Aalborg AFM Operating Manual

OPERATING MANUAL
AFM and AFC
MASS FLOW METERS
and CONTROLLERS
Technical Data Sheet No. TD9305M Rev. M Date of Issue: August 2009
QUALITY SYSTEM REGISTERED
1. UNPACKING THE AFM/AFC MASS FLOW METER.....................
1.1 Inspect Package for External Damage.........................................
1.2 Unpack the Mass Flow Meter/Controller.......................................
1.3 Returning Merchandise for Repair...............................................
2. INSTALLATION............................................................
2.1 Primary Gas Connections............................................................
2.2 Electrical Connections.................................................................
3. PRINCIPLE OF OPERATION..............................................
4. SPECIFICATIONS...........................................................
4.1 AFM 26/36/46 Mass Flow Meters.................................................
4.2 AFC 26/36/46 Mass Flow Controllers..........................................
4.3 CE Compliance............................................................................
5. OPERATING INSTRUCTIONS.............................................
5.1 Preparation and Warm Up...........................................................
5.2 Flow Signal Output Readings.......................................................
5.3 Swamping Condition...................................................................
5.4 Set Point Reference Signal (AFC)................................................
5.5 TTL, Valve OFF Control (AFC)......................................................
5.6 Valve Test/Purge (AFC)................................................................
6. MAINTENANCE............................................................
6.1 Introduction.................................................................................
6.2 Flow Path Cleaning......................................................................
6.2.1 Restrictor Flow Element (RFE).................................................
6.2.2 AFM 26 and AFC 26 models.....................................................
6.2.3 AFM 36/46 and AFC 36/46 models..........................................
6.2.4 Valve Maintenance (AFC).........................................................
7. CALIBRATION PROCEDURES..............................................
7.1 Flow Calibration..............................................................................
7.2 Calibration of AFM Mass Flow Meters............................................
7.2.1 Connections and Initial Warm Up..........................................
7.2.2 ZERO Adjustment.................................................................
7.2.3 SPAN Adjustment.................................................................
1
1 1 1
2
2 2
4
5
5 6 7
10
10 10 11 11 12 12
13
13 13 13 13 14 14
15
15 16 16 17 17
7.3 Linearity Adjustment......................................................................
7.3.1 Connections and Initial Warm Up...........................................
7.3.2 ZERO Adjustment.................................................................
7.3.3 25% Flow Adjustment.............................................................
7.3.4 50% Flow Adjustment............................................................
7.3.5 75% Flow Adjustment.............................................................
7.3.6 100% Flow Adjustment.......................................................
7.4 Calibration of AFC Mass Flow Controllers......................................
7.4.1 Disable Solenoid Valve.........................................................
7.4.2 Valve Adjustment..................................................................
7.4.3 Full Scale Flow Adjustment...................................................
7.4.4 25% Flow Adjustment...........................................................
7.4.5 50% Flow Adjustment...........................................................
7.4.6 75% Flow Adjustment.........................................................
7.4.7 100% Flow Adjustment..........................................................
8. TROUBLESHOOTING.........................................................
8.1 Common Conditions......................................................................
8.2 Troubleshooting Guide...................................................................
8.3 Technical Assistance...................................................................
9. CALIBRATION CONVERSIONS FROM REFERENCE GASES...........
APPENDIX 1 COMPONENT DIAGRAMS..................................................
APPENDIX 2 GAS FACTOR TABLE ("K" FACTORS)...................................
APPENDIX 3 DIMENSIONAL DRAWINGS................................................
APPENDIX 4 WARRANTY.........................................................................
17 17 18 18 18 18 18 18 18 19 19 19 19 19 19
20
20 21 23
23
24
25
29
33
1
1. UNPACKING THE AFM/AFC MASS FLOW METER
1.1 Inspect Package for External Damage
Your AFM/AFC Mass Flow Meter/Controller was carefully packed in a sturdy card­board carton, with anti-static cushioning materials to withstand shipping shock. Upon receipt, inspect the package for possible external damage. In case of exter­nal damage to the package contact the shipping company immediately.
1.2 Unpack the Mass Flow Meter/Controller
Open the carton carefully from the top and inspect for any sign of concealed ship­ping damage. In addition to contacting the shipping carrier please forward a copy of any damage report to your distributor or Aalborg7 directly.
When unpacking the instrument please make sure that you have all the items indi­cated on the Packing List. Please report any shortages promptly.
1.3 Returning Merchandise for Repair
Please contact the customer service representative of your distributor or Aalborg if you purchased your Mass Flow Meter/Controller directly, and request a Return
Authorization Number (RAN). Equipment returned without an RAN will not be accepted. Aalborg7 reserves the right to charge a fee to the customer for
equipment returned under warranty claims if the instruments are tested to be free from warrantied defects.
Shipping charges are borne by the customer. Meters returned "collect" will not be accepted!
It is mandatory that any equipment returned for servicing be purged and neutral­ized of any dangerous contents including but not limited to toxic, bacterially infec­tious, corrosive or radioactive substances. No work shall be performed on a returned product unless the customer submits a fully executed, signed SAFETY CERTIFICATE. Please request form from the Service Manager.
2
2. INSTALLATION
2.1 Primary Gas Connections
Please note that the AFM/AFC Mass Flow Meter/Controller will not operate with liquids. Only clean gases are allowed to be introduced into the instrument. If gases are contaminated they must be filtered to prevent the introduction of imped­iments into the sensor.
Attitude sensitivity of the Mass Flow Meter is +
15F. This means that the gas flow path of the Flow meter/Controller must be horizontal within those stated limits. Should there be need for a different orientation of the meter, re calibration may be necessary. It is also preferable to install the AFM/AFC transducer in a stable environment, free of frequent and sudden temperature changes, high moisture, and drafts.
Prior to connecting gas lines inspect all parts of the piping system including fer­rules and fittings for dust or other contaminants.
Be sure to observe the direction of gas flow as indicated by the arrow on the front of the meter when connecting the gas system to be monitored.
Insert tubing into the compression fittings until the ends of the properly sized tub­ings home flush against the shoulders of the fittings. Compression fittings are to be tightened according to the manufacturer's instructions to one and one quarter turns. Avoid over tightening which will seriously damage the Restrictor Flow Elements (RFE's)!
AFM/AFC transducers are supplied with standard 1/4 inch (AFM/AFC 26 and 36) or 3/8 inch (AFM/AFC 46), or optional 1/8 inch inlet and outlet compression fit­tings which should not be removed unless the meter is being cleaned or calibrat­ed for a new flow range.
Using a Helium Leak Detector or other equivalent method perform a thorough leak test of the entire
system. (All AFM/AFC's are checked prior to shipment for
leakage within stated limits. See specifications in this manual.)
2.2 Electrical Connections
AFM/AFC transducers require a +15VDC and -15VDC power supply to operate. Additionally, a readout panel meter, digital multimeter, or other equivalent device is required to observe the flow signal. A variable analog 0-5VDC reference input is required for AFC models. The Aalborg7 SDPROC accessory Command Modules offer a convenient and compact means to fulfill these needs.
AFM/AFC transducers come with a 15 pin "D" connector. The pin diagram is pro­vided on figure 2-3.
