Analytical Industries Inc (AII) GPR-1200 MS Operating Manual

Technical Specifications *
Accuracy: < 2% of FS range under constant conditions Analysis Ranges: 0-1, 0-10, 0-100, 0-1000 PPM FS ranges;
Auto-ranging or manual lock on a single range
Application: Oxygen analysis in inert, helium, hydrogen and mixed
gas streams Area Classification: General purpose Calibration: Max interval3 months. Use certified span gas with O2
content (balance N2) approximating 80% of full scale.
For optimum accuracy, calibrate one range higher than
the range of interest. Compensation: Temperature
Connections: 1/8" compression tube fittings Controls: Water resistant keypad; menu driven range selection,
calibration and system functions Display: Graphical LCD 2.75 x 1.375”; resolution .001 PPM Enclosure: Painted aluminum NEMA 4X, 8.6 x 9 x 3", 12 lbs.
Flow: Sensitive; recommended flow rate 2 SCFH
LED Indicators: LOW BATT (72 hr. warning); CHARGE mode
GPR-1200 MS
Portable PPB O2 Analyzer
Rechargeable Battery Powered
Linearity: > .995 over all ranges Pressure: Inlet - regulate to 5-30 psig to deliver 2 SCFH flow;
vent - atmospheric Power: Rechargeable battery, 60 day cycle, 8 hrs with pump Recovery Time: 2 minutes at 9 PPM to 10 PPB in < 10 min on N2 purge
30 seconds in air to < 1 PPM in < 45 min on N2 purge
Response Time: 90% of final FS reading in 10 seconds Sample System: Flow control and sample/bypass valves; flow indicator Sensitivity: < 0.5% of FS range
Sensor Model: GPR-12-2000MS Sensor Life: 24 months in < 100 PPM O2 at 25ºC and 1 atm Signal Output: 0-1V FS
Temp. Range: 5ºC to 45ºC Warranty: 12 months analyzer; 12 months sensor
Wetted Parts: Stainless steel
Optional Equipment
Integral stainless steel bypass sample system significantly in-
Innovative Sensor Technology
Fast Recovery to < 1 PPM from Exposure to Air Unmatched Performance Unmatched Sensor Life and Warranty Excellent Stability
Sensitivity 0.5% Full Scale Auto Ranging or Fixed Single 0-1 V Signal Output Operates in Charging Mode Low Battery Warning LED Stainless Steel Wetted Parts
Carrying case with custom foam insert Sample conditioning - pump, filter, scrubbers - contact factory
ISO 9001:2008 Certified
INTERTEK Certificate No. 485
* Subject to change without notice.
2855 Metropolitan Place, Pomona, CA 91767 USA Tel: 909-392-6900, Fax: 909-392-3665, www.aii1.com, e-mail: info@aii1.com Rev 6/15
Portable ppm Oxygen Analyzer
GPR-1200 MS
Owner’s Manual
2855 Metropolitan Place, Pomona, CA 91767 USA Tel: 909-392-6900, Fax: 909-392-3665, e-mail: info@aii1.com, www.aii1.com
10/09
Table of Contents
Introduction Quality Control Certification Safety Specifications Operation Maintenance Spare Parts Troubleshooting Warranty Material Safety Data Sheets Appendix C – Pump Options
1 2 3 4 5 6 7 8 9 10
1 Introduction
Your new portable oxygen analyzer incorporates an advanced electrochemical sensor specific to oxygen along with state-of-the-art digital electronics designed to give you years of reliable precise oxygen measurements in variety of industrial oxygen applications. To obtain maximum performance from your new oxygen analyzer, please read and follow the guidelines provided in this Owner’s Manual.
Every effort has been made to select the most reliable state of the art materials and components; and, to design the analyzer for superior performance and minimal cost of ownership. This analyzer was tested thoroughly by the manufacturer prior to shipment for best performance.
However, modern electronic devices do require service from time to time. The warranty included herein plus a staff of trained professional technicians to quickly service your analyzer is your assurance that we stand behind every analyzer sold.
The serial number of this analyzer may be found on the inside the analyzer. You should note the serial number in the space provided and retains this Owner’s Manual as a permanent record of your purchase, for future reference and for warranty considerations.
Serial Number: _______________________ Advanced Instruments Inc. appreciates your business and pledges to make every effort to maintain the highest
possible quality standards with respect to product design, manufacturing and service.
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2 Quality Control Certification
Date: Customer:
Order No.:
Model GPR-1200 MSMS Portable ppm Oxygen Analyzer Sensor ( ) GPR-12-2000MS ppm Oxygen Sensor
Serial Nos.
