ADWA AD332, AD331 User guide

Page 1
USER MANUAL
AD331 • AD332
Waterproof Portable Meters for
EC and TDS Measurements
www.adwainstruments.com
Page 2
Dear Customer,
Thank you for choosing an Adwa product. Please read carefully this manual before starting operations.
This instrument is in compliance with the EMC directive 2004/ 108/EC and its standards, and Low Voltage Directive 2006/95/ EC and its standards for electrical equipments.
For additional technical information, please e-mail us at [email protected].
WARRANTY
Adwa warrants this product to be free of defects in material and workmanship as stated in the operating manual. If repair or adjustment is necessary and has not been the result of abuse, misuse or improper handling within the warranty pe­riod, please contact your dealer or the nearest Adwa Office for the RGA (Return Goods Authorization) number to put on the outside of your package. Warranted service will be made with­out charge. The meter is warranted for a period of 2 years, while probes are warranted for 6 months. The warranty pe­riod commences from the original date of sale. Warranty is only valid when the product is used under normal conditions and in accordance with the instruction manual. The warranty is void if the instrument is repaired or serviced by unautho­rized personnel, not used in accordance to the instructions, or if non-Adwa accessories such as buffer solutions, probes, etc. are used in conjunction with the meter. Adwa will not be held responsible for any accident whether directly or indi­rectly, caused by the use of this instrument.
2
Page 3
TABLE OF CONTENTS
Introduction ................................................................ 4
Technical Data .......................................................... 6
Front and Top Panels ................................................ 8
Operational Guide .................................................... 10
Autoranging ............................................................. 14
Temperature Compensation .................................... 15
EC Calibration ......................................................... 17
Temperature Adjustment ........................................ 22
Setup ........................................................................ 23
Good Laboratory Practice ....................................... 26
Log-on-Demand ....................................................... 29
Hold Function .......................................................... 33
Printing
PC interface
Battery Replacement .............................................. 37
Probe Maintenance ................................................. 38
Probes and Solutions ............................................... 39
(AD332 only) ............................................................ 34
(AD332 only) .................................................. 36
3
Page 4
INTRODUCTION
AD331 and AD332 are waterproof portable meters.
AD331 reads EC in 5 ranges and AD332 can measure
EC and TDS. Both models also read temperature.
The autoranging feature of the EC and TDS ranges automatically sets the instrument to the scale with the highest resolution.
Measurements are compensated for temperature ef­fect automatically (ATC) or manually (MTC). It is also possible to disable the temperature compensation feature to measure the actual conductivity.
The temperature coefficient is user selectable.
These instruments also feature a measurement stabil­ity indicator, GLP capability, and a user selectable ID code to uniquely identify the instrument.
Moreover, AD332 includes PC interface and printing function. Connect the meter to an external serial printer with the following printer specifications:
• at least 16 characters / line
• baud rate 9600
• 9-pin RS232 input
4
Page 5
All models are supplied complete with:
• AD76309 conductivity probe with built-in tempera-
ture sensor and 1 m cable
• Calibration solution (20 ml sachet each):
• 1413 μS/cm EC standard solution
• 12,88 mS/cm EC standard solution
• 1.5 V AA alkaline batteries (4 pcs)
• User manual
5
Page 6