Caution: AFM/AFC transducers should not be used for monitoring OXYGEN gas unless specifically cleaned and prepared for such application. For more information, contact your distributor or Aalborg7.
FIGURE 2-1, WIRING DIAGRAM FOR AFM/AFC TRANSDUCERS.
FIGURE 2-3, AFM/AFC 15 PIN "D" CONNECTOR CONFIGURATION.
3
PIN FUNCTION
1
Chassis Ground
2 Common, Signal Ground For Pin 3 3 0-5 VDC Flow Signal 4 +15 VDC Power Supply 5 (-) 4-20 mA Flow Signal (optional) 6 +7 VDC for Local Set Point 7 (unassigned) 8 TTL Valve Off Control (AFC) 9 Control Set Point Input 0 5 VDC (AFC) 10 Common, Signal Ground for Pin 9 11 Common, Power Supply 12 Valve Test Point/Purge (AFC) 13 (unassigned) 14 -15 VDC Power Supply 15 (+) 4-20 mA Flow Signal (optional)
Important notes:
In general, "D" Connector numbering patterns are standardized. There are, how­ever, some connectors with nonconforming patterns and the numbering sequence on your mating connector may or may not coincide with the numbering sequence shown in our pin configuration table above. It is imperative that you match the appropriate wires in accordance with the correct sequence regardless of the par­ticular numbers displayed on your mating connector.
Make sure power is OFF when connecting or disconnecting any cables in the system.
The (+) and (-) power inputs are each protected by a 750mA M (medium time-lag) resettable fuse. If a shorting condition or polarity reversal occurs, the fuse will cut power to the flow transducer circuit. Disconnect the power to the unit, remove the faulty condition, and reconnect the power. The fuse will reset once the faulty con­dition has been removed.
Cable length may not exceed 9.5 feet (3 meters).
Use of the AFM/AFC flow transducer in a manner other than that specified in this manual or in writing from Aalborg7, may impair the protection provided by the
equipment.
3. PRINCIPLE OF OPERATION
The stream of gas entering the Mass Flow transducer is split by shunting a small portion of the flow through a capillary stainless steel sensor tube. The remainder of the gas flows through the primary flow conduit. The geometry of the primary conduit and the sensor tube are designed to ensure laminar flow in each branch. According to principles of fluid dynamics the flow rates of a gas in the two laminar flow conduits are proportional to one another. Therefore, the flow rates measured in the sensor tube are directly proportional to the total flow through the transducer.
In order to sense the flow in the sensor tube, heat flux is introduced at two sec­tions of the sensor tube by means of precision wound heater-sensor coils. Heat is transferred through the thin wall of the sensor tube to the gas flowing inside. As gas flow takes place heat is carried by the gas stream from the upstream coil to the downstream coil windings. The resultant temperature dependent resistance differential is detected by the electronic control circuit. The measured gradient at the sensor windings is linearly proportional to the instantaneous rate of flow tak­ing place.
An output signal is generated that is a function of the amount of heat carried by the gases to indicate mass-molecular based flow rates.
Additionally, AFC model Mass Flow Controllers incorporate a proportionating solenoid valve. The closed loop control circuit of the AFC continuously compares the mass flow output with the selected flow rate. Deviations from the set point are corrected by compensating valve adjustments, thus maintaining the desired flow parameters.
4
4. SPECIFICATIONS
FLOW MEDIUM: Please note that AFM26/36/46 Mass Flow Meters and AFC26/36/46 Mass Flow Controllers are designed to work with clean gases only. Never try to meter or control flow rates of liquids with any AFM's or AFC's.
CALIBRATIONS: Performed at standard conditions [14.7 psia (1.01 bars) and 70
F
F
(21.1
F
C)] unless otherwise requested or stated.
ENVIRONMENTAL (per IEC 664): Installation Level II; Pollution Degree II
4.1 AFM 26/36/46 Mass Flow Meters
ACCURACY: +
1% of full scale, including linearity for gas temperatures ranging from
59
F
F to 77FF (15FC to 25FC) and pressures of 10 to 60 psia (0.7 to 4.1 bars).
REPEATABILITY: +
0.2% of full scale.
TEMPERATURE COEFFICIENT: 0.1% of full scale/
F
C.
PRESSURE COEFFICIENT: 0.01% of full scale/psi (0.07 bar).
RESPONSE TIME: 300ms time constant; approximately 1 second to within +
2% of set
flow rate for 25% to 100% of full scale flow rate.
GAS PRESSURE: 500 psig (34.5 bars) maximum; optimum pressure is 20 psig (1.4 bars).
GAS AND AMBIENT TEMPERATURE: 32
F
F to 122 FF (0 FC to 50 FC). 14 FF to 122 FF
(-10
F
C to 50 FC) - Dry gases only.
RELATIVE GAS HUMIDITY: Up to 70%.
LEAK INTEGRITY: 1 x 10
-9
sccs He maximum to the outside environment.
ATTITUDE SENSITIVITY: 1% shift for a 90 degree rotation from horizontal to vertical; standard calibration is in horizontal position.
OUTPUT SIGNALS: Linear 0-5 VDC (2000 minimum load impedance); 4-20 mA optional (50-500 maximum loop resistance); 20 mV peak to peak max noise.
Contact your distributor or Aalborg7for optional RS232 or IEEE488 interfaces.
TRANSDUCER INPUT POWER: +15 +5% VDC, 80 mA max, 1.2 watts; -15 +5% VDC, 10 mA max, 0.15 watts.
Power inputs are each protected by a 750mA M (medium time-lag) resettable fuse, and a rectifier diode for polarity protection.
WETTED MATERIALS: 316 stainless steel, VITON7 O-rings; BUNA-N7, NEOPRENE7 or KALREZ7 O-rings are optional.
5
Aalborg7 makes no expressed or implied guarantees of corrosion resistance of mass flow meters as pertains to different flow media reacting with components of meters. It is the customers' sole responsibility to select the model suitable for a particular gas based on the fluid contacting (wetted) materials offered in the different models.
INLET AND OUTLET CONNECTIONS: 1/4" (AFM 26/AFM 36) or 3/8" (AFM 46) compres­sion fittings standard; 1/8" or 3/8" compression fittings and 1/4" VCR7 fittings are optional.
TRANSDUCER INTERFACE CABLE: Flat cable with male 15-pin "D" connector is standard. Optional shielded cable is available with male/female 15-pin "D" connector ends. [Cable length may not exceed 9.5 feet (3 meters)].
4.2 AFC 26/36/46 Mass Flow Controllers
ACCURACY: +
1% of full scale, including linearity for gas temperatures ranging from
59
F
F to 77FF (15FC to 25FC) and pressures of 10 to 60 psia (0.7 to 4.1 bars).
REPEATABILITY: +
0.2% of full scale.
TEMPERATURE COEFFICIENT: 0.1% of full scale/
F
C.
PRESSURE COEFFICIENT: 0.01% of full scale/psi (0.07 bar).
RESPONSE TIME: AFC26: 300ms time constant; approximately 1 second to within
+
2% of set flow rate for 25% to 100% of full scale flow.