Accessories Owner’s Manual ( ) PWRS-1002 9VDC Battery Charger/Adapter 110VAC
CONN-1034 Plug Mini Phone .141 dia. Black Handle TOOL-1001 5/16 Combination Wrench
Configuration A-1151-E-B6-NB PCB Assembly Main/Display Range: 0-1 ppm, 0-1 ppm, 0-100 ppm, 0-1000 ppm Wetted parts: Stainless steel Crossover bypass/shut off valve
Electronics Test LED indicators: Low battery, charge Electronic offset Analog signal output 0-1V Gas Phase Test
Span adjustment within 10-50% FS Final Overall inspection for physical defects
Options NA Notes 1 of 1 analyzers due ASAP
Analyzer_________________________ Sensor _____________________________
( ) PWRS-1003 9VDC Battery Charger/Adapter 220VAC ( ) PWRS-1008 9VDC Battery Charger/Adapter 12VDC Auto Cigarette Lighter
Baseline drift on zero gas < ± 2% FS over 24 hour period on 0-1% range Noise level < ± 0.5% FS
Pass
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3 Safety
General
This section summarizes the essential precautions applicable to the GPR-1200 MS Series Portable ppm Oxygen Analyzer. Additional precautions specific to individual analyzer are contained in the following sections of this manual. To operate the analyzer safely and obtain maximum performance follow the basic guidelines outlined in this Owner’s Manual.
Caution: This symbol is used throughout the Owner’s Manual to CAUTION and alert the user to recommended safety and/or operating guidelines.
Danger: This symbol is used throughout the Owner’s Manual to identify sources of immediate DANGER such as the presence of hazardous voltages.
Read Instructions: Before operating the analyzer read the instructions. Retain Instructions: The safety precautions and operating instructions found in the Owner’s Manual should be
retained for future reference.
Heed Warnings: Follow all warnings on the analyzer, accessories (if any) and in this Owner’s Manual. Follow Instructions: Observe all precautions and operating instructions. Failure to do so may result in personal
injury or damage to the analyzer.
Installation
Oxygen Sensor: DO NOT open the sensor. The sensor contains a corrosive liquid electrolyte that could be harmful if touched or ingested, refer to the Material Safety Data Sheet contained in the Owner’s Manual appendix. Avoid contact with any liquid or crystal type powder in or around the sensor or sensor housing, as either could be a form of electrolyte. Leaking sensors should be disposed of in accordance with l ocal regulations.
Exposure to air: Minimize the time the sensor is exposed to air during installation. Inlet Pressure: The analyzer is designed for flowing samples are intended to operate at positive pressure
regulated to between 5-30 psig.
Outlet Pressure: The sample gas vent pressure should be atmospheric. Flow Rate: Recommended – 1 SCFH Mounting: Mount as recommended by the manufacturer. The analyzer is approved for indoor or outdoor use. Power: Supply power to the analyzer only as rated by the specification or markings on the analyzer enclosure. The
wiring that connects the analyzer to the power source should be installed in accordance with recognized electrical standards and so they are not pinched particularly near the power source and the point where they attach to the analyzer. Never yank wiring to remove it from an outlet or from the analyzer.
Operating Temperature: The maximum operating temperature is 45º C. Heat: Situate and store the analyzer away from sources of heat. Liquid and Object Entry: The analyzer should not be immersed in any liquid. Care should be taken so that
liquids are not spilled into and objects do not fall into the inside of the analyzer. Handling: Do not use force when using the switches and knobs. Before moving your analyzer be sure to
disconnect the wiring/power cord and any cables connected to the output terminals located on the analyzer.
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Maintenance
Serviceability: Except for replacing the oxygen sensor, there are no parts inside the analyzer for the operator to service.
Only trained personnel with the authorization of their supervisor should conduct maintenance. Oxygen Sensor: DO NOT open the sensor. The sensor contains a corrosive liquid electrolyte that could be
harmful if touched or ingested, refer to the Material Safety Data Sheet contained in the Owner’s Manual appendix. Avoid contact with any liquid or crystal type powder in or around the sensor or sensor housing, as either could be a form of electrolyte. Leaking sensors should be disposed of in accordance with l ocal regulations.
Troubleshooting: Consult the guidelines in Section 8 for advice on the common operating errors before concluding that your analyzer is faulty.
Do not attempt to service the analyzer beyond those means described in this Owner’s Manual. Do not attempt to make repairs by yourself as this will void the warranty as per Section 10 and may result in electrical shock, injury or damage. All other servicing should be referred to qualified service personnel.
Cleaning: The analyzer should be cleaned only as recommended by the manufacturer. Wipe off dust and dirt from the outside of the unit with a soft damp cloth then dry immediately. Do not use solvents or chemicals.