TECHNICAL DATA
EC Range 19.99 ; 199.9 ; 1999 μS/cm
19.99 ; 199.9 mS/cm
TDS Range 9.99 ; 99.9 ; 999 ppm
(AD332) 9.99 ; 99.9 ppt
Temperature Range -9.9 to 120.0 °C
Resolution 0.01 ; 0.1 ; 1 μS/cm
0.01 ; 0.1 mS/cm
0.01 ; 0.1 ; 1 ppm / 0.01 ; 0.1 ppt
0.1°C
Accuracy ±1% f.s. (EC and TDS)
(@20°C/68°F) ±0.5 °C
EC Calibration Offset: 0.0 μS/cm;
Slope: 1 point with 6
memorized standards (84.0, 1413 μS/cm; 5.00,
12.88, 80.0, 111.8 mS/cm) or one custom value
Temperature Automatic or manual, Compensation -9.9 to 120 °C
Temperature Selectable Coefficient from 0.00 to 10.00% / °C
6
Page 7
TDS Factor Selectable from 0.40 to 1.00
(AD332 only) (default value: 0.50)
Reference Temperature
Selectable from 15.0 to 30.0 °C
Log-on-demand Up to 250 samples
Probe (included) AD76309
PC Interface & Printer
(AD332 only)
RS232 port; external serial printer
Battery Type 4 x 1.5 V AA alkaline batteries
Battery Life Approx. 200 h of continuous use
Auto-Off User selectable: 5 min or disabled
Environment 0 to 50°C; RH max 95%
Dimensions 188 x 96 x 70 mm
Weight 460 g
7
Page 8
FRONT AND TOP PANELS
8
Page 9
1. Probe holder
2. ON/OFF key, to turn the instrument ON and OFF
3. STORE/MRCL key, to store the measured data and to recall stored data
4. CAL/SETUP key, to enter/exit calibration and setup mode
5. CFM key, to confirm values
6. SHIFT key, to activate the key alternate function Press and hold first the SHIFT key and then the second desired key
7. Down arrow/PAPER key, to manually decrease the value of temperature or other parameters and to pull out the printer paper
8. Up arrow/PRINT key, to manually increase the value of temperature or other parameters and to ob­tain a printout or cancel printing
9. RANGE (
AD332) or NEXT (AD331)/“lock” key, to
select measurement unit or switch the focused data, and to freeze current range on the LCD
10. HOLD/GLP key, to freeze the first stable reading on the LCD and to display Good Laboratory Prac­tice information
11. Liquid Crystal Display (LCD)
12. DIN connector for conductivity probe
13. RS232 port for serial printer or PC connection
9
Page 10
OPERATIONAL GUIDE
• The meter is supplied complete with four 1.5 V AA
alkaline batteries. Remove the battery cover, unwrap the batteries and install them while paying attention to their polarity (see “Battery Replacement” section for details).
• Connect the supplied probe to the DIN connector and
tighten the threaded ring. Make sure the probe sleeve is properly inserted.
10
Page 11
INSTRUMENT START-UP
• Turn the instrument on by pressing
the ON/OFF key.
• At start-up the display will show all used segments for
a few seconds (or while the button is held), followed by the reference temperature value with “rEF” indi­cation, then enters the measurement mode.
• To save battery life, the auto-off feature automatically
turns the meter off after 5 minutes with no button pressed. This feature can be disabled through the “AoFF” setup item (see “Setup” section for details).
11
Page 12
TAKING MEASUREMENTS
• Immerse the probe into the solution
to be tested. The sleeve holes must be completely submerged.
• Tap the probe repeatedly to remove
any air bubbles that may be trapped inside the sleeve.
• If needed, press RANGE (AD332)
until the EC or TDS range is selected on the LCD.
• Allow for the reading to stabilize. The primary LCD
displays the measurement in the selected range, while the secondary LCD shows the temperature reading.
12
Page 13
Notes:
• If the meter displays only dashes "----", the read-
ing is out of range.
• If the stability indicator (hourglass symbol) blinks,
the reading is not stable.
• Make sure the meter is calibrated before taking
measurements.
• If measurements are taken successively in dif-
ferent samples, for accurate reading it is recom­mended to rinse the probe thoroughly with deion­ized water before immersing it into the next sample.
• For AD332: the TDS reading is obtained by mul-
tiplying the EC value by the TDS factor (de­fault: 0.50). This factor can be selected by the user (0.40 to 1.00) through the "tdS" setup item (see “Setup” section for details).