AFC36/46: 600ms time constant; approximately 2 seconds to within
+
2% of set flow rate for 25% to 100% of full scale flow.
GAS PRESSURE: 500 psig (34.5 bars) maximum; optimum pressure is 20 psig (1.4 bars); 25 psig (1.7 bars gauge) for AFC46.
MAXIMUM DIFFERENTIAL PRESSURES: 40 psig (2.61 bars) for AFC 46. 50 psig (3.34 bars) for AFC 26/36. Optimum differential pressure is 25 psid (1.7 bars). See Table IV for pressure drops associated with various models and flow rates.
GAS AND AMBIENT TEMPERATURE: 41
F
F to 122FF (5FC to 50FC).
RELATIVE GAS HUMIDITY: up to 70%.
LEAK INTEGRITY: 1 x 10
-9
sccs He maximum to the outside environment.
ATTITUDE SENSITIVITY: 1% shift for a 90 degree rotation from horizontal to vertical; standard calibration is in horizontal position.
OUTPUT SIGNALS: Linear 0-5 VDC (2000 minimum load impedance); 4-20 mA optional (50-500 loop resistance); 20 mV peak to peak max noise.
Contact your distributor or Aalborg7 for optional RS232 or IEEE488 interfaces.
6
COMMAND SIGNAL: 0-5 VDC (200K input impedance).
TRANSDUCER INPUT POWER:
AFC26: (10 sLit/min max) +15 +
5% VDC, 80 mA max,
1.2 watts max; -15 +
5% VDC, 200 mA max; 3 watts max;
AFC36: (50 sLit/min max) +15 +5% VDC, 80 mA max,
1.2 watts max; -15 +5% VDC, 600 mA max, 9 watts max.
AFC46 (100 sLit/min max) +15 +
5% VDC, 80 mA max,
1.2 watts max; -15 +5% VDC, 600 mA max, 9 watts max.
Power inputs are each protected by a 750mA M (medium time-lag) resettable fuse, and a rectifier diode for polarity protection.
WETTED MATERIALS: 316 stainless steel, 416 stainless steel, VITON7 O-rings; BUNA-N7, NEOPRENE7 or KALREZ7 O-rings are optional.
Aalborg7 makes no expressed or implied guarantees of corrosion resistance of mass flow meters as pertains to different flow media reacting with components of meters. It is the customers' sole responsibility to select the model suitable for a particular gas based on the fluid contacting (wetted) materials offered in the different models.
INLET AND OUTLET CONNECTIONS: 1/4" (AFC 26/AFC 36) or 3/8" (AFC 46) compression fittings standard; 1/8" or 3/8" compression fittings and 1/4" VCR7 fittings are optional.
TRANSDUCER INTERFACE CABLE: Flat cable with female 15-pin "D" connector ends is standard. Optional shielded cable is available with male/female 15-pin “D” connector ends. [Cable length may not exceed 9.5 feet (3 meters)]
4.3 CE Compliance
Any model AFM or AFC bearing a CE marking on it, is in compliance with the below stated test standards currently accepted.
EMC Compliance with 89/336/EEC as amended; Emission Standard: EN 55011:1991, Group 1, Class A Immunity Standard: EN 55082 1:1992
7
FLOW RANGES
TABLE I AFM 26 AND AFC 26 LOW FLOW MASS FLOW METER/CONTROLLERS*
TABLE II AFM 36 AND AFC 36 MEDIUM FLOW MASS FLOW METER/CONTROLLERS*
TABLE III AFM 46 AND AFC 46 HIGH FLOW MASS FLOW METER/CONTROLLERS*
* Flow rates are stated for Nitrogen at STP conditions [i.e. 70
F
F (21.1FC) at 1 atm].
For other gases use the K factor as a multiplier from APPENDIX 2.
8
CODE scc/min [N2]
CODE
std liters/min [N
2
]
01 0 to 10 07 0 to 1
02 0 to 20 08 0 to 2
03 0 to 50 09 0 to 5
04 0 to 100 10 0 to 10
05 0 to 200
06 0 to 500
CODE standard liters/min [N2]
11 0 to 15
30 20
31 30
32 40
33 50
CODE standard liters/min [N2]
40 60
41 80
42 100
TABLE IV PRESSURE DROPS AFM
TABLE IV PRESSURE DROPS AFC
TABLE V APPROXIMATE WEIGHTS
9
MODEL WEIGHT SHIPPING WEIGHT
AFM 26 transmitter 1.71 lbs (0.78 kg) 3.21 lbs (1.46 kg)
AFM 36/46 transmitter 2.42 lbs (1.10 kg) 3.92 lbs (1.78 kg)
AFC 26 transmitter 2.20 lbs (1.00 kg) 3.70 lbs (1.68 kg)
AFC 36/46 transmitter 2.84 lbs (1.29 kg) 4.34 lbs (1.97 kg)
MODEL
FLOW RATE
[std liters/min]
MAXIMUM PRESSURE DROP
[mm H2O]
[psid] [mbar]
AFM 26 up to 10 25 0.04 2.5
AFM 36
15 63 0.09 6.4 20 300 0.44 30 30 800 1.18 81 40 1480 2.18 150 50 2200 3.23 223
AFM 46
60 3100 4.56 314
100 5500 8.08 557
MODEL
FLOW RATE
[std liters/min]
MAXIMUM PRESSURE DROP
[mm H2O]
[psid] [mbar]
AFC 26 up to 10 720 1.06 75
AFC 36
15 2630 3.87 266 20 1360 2.00 138 30 2380 3.50 241 40 3740 5.50 379 50 5440 8.00 551
AFC 46
60 7480 11.00 758
100 12850 18.89 1302
5. OPERATING INSTRUCTIONS
5.1 Preparation and Warm Up
It is assumed that the Mass Flow Meter or Controller has been correctly installed and thoroughly leak tested as described in section 2. Make sure the flow source is OFF. Power up the transducer using your own power supply (or turn the POWER switch to the ON position at the front panel of your SDPROC Command Module). Allow the Mass Flow Meter or Controller to warm-up for a minimum of 15 minutes.
During initial powering of the AFM/AFC transducer, the flow output signal will be indicating a higher than usual output. This is indication that the AFM/AFC trans­ducer has not yet attained it's minimum operating temperature. This condition will automatically cancel within a few minutes and the transducer should eventually zero.
Caution: If the valve is left in the AUTO (control) or OPEN mode for an extended period of time, it may become warm or even hot to the the touch. Use care in avoiding direct contact with the valve during operation.
5.2 Flow Signal Output Readings
The flow signal output can be viewed on the panel meter, digital multimeter, or other display device used as shown in figure 2-1.
When using the accessory SDPROC Command Module the flow rate will appear on the display at the front panel. The observed reading is a 0 to 100% indication (direct engineering units are optional). [If using a multichannel readout, be sure that the CHANNEL selector switch is set to the correct channel.]
Analog output flow signals of 0 to 5 VDC or optional 4 to 20 mA are attained at the appropriate pins of the 15-pin "D" connector (see Figure 2-3) on the top of the AFM/AFC transducer. The output flow signal is also available at the DATA con­nector on the rear panel of the SDPROC Command Module.