Nonuse Periods: If the analyzer is equipped with a range switch advance the switch to the OFF position and disconnect the power when the analyzer is left unused for a long period of time.
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A
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4 Specifications *
Accuracy: < 1% of FS range under constant conditions Analysis: 0-1 ppm, 0-10, 0-100, 0-1000 ppm FS ranges;
Application:
Approvals: CE, Intrinsic Safety (pending) Area Classification: Meets recognized intrinsic safe ty standard s for us e in Class
Calibration: Certified gas of O
Compensation: Temperature and barometric pressure Connections: 1/8" compression tube fittings Controls: Water resistant keypad; menu driven ran
Display: Graphical LCD 2.75 x 1.375; resolution .001 ppb; displays
Enclosure: Painted aluminum NEMA 4X, 8.6x9x3", 12 lbs. Flow Sensitivity: None between 1-3 SCFH, 1 SCFH recommended LED Indicators: LOW BATT (72 hr. warning); CHARGE mode Linearity: > .995 over all ranges Pressure: Inlet - regulate to 5-30 psig; vent - atmospheric Power: Rechargeable battery, 60 day duty cycle (pump 1 day) Recovery Time: 60 seconds in air to < 1 ppm in < 20 minutes on N Response Time: 90% of final FS reading in 10 sec onds Sample System: Flow control, bypass and isolation valves; flow indicator Sensitivity: < 0.5% of FS range Sensor Model: GPR-12-2000MS Sensor Life: 24 months at 25ºC and 1 atm; average O Signal Output: 0-1V Temp. Range: 5º to 45ºC Warranty: 12 months analyzer; 12 months sensor Wetted Parts: Stainless steel
Optional Equipment
auto-ranging or manually lock on single range
nalyze oxygen concentrations from 10 ppb to 1000 ppm
in inert, hydrocarbon, helium, hydrogen and gas streams
1, Division 1, Group C, D hazardous areas (see Options)
balance N2 approximating 80% of
analysis range or one range above analysis range
calibration and system functions
real time ambient temperature and pressure
2
e selection,
purge
2
< 100 ppm
2
GPR-1200 MS
Portable ppm O2 Analyzer
Advanced Sensor Technology Accuracy < 1% FS Range Sensitivity < 0.5% FS Range Fast Recovery to < 1 ppm 24 Month Expected Life No Maintenance Intrinsically Safe Design 4 Standard Analysis Ranges Auto or Manual Ranging SS Bypass Sample System Water Resistant Enclosure ISO 9001:2008 Approved QA System
Integral sampling pump - general purpose or intrinsically safe designs Carrying case with custom foam insert Sample conditioning accessories - contac t factory
* Specifications subject to change without notice
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Integral bypass sample system increases productivity.
5 Operation
Principle of Operation
The GPR-1200 MS portable oxygen analyzer incorporates a proprietary Pico-Ion oxygen sensor. The analyzer is configured in a general purpose NEMA 4 rated enclosure and meets the intrinsic safety standards required for use in Class 1, Division 1, Groups A, B, C, D hazardous areas. Two integral sampling pump options are available – one that meets the intrinsic safety standards and a less expensive option for general purpose service.
Breakthrough Sensor Technology:
A breakthrough sensor technology measures the partial pressure of oxygen from less than 10 ppb to 1000 ppm level in inert gases, gaseous hydrocarbons, helium, hydrogen and mixed gas streams. The “Pico-Ion” sensor design and chemistry have been combined to produce a significant advancement in oxygen sensor technology.
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Oxygen, the fuel for this electrochemical transducer, reacts chemically at the sensing electrode to produce an electrical current output proportional to the oxygen concentration in the gas phase. The sensor’s signal output is linear over all four ranges and remains virtually constant over its useful life. The sensor requires no maintenance or electrolyte addition and is easily and safely replaced at the end of its useful life.
The signal generated by the sensor is processed by state of the art low power micro-processor based digital circuitry. The first stage amplifies the signal. The second stage eliminates the low frequency noise. The third stage employs a high frequency filter and compensates for signal output variations caused by ambient temperature changes. The result is a very stable signal. Several selectable averaging modes are available to enhance the stability of the analyzer and eliminate anomalies if desired. Sample oxygen is analyzed very accurately. Response time of 90% of full scale is less than 10 seconds on the 0-1 ppm range (actual experience may vary due to the integrity of sample line connections, dead volume and flow rate selected).
