission settings:
Baud Rate 1200, 2400, 4800, 9600 Data Bits 8 Parity None Stop Bit 1 Start Bit 1 Flow Control Hardware
NOTE: The baud rate selected in Hyper Terminal must match the V-2000 baud rate. See Chapter 2, Section
2-5 Baud Rate.
11. From the HyperTerminal menu, select Transfer. Click on Capture Text. Enter the path and name of the file created in Step 1. Click on Start.
12. Make sure that the desired V-2000 printout format has been chosen as outlined in Chapter 2, Section 2-6 Print.
13. Press and hold the log key for approximately 4 seconds.
14. Press and hold the print key for approximately 4 seconds to download all saved data.
15. Log #, test results, program #, parameter, and date/time tag should appear in the Hyper Terminal window. When transmission is complete, click the Disconnect icon. Click on Transfer/Capture Text and Stop. Exit the HyperTerminal program.
16. The text file which captured the V-2000 data can now be opened in the appropriate software application. Data may be reformatted as needed for spreadsheet or database manipulation.
5-3 Uploading Method Revisions
The V-2000 method program can be updated by logging onto the CHEMetrics website, www.chemetrics.com and clicking on the V-2000 Upload New Methods link. The CHEMetrics website will inform customers when new methods are available or existing methods have been updated. Also, the parameter specific test kits will have information about method updates as they occur. To ensure that the most current method calibrations are being used, it is recommended that every V-2000 user check the CHEMetrics website frequently.
To determine which method revision is currently present on your V-2000 instrument, simply turn the instrument on. On start up, the V-2000 briefly displays the current method revision.
Note: Uploading a new method revision does not overwrite any user generated custom methods.
Automatic Method Revision Update:
Instructions:
1. With the V-2000 power off, connect the V-2000 to a computer using the supplied RS-232
serial cable.
2. Press the power key to turn the meter on.
3. Then press the setup key.
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4. Press the or – keys until “UPLOAD” is displayed, then press the yes key to accept.
5. Meter should read “WAITING”, indicating meter is ready for the Method Revision Update.
NOTE: To abort the upload process, press yes key again.
6. Click on the link provided on the CHEMetrics website and open the program.
7. Follow the instructions provided in the file.
8. When the program is complete, the instrument will display “ALL DONE” along with the
new method revision number.
NOTE: If the above Automatic Method Revision Update does not complete successfully, contact
CHEMetrics Technical Support at 540-788-9026 or technical@chemetrics.com.
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Chapter 6
Error Messages
Error code Explanation
E11 420 nm LED Failure
E12 520 nm LED Failure
E13 580 nm LED Failure
E14 610 nm LED Failure
E19 LCD Driver Error
OVERRNG Over-range: Test result is more than 110% above
claimed operational range; dilute that sample and repeat the test
UNDRRNG Under-range: Test result is less than zero.
14
Chapter 7
Custom User Programs
The V-2000 has the capacity to store up to 10 custom user programs. This function allows the user to establish and input their own calibration data. The V-2000 can then be used to generate test results that are based on this custom calibration.
7-1 Creating a Custom User Program
1. Install the appropriate sample cell adapter into the photometer.
2. Turn the photometer on by pressing the power key.
3. Insert the zeroing vial into the V-2000, cover the zeroing vial with the light shield, and press the zero key. “Wait” is displayed, then the result is displayed as “0.000".
4. Press the prgm key, enter the desired program number (190 -199 only), The instrument will display “No User X” if no user program is currently stored at that location.
5. Press the setup key and use the or – keys until “USR PRGM” is displayed, then press the yes key.
6. “WAVELENGTH?” will be displayed. Use the or – keys to select the desired wavelength. When the desired wavelength is displayed, press the yes key.
7. “UNITS” will be displayed. Use the or – keys to select the desired units. When the desired units are displayed, press the yes key.
8. “TIMER 1” will be displayed. Press the yes key to set the first timer, then use the or – keys to select the desired length of time (10 second intervals). When the desired length of time is displayed, press the yes key.
9. “TIMER 2” will be displayed. Press the yes key to set the second timer, then use the or – keys to select the desired length of time (10 second intervals). When the desired length of time is displayed, press the yes key.
10. “SAVE USR ?” will be displayed. Press the yes key to save the new user program. “—SAVED—“ will be displayed. The instrument will automatically proceed to “CAL USR”.
7-2 Calibrating a Custom User Program
A calibration must be entered to use a new custom user program. Calibrating a user program requires a minimum of 2 calibration standards, selected to bracket the anticipated sample concentration. However, the V-2000 will accept up to 5 calibration standards which cover the expected range of the test.
1. Follow the parameter specific Test Procedure to generate 2 to 5 fully reacted test vials for the selected standard concentrations.