13
Page 14
AUTORANGING
The EC and TDS scales are autoranging. The meter automatically sets the scale with the highest possible resolution. By pressing SHIFT and “lock” keys, the autoranging feature is disabled and the current range is frozen on the LCD. The μS, mS, ppm or ppt tag (depend- ing on the selected measurement mode and range) starts blinking. To restore the autoranging option press the SHIFT and “lock” keys again.
Note: Autoranging is automatically restored if range is
changed, if setup or calibration mode is entered, or if meter is turned off and back on again.
14
Page 15
TEMPERATURE COMPENSATION
Three options are available for temperature compensa­tion:
1. Automatic (ATC): the EC probe features a built-in
temperature sensor, which allows automatic compen­sation of the EC or TDS measurements.
2. Manual (MTC): the temperature value can be manu-
ally set using the arrow keys. The compensation is referenced to the selected reference temperature. While in MTC mode, the °C tag blinks on the second­ary LCD.
3. No compensation (No TC): the temperature is not
taken into account. The reading displayed on the pri­mary LCD is the actual EC or TDS value.
Notes:
• The default compensation mode is ATC.
• Temperature compensation setting can be ac­cessed through the "tcE" setup item (see “Setup” section for details).
• If the temperature compensation is active, mea­surements are compensated using the tempera­ture coefficient (default value 1.90 %/°C).
15
Page 16
The temperature coefficient can be modified through the “tc” setup item (see “Setup” section for details).
• If the temperature reading is out of the -9.9 to
120.0°C range and the ATC option is selected, the temperature full scale value and the °C tag will blink on the secondary LCD.
• The reference temperature can be set from 15 to 30°C. When the reference temperature is changed, the temperature coefficient must be manually adjusted by the user. For example, if α is the coefficient with refer- ence temperature of 25°C, when changing the temperature to 20°C, the new coefficient can be calculated with the following formula:
β=α/(1-α/20)
If α=1.90%/°C, then β=2.10%/°C.
• For AD332, always set reference tempera-
ture to 25°C when measuring TDS.
16
Page 17
EC CALIBRATION
EC calibration is performed for both meters. For AD332, since the TDS values are automatically derived from the EC readings, no specific calibration for TDS is needed.
Selectable points for EC calibration are 0.00, 84.0 and 1413 μS/cm, 5.00, 12.88, 80.0 and 111.8 mS/cm.
• Rinse the probe with selected standard or deionized water, then immerse it into the cali­bration solution. The sleeve holes must be completely submerged.
• Tap the probe repeatedly to remove any air bubbles that may be trapped inside the sleeve.
• To enter calibration mode, press the CAL key from the corresponding measurement range.
Note: For AD332, pressing CAL
when TDS range is selected has no effect.
17
Page 18
• For zero calibration, simply leave the dry probe in the air. The "CAL" and "BUFFER" tags light up.
• The primary LCD displays the not calibrated EC or TDS reading, while the secondary LCD shows one of the available standard values. The hourglass symbol blinks.
• If necessary, use the arrow keys to select the desired standard value.
• When the reading is stable, the CFM tag starts blink­ing. Press CFM to confirm calibration.
• The instrument displays the "Stor Good" message and returns to measurement mode.
18
Page 19
Notes:
• If the temperature is out of range, the "WRONG BUFFER TEMP" message blinks on the LCD. If the reading is too far from the expected value, "WRONG BUFFER" blinks.
• For best results, use a calibration solution with EC (or TDS) value close to the sample to be measured.
• During calibration the meter compensates using the 1.90%/°C coefficient. If the setup item "tc" has been set to a different value, when exiting calibration mode, the displayed value might be different from the nominal standard value.
CUSTOM CALIBRATION
Calibration can be also performed with a custom cali­bration solution.
• Immerse the probe into the custom calibration solution and select the proper EC (or TDS) range. Press first CAL to enter the calibration mode and then RANGE (or NEXT) to enter the custom calibration.