The default calibration is performed for 0-5 VDC output signal. If 4-20 mA output signal is used for flow indication on the AFC, the accuracy of the actual flow rate will be in the specified range (+
1.0%) of full scale, but the total uncertainty of the output reading may be in the range of +2.0% of full scale. Optional calibration for 4-20 mA output signal is available upon request at time of order.
Meter signal output is linearly proportional to the mass molecular flow rate of the gas being metered. The full scale range and gas for which your meter has been calibrated are shown on the flow transducer's front label.
For optional RS232 or IEEE488 interfaces please contact your distributor or Aalborg7.
10
11
5.3 Swamping Condition
If a flow of more than 10% above the maximum flow rate of the Mass Flow Meter is taking place, a condition known as "swamping" may occur. Readings of a "swamped" meter cannot be assumed to be either accurate or linear. Flow must be restored to below 110% of maximum meter range. Once flow rates are lowered to within calibrated range, the swamping condition will end. Operation of the meter above 110% of maximum calibrated flow may increase recovery time.
5.4 Set Point Reference Signal (AFC)
AFC flow controllers have a built-in solenoid valve and allow the user to set the flow to any desired flow rate within the range of the particular model installed. This valve is normally closed when no power is applied.
The set point input responds to an analog 0 to 5 VDC reference voltage. This volt­age is a linear representation of 0 to 100% of the full scale mass flow rate. Response time to set point changes are 1 second (AFC26) and 2 seconds (AFC36/46) to within 2% of the final flow over 25 to 100% of full scale.
On pin 6 of the AFC transducer is a regulated and constant +5VDC output signal.
This signal may be used in conjunction with a local set point potentiometer for
flow setting.
FIGURE 5-1, LOCAL SET POINT POTENTIOMETER CONNECTIONS
It is recommended that a potentiometer between 5K to 100K ohm and capable of at least 10-turns or more for adjustment be used. Use the control potentiometer to command the percentage of flow desired.
Alternatively, a variable 0 to 5VDC analog signal may be applied directly to the SET POINT and COMMON connections of the AFC transducer (see Figure 2-1).
5.5 TTL, Valve OFF Control (AFC)
It may, at times, be desirable to set the flow and maintain that setting while being able to turn the flow control valve off and on again. This can be accomplished by applying a (TTL compatible) high and low signal of +5 VDC and 0 VDC to pin 8, on the 15-pin "D" connector. When 0 VDC (LOW) signal is applied, the solenoid valve is not powered and therefore will remain normally closed. Conversely, a +5 VDC (HIGH) signal applied will allow the solenoid valve to remain active. The solenoid valve will remain active when the VALVE OFF pin remains "floating".
The simplest means for utilizing the VALVE OFF control feature, is to connect a toggle switch between the COMMON and VALVE OFF pins of the AFC transduc­er. Toggling the switch on and off will allow for activating and deactivating the sole­noid valve.
5.6 Valve Test/Purge (AFC)
At times, it may be necessary to purge the flow system with a neutralizing gas such as pure dry nitrogen. The AFC transducer is capable of a full open condition for the solenoid valve, regardless of set point conditions. For AFC's utilizing +15VDC valve configuration, connecting the TEST pin 12 on 15-pin "D" connec­tors) to ground will fully open the valve. For AFC's with a +30VDC valve configu­ration, connecting the TEST pin to +15VDC will fully open the valve.
12
6. MAINTENANCE
6.1 Introduction
It is important that the Mass Flow Meter/Controller is used with clean, filtered gases only. Liquids may not be metered. Since the RTD sensor consists, in part, of a small capillary stainless steel tube, it is prone to occlusion due to impedi­ments or gas crystallization. Other flow passages are also easily obstructed. Therefore, great care must be exercised to avoid the introduction of any potential flow impediment. To protect the instrument a 50 micron (AFM26/ AFC26) or 60 micron (AFM36/46, AFC36/46) filter is built into the inlet of the flow transducer. The filter screen and the flow paths may require occasional cleaning as described below. There is no other recommended maintenance required. It is good practice, however, to keep the meter away from vibration, hot or corrosive environments and excessive RF or magnetic interference.
If periodic calibrations are required they should be performed by qualified per­sonnel and calibrating instruments, as described in section 7. It is recommended that units are returned to Aalborg7 for repair service and calibration.
CAUTION: TO PROTECT SERVICING PERSONNEL IT IS MANDATORY THAT ANY INSTRUMENT BEING SERVICED IS COMPLETELY PURGED AND NEUTRALIZED OF TOXIC, BACTERIOLOGICALLY INFECTED, CORROSIVE OR RADIOACTIVE CONTENTS.
6.2 Flow Path Cleaning
Before attempting any disassembly of the unit for cleaning, try inspecting the flow paths by looking into the inlet and outlet ends of the meter for any debris that may be clogging the flow through the meter. Remove debris as necessary. If the flow path is not unclogged, then proceed with steps below.
Do not attempt to disassemble the sensor. If blockage of the sensor tube is not alleviated by flushing through with cleaning fluids, please return meter to Aalborg for servicing.
6.2.1 Restrictor Flow Element (RFE)
The Restrictor Flow Element (RFE) is a precision flow divider inside the trans­ducer, which splits the inlet gas flow by a preset amount to the sensor and main flow paths. The particular RFE used in a given Mass Flow Meter/Controller depends on the gas and flow range of the instrument.
6.2.2 AFM 26 and AFC 26 models
Unscrew the inlet compression fitting of meter. Note that the Restrictor Flow Element (RFE) is connected to the inlet fitting.
Carefully disassemble the RFE from the inlet connection. The 50 micron filter
13
14
screen will now become visible. Push the screen out through the inlet fitting. Clean or replace each of the removed parts as necessary. If alcohol is used for clean­ing, allow time for drying.
Inspect the flow path inside the transducer for any visible signs of contaminant's. If necessary, flush the flow path through with alcohol. Thoroughly dry the flow paths by flowing clean dry gas through.
Carefully re-install the RFE and inlet fitting, avoiding any twisting and deforming the RFE. Be sure that no dust has collected on the O-ring seal.
NOTE: Over tightening will deform and render the RFE defective.
It is advisable that at least one calibration point be checked after re-installing the inlet fitting - see section 7.
6.2.3 AFM 36/46 and AFC 36/46 models
Unscrew the four socket head cap screws (two 10-24 and two 6-32) at the inlet side of the meter. This will release the short square block containing the inlet com­pression fitting.
The 60 micron filter screen will now become visible. Remove the screen. DO NOT remove the RFE inside the flow transducer! Clean or replace each of the removed parts as necessary. If alcohol is used for cleaning, allow time for drying.
Inspect the flow path inside the transducer for any visible signs of contaminant's. If necessary, flush the flow path through with alcohol. Thoroughly dry the flow paths by flowing clean dry gas through.
Re-install the inlet parts and filter screen. Be sure that no dust has collected on the O-ring seal.
It is advisable that at least one calibration point be checked after re-installing the inlet fitting - see section 7.
6.2.4 Valve Maintenance (AFC)
The solenoid valve consists of 316 and 416 stainless steel, and VITON7 (or optional NEOPRENE7 or KALREZ7) O-rings and seals. No regular maintenance is required except for periodic cleaning.