15
2. While “CAL USR” is displayed, press the yes key.
3. “3 CAL PTS?” will be displayed. Use the or – keys until the desired number of calibration points is displayed, then press the yes key.
4. “PT1 CONC?” will be displayed. Insert the first reacted standard into the V-2000 and cover it with the light shield. Enter the value for the first standard using the numeric keypad. Press the yes key to accept the value entered. The V-2000 will read the first standard and automatically proceed to the next standard.
NOTE: If no decimal point is used in the concentration value, press the yes key again to accept the value.
5. Repeat Step 4 for each of the remaining standard concentrations.
6. “CAL OK” will be displayed at the completion of the calibration.
7-3 Replacing or Reviewing a Custom User Program
1. Install the appropriate sample cell adapter into the photometer.
2. Turn the photometer on by pressing the power key.
3. Insert the zeroing vial into the V-2000, cover the zeroing vial with the light shield, and press the zero key. “Wait” is displayed, then the result is displayed as “0.000".
4. Press the prgm key, enter the desired program number (190 -199 only), The instrument will display “No User X” if no user program is currently stored at that location or “**USR X” if a program is stored at that location.
5. Press the setup key and use the or – keys until “USR PRGM” is displayed, then press the yes key.
6. If a stored user program exists, “REPL OLD?” will be displayed. Use the or – keys to toggle between “REPL OLD?” and “REVIEW?”. To view program settings, press the yes key to select “REVIEW?”. To replace the existing program or change certain settings, press the yes key to select “REPL OLD?”.
16
Chapter 8
Specifications & Features
Wavelength (nm) 420, 520, 580, 610
Wavelength Accuracy ± 2 nm
Wavelength Selection Automatic
Photometric Reproducibility ± 0.005A (0-1A)
Photometric Accuracy ± 0.005A @ 1.0 Abs Nominal
Photometric Range 0 - 2 A
Light Source Light Emitting Diode (LED)
Detector Photodiode
Bandwidth 10 ± 2 nm
Operating Temperature 0.0 to 45.0 °C
Humidity 90% at 50.0 °C max
Waterproof IP67
Cell Adapter(s) 16 mm, 13 mm
Output Units mg/L, ppm, μg/L, ppb, g/L, Absorbance, or
% Transmittance
Datalogging 100 points, Date and Time Tag
Download Capability Data to Spreadsheet and Printer, RS232 Output
Upload Capability Methods Update, RS232 Input
Power Supply 4 AA Alkaline Batteries
Compliance European CE Mark
Programmed Method Capacity 185 and 10 User Defined
Timing Capability Built-in Timer
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Chapter 9
Product Information
9-1 Instrument & Accessories
Catalog Number Description
V-2000 V-2000 Photometer, comes with 13 mm sample cell adapter
(installed), 16 mm sample cell adapter, COD ZEROING Vial, RS­232 cable, serial connector, light shield, operator’s manual, 4 AA batteries.
A-0182 V-2000 Carrying case, hard plastic kit case with handle and foam
insert that holds V-2000 Photometer and up to 4 Vacu-vials Test Kits.
A-0183 COD ZEROING Vial, package of one
9-2 Warranty Information
The V-2000 Photometer, other than its expendable components (sample cell adapters, light shield, RS-232 cable and serial connector), carries an unconditional guarantee of freedom from defects in material and workmanship for a period of two years from date of shipment. User access to the interior of the instrument may impair its function and will void this warranty. Improper use, application or servicing also voids this warranty. Manufacturer’s liability shall not exceed cost of replacement of the photometer.
9-3 European Union’s WEEE Directive 2002/96/EC
This product is required to comply with European Union’s Waste Electrical & Electronic Equipment (WEEE) Directive 2002/96/EC. It is marked with the WEEE symbol. For information on recycling this instrument, contact the instrument distributor.
Marking of electrical and electronic equipment, which applies to electrical and electronic equipment falling under the Directive 2002/96/EC (WEEE) and the equipment that has been put on the market after 13 August 2005.