Electronics:
The signal generated by the sensor is processed by state of the art low power micro-processor based digital circuitry. The first stage amplifies the signal. The second stage eliminates the low frequency noise. The third stage employs a high frequency filter and compensates for signal output variations caused by ambient temperature changes. The result is a very stable signal. Sample oxygen is analyzed very accurately. Response time of 90% of full scale is less than 10 seconds (actual experience may vary due to the integrity of sample line connections, dead volume and flow rate selected) on all ranges under ambient monitoring conditions. Sensitivity is typically 0.5% of full scale low range. Oxygen readings may be recorded by an external device via the 0-1V signal output jack.
Power is supplied by an integral rechargeable lead acid battery which provides enough power to operate the analyzer continuously for approximately 60 days. An LED located on the front panel provides a blinking 72 hour warning to recharge the battery. A 9VAC adapter (positive pole located on the inside of the female connector) can be used to recharge the battery from a convenience outlet. The analyzer is designed to be fully operational during the 8-10 hour charging cycle which is indicated by a second continuously lit LED.
Sample System:
The GPR-1200 MS is supplied with a bypass sample system which enables the user to isolate the sensor from exposure to high oxygen concentration which results is a substantial increase is user productivity. The bypass feature has two important features: One, the sensor can be isolated from exposure to high oxygen levels when changing sample lines, during transport and during standby intervals making it ideal for mobile cart applications. Two, it enables the user to purge newly connected gas lines of the oxygen trapped inside. The result is an analyzer that comes on-line at ppb levels in a matter of minutes and provides users with a significant increase in productivity.
However the sample must be properly presented to the sensor to ensure an accurate measurement. Users interested in adding their own sample conditioning system should consult the factory. Advanced Instruments Inc. offers a full line of sample handling, conditioning and expertise to meet your appl ication requirements. Contact us at 909-392-6900 or e-mail us at info@aii1.com
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Pressure & Flow
All electrochemical oxygen sensors respond to partial pressure changes in oxygen. The inlet pressure must always be higher than the pressure at the outlet vent which is normally at atmospheric pressure.
The sensor is exposed to sample gas that must flow or be drawn through the analyzer’s internal sample system. Flow rates of 1-5 SCFH cause no appreciable change in the oxygen reading. However, flow rates above 5 SCFH generate backpressure and erroneous oxygen readings because the diameter of the integral tubing cannot evacuate the sample gas at the higher flow rate.
A flow control valve upstream of the sensor controls the flow rate of the sample gas which is displayed by the flow indicator downstream of the sensor. A flow rate of 2 SCFH or 1 liter per minute is recommended for optimum performance.
Caution: Do not place your finger over the vent (it pressurizes the sensor) to test the flow indicator when gas is flowing to the sensor. Removing your finger (the restriction) generates a vacuum on the sensor and may damage the sensor (voiding the sensor warranty).
Positive Pressure Applications:
If the sample pressure is greater than 30 psig an external pressure regulator (optional) is required upstream of the analyzer to control of sample flow. A pressure regulator with a metallic diaphragm is recommended to prevent high oxygen readings that could result from the use of diaphragms constructed of more gas permeable materials.
If other optional sample system components such as coiled metal tubing (samples must be cooled to at least 35­40º C for continuous use), coalescing filters, scrubbers, etc. are required install the pressure regulator after the coiled tubing and before the other components and the analyzer. Note: A scrubber requires a flow valve upstream for optimum efficiency and response time and that the analyzer flow valve is opened completely.
Atmospheric or Slightly Negative Pressure Applications:
For accurate high ppb and/or low ppm range measurements, an optional sample pump is required downstream of the analyzer to draw the sample through the analyzer. The vacuum drawn on the analyzer and sensor should not exceed 4” of water.
Caution: Use of pump downstream of the sensor requires the flow control valve upstream of the sensor be completely opened to avoid drawing excessive vacuum on the sensor, which can damage the sensor.
If pump over-loading (due to the limitation of low flow rate of the sample gas) is a consideration, a second throttle valve on the pump’s inlet side may be necessary to provide a bypass path, as illustrated below, to prevent the pump from over-loading and over-heating while maintaining the required sample flow rate within the above­mentioned parameters.
Standard Bypass Sample System
The GPR-1200MS Portable 0-1 ppm Oxygen Analyzer is equipped with a bypass sample system featured below:
1. Manufacturer supplies the analyzer with the sensor it was qualified with.
2. Isolate the sensor during transport and maintenance intervals and extend sensor life.
3. Isolate the sensor from exposure to high oxygen levels during upset conditions and extend sensor life.
4. Purge the high oxygen levels or air trapped in the sample system following a process upset, changing sample gas lines or connecting span gas lines.
5. Increase productivity by complimenting the recovery capability of the sensor to reduce downtime.
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