Various corrosive gases may demand more frequent replacement of VITON7 O- rings and seals inside the valve. Be sure to use an elastomer material, appropri-
ate for your specific gas application. Contact your distributor or Aalborg7 for optional sealing materials available.
Set the AFC into PURGE mode, and attempt to flush through with a clean, filtered, and neutral gas such as nitrogen. [Another option for fully opening the valve is to
remove the plastic cap on top of the valve, and turn the set screw counterclock­wise until it stops. See section 7.4 for valve adjustment, to return the valve to func­tional use.]
7. CALIBRATION PROCEDURES
Note: Removal of the factory installed calibration seals and/or any adjustments made to the meter, as described in this section, will void any calibration warranty applicable.
7.1 Flow Calibration
Aalborg7 Instruments' Flow Calibration Laboratory offers professional calibration support for Mass Flow Meters and Controllers, using precision calibrators under strictly controlled conditions. NIST traceable calibrations are available. Calibrations can also be performed at customers' site using available standards.
Factory calibrations are performed using NIST traceable precision volumetric cal­ibrators incorporating liquid sealed frictionless actuators.
Generally, calibrations are performed using dry nitrogen gas. The calibration can then be corrected to the appropriate gas desired based on relative correction [K] factors shown in the gas factor table see Appendix 2. A reference gas, other than nitrogen, may be used to closer approximate the flow characteristics of certain gases. This practice is recommended when a reference gas is found with ther­modynamic properties similar to the actual gas under consideration. The appro­priate relative correction factor should be recalculated - see section 9.
It is standard practice to calibrate Mass Flow Meters/Controllers with dry nitrogen gas at 70
F
F (21.1FC), 20 psig (1.4 bars) [25 psig (1.7 bars) for AFC46] inlet pres­sure and 0 psig (0 bar) outlet pressure. It is best to calibrate the AFM/AFC trans­ducers to actual operating conditions. Specific gas calibrations of non-toxic and non-corrosive gases are available at specific conditions. Please contact your dis-
tributor or Aalborg7 for a price quotation.
It is recommended that a flow calibrator of at least four times better collective accuracy than that of the Mass Flow Meter/Controller to be calibrated be used. Equipment required for calibration includes a flow calibration standard and a cer­tified high sensitivity multimeter (which together have a collective accuracy of +
0.25% or better), an insulated (plastic) screwdriver, a flow regulator (example: metering needle valve) installed upstream from the Mass Flow Meter and a pres­sure regulated source of dry filtered nitrogen gas (or other suitable reference gas). The gas and ambient temperature, as well as inlet and outlet pressure conditions should be set up in accordance with actual operating conditions.
Calibration potentiometer locations are illustrated in Figure 7-1.
15
FIGURE 7-1, CALIBRATION POTENTIOMETER LOCATIONS
7.2 Calibration of AFM Mass Flow Meters
All adjustments in this section are made from the outside of the meter, there is no need to disassemble any part of the instrument.
AFM Mass Flow Meters may be field recalibrated/checked for the same range they were originally factory calibrated for. When linearity adjustment is needed, or flow range changes are being made proceed to step 7.3. Flow range changes may require a different Restrictor Flow Element (RFE). Additionally, a different Solenoid Valve Orifice for the AFC Mass Flow Controller (see Table VI) may also be required. Consult your distributor or Aalborg7 for more information.
7.2.1 Connections and Initial Warm Up
Connect the multimeter to output pins* [2] and [3] of the 15-pin “D” connector for 0-5 VDC (or pins [5] and [15] for optional 4-20 mA) (see Figure 2-3).
* If you are calibrating a Mass Flow Meter System that incorporates a
DSPROC Command Module, the multimeter may be connected via the DATA connector which is located at the back of the Command Module.
Power up the Mass Flow Meter for at least 30 minutes prior to commencing the calibration procedure.
16
7.2.2 ZERO Adjustment
Shut off the flow of gas into the Mass Flow Meter. To ensure that no seepage or leak occurs into the meter, it is good practice to temporarily disconnect the gas source. Using the multimeter and the insulated screwdriver, adjust the ZERO potentiometer [R29] through the access window for 0 VDC (or 4 mA respectively) at zero flow.
7.2.3 SPAN Adjustment
Reconnect the gas source. Using the flow regulator, adjust the flow rate to 100% of full scale flow. Check the flow rate indicated against the flow calibrator. If the deviation is less than +
10% of full scale reading, correct the SPAN potentiometer
[R21] setting by using the insulated screwdriver through the access window, to eliminate any deviation. If the deviation is larger than +10% of full scale reading, a defective condition may be present.
LIKELY REASONS FOR A MALFUNCTIONING SIGNAL MAY BE:
M Occluded or contaminated sensor tube. M Leaking condition in the AFM transducer or the gas line and fittings. M For gases other than nitrogen, recheck appropriate "K" factor from Gas Factor Table. M Temperature and/or pressure correction errors.
See also section 8 TROUBLESHOOTING. If after attempting to remedy the above conditions, a malfunction still persists, return the meter for factory service, see section 1.1.
At this point the calibration is complete. However, it is advisable that several addi­tional points between 0 and 100%, such as 25%, 50%, and 75% flow be checked. If discrepancies are found, proceed to step 7.3 for Linearity Adjustment.
7.3 Linearity Adjustment
All adjustments in this section are made from the outside of the meter, there is no need to disassemble any part of the instrument.
7.3.1 Connections and Initial Warm Up
Connect the multimeter to output pins* [2] and [3] for 0 5 VDC (or pins [5] and [15] for optional 4-20 mA) (see Figure 2-3).
* If you are calibrating a Mass Flow Meter System that incorporates a
SDPROC Command Module, the multimeter may be connected via the DATA connector which is located at the back of the Command Module.
Power up the Mass Flow Meter for at least 30 minutes prior to commencing the calibration procedure.
17
7.3.2 ZERO Adjustment
Shut off the flow of gas into the Mass Flow Meter. To ensure that no seepage or leak occurs into the meter, it is good practice to temporarily disconnect the gas source. Using the multimeter and the insulated screwdriver, adjust the ZERO potentiometer [R29] through the access window for 0 VDC (or 4 mA respectively) at zero flow.
7.3.3 25% Flow Adjustment
Reconnect the gas source. Using the flow regulator, adjust the flow rate to 25% of full scale flow. Check the flow rate indicated against the flow calibrator. Adjust the set­ting for potentiometer [R21] by using the insulated screwdriver through the access window, until the output of the flow meter reads 1.25VDC +
37mV (or 8mA +0.12mA).
7.3.4 50% Flow Adjustment
Using the flow regulator, increase the flow rate to 50% of full scale flow. Check the flow rate indicated against the flow calibrator. Adjust the setting for potentiometer [R45] by using the insulated screwdriver through the access window, until the out­put of the flow meter reads 2.50VDC +37mV (or 12mA +0.12mA).
7.3.5 75% Flow Adjustment
Increase the flow rate to 75% of full scale flow. Check the flow rate indicated against the flow calibrator. Adjust the setting for potentiometer [R44] by using the insulated screwdriver through the access window, until the output of the flow meter reads 3.75VDC +
37mV (or 16mA +0.12mA).