19
Page 20
• The "CAL", "BUFFER" and "Cal Point Custom" tags light up. The primary LCD displays the not calibrated temperature compensated reading, while the second­ary LCD shows the temperature compensated read­ing, factory calibrated with cell value k=1. The hour­glass symbol blinks.
• Using the arrow keys, adjust the reading displayed on the primary LCD to the desired value.
• The maximum adjustment is ±40% around the value displayed on the secondary LCD.
• When the reading is stable, the CFM tag starts blink­ing. Press CFM to confirm calibration.
20
Page 21
• The instrument displays the "Stor Good" message and returns to measurement mode.
Notes:
• Zero calibration is not allowed in custom mode.
• The calibrated custom value is considered the value of the calibration solution at the selected reference temperature.
• The cell constant value can be set directly through
the "CELL" setup item, without following the cali­bration procedure (see “Setup” section for de­tails).
• Temperature reading is not used during custom calibration.
21
Page 22
TEMPERATURE ADJUSTMENT
Temperature reading can be manually fine-tuned as ex­plained in this section.
Press SHIFT and CFM keys to enter the temperature adjustment mode. Both primary and secondary LCDs will display the current temperature reading for a few seconds, followed by the default temperature reading.
Adjust the temperature value on the primary LCD using the arrow keys. The maximum allowed adjustment is ±1.0
ºC around the current reading.
Press CFM to confirm. The meter returns to measure­ment mode and displays the new temperature.
Notes:
• Press SHIFT and CFM keys to escape without
changing.
• To enter temperature adjustment mode, the probe must be connected and the meter must be in ATC mode.
22
Page 23
SETUP
Setup mode allows to view and modify the instrument parameters.
To enter setup mode, press SHIFT and then SETUP key from measurement mode. The SETUP tag lights up. The primary LCD will display the temperature coef­ficient (default value 1.90%/ LCD shows the code of the current setup item.
Select the desired setup item using the arrow keys, then press CFM to select and edit the setup item. The cur­rent value of the selected item starts blinking (if the pa­rameter can be modified).
ºC), while the secondary
23
Page 24
Use the arrow keys to change the value. If there is another part of the item to be set (e.g. month in setting up the current date), press RANGE (or NEXT) and the part to be changed will start blinking.
Use the arrow keys to change the value and then press CFM to confirm.
Note: To escape without changing the previously set
value, press SHIFT and then SETUP before confirming.
24
Page 25
The following table lists the setup items, their valid range and the factory settings (default):
Item
tc
tcE
rEF
tdS
CELL
AoFF
YEAr
DATE
TIME
id
vEr
(*) For AD332 only.
Description
Temperature coefficient
Temp.compensation mode
Reference temperature
TDS factor (*)
Cell constant (K)
Auto-off feature
Printer Status (*)
Year
Date (DD.MM)
Time (hh:mm)
Meter identification code
Firmware release
Valid values Default
0.00 to 10.00% / ºC 1.90
Atc, Mtc, notc Atc
15.0 to 30.0 ºC 25.0 ºC
0.40 to 1.00 0.50
0.500 to 1.700 1.000
On, Off Off
On/Off Off
2000 to 2098 2000
01.01 to 31.12 01.01
01:01 to 23:59 00:00
0000 to 9999 0000
25
Page 26
GOOD LABORATORY PRACTICE
Good Laboratory Practice (GLP) is a set of functions that allows storage and retrieval of data regarding the status of the system. After a successful calibration, the meter automatically stores the date and time of calibration, the used calibra­tion solution and the resulting cell constant value. All this information can be recalled by the user. To view the last calibration data, press SHIFT and then GLP keys. The first information appearing on the LCD is the meter "id" code.
By repeatedly pressing RANGE (or NEXT) key, all GLP data are displayed as shown in the next pages.
26
Page 27
Last calibration date (day and month).
Last calibration date (year).