18
9-4 List of Supported Parameters
Kit Catalog
Parameter
Aluminum K-0603 9 520 0.04 - 0.25 Eriochrome Cyanine R
Ammonia 3 K-1403 14 610
Ammonia K-1503 15 420
Ammonia 2 K-1523 16 420
Bromine K-1603 21 610 0.90 - 9.00 DDPD
Chloride K-2103 26 420 2.5 - 40.0 Ferric Thiocyanate
Chlorine 2 K-2513 32 520 0.40 - 5.00 DPD
Chlorine 3 K-2523 32 520 0.40 - 5.00 DPD
Number
Program
Code Wavelength
Range
ppm Method
0.20 - 3.00 (as N)
0.50 - 7.00 (as N)
1.0 - 14.0 (as N)
Salicylate
Direct Nesslerization
Direct Nesslerization
Chlorine Dioxide
Chromate K-2803 42 520 0.20 - 3.50 Diphenylcarbazide
Chromate 2 K-2823 43 580 0.70 - 13.00 Diphenylcarbazide
Copper K-3503 55 420 0.50 - 12.00 Bathocuproine
Cyanide K-3803 60 610 0.040 - 0.400
DEHA 1 K-3903 64 580 0.15 - 2.00 PDTS
Fluoride K-4003 73 580 0.50 - 2.00 SPADNS
Formaldehyde K-4203 78 520
Glycol K-4403 83 520
K-2703 37 520 0.80 - 11.00 DPD
Isonicotinic/Barbituric Acid
0.40 - 8.00
0.60 - 10.00 (as ethylene
glycol)
Purpald
Purpald/Periodate
Glycol 2 K-4423 84 520
19
5.0 - 65.0
(as propylene
glycol)
Purpald/Periodate
Parameter
Kit Catalog
Number
Program
Code Wavelength
Range
ppm Method
Hydrazine K-5003 89 420 0.10 - 1.20 PDMAB
Peroxide 1 K-5503 94 610 0.20 - 2.00 DDPD
Peroxide 2 K-5543 95 520 0.15 - 6.00 Ferric Thiocyanate
Iron 1 K-6003 100 520 0.20 - 6.00 Phenanthroline
Iron 3 K-6013 101 420 1.0 - 25.0 Phenanthroline
Iron 2 K-6023 102 580 0.10 - 2.50 PDTS
Iron 4 K-6203 100 520 0.20 - 6.00 Phenanthroline
Manganese K-6503 110 520 1.0 - 30.0 Periodate
Molybdate K-6703 115 420
Nitrate K-6903 119 520
Nitrate 4 K-6913 122 520
Nitrate 2 K-6923 120 520
Nitrate 3 K-6933 121 520
Nitrite K-7003 125 520
COD LR, EPA Approved
COD LR, Mercury Free
COD HR, EPA Approved
K-7350 48 420 20 - 150
K-7351 48 420 20 - 150
K-7360 49 610 100 - 1500
1.0 - 25.0
(as Mo)
0.20 - 1.50 (as N)
0.10 - 1.00 (as N)
0.40 - 3.00 (as N)
5.0 - 50.0 (as NO
)
3
0.080 - 0.800 (as N)
Catechol
Cadmium Reduction
Zinc Reduction
Cadmium Reduction
Cadmium Reduction
Azo Dye Formation
Dichromate Reactor Digestion
Dichromate Reactor Digestion
Dichromate Reactor Digestion
COD HR, Mercury Free
COD HR+, EPA Approved
COD HR+, Mercury Free
K-7361 49 610 100 - 1500
K-7370 49 610 1,000 - 15,000
K-7371 49 610 1,000 - 15,000
Dichromate Reactor Digestion
Dichromate Reactor Digestion
Dichromate Reactor Digestion
20
Parameter
Kit Catalog
Number
Program
Code Wavelength
Range
ppm Method
Ozone K-7403 134 610 0.20 - 2.50 DDPD
Ozone 2 K-7413 135 610 0.30-1.00 Indigo
Oxygen 1 K-7503 140 610 0.20 - 2.00 Indigo Carmine
Oxygen 2 K-7513 141 520 2.0 - 15.0 Indigo Carmine
Oxygen 3 K-7553 142 520 0.100 - 1.400 Rhodazine D™
Peracetic Acid K-7903 147 610 0.40 - 4.00 DDPD
Phenols K-8003 152 520 0.40 - 8.00 4-Aminoantipyrine
Phenols 2 K-8023 153 520 1.0 - 20.0 4-Aminoantipyrine
Phosphate 1 K-8503 158 420
Phosphate 2 K-8513 159 610
Phosphate 2 K-8513 160 610
Silica K-9003 168 610
5.0 - 80.0 (as PO
0.30 - 8.00 (as PO
0.10 - 2.64
(as P)
0.50 - 10.00 (as SiO
Vanadomolybdo-
)
phosphoric Acid
4
Stannous Chloride
)
4
Stannous Chloride
Heteropoly Blue
)
2
Sulfate K-9203 174 420 8.0 - 100.0 Turbidimetric
Sulfide K-9503 179 610 0.20 - 3.00 Methylene Blue
Sulfide 2 K-9523 180 610 0.60 - 6.00 Methylene Blue
Zinc K-9903 187 610 0.30 - 3.00 Zincon
Zinc 2 K-9923 188 610 0.60 - 6.00 Zincon
21
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