7.3.6 100% Flow Adjustment
Increase the flow rate to 100% of full scale flow. Check the flow rate indicated against the flow calibrator. Adjust the setting for potentiometer [R43] by using the insulated screwdriver through the access window, until the output of the flow meter reads 5.00VDC +
37mV (or 20mA +0.12mA).
Repeat steps 7.3.3 to 7.3.6 at least once more.
7.4 Calibration of AFC Mass Flow Controllers
All adjustments in this section are made from the outside of the meter, there is no need to disassemble any part of the instrument.
AFC Mass Flow Controllers may be field recalibrated/checked for the same range they were originally factory calibrated for.
7.4.1 Disable Solenoid Valve
Remove the round plastic cap on top of the solenoid valve. Turn the set screw on top of the valve counterclockwise until it stops, to open the valve. Set the valve into PURGE mode. This step essentially bypasses the flow control properties of
18
the transducer. The unit will now act as a mass flow meter.
CAUTION: If the valve is left in the AUTO (control) or OPEN mode for an extended period of time, it may become warm or even hot to the touch. Use care in avoiding direct contact with the valve during operation.
Follow steps outlined in section 7.2 and 7.3, then continue with step 7.4.2 below.
7.4.2 Valve Adjustment
Discontinue the PURGE mode (set valve for the closed position). Apply an inlet pressure of 5 psig, and atmospheric pressure at the outlet. If a small flow occurs, turn the set screw on top of the solenoid valve clockwise until the flow through the AFC just stops.
7.4.3 Full Scale Flow Adjustment
Fully open the flow regulator upstream of the AFC. Increase the inlet pressure to 20 psig (25 psig for AFC46). Apply a +5.00 VDC set point reference. Using the cal­ibrator check the flow rate. If necessary, adjust R21 to match the desired full scale flow rate. [In control mode, turning R21 clockwise will decrease the flow. Conversely, turning R21 counterclockwise will increase the flow through the AFC.]
7.4.4 25% Flow Adjustment
Change the set point to 1.25 VDC to control at 25% of full scale flow. Check the flow rate indicated against the flow calibrator. If the flow rate is not within +
0.75% of full scale, re-adjust the setting for potentiometer [R21], until the flow output is correct.
7.4.5 50% Flow Adjustment
Change the set point to 2.50 VDC to control at 50% of full scale flow. Check the flow rate indicated against the flow calibrator. If the flow rate is not within +
0.75% of full
scale, re-adjust the setting for potentiometer [R45], until the flow output is correct.
7.4.6 75% Flow Adjustment
Change the set point to 3.75 VDC to control at 75% of full scale flow. Check the flow rate indicated against the flow calibrator. If the flow rate is not within +0.75% of full scale, re-adjust the setting for potentiometer [R44], until the flow output is correct.
7.4.7 100% Flow Adjustment
Change the set point to 5.00 VDC to control at 100% of full scale flow. Check the flow rate indicated against the flow calibrator. If the flow rate is not within +
0.75% of full
scale, re-adjust the setting for potentiometer [R43], until the flow output is correct.
Repeat steps 7.4.4 to 7.4.7 at least once more.
19
TABLE VI AFC SOLENOID VALVE ORIFICE SELECTION TABLE
8. TROUBLESHOOTING
8.1 Common Conditions
Your Mass Flow Meter/Controller was thoroughly checked at numerous quality control points during and after manufacturing and assembly operations. It was cal­ibrated in accordance to your desired flow and pressure conditions for a given gas or a mixture of gases.
It was carefully packed to prevent damage during shipment. Should you feel that the instrument is not functioning properly please check for the following common conditions first:
Are all cables connected correctly?
Are there any leaks in the installation?
Is the power supply correctly selected according to requirements?
When several meters are used a power supply with appropriate current rating should be selected.
Were the connector pinouts matched properly?
When interchanging with other manufacturers' equipment, cables and connectors must be carefully wired for correct pin configurations.
Is the pressure differential across the instrument sufficient?
20
ORIFICE PART NUMBER FLOW RATE [N2]
OR.010 under 10 sccm
OR.020 10 to 1000 sccm
OR.040
1 to 5 slpm
OR.055 5 to 10 slpm
OR.063 10 to 15 slpm
OR.073 15 to 20 slpm
OR.094
20 to 50 slpm
OR.125 50 to 100 slpm
8.2 Troubleshooting Guide
21
REMEDY
check connection of power supply
disconnect AFM/AFC transducer from power supply; remove the shorting condition or check polarities; fuse resets automatically
disconnect power cord from AC supply; remove and inspect fuses at AC power input connector of SDPROC; replace as necessary
REMOVE CAUSE OF SHORT CIRCUIT!
flush clean or disassemble to remove impediments or replace
flush clean or disassemble to remove impediments or return to factory for replacement
return to factory for replacement
re-adjust valve (section 7.4)
disconnect AFM/AFC transducer from power supply; remove the shorting condition or check polarities; fuse resets automatically
REMOVE CAUSE OF SHORT CIRCUIT!
apply appropriate gas pressure
flush clean or disassemble to remove impediments or replace
signal and power supply commons are different
apply appropriate gas pressure
check cables and all connections or replace
re-adjust set point
re-adjust valve (section 7.4)
LIKELY REASON
power supply off
fuse blown (AFM/AFC)
fuse blown (SDPROC)
filter screen obstructed at inlet
occluded sensor tube
pc board defect
valve adjustment wrong
fuse blown (AFM/AFC)
inadequate gas pressure
filter screen obstructed at inlet
ground loop
inadequate gas pressure
cable or connector malfunction
set point is too low (<2% of full scale)
valve adjustment wrong
INDICATION
lack of reading or output
output reads at (+) or (- ) saturation only
flow reading does not coincide with the set point (AFC models only)
no response to set point (AFC models only)
22
REMEDY
locate and correct
return to factory for replacement
return to factory for replacement
locate and repair
use matched calibration
see K factor tables in APPENDIX 2
locate and correct
return to factory for replacement
flush clean or disassemble to remove impediments
flush clean or disassemble to remove impediments or return to factory for replacement
flush clean or disassemble to remove impediments or replace
check for any tilt or change in the mounting of the transducer; generally, units are calibrated for horizontal installation (relative to the sensor tube)
re-adjust valve (section 7.4)
return to factory for replacement
check cable and connectors or replace
decrease pressure to correct level
adjust appropriately
re-adjust valve (section 7.4)
return to factory for replacement
check cable and connectors or replace
disassemble to remove impediments or return to factory
LIKELY REASON
gas leak
pc board defective
defective sensor
gas Leak
gas metered is not the same as what meter was calibrated for
composition of gas changed
gas leak
pc board defective
RFE dirty
occluded sensor tube
filter screen obstructed at inlet
transducer is not mounted properly
incorrect valve adjustment
pc board defect
cable or connectors malfunction
differential pressure too high
insufficient inlet pressure
incorrect valve adjustment
pc board defect
cable or connectors malfunction
orifice obstructed
INDICATION
unstable or no zero reading
full scale out­put at "no flow" condition or with valve closed
calibration off
AFC valve does not work in open position
AFC valve does not work in close position
For best results it is recommended that instruments are returned to the factory for servicing. See section 1.3 for return procedures.