Last calibration time.
Cell constant (K)
Calibration with standard so­lution.
27
Page 28
Calibration with custom solu­tion.
If the cell constant was changed after calibration (through the “CELL” setup item), this information is not displayed.
If RANGE (or NEXT) is pressed while the last param­eter is displayed, the meter returns to measurement mode.
Notes:
• To exit GLP mode at any time, press SHIFT+GLP.
• If calibration has never been performed, after display­ing the ID code, the meter will show the "no CAL" message blinking. Press RANGE (or NEXT) or SHIFT+GLP to return to measurement mode.
•For AD332, only last EC calibration data are avail- able. No calibration data can be recalled for TDS. If SHIFT+GLP are pressed from TDS measurement mode, the meter will display the ID code only. Press SHIFT+GLP again to return to measurement mode.
• GLP data are not affected by zero calibrations.
28
Page 29
LOG-ON-DEMAND
To store current reading into memory, press STORE key from measurement mode.
The LCD will display for a few seconds the "Stor" mes­sage together with the "Log" tag and the sample number.
By pressing the STORE key a complete set of informa­tion is memorized: date, time, EC or TDS and tempera­ture readings.
Up to 250 samples can be stored into memory. When the memory is full and
the STORE key is pressed, the sample will not be stored and the LCD will display the "FULL" message.
In this case, it is necessary to delete the last sample or all logged data to proceed.
29
Page 30
VIEWING STORED DATA
To retrieve memorized information, press SHIFT and then MRCL keys.
The primary LCD displays the date (day & month) and the secondary LCD shows the number of last stored sample.
If no samples are stored into memory, the "ZERO" mes­sage is displayed.
• Select the desired sample number using the arrow keys.
If the up arrow key is pressed while the last sample is displayed, the meter returns to the first sample.
• Press RANGE (or NEXT) to view the remaining data for the selected sample as shown in the next page.
30
Page 31
• Year
• Time
• EC or TDS reading (only dashes "----" means reading out of range or probe not connected)
• Temperature reading (only dashes "----" means reading out of range)
• To skip to next or previous sample, use the up or down arrow key respectively. For example, if the up arrow key is pressed while a sample reading is displayed, the meter shows the reading of next sample.
• To return to measurement mode, press SHIFT+MRCL at any time.
31
Page 32
DELETING STORED DATA
The meter allows to delete a single sample or all the memory at one time.
To delete a single sample proceed as follows:
• Enter the viewing stored data mode and select the de­sired sample number.
• Press the HOLD key. "dEL" and "CFM" will start blinking.
• Press CFM to confirm deletion or HOLD again to escape without deleting data. When scrolling through stored data, if a deleted sample is selected, the meter will display the "nuLL" message.
To delete all data in memory:
• Enter the viewing stored data mode.
• Press SHIFT+HOLD keys. "dEL" and "CFM" will start blinking and the "ALL" message is displayed on the secondary LCD.
32
Page 33
• Press CFM to confirm deletion or SHIFT+HOLD again to escape without deleting data.
Note: If no samples are stored in memory and a dele-
tion is attempted, the meter shows the "Zero" message and then returns to measurement mode.
HOLD FUNCTION
To freeze the first stable reading on the LCD, press the HOLD key from measurement mode.
The “Auto” and “H” tags will blink on the LCD until the reading is stabilized.
When the reading becomes stable, the “Auto” and “H” tags stop blinking and the read­ing is frozen.
Press the HOLD key again to return to normal mea­surement mode.
33
Page 34
PRINTING (AD332 only)
When connected to an external serial printer, a com­plete set of information can be printed. Use the AD9551 serial communication cable (optional).
Printer specifications:
• at least 16 characters / line
• baud rate 9600
• 9-pin RS232 input
Data can be printed on demand (from measurement, GLP and SETUP modes) by pressing SHIFT+PRINT keys, or automatically for log-on-demand mode.
Note: To cancel printing, press SHIFT+PRINT again.
While in EC measurement mode, the printout provides the following information.
Date 2000/01/01 Time 00:19 EC 83.2 mS
°C 25.0
Note: For TDS measurement mode, the TDS reading
will be printed.
34
Page 35
When in GLP mode, the printout pro­vides the following information:
GL P Instr ID 0005 Date 2000/01/01 Time 00:34 Cell 0.961 Cal Buffer EC 8.00 mS
When in SETUP mode, the follow­ing information are printed:
SETUP REPORT Instr ID 0005 Date 2000/01/01 Time 00:34 TC 01.90 % TCE Atc Temp REF 25.0 TDS Factor 0.50 Cell 1.000 AutoOff OFF Printer On Version 1.0
When exiting the setup mode, the instrument asks if the setup report has to be printed. The “Prn” message will be displayed together with the printer symbol ( ) and the CFM tag blinking.
35
Page 36
Press CFM to print the setup report or CAL to exit with­out printing.
When a reading is logged on-demand, an automatic printout will provide the following information for EC or TDS:
LO G Record No 001 Date 2000/01/01 Time 00:19 EC 83.2 mS
°C 25.0
PC INTERFACE (AD332 only)
Data transmission from the instrument to the PC can be done with the ADSW10 Windows® compatible software (optional). ADSW10 offers graphing and on-line help feature, and data can be exported to the most popular spreadsheet programs for further analysis.
To connect the instrument to a PC, use the AD9551 serial communication cable (optional). Make sure that the instrument is switched off and plug the cable to the instrument RS232 socket and to the PC serial port.
Specifications:
Isolated 8-bit data transmission Baud rate: 2400 Start bit: 1 Stop bit: 1 Parity bit: none
36
Page 37
BATTERY REPLACEMENT
When batteries become too weak, the “bAtt” message ap­pears. It is recommended to re­place the batteries soon.
When the battery level is too low to ensure reliable read­ings, the meter automatically turns off.
Battery replacement must only take place in a safe area and us­ing the battery type specified in this instruction manual. To replace rundown batteries, re­move the battery cover and sub­stitute all four 1.5 V AA alkaline batteries with new ones, while paying attention to the correct po­larity. Reattach and tighten the battery cover making sure that the gas­ket is in place.
Note: When batteries are removed, the meter can re-
member date & time for about 5 minutes. After that, it will be necessary to set again date & time through the setup procedure.
37
Page 38
PROBE MAINTENANCE
After measurements, rinse the probe with clean water.
If a more thorough cleaning is required, remove the probe sleeve and clean the probe with a cloth or a non-abra­sive detergent.
Make sure to reinsert the sleeve onto the probe properly and in the right direction.
After cleaning the probe, recalibrate the instrument.
38
Page 39
PROBES AND SOLUTIONS
AD76309 Conductivity probe with built-in tem-
perature sensor, DIN connector and 1 m cable
AD70030P 12.88 mS/cm EC solution, 20 ml sachet,
25 pcs
AD7030 12.88 mS/cm EC standard solution, 230
ml bottle
AD70031P 1413 μS/cm EC standard solution, 20 ml
sachet, 25 pcs
AD7031 1413 μS/cm EC standard solution, 230
ml bottle
AD7033 84 μS/cm solution, 230 ml bottle
AD7034 80.00 mS/cm EC standard solution, 230
ml bottle
AD7035 111.80 mS/cm EC standard solution, 230
ml bottle
AD7039 5000 μS/cm EC standard solution, 230
ml bottle
AD70442 1500 ppm TDS standard solution, 230
ml bottle
AD9551 Serial communication cable
39
Page 40
ADWA HUNGARY Kft.
Alsókikötõ sor 11, 6726 Szeged, Hungary
Tel. +36 62 317 878
Fax +36 62 550 610
www.adwainstruments.com
MANAD331 09/14
Loading...