8.3 Technical Assistance
Aalborg7 Instruments will provide technical assistance over the phone to qualified repair personnel. Please call our Technical Assistance at (845) 770-3000. Please have your Serial Number and Model Number ready when you call.
APPENDIX 1
23
Q
O
= Q
a
= Q
r
x K = 1000 X 0.9926 = 992.6 sccm
where K = relative K factor to reference gas (oxygen to nitrogen)
1
d X C
p
where d = gas density (gram/liter) C
p
= coefficient of specific heat (cal/gram)
Q
a
K
a
Q
r
K
r
where Qa= mass flow rate of an actual gas (sccm) Q
r
= mass flow rate of a reference gas (sccm)
K
a
= K factor of an actual gas
K
r
= K factor of a reference gas
=
9. CALIBRATION CONVERSIONS FROM
REFERENCE GASES
The calibration conversion incorporates the K factor. The K factor is derived from gas density and coefficient of specific heat. For diatomic gases:
=
K
=
K
gas
Note in the above relationship that d and Cp are usually chosen at standard con­ditions of one atmosphere and 25
F
C.
If the flow range of a Mass Flow Controller or Controller remains unchanged, a relative K factor is used to relate the calibration of the actual gas to the reference gas.
For example, if we want to know the flow rate of oxygen and wish to calibrate with nitrogen at 1000 SCCM, the flow rate of oxygen is:
2
APPENDIX 1
COMPONENTS DIAGRAMS
24
AFM METERING PC BOARD
(ALSO INCORPORATED IN AFC)
AFC CONTROL PC BOARD
25
APPENDIX 2
GAS FACTOR TABLE (“K” FACTORS)
CAUTION: K-Factors at best are only an approximation. K factors should not
be used in applications that require accuracy better than +/- 5 to 10%.
ACTUAL GAS
K FACTOR
Relative to N
2
Cp
[Cal/g]
Density
[g/I]
Acetylene C2H
2
.5829 .4036 1.162 Air 1.0000 .240 1.293 Allene (Propadiene) C3H
4
.4346 .352 1.787 Ammonia NH
3
.7310 .492 .760 Argon Ar
Argon AR-1 (>=10 L/min)
1.4573
1.205
.1244 .1244
1.782
1.782
Arsine AsH
3
.6735 .1167 3.478 Boron Trichloride BCl
3
.4089 .1279 5.227 Boron Trifluoride BF
3
.5082 .1778 3.025 Bromine Br
2
.8083 .0539 7.130 Boron Tribromide Br
3
.38 .0647 11.18 Bromine PentaTrifluoride BrF
5
.26 .1369 7.803 Bromine Trifluoride BrF
3
.3855 .1161 6.108 Bromotrifluoromethane (Freon-13 B1) CBrF
3
.3697 .1113 6.644
1,3-Butadiene C4H
6
.3224 .3514 2.413
Butane C4H
10
.2631 .4007 2.593
1-Butene C4H
8
.2994 .3648 2.503
2-Butene C4H8 CIS
.324 .336 2.503
2-Butene C4H8TRANS
.291 .374 2.503
Carbon Dioxide CO
2
Carbon Dioxide CO2-1 (>10 L/min)
.7382 .658
.2016 .2016
1.964
1.964
Carbon Disulfide CS
2
.6026 .1428 3.397
Carbon Monoxide C0
1.00 .2488 1.250
Carbon Tetrachloride CCl
4
.31 .1655 6.860
Carbon Tetrafluoride (Freon-14)CF
4
.42 .1654 3.926
Carbonyl Fluoride COF
2
.5428 .1710 2.945
Carbonyl Sulfide COS
.6606 .1651 2.680
Chlorine Cl
2
.86 .114 3.163
Chlorine Trifluoride ClF
3
.4016 .1650 4.125
Chlorodifluoromethane (Freon-22)CHClF
2
.4589 .1544 3.858
Chloroform CHCl
3
.3912 .1309 5.326
Chloropentafluoroethane(Freon-115)C2ClF
5
.2418 .164 6.892
Chlorotrifluromethane (Freon-13) CClF
3
.3834 .153 4.660
CyanogenC2N
2
.61 .2613 2.322
CyanogenChloride CICN
.6130 .1739 2.742
Cyclopropane C3H
5
.4584 .3177 1.877
26
ACTUAL GAS
K FACTOR
Relative to N
2
Cp
[Cal/g]
Density
[g/I]
Deuterium D
2
1.00 1.722 1.799
Diborane B2H
6
.4357 .508 1.235
Dibromodifluoromethane CBr2F
2
.1947 .15 9.362
Dichlorodifluoromethane (Freon-12) CCl2F
2
.3538 .1432 5.395
Dichlofluoromethane (Freon-21) CHCl2F
.4252 .140 4.592
Dichloromethylsilane (CH3)2SiCl
2
.2522 .1882 5.758
Dichlorosilane SiH2Cl
2
.4044 .150 4.506
Dichlorotetrafluoroethane (Freon-114) C2Cl2F
4
.2235 .1604 7.626
1,1-Difluoroethylene (Freon-1132A) C2H2F
2
.4271 .224 2.857
Dimethylamine (CH3)2NH
.3714 .366 2.011
Dimethyl Ether (CH3)2O
.3896 .3414 2.055
2,2-Dimethylpropane C3H
12
.2170 .3914 3.219
Ethane C2H
6
.50 .420 1.342
Ethanol C2H6O
.3918 .3395 2.055
Ethyl Acetylene C4H
6
.3225 .3513 2.413
Ethyl Chloride C2H5Cl
.3891 .244 2.879
Ethylene C2H
4
.60 .365 1.251
Ethylene Oxide C2H4O
.5191 .268 1.965
Fluorine F
2
.9784 .1873 1.695
Fluoroform (Freon-23) CHF
3
.4967 .176 3.127
Freon-11 CCl3F
.3287 .1357 6.129
Freon-12 CCl2F
2
.3538 .1432 5.395
Freon-13 CClF
3
.3834 .153 4.660
Freon-13B1 CBrF
3
.3697 .1113 6.644
Freon-14 CF
4
.4210 .1654 3.926
Freon-21 CHCl2F
.4252 .140 4.592
Freon-22 CHClF
2
.4589 .1544 3.858
Freon-113 CCl2FCClF
2
.2031 .161 8.360
Freon-114 C2Cl2F
4
.2240 .160 7.626
Freon-115 C2ClF
5
.2418 .164 6.892
Freon-C318 C4F
8
.1760 .185 8.397
Germane GeH
4
.5696 .1404 3.418
Germanium Tetrachloride GeCl
4
.2668 .1071 9.565
Helium He Helium He-1 (>50 L/min) Helium He-2 (>10-50 L/min)
1.454
2.43
2.05
1.241
1.241
1.241
.1786 .1786 .1786
Hexafluoroethane C2F6(Freon-116)
.2421 .1834 6.157
Hexane C6H
14
.1792 .3968 3.845
Hydrogen H2-1 Hydrogen H
2
-2 (>10-100 L)
Hydrogen H
2
-3 (>100 L)
1.0106
1.35
1.9
3.419
3.419
3.419
.0899 .0899 .0899
27
ACTUAL GAS
K FACTOR
Relative to N
2
Cp
[Cal/g]
Density
[g/I]
Hydrogen Bromide HBr
1.000 .0861 3.610
Hydrogen Chloride HCl
1.000 .1912 1.627
Hydrogen Cyanide HCN
.764 .3171 1.206
Hydrogen Fluoride HF
.9998 .3479 .893
Hydrogen Iodide HI
.9987 .0545 5.707
Hydrogen Selenide H2Se
.7893 .1025 3.613
Hydrogen Sulfide H2S
.80 .2397 1.520
Iodine Pentafluoride IF
5
.2492 .1108 9.90
Isobutane CH(CH3)
3
.27 .3872 3.593
Isobutylene C4H
6
.2951 .3701 2.503
Krypton Kr
1.453 .0593 3.739
Methane CH4 (<=10 L/min) Methane CH
4
-1 (>=10 L/min)
.7175 .75
.5328 .5328
.715 .715
Methanol CH
3
.5843 .3274 1.429
Methyl Acetylene C3H
4
.4313 .3547 1.787
Methyl Bromide CH2Br
.5835 .1106 4.236
Methyl Chloride CH3Cl
.6299 .1926 2.253
Methyl Fluoride CH3F
.68 .3221 1.518
Methyl Mercaptan CH3SH
.5180 .2459 2.146
Methyl Trichlorosilane (CH3)SiCl
3
.2499 .164 6.669
Molybdenum Hexafluoride MoF
6
.2126 .1373 9.366
Monoethylamine C2H5NH
2
.3512 .387 2.011
Monomethylamine CH3NH
2
.51 .4343 1.386
Neon NE
1.46 .246 .900
Nitric Oxide NO
.990 .2328 1.339
Nitrogen N
2
1.000 .2485 1.25
Nitrogen Dioxide NO
2
.737 .1933 2.052
Nitrogen Trifluoride NF
3
.4802 .1797 3.168
Nitrosyl Chloride NOCl
.6134 .1632 2.920
Nitrous Oxide N2O
.7128 .2088 1.964
Octafluorocyclobutane (Freon-C318) C4F
8
.176 .185 8.397
Oxygen O
2
.9926 .2193 1.427
Oxygen Difluoride OF
2
.6337 .1917 2.406
Ozone
.446 .195 2.144
Pentaborane B5H
9
.2554 .38 2.816
Pentane C5H
12
.2134 .398 3.219
Perchloryl Fluoride ClO3F
.3950 .1514 4.571
Perfluoropropane C3F
8
.174 .197 8.388
Phosgene COCl
2
.4438 .1394 4.418
Phosphine PH
3
.759 .2374 1.517
28
ACTUAL GAS
K FACTOR
Relative to N
2
Cp
[Cal/g]
Density
[g/I]
Phosphorous Oxychloride POCl
3
.36 .1324 6.843
Phosphorous Pentafluoride PH
5
.3021 .1610 5.620
Phosphorous Trichloride PCl
3
.30 .1250 6.127
Propane C3H
8
.35 .399 1.967
Propylene C3H
6
.40 .366 1.877
Silane SiH
4
.5982 .3189 1.433
Silicon Tetrachloride SiCl
4
.284 .1270 7.580
Silicon Tetrafluoride SiF
4
.3482 .1691 4.643
Sulfur Dioxide SO
2
.69 .1488 2.858
Sulfur Hexafluoride SF
6
.2635 .1592 6.516
Sulfuryl Fluoride SO2F
2
.3883 .1543 4.562
Tetrafluoroethane (Forane 134A) CF3CH2F
.5096 .127 4.224
Tetrafluorohydrazine N2F
4
.3237 .182 4.64
Trichlorofluoromethane (Freon-11) CCl3F
.3287 .1357 6.129
Trichlorosilane SiHCl
3
.3278 .1380 6.043
1,1,2-Trichloro-1,2,2 Trifluoroethane (Freon-113) CCl
2
FCClF
2
.2031 .161 8.36
Triisobutyl Aluminum (C4H9)AL
.0608 .508 8.848
Titanium Tetrachloride TiCl
4
.2691 .120 8.465
Trichloro Ethylene C2HCl
3
.32 .163 5.95
Trimethylamine (CH3)3N
.2792 .3710 2.639
Tungsten Hexafluoride WF
6
.2541 .0810 13.28
Uranium Hexafluoride UF
6
.1961 .0888 15.70
Vinyl Bromide CH2CHBr
.4616 .1241 4.772
Vinyl Chloride CH2CHCl
.48 .12054 2.788
Xenon Xe
1.44 .0378 5.858
APPENDIX 3
DIMENSIONAL DRAWINGS
AFM 26 MASS FLOW METER
NOTES: Aalborg7 reserves the right to change designs and dimensions at its
sole discretion at any time without notice. For certified dimensions please contact Aalborg7.
29
AFM 36/46 MASS FLOW METER
NOTES: Aalborg7 reserves the right to change designs and dimensions at
its sole discretion at any time without notice. For certified dimensions please contact Aalborg7.
30
AFC 26 MASS FLOW CONTROLLER
NOTES: Aalborg7 reserves the right to change designs and dimensions at its
sole discretion at any time without notice. For certified dimensions please contact Aalborg7.
31
AFC 36/46 MASS FLOW CONTROLLER
NOTES: Aalborg7 reserves the right to change designs and dimensions at its
sole discretion at any time without notice. For certified dimensions please contact Aalborg7.
32
NOTE: Follow Return Procedures In section 1.3.
33
APPENDIX 4
WARRANTY
Aalborg7 Mass Flow Systems are warranted against parts and workmanship for a period of one year from the date of purchase. Calibrations are warrant­ed for up to six months after date of purchase, provided calibration seals have not been tampered with. It is assumed that equipment selected by the customer is constructed of materials compatible with gases used. Proper selection is the responsibility of the customer. It is understood that gases under pressure present inherent hazards to the user and to equipment, and it is deemed the responsibility of the customer that only operators with basic knowledge of the equipment and its limitations are permitted to control and operate the equipment covered by this warranty. Anything to the contrary will
automatically void the liability of Aalborg7 and the provisions of this warran­ty. Defective products will be repaired or replaced solely at the discretion of
Aalborg7 at no charge. Shipping charges are borne by the customer. This warranty is void if the equipment is damaged by accident or misuse, or has
been repaired or modified by anyone other than Aalborg7 or factory author­ized service facility. This warranty defines the obligation of Aalborg7 and no other warranties expressed or implied are recognized.
TRADEMARKS
Aalborg®-is a registered trademark of Aalborg Instruments & Controls. Buna®-is a registered trademark of DuPont Dow Elastometers. Kalrez
®
-is a registered trademark of DuPont Dow Elastomers.
Neoprene
®
-is a registered trademark of DuPont.
VCR®-is a registered trademark of Swagelok Marketing Co